== Соединения W (томa 33-34) == |
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189. 33-0054 NH4Er{WO4}2*3H2O Rombik Groupa 17
Dexp. Dcal. d(D) h k l 5.0500 5.0410 .0090 0 2 1 3.8500 3.8465 .0035 0 3 0 3.4500 3.4540 -.0040 0 0 3 3.1800 3.1788 .0012 1 0 1 2.9600 2.9636 -.0036 0 2 3 2.5300 2.5276 .0024 0 1 4 1.9180 1.9189 -.0009 0 5 3 1.5870 1.5866 .0004 1 6 2 1.5150 1.5153 -.0003 2 3 1 1.4910 1.4908 .0002 2 1 3
a= 3.340 b=11.539 c=10.362 da= .001 db= .001 dc= .003 V= 399.3
190. 33-0055 NH4Er{WO4}2*3H2O Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 5.0900 5.0940 -.0040 0 1 1 3.9100 3.9087 .0013 -2 1 1 3.4800 3.4784 .0016 -2 1 2 3.2300 3.2277 .0023 3 0 0 3.0100 3.0120 -.0020 0 2 0 2.5800 2.5808 -.0008 -4 0 1 2.2100 2.2099 .0001 -3 1 4 1.9600 1.9598 .0002 -4 2 1 1.7460 1.7459 .0001 1 2 4 1.7120 1.7123 -.0003 -6 0 3 1.6120 1.6122 -.0002 0 2 5 1.5390 1.5388 .0002 -6 0 5 1.5060 1.5060 .0000 0 4 0
a= 10.3950 b= 6.0240 c= 10.2450 beta= 111.325 da=.00084 db=.0007 dc=.0002 dbet=.001 V= 597.6
191. 33-0077 {NH4}4Na6W12O41*32H2O Monoklin Grupa 14
Dexp Dcal d(D) h k l 17.3000 15.9715 1.3285 1 0 0 15.6000 15.9715 -.3715 1 0 0 13.2000 13.0888 .1112 0 1 1 11.9000 11.8652 .0348 1 1 0 10.8000 10.9083 -.1083 -1 1 1 8.5300 8.5126 .0174 0 1 2 7.2700 7.2809 -.0109 2 1 0 6.5400 6.5444 -.0044 0 2 2 5.7800 5.7758 .0042 1 2 2 4.8500 4.8526 -.0026 0 0 4 4.2600 4.2563 .0037 0 2 4 3.9900 3.9929 -.0029 4 0 0
a= 16.3350 b=17.7250 c= 19.8520 beta= 102.104 da= .0004 db=.0008 dc.0007 dbet=.001 V= 5620.0
Triklin
Dexp Dcal d(D) h k l 17.3000 17.3225 -.0225 1 0 0 15.6000 15.5944 .0056 0 1 0 13.2000 13.1980 .0020 0 0 1 11.9000 11.9085 -.0085 1 0 1 10.8000 10.8015 -.0015 1 1 1 8.5300 8.5261 .0039 1 -1 1 7.2700 7.2755 -.0055 2 2 0 6.5400 6.5773 -.0373 -2 0 1 5.7800 5.7742 .0058 3 0 0 4.8500 4.8504 -.0004 3 3 0 4.2600 4.2630 -.0030 2 -2 2 3.9900 3.9913 -.0013 -3 2 0
A= 19.204 DA= .004 B= 16.822 DB= .007 C= 13.608 DC= .001 GAMMA= 68.00 DGAMMA= .03 BETA = 75.92 DBETA = .07 ALPHA= 85.46 DALPHA= .05 V=3948.2
192. 33-0078 {NH4}2Na8W12O41*25H2O Monoklin Grupa 3
