== Соединения W (том 32) == |
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170. 32-0604 La2WO6 Triklin
Dexp Dcal d(D) h k l 6.3900 6.3963 -.0063 1 0 1 5.4900 5.4996 -.0096 0 1 1 4.8700 4.8732 -.0032 0 0 2 4.8000 4.8016 -.0016 -2 1 1 4.4100 4.4179 -.0079 2 -1 1 4.0400 4.0408 -.0008 -2 0 2 3.8100 3.8100 .0000 -2 -1 1 3.7600 3.7574 .0026 -2 2 0 3.7100 3.7090 .0010 2 1 0 3.6100 3.6137 -.0037 -3 1 1 3.4800 3.4789 .0011 -2 2 1 3.4100 3.4072 .0028 -2 -1 2
A= 11.229 DA= .001 B= 8.177 DB= .002 C= 10.091 DC= .001 GAMMA=108.845 DGAMMA= .002 BETA =100.183 DBETA = .005 ALPHA= 97.03 DALPHA= .01 V=847.0
171. 32-0843 K3Na6.6W12O41*22H2O Triklin
Dexp Dcal d(D) h k l 13.7000 13.7385 -.0385 0 1 1 12.8000 12.7991 .0009 0 -1 1 11.3000 11.2699 .0301 1 1 0 10.9000 10.8816 .0184 1 0 1 9.8000 9.8088 -.0088 -1 1 0 8.4000 8.4000 .0000 -1 1 1 8.3000 8.2983 .0017 1 2 0 8.0000 7.9901 .0099 1 2 1 6.1000 6.1062 -.0062 2 0 1 5.7000 5.7044 -.0044 1 0 3 5.6000 5.6047 -.0047 -1 -3 1 5.5000 5.4972 .0028 2 1 2
A= 12.6734 DA= .0004 B= 19.7895 DB= .0004 C= 18.2829 DC= .0007 GAMMA= 80.637 DGAMMA= .001 BETA = 82.080 DBETA = .002 ALPHA= 84.742 DALPHA= .003 V=4470.7
172. 32-1003 AgDy{WO4}2 Triklin
Dexp Dcal d(D) h k l 6.4000 6.3987 .0013 1 0 0 5.8900 5.8865 .0035 0 1 0 5.3300 5.3430 -.0130 -1 0 1 4.9000 4.8985 .0015 0 -1 1 3.9400 3.9433 -.0033 1 0 1 3.7200 3.7248 -.0048 -1 -1 1 3.1900 3.1842 .0058 1 -2 0 3.0900 3.0863 .0037 0 -1 2 2.9630 2.9663 -.0033 1 -2 1 2.8800 2.8778 .0022 -1 -1 2 2.6760 2.6715 .0045 -2 0 2 2.5710 2.5706 .0004 -2 -1 1
A= 7.133 DA= .003 B= 6.444 DB= .002 C= 6.644 DC= .003 GAMMA=110.16 DGAMMA= .01 BETA =103.25 DBETA = .08 ALPHA= 97.562 DALPHA= .001 V= 271.6
173. 32-1013 AgLa{WO4} Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 4.9300 4.9273 .0027 1 1 0 3.2100 3.2107 -.0007 0 1 2 2.9500 2.9495 .0005 0 2 1 2.7110 2.7092 .0018 -2 0 2 2.3920 2.3926 -.0006 3 0 1 1.9930 1.9931 -.0001 -1 3 1 1.9100 1.9099 .0001 -1 2 3 1.7480 1.7482 -.0002 3 0 3 1.6840 1.6869 -.0029 3 1 3 1.6390 1.6424 -.0034 3 3 0 1.6000 1.5980 .0020 4 2 1 1.4830 1.4823 .0007 0 0 5
a= 7.673 b= 6.430 c= 7.4153 beta= 91.863 da=.001 db=.001 dc=.0005 dbet=.006 V= 365.7
Triklin