Dexp Dcal d(D) h k l 24.9000 25.0361 -.1361 1 0 0 15.2000 15.1553 .0447 1 1 0 13.0000 13.1333 -.1333 1 0 1 10.8000 10.8109 -.0109 1 1 1 8.9000 8.8984 .0016 1 2 0 8.3400 8.3454 -.0054 3 0 0 7.4000 7.4108 -.0108 3 0 1 6.7300 6.7085 .0215 -1 1 2 6.0400 5.9460 .0940 4 1 0 5.7900 5.7937 -.0037 1 2 2 5.4600 5.4576 .0024 3 1 2 5.3000 5.2935 .0065 -3 1 2
a= 25.050 b= 19.0400 c= 15.1210 beta= 88.083 da=.001 db=.0002 dc= .0004 dbet=.001 V= 7208
Triklin
Dexp Dcal d(D) h k l 24.9000 24.8526 .0474 1 0 0 15.2000 15.2119 -.0119 1 1 0 13.0000 12.9842 .0158 0 1 1 10.8000 10.7959 .0041 2 1 0 8.9000 8.8954 .0046 0 2 1 8.3400 8.3402 -.0002 -2 -1 1 7.4000 7.3963 .0037 -2 2 1 6.7300 6.7303 -.0003 -2 2 0 6.0400 6.0430 -.0030 1 3 1 5.7900 5.7871 .0029 1 -2 1 5.4600 5.4605 -.0005 3 -1 1 5.3000 5.2999 .0001 -4 1 2
A= 25.776 DA= .001 B= 18.70350 DB= .0007 C= 14.467 DC= .001 GAMMA= 87.857 DGAMMA= .006 BETA =103.51 DBETA = .01 ALPHA= 69.798 DALPHA= .002 V= 6310.7
193. 33-0822 Li0.05Na0.65WO3 Monoklin Grupa 3
Dexp Dcal d(D) h k l 4.2500 4.2485 .0015 1 1 0 3.8500 3.8538 -.0038 0 1 1 2.7100 2.7082 .0018 2 1 1 2.2200 2.2213 -.0013 1 2 1 1.9210 1.9206 .0004 3 0 2 1.7220 1.7225 -.0005 3 2 1 1.5700 1.5703 -.0003 -3 2 2 1.3610 1.3610 .0000 5 0 2 1.2850 1.2848 .0002 -6 0 1 1.2170 1.2172 -.0002 -5 1 3 1.1580 1.1579 .0001 0 1 5 1.0650 1.0653 -.0003 3 0 5 1.0280 1.0278 .0002 2 2 5 .9340 .9340 .0000 -3 5 1
a= 7.828 b= 5.060 c= 5.952 beta= 92.41 da= .004 db=.001 dc=.001 dbeta=.02 V= 235.6
194. 33-0823 Li0.33Na0.06WO3 Monoklin Grupa 14
Dexp Dcal d(D) h k l 3.7700 3.7693 .0007 3 0 0 2.6600 2.6600 .0000 -1 1 2 2.1600 2.1603 -.0003 5 0 2 2.1600 2.1640 -.0040 -2 1 3 1.8700 1.8698 .0002 -4 0 4 1.6750 1.6748 .0002 -2 0 6 1.5280 1.5280 .0000 -2 2 1 1.3210 1.3210 -.0000 7 1 4 1.2500 1.2500 -.0000 9 0 2
a= 11.358 b= 3.222 c= 10.88000 beta= 84.606 da= .001 db=.001 dc=.00002 dbet=.006 V= 396.3
195.33-0824 Li0.1Na0.75WO3 Rombik Groupa 30,53
Dexp. Dcal. d(D) h k l 3.8500 3.8358 .0142 1 0 2 2.7300 2.7276 .0024 2 1 1 2.2100 2.2167 -.0067 1 1 3 1.9250 1.9274 -.0024 0 2 0 1.7300 1.7299 .0001 5 0 0 1.5720 1.5733 -.0013 4 1 3 1.3640 1.3638 .0002 4 2 2 1.2880 1.2877 .0003 6 1 2 1.2190 1.2191 -.0001 2 3 1 1.0810 1.0812 -.0002 8 0 0 .9360 .9360 .0000 6 3 2
a= 8.649 b= 3.855 c= 8.56 da= .001 db= .001 dc= .02 V= 285.4
196. 33-0825 Li0.28Na0.06WO3 Monoklin Grupa 14
Dexp Dcal d(D) h k l 6.0300 6.0274 .0026 -1 1 1 5.4700 5.4207 .0493 2 1 0 4.2900 4.2913 -.0013 2 2 0 3.8300 3.8313 -.0013 3 1 0 3.3800 3.3815 -.0015 1 3 1 2.9400 2.9379 .0021 4 1 0 2.9400 2.9497 -.0097 1 4 0 2.7100 2.7104 -.0004 4 2 0 2.6900 2.6887 .0013 -3 2 2 2.5000 2.5006 -.0006 -4 1 2 2.3200 2.3198 .0002 0 5 1 2.2500 2.2502 -.0002 5 2 0 1.9100 1.9101 -.0001 5 1 2
a= 12.2250 b= 12.1650 c= 7.7690 beta= 97.854 da=.0009 db= .0002 dc=.0009 dbet=.002 V= 1144.5
197. 33-1036 KRb3W5O17 Triklin
Dexp Dcal d(D) h k l 5.9100 5.9096 .0004 -1 0 1 5.1500 5.1530 -.0030 -1 1 1 4.8000 4.7930 .0070 1 -1 1 4.1500 4.1523 -.0023 -1 -1 1 3.7700 3.7705 -.0005 0 0 2 3.6500 3.6476 .0024 -2 0 1 3.3400 3.3424 -.0024 2 -1 1 3.2100 3.2100 -.0000 0 1 2 3.1800 3.1747 .0053 1 -1 2 3.1000 3.1045 -.0045 -2 2 1 2.5780 2.5765 .0015 -2 2 2 2.4680 2.4670 .0010 -1 -2 2
A= 8.218 DA= .002 B= 7.7981 DB= .0006 C= 7.684 DC= .002 GAMMA=111.51 DGAMMA= .05 BETA = 99.43 DBETA = .04 ALPHA= 91.94 DALPHA= .02 V= 449.7
198. 33-1044 K5Na5W12O41*26H2O Triklin
Dexp Dcal d(D) h k l 33.9000 33.7415 .1585 1 0 0 25.2000 25.1961 .0039 0 1 0 20.0000 19.9976 .0024 1 0 2 16.0000 16.0215 -.0215 2 -1 1 10.9000 10.8838 .0162 0 -1 4 10.0000 9.9988 .0012 2 0 4 8.1000 8.0991 .0009 -2 3 0 7.4000 7.4030 -.0030 0 -1 6 6.8000 6.8017 -.0017 3 2 3 6.4000 6.3951 .0049 2 1 6 5.6000 5.6002 -.0002 6 0 3 5.5000 5.5008 -.0008 4 0 7
A= 35.215 DA= .002 B= 26.51 DB= .03 C= 45.757 DC= .008 GAMMA=102.92 DGAMMA= .09 BETA = 76.63 DBETA = .02 ALPHA=105.24 DALPHA= .04 V=39671
199. 33-1132 Rb2WO4 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 5.9600 5.9721 -.0121 1 1 1 4.8700 4.8787 -.0087 1 0 2 3.9700 3.9727 -.0027 1 2 0 3.8700 3.8655 .0045 -1 0 2 3.5500 3.5563 -.0063 3 0 1 3.3000 3.2995 .0005 1 0 3 3.1600 3.1627 -.0027 3 1 0 3.0500 3.0505 -.0005 3 1 2 2.3560 2.3568 -.0008 4 0 3 2.1220 2.1231 -.0011 0 3 3 2.0530 2.0526 .0004 -3 3 1 1.9260 1.9252 .0008 4 3 2