Dexp Dcal d(D) h k l 4.9300 4.9301 -.0001 -1 0 1 3.2100 3.2100 .0000 2 1 1 2.9500 2.9499 .0001 -2 -1 1 2.7110 2.7107 .0003 -1 -1 2 2.3920 2.3922 -.0002 2 2 0 1.9930 1.9928 .0002 4 1 0 1.9100 1.9105 -.0005 -2 -2 2 1.7480 1.7477 .0003 2 3 0 1.6840 1.6841 -.0001 -3 -2 2 1.6390 1.6389 .0001 1 1 4 1.6000 1.5993 .0007 -3 2 2 1.4830 1.4827 .0003 0 -3 3
A= 8.494 DA= .005 B= 5.665 DB= .002 C= 6.9281 DC= .0007 GAMMA= 87.90 DGAMMA= .03 BETA = 81.00 DBETA = .01 ALPHA= 91.97 DALPHA= .02 V= 328.8
174. 32-1030 Ag2W2O7 Triklin
Dexp Dcal d(D) h k l 6.5200 6.5167 .0033 0 1 2 5.7700 5.7657 .0043 0 -1 2 4.5500 4.5515 -.0015 -1 0 2 3.7000 3.7010 -.0010 1 -1 4 3.2900 3.2882 .0018 1 1 5 3.0900 3.0924 -.0024 2 0 4 2.9860 2.9846 .0014 2 1 0 2.9700 2.9703 -.0003 0 3 0 2.9190 2.9139 .0051 1 0 6 2.8240 2.8228 .0012 2 0 5 2.7560 2.7567 -.0007 -1 2 4 2.6730 2.6717 .0013 -1 1 5
A= 6.9506 DA= .0005 B= 9.007 DB= .003 C= 17.692 DC= .001 GAMMA= 94.63 DGAMMA= .01 BETA = 72.77 DBETA = .01 ALPHA= 84.708 DALPHA= .002 V=1046.4
175. 32-1064 NaCr{WO4}2 Triklin
Dexp Dcal d(D) h k l 5.7200 5.7088 .0112 1 1 0 4.9300 4.9300 .0000 0 0 1 3.9100 3.9084 .0016 0 -2 1 3.7300 3.7307 -.0007 2 -1 1 2.9780 2.9780 .0000 -3 2 0 2.8540 2.8544 -.0004 2 2 0 2.4650 2.4650 .0000 0 0 2 2.2590 2.2622 -.0032 3 2 0 2.2090 2.2091 -.0001 -2 -3 1 2.0540 2.0534 .0006 3 -3 2 1.9690 1.9702 -.0012 2 -5 1 1.9030 1.9029 .0001 3 3 0
A= 9.69325 DA= .00000 B= 9.954 DB= .004 C= 5.1517 DC= .0003 GAMMA=108.024 DGAMMA= .006 BETA = 83.22 DBETA = .04 ALPHA=106.78 DALPHA= .01 V=452.8
176. 32-1185 Na2W2O7 Triklin
Dexp Dcal d(D) h k l 7.3100 7.2991 .0109 0 0 1 5.9700 5.9680 .0020 0 1 1 5.5300 5.5290 .0010 0 -1 1 4.7300 4.7227 .0073 -1 -1 1 4.6500 4.6436 .0064 2 0 1 3.8000 3.7962 .0038 -1 2 1 3.6900 3.6887 .0013 -2 -1 1 3.2500 3.2499 .0001 -1 1 2 3.1400 3.1406 -.0006 -3 0 1 3.0890 3.0917 -.0027 0 3 0 3.0240 3.0217 .0023 -1 3 0 2.9840 2.9840 .0000 0 2 2
A= 11.0777 DA= .0002 B= 9.3149 DB= .0005 C= 7.3629 DC= .0008 GAMMA= 92.818 DGAMMA= .006 BETA = 83.938 DBETA = .004 ALPHA= 85.8357 DALPHA= .0005 V=752.3
177. 32-1186 Na2W2O7 Triklin