a= 10.690 b= 8.627 c= 9.8990 beta= 72.542 da= .001 db=.001 dc=.0005 dbet=.007 V= 870.9
Triklin
Dexp Dcal d(D) h k l 5.9600 5.9609 -.0009 1 1 1 4.8700 4.8712 -.0012 -1 -1 1 3.9700 3.9700 .0000 2 1 0 3.8700 3.8705 -.0005 2 0 1 3.5500 3.5512 -.0012 -1 -1 2 3.3000 3.3038 -.0038 0 1 3 3.1600 3.1587 .0013 1 0 3 3.0500 3.0499 .0001 -2 0 2 2.3560 2.3556 .0004 -2 -1 3 2.1220 2.1218 .0002 -1 2 4 2.0530 2.0532 -.0002 1 3 4 1.9260 1.9259 .0001 0 4 0
A= 8.403 DA= .005 B= 8.088 DB= .005 C= 10.256 DC= .001 GAMMA= 76.49 DGAMMA= .05 BETA = 83.11 DBETA = .02 ALPHA= 77.17 DALPHA= .01 V= 659.1 |
200. 33-1196 Ag2WO4 Triklin
Dexp Dcal d(D) h k l 2.9700 2.9706 -.0006 2 0 0 2.8600 2.8600 .0000 0 -2 1 2.7500 2.7505 -.0005 -2 0 1 2.6400 2.6395 .0005 2 0 1 2.0100 2.0100 .0000 0 2 2 1.6950 1.6942 .0008 2 -2 1 1.6850 1.6850 .0000 2 1 3 1.6610 1.6620 -.0010 1 3 2 1.6210 1.6203 .0007 1 4 0 1.5970 1.5958 .0012 0 0 4 1.2690 1.2698 -.0008 -2 -2 5 1.2400 1.2400 .0000 5 1 1
A= 6.805 DA= .007 B= 6.837 DB= .004 C= 6.542 DC= .002 GAMMA= 60.98 DGAMMA= .09 BETA = 98.58 DBETA = .03 ALPHA=102.27 DALPHA= .02 V=258.4
201. 33-1237 Na2CrWO7 Triklin
Dexp Dcal d(D) h k l 7.2000 7.1998 .0002 1 0 0 5.4400 5.4394 .0006 -1 1 0 4.6600 4.6649 -.0049 0 0 2 4.5700 4.5692 .0008 -1 1 2 3.7200 3.7238 -.0038 -1 2 0 3.6000 3.5999 .0001 2 0 0 3.2100 3.2097 .0003 -1 0 3 3.0750 3.0754 -.0004 2 0 1 2.9940 2.9934 .0006 1 -1 2 2.8850 2.8852 -.0002 -1 -2 2 2.7300 2.7293 .0007 -1 3 0 2.5890 2.5889 .0001 2 1 2
A= 7.5156 DA= .0008 B= 9.660 DB= .001 C= 10.227 DC= .001 GAMMA= 90.30 DGAMMA= .07 BETA =105.95 DBETA = .07 ALPHA= 72.239 DALPHA= .07 V=676.1
202. 33-1544 C10H24BaN2O12W2*3.5H2O Triklin
Dexp Dcal d(D) h k l 9.6000 9.6009 -.0009 1 0 0 7.1000 7.0931 .0069 -1 1 0 6.3000 6.2989 .0011 1 0 1 5.9200 5.9553 -.0353 1 1 0 4.7400 4.7405 -.0005 0 -1 2 4.5200 4.5233 -.0033 1 -2 1 4.3700 4.3824 -.0124 0 0 2 3.9250 3.9253 -.0003 2 1 0 3.3140 3.3154 -.0014 2 1 1 3.0480 3.0481 -.0001 0 -2 3 2.9120 2.9113 .0007 -2 -2 2 2.8530 2.8538 -.0008 -1 -2 3