Dexp Dcal d(D) h k l 7.3600 7.3725 -.0125 -1 1 0 5.9500 5.9468 .0032 1 1 0 5.5200 5.5132 .0068 1 0 1 4.7300 4.7263 .0037 -1 0 1 4.6200 4.6282 -.0082 2 0 1 3.8600 3.8616 -.0016 0 2 0 3.7800 3.7806 -.0006 2 1 1 3.6800 3.6776 .0024 -2 1 1 3.2400 3.2407 -.0007 -1 2 1 3.1600 3.1556 .0044 -2 -1 1 3.1500 3.1511 -.0011 2 -2 1 3.1300 3.1286 .0014 -4 1 0
A= 12.933 DA= .003 B= 7.9489 DB= .0009 C= 5.689 DC= .001 GAMMA=103.06 DGAMMA= .01 BETA = 78.900 DBETA = .003 ALPHA= 88.53876 DALPHA= .00602 V=557.6
178. 32-1187 Na2W2O7 Triklin
Dexp Dcal d(D) h k l 8.4800 8.4501 .0299 0 1 1 7.6000 7.5845 .0155 0 -1 1 5.6600 5.6690 -.0090 1 1 0 4.8300 4.8258 .0042 -1 1 0 4.3500 4.3485 .0015 1 2 0 4.1400 4.1447 -.0047 0 0 3 3.8500 3.8480 .0020 1 2 2 3.5500 3.5507 -.0007 1 0 3 3.2900 3.2921 -.0021 1 3 1 3.1800 3.1819 -.0019 0 3 2 3.1200 3.1193 .0007 -1 1 3 3.0700 3.0721 -.0021 0 1 4
A= 6.1367 DA= .00080 B= 10.67974 DB= .00004 C= 12.5798 DC= .0007 GAMMA= 78.732 DGAMMA= .003 BETA = 83.932 DBETA = .004 ALPHA= 82.69 DALPHA= .01 V=799.1
179. 32-1313 TlIn{WO4} Triklin
Dexp. Dcal. d(D) h k l 4.1700 4.1697 .0003 1 -2 0 4.0400 4.0401 -.0001 -3 -1 0 3.7700 3.7674 .0026 3 0 0 3.4500 3.4501 -.0001 0 -3 0 3.2100 3.2099 .0001 1 0 1 3.1800 3.1799 .0001 -3 -3 0 2.9800 2.9777 .0023 -2 0 1 2.8500 2.8499 .0001 2 0 1 2.6500 2.6512 -.0012 2 -1 1 2.6100 2.6112 -.0012 -1 2 1 2.5600 2.5618 -.0018 2 -3 0 2.1030 2.1043 -.0013 0 -4 1
A= 12.1508 DA= .0002 B= 11.125 DB= .001 C= 3.4092 DC= .0002 GAMMA= 68.65 DGAMMA= .01 BETA = 94.06 DBETA = .01 ALPHA= 93.86 DALPHA= .02 V= 427.7
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180. 32-1314 Tl3In{WO4}3 Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.6800 3.6644 .0156 -1 1 1 3.5600 3.5608 -.0008 -2 1 1 3.3900 3.3906 -.0006 -3 1 1 3.0700 3.0700 -.0000 2 1 2 2.9600 2.9619 -.0019 1 0 4 2.7300 2.7315 -.0015 6 1 0 2.6100 2.6108 -.0008 -9 0 1 2.5800 2.5765 .0035 9 0 0 2.3800 2.3812 -.0012 7 0 3 2.3200 2.3189 .0011 10 0 0 2.3000 2.2991 .0009 -10 0 2 2.2400 2.2400 .0000 -6 0 5
a= 23.5200 b= 3.8610 c= 12.380 beta= 99.624 da= .0009 db=.0001 dc=.001 dbet=.001 V= 1108.4
Triklin
Dexp. Dcal. d(D) h k l 3.6800 3.6785 .0015 -2 -1 0 3.5600 3.5611 -.0011 1 -1 1 3.3900 3.3902 -.0002 1 -3 0 3.0700 3.0659 .0041 2 -1 1 2.9600 2.9601 -.0001 2 -3 0 2.9600 2.9587 .0013 2 0 1 2.7300 2.7300 .0000 3 -2 0 2.6100 2.6070 .0030 -3 -1 0 2.6100 2.6119 -.0019 1 2 1 2.5800 2.5799 .0001 1 -4 0 2.5800 2.5823 -.0023 -2 0 1 2.3800 2.3794 .0006 -1 -3 1