A= 9.7504 DA= .0008 B= 9.616 DB= .004 C= 9.546 DC= .003 GAMMA= 99.525 DGAMMA= .002 BETA = 89.210 DBETA = .01 ALPHA=113.143 DALPHA= .001 V= 810.5
203. 33-1844 C10H24K2N2O12W2*2H2O Triklin
Dexp Dcal d(D) h k l 7.2000 7.1783 .0217 -1 0 1 6.5100 6.5048 .0052 0 -1 1 5.7900 5.7944 -.0044 -1 1 1 5.4000 5.4009 -.0009 1 0 1 4.0000 4.0004 -.0004 2 0 0 3.6930 3.6945 -.0015 0 2 2 3.4270 3.4264 .0006 1 -2 1 3.2670 3.2661 .0009 1 -1 2 3.1000 3.0975 .0025 1 3 1 2.9030 2.9021 .0009 0 -1 3 2.6600 2.6644 -.0044 -3 0 2 2.5450 2.5472 -.0022 -3 -2 1
A= 8.3803 DA= .0002 B= 10.2627 DB= .0003 C= 9.879 DC= .001 GAMMA= 84.139 DGAMMA= .006 BETA =105.583 DBETA = .004 ALPHA= 84.59 DALPHA= .01 V=806.9
204. 33-1881 C10H24N2Na2O12W2*3H2O Triklin
Dexp Dcal d(D) h k l 7.1000 7.0953 .0047 -1 2 0 6.1900 6.1878 .0022 1 2 0 5.5000 5.5153 -.0153 0 -2 1 5.1300 5.1255 .0045 1 0 1 4.7700 4.7619 .0081 0 -3 1 4.4000 4.3985 .0015 2 0 0 4.1000 4.1013 -.0013 1 4 0 3.5900 3.5910 -.0010 2 -2 1 3.4400 3.4400 .0000 -2 2 1 3.3020 3.3045 -.0025 -2 -2 1 3.1000 3.0939 .0061 2 4 0 2.9880 2.9815 .0065 1 -1 2
A= 8.883 DA= .005 B= 20.20 DB= .01 C= 6.284 DC= .006 GAMMA= 97.97 DGAMMA= .05 BETA = 88.72 DBETA = .04 ALPHA= 95.00 DALPHA= .06 V=1109.3
205. 33-1945 C20H16F2N4O5W2 Triklin
Dexp Dcal d(D) h k l 10.4000 10.4187 -.0187 1 0 0 9.2600 9.2550 .0050 1 1 0 8.0400 8.0531 -.0131 -1 0 1 7.3700 7.3479 .0221 -1 -1 1 6.6100 6.6210 -.0110 0 -1 1 6.0000 5.9990 .0010 1 0 1 5.8100 5.8114 -.0014 1 1 1 5.2100 5.2093 .0007 2 0 0 4.9200 4.9275 -.0075 -1 -2 1 4.6400 4.6419 -.0019 -1 0 2 4.3600 4.3522 .0078 0 -2 1 4.1500 4.1499 .0001 0 1 2
A= 11.8429 DA= .0003 B= 11.00646 DB= .00001 C= 9.4263 DC= .0005 GAMMA= 66.794 DGAMMA= .003 BETA =107.563 DBETA = .001 ALPHA= 95.368 DALPHA= .001 V=1075.0
206. 34-0704 alfa-La2W2O9 Triklin
Dexp Dcal d(D) h k l 6.9600 6.9600 .0000 1 0 1 4.9900 4.9919 -.0019 0 2 1 4.7900 4.7916 -.0016 1 0 2 4.2500 4.2477 .0023 1 -2 1 4.1700 4.1680 .0020 0 2 2 3.5500 3.5494 .0006 1 2 2 3.4900 3.4918 -.0018 1 0 3 3.4100 3.4089 .0011 0 3 0 3.2300 3.2319 -.0019 1 -1 3 3.1700 3.1706 -.0006 0 3 2 3.1200 3.1210 -.0010 0 -3 1 3.0500 3.0492 .0008 -1 -1 3