A= 8.854 DA= .001 B= 10.546 DB= .001 C= 3.695 DC= .001 GAMMA=103.18 DGAMMA= .02 BETA = 80.04 DBETA = .02 ALPHA=100.56 DALPHA= .01 V= 327.1
181. 32-1317 TlLa{WO4}2 Triklin
Dexp Dcal d(D) h k l 5.5400 5.5410 -.0010 -2 1 0 5.0700 5.0653 .0047 -1 0 1 3.7300 3.7293 .0007 1 -2 1 3.5400 3.5411 -.0011 1 2 0 3.3500 3.3520 -.0020 -2 -1 1 3.2500 3.2458 .0042 0 2 1 3.1200 3.1213 -.0013 3 -2 1 2.9300 2.9319 -.0019 2 2 0 2.7520 2.7510 .0010 0 3 0 2.7120 2.7142 -.0022 2 0 2 2.6140 2.6148 -.0008 1 1 2 2.5620 2.5613 .0007 3 -3 1
A= 12.007 DA= .001 B= 8.747 DB= .001 C= 5.9730 DC= .0006 GAMMA=108.66 DGAMMA= .04 BETA = 83.169 DBETA = .003 ALPHA= 97.15 DALPHA= .02 V=587.7
182. 32-1323 TlSm{WO4}2 Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.3800 3.3810 -.0010 2 1 0 3.2900 3.2953 -.0053 1 1 2 3.1000 3.0987 .0013 2 1 1 2.9300 2.9291 .0009 0 2 2 2.7190 2.7173 .0017 0 3 0 2.5530 2.5520 .0010 1 3 0 2.4320 2.4331 -.0011 1 3 1 2.3120 2.3125 -.0005 0 2 3 2.2010 2.2002 .0008 -2 1 3 2.1220 2.1223 -.0003 2 1 3 2.0700 2.0699 .0001 -3 2 1 1.9800 1.9808 -.0008 0 4 1
a= 7.4373 b= 8.152 c= 8.4312 beta= 92.30 da=.0002 db=.002 dc=.0008 dbeta=.01 V= 510.7
183. 32-1325 TlSc{WO4}2 Monoklin Grupa 3
Dexp Dcal d(D) h k l 4.3400 4.3394 .0006 0 0 4 4.2500 4.2506 -.0006 2 1 0 3.6400 3.6391 .0009 -3 0 3 3.3000 3.2989 .0011 -3 1 2 3.0600 3.0595 .0005 0 2 0 3.0000 2.9998 .0002 -4 0 2 2.8830 2.8855 -.0025 0 2 2 2.6950 2.6935 .0015 -4 1 2 2.4920 2.4926 -.0006 -4 1 4 2.3650 2.3653 -.0003 3 0 5 2.2960 2.2953 .0007 0 2 5 2.2300 2.2300 -.0000 4 0 4
a= 12.0990 b= 6.119 c= 17.7700 beta= 102.364 da= .0007 db=.002 dc= .0001 dbet= .003 V= 1285.0
184. 32-1326 TlSc{WO4}2 Triklin
Dexp Dcal d(D) h k l 5.6900 5.6893 .0007 0 1 0 4.5800 4.5790 .0010 -1 1 1 4.2400 4.2405 -.0005 0 -1 2 4.0900 4.0878 .0022 1 -1 1 3.8000 3.7995 .0005 -1 1 3 3.4800 3.4787 .0013 0 1 4 3.4400 3.4405 -.0005 2 0 2 3.1900 3.1905 -.0005 -2 -1 2 3.1300 3.1299 .0001 1 1 4 2.9600 2.9611 -.0011 0 -1 4 2.9200 2.9279 -.0079 0 1 5 2.8300 2.8315 -.0015 0 2 2