A= 8.8719 DA= .0001 B= 10.6095 DB= .0001 C= 11.512 DC= .003 GAMMA=101.965 DGAMMA= .003 BETA = 90.91 DBETA = .01 ALPHA= 80.1980 DALPHA= .0005 V=1044.1
207. 34-0805 NH4Dy{WO4}2*3H2O Rombik Groupa 34,58
Dexp. Dcal. d(D) h k l 5.0900 5.1005 -.0105 1 1 0 3.8700 3.8644 .0056 0 1 1 3.1900 3.1893 .0007 1 1 1 2.9700 2.9694 .0006 0 4 0 2.5400 2.5398 .0002 1 3 1 1.9320 1.9322 -.0002 0 2 2 1.5900 1.5900 .0000 3 4 0 1.5100 1.5100 -.0000 1 7 1
a= 5.6478 b=11.877 c= 4.08678 da= .0003 db= .002 dc= .00008 V= 274.15
208. 34- 0877 NH4Tm{WO4}2*3H2O Tetragon Groupa 114
Dexp. Dcal. d(D) h k l 5.0900 5.1274 -.0374 1 0 1 3.9100 3.9077 .0023 2 1 0 3.1800 3.1661 .0139 0 0 2 2.9800 2.9767 .0033 1 0 2 2.5300 2.5326 -.0026 3 1 1 1.9210 1.9244 -.0034 3 2 2 1.5920 1.5917 .0003 3 2 3 1.5080 1.5071 .0009 5 1 2 1.4880 1.4884 -.0004 2 0 4
a= 8.74 c= 6.332 da= .0191 dc= .003 V= 483.5
209. 34-1358 {NH4}6Na4W12O41*18H2O Triklin
Dexp Dcal d(D) h k l 24.6000 24.5742 .0258 1 0 0 10.9000 10.6272 .2728 -2 1 0 7.4000 7.4095 -.0095 0 2 0 6.1400 6.1435 -.0035 4 0 0 5.3000 5.2930 .0070 4 1 0 4.7600 4.7598 .0002 0 0 1 4.2800 4.2806 -.0006 2 3 0 3.7300 3.7315 -.0015 3 -2 1 3.5100 3.5106 -.0006 7 0 0 3.2000 3.2000 .0000 -6 1 1 2.9400 2.9410 -.0010 7 2 0 2.7400 2.7398 .0002 -7 -1 1
A= 25.16 DA= .03 B= 15.16 DB= .04 C= 4.763 DC= .002 GAMMA=102.2 DGAMMA= .2 BETA = 92.14 DBETA = .1 ALPHA= 89.96 DALPHA= .03 V=1769.4
210. 34-1460 {NH4}7.4Na2.6W12O40*15H2O Triklin
Dexp Dcal d(D) h k l 18.1000 18.0822 .0178 0 1 0 13.3000 13.2960 .0040 1 0 0 12.1000 12.0914 .0086 -1 1 0 10.5000 10.4578 .0422 -1 0 1 8.9200 8.9259 -.0059 0 1 1 7.6300 7.5993 .0307 0 -2 1 6.5400 6.5657 -.0257 0 2 1 5.8500 5.8469 .0031 -2 2 1 5.5600 5.5720 -.0120 0 -1 2 5.2300 5.2289 .0011 -2 0 2 4.9700 4.9725 -.0025 -2 -1 2 4.2800 4.2760 .0040 1 1 2
A= 14.3777 DA= .0007 B= 18.6181 DB= .0006 C= 11.8937 DC= .0002 GAMMA=100.868 DGAMMA= .003 BETA =108.3498 DBETA = .0001 ALPHA= 94.5409 DALPHA= .0004 V=2935 |
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