A= 8.3297 DA= .0007 B= 5.789 DB= .003 C= 15.754 DC= .005 GAMMA= 86.01 DGAMMA= .02 BETA = 97.06 DBETA = .01 ALPHA= 80.695 DALPHA= .007 V=741.0
185. 32-1389 W2F9NO3 Monoklin Grupa 3
Dexp Dcal d(D) h k l 5.3700 5.3726 -.0026 1 1 0 5.0000 4.9977 .0023 -2 0 1 3.8600 3.8597 .0003 3 0 0 3.6000 3.5972 .0028 -1 1 3 3.4900 3.4884 .0016 1 0 5 2.7900 2.7889 .0011 -3 1 2 2.7300 2.7230 .0070 4 1 2 2.6730 2.6729 .0001 4 1 3 2.5610 2.5619 -.0009 4 1 4 2.4790 2.4807 -.0017 2 0 7 2.4150 2.4124 .0026 4 0 6 2.3780 2.3780 .0000 3 0 7
a= 12.198 b= 6.065 c= 17.4500 beta= 71.66 da= .001 db=.003 dc=.0001 dbet=.01 V= 1225.5
186. 32-1394 WO3 Triklin
Dexp Dcal d(D) h k l 3.8300 3.8316 -.0016 0 1 1 3.4300 3.4305 -.0005 0 -1 1 3.1600 3.1612 -.0012 -1 0 1 2.7000 2.7001 -.0001 0 0 2 2.5600 2.5593 .0007 -1 -1 1 2.1800 2.1785 .0015 -1 0 2 2.0400 2.0390 .0010 1 2 1 1.9400 1.9370 .0030 1 -2 1 1.8300 1.8332 -.0032 2 -1 1 1.7200 1.7199 .0001 2 0 2 1.6500 1.6500 .0000 2 1 2 1.5400 1.5397 .0003 -2 1 2
A= 4.1683 DA= .0006 B= 4.895 DB= .002 C= 5.454 DC= .001 GAMMA= 90.57 DGAMMA= .02 BETA = 85.10 DBETA = .02 ALPHA= 83.72 DALPHA= .04 V= 110.2
187. 32-1446 Y2{ReO4}3{WO4}3 Triklin
Dexp Dcal d(D) h k l 5.0700 5.0669 .0031 0 1 2 4.6700 4.6478 .0222 0 2 0 4.4700 4.4583 .0117 2 0 0 3.9700 3.9592 .0108 0 -1 2 3.8300 3.8308 -.0008 -2 -1 1 3.7800 3.7813 -.0013 -1 2 0 3.7000 3.7023 -.0023 -2 1 0 3.6300 3.6306 -.0006 2 1 2 3.5800 3.5839 -.0039 -2 1 1 3.4100 3.4088 .0012 -1 2 2 3.2900 3.2890 .0010 -2 0 2 3.1600 3.1602 -.0002 1 3 0
A= 9.20616 DA= .00000 B= 10.02328 DB= .00002 C= 10.52512 DC= .00003 GAMMA= 75.6716 DGAMMA= .0002 BETA = 84.3141 DBETA = .0001 ALPHA= 72.3329 DALPHA= .0001 V=896.6
188. 32-1447 Y2{ReO4}4{WO4} Triklin
Dexp Dcal d(D) h k l 10.1000 10.1558 -.0558 0 -1 1 5.8700 5.8686 .0014 0 -3 1 5.2800 5.2745 .0055 1 0 0 5.1100 5.1133 -.0033 0 0 2 4.5600 4.5529 .0071 0 -4 1 4.2700 4.2667 .0033 -1 -1 2 4.1900 4.1831 .0069 -1 0 2 4.1100 4.1077 .0023 1 -2 1 4.0500 4.0507 -.0007 1 1 1 4.0000 4.0008 -.0008 -1 3 0 3.9300 3.9300 .0000 0 -4 2 3.7400 3.7418 -.0018 1 -3 1
A= 5.423 DA= .001 B= 18.465 DB= .001 C= 10.933 DC= .001 GAMMA= 88.1049 DGAMMA= .0004 BETA =103.30 DBETA = .03 ALPHA=106.04 DALPHA= .02 V=1024.2 |
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