== Соединения W (томa 22-27) == |
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70. 22-0203 Cs11{WO3}5F11*5H2O Triklin
Dexp Dcal d(D) h k l 5.9100 5.9106 -.0006 -1 0 1 5.2900 5.2890 .0010 -1 1 0 4.5900 4.5897 .0003 1 -1 2 3.7200 3.7175 .0025 2 -1 2 3.6500 3.6492 .0008 -2 1 0 3.4000 3.4000 .0000 1 -2 1 3.3000 3.3075 -.0075 0 0 3 3.2400 3.2393 .0007 1 -2 2 3.0400 3.0405 -.0005 -2 -2 1 2.8590 2.8593 -.0003 2 1 3 2.6430 2.6445 -.0015 2 -2 0 2.4910 2.4915 -.0005 4 0 1
A= 10.090 DA= .002 B= 7.588 DB= .001 C= 10.789 DC= .003 GAMMA= 83.38 DGAMMA= .05 BETA = 72.31 DBETA = .02 ALPHA=102.23 DALPHA= .05 V= 754.7
71. 22-0694 LiY5W8O32 Triklin
Dexp Dcal d(D) h k l 5.5500 5.5488 .0012 -1 1 1 5.3600 5.3647 -.0047 0 -1 2 4.9900 4.9901 -.0001 0 0 2 4.6000 4.5904 .0096 1 -2 1 4.2600 4.2580 .0020 -2 1 1 4.0900 4.0805 .0095 1 1 1 3.9800 3.9811 -.0011 1 -2 2 3.8500 3.8561 -.0061 -1 1 2 3.7800 3.7807 -.0007 -2 -1 1 3.7300 3.7303 -.0003 2 -2 1 3.1600 3.1586 .0014 1 -3 1 3.1300 3.1289 .0011 -3 1 1
A= 9.6641 DA= .0001 B= 9.520 DB= .003 C= 11.0211 DC= .0008 GAMMA=105.13 DGAMMA= .01 BETA = 96.65 DBETA = .03 ALPHA=111.347 DALPHA= .002 V=886.4
72. 22-0836 beta-KNdW2O8 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 6.5400 6.5406 -.0006 0 1 1 6.0900 6.0872 .0028 1 1 1 5.0500 5.0443 .0057 -1 0 1 4.1100 4.1097 .0003 0 1 2 4.0300 4.0301 -.0001 2 1 1 3.6900 3.6918 -.0018 2 1 0 3.2700 3.2703 -.0003 0 2 2 3.2300 3.2298 .0002 2 2 1 3.2000 3.2005 -.0005 -2 0 1 3.0500 3.0500 -.0000 0 0 3 3.0300 3.0281 .0019 -2 1 1
a= 8.932 b= 9.353 c= 10.170 beta= 64.11 da= .001 db=.002 dc= .001 dbet=.01 V= 764.4
73. 23-0710 WOCl2 Triklin
Dexp Dcal d(D) h k l 6.7800 6.7879 -.0079 0 1 1 6.1400 6.1387 .0013 -1 1 0 4.5700 4.5688 .0012 0 -1 1 3.6200 3.6185 .0015 0 0 2 3.1800 3.1799 .0001 1 -2 1 3.0800 3.0839 -.0039 -2 1 1 2.8140 2.8116 .0024 -1 3 0 2.5540 2.5550 -.0010 -2 3 1 2.2820 2.2844 -.0024 0 -2 2 2.1660 2.1658 .0002 3 0 0 2.1180 2.1179 .0001 0 4 2 2.0580 2.0586 -.0006 1 3 3
A= 6.9001 DA= .0003 B= 9.0201 DB= .0003 C= 7.827 DC= .002 GAMMA=107.17 DGAMMA= .02 BETA = 87.16 DBETA = .02 ALPHA= 69.747 DALPHA= .005 V= 430.4
74. 23-1330 KErW2O8 Monoklin Grupa 14
Dexp Dcal d(D) h k l 5.7900 5.8030 -.0130 1 1 0 5.2800 5.2811 -.0011 -1 1 1 4.8700 4.8582 .0118 -1 0 2 4.0000 3.9989 .0011 1 0 2 3.8700 3.8678 .0022 0 1 2 4.0000 3.9989 .0011 1 0 2 3.8700 3.8678 .0022 0 1 2 3.6000 3.5971 .0029 -2 1 2 3.3900 3.3908 -.0008 -3 1 1 3.3200 3.3168 .0032 3 1 0 3.1400 3.1312 .0088 -1 2 1 3.0700 3.0794 -.0094 -3 1 2
a= 11.882 b= 6.7350 c= 9.8200 beta= 105.794 da= .001 db=.0004 dc= .0001 dbet= .001 V= 756.2
75. 23-1451 WOCl2 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 6.1500 6.1468 .0032 1 1 0 4.0000 3.9993 .0007 -1 1 1 3.6200 3.6233 -.0033 1 2 0 3.2600 3.2608 -.0008 1 2 1 3.0800 3.0809 -.0009 3 1 1 2.5400 2.5395 .0005 3 2 1 2.0900 2.0898 .0002 5 0 1 2.0100 2.0102 -.0002 5 0 0 1.8900 1.8903 -.0003 -1 0 3 1.8000 1.8003 -.0003 4 1 3 1.7000 1.6997 .0003 -1 2 3
a= 10.464 b= 7.7690 c= 6.3400 beta= 73.839 da= .001 db= .0003 dc= .0004 dbet=.005 V= 495.1
76. 23-1956 C60H20As2N6S6W Triklin
Dexp Dcal d(D) h k l 9.9700 10.0007 -.0307 0 1 1 9.2100 9.2341 -.0241 1 0 0 8.4300 8.4281 .0019 0 -1 1 7.5500 7.5457 .0043 1 0 1 7.3000 7.2823 .0177 1 1 0 7.2000 7.2168 -.0168 -1 0 1 6.8100 6.8140 -.0040 0 2 0 6.1000 6.1296 -.0296 0 0 2 5.8000 5.7952 .0048 -1 2 0 5.5000 5.4907 .0093 -1 2 1 5.1000 5.0958 .0042 1 2 1 5.0000 5.0004 -.0004 0 2 2
A= 9.2938 DA= .0005 B= 13.905 DB= .001 C= 12.44609 DC= .00007 GAMMA= 95.947 DGAMMA= .001 BETA = 88.389 DBETA = .001 ALPHA= 80.423 DALPHA= .002 V=1575.7
77. 24-0284 Cs4{MoO4}{WO4} Triklin
Dexp Dcal d(D) h k l 4.6600 4.6588 .0012 -1 1 1 4.1700 4.1721 -.0021 -2 0 1 3.5200 3.5232 -.0032 -1 -1 1 3.3900 3.3906 -.0006 -3 1 1 3.3100 3.3098 .0002 -1 2 1 3.2700 3.2712 -.0012 0 2 1 2.8500 2.8472 .0028 3 0 1 2.5900 2.5902 -.0002 -1 1 2 2.5300 2.5292 .0008 0 -2 1 2.3700 2.3694 .0006 -1 3 1 2.1400 2.1383 .0017 0 -1 2 2.1100 2.1098 .0002 2 3 0
A= 12.206 DA= .007 B= 7.242 DB= .001 C= 5.1963 DC= .0003 GAMMA= 96.73 DGAMMA= .03 BETA =101.80 DBETA = .03 ALPHA= 73.54 DALPHA= .01 V=430.2
78. 24-0480 Ho4W4O33 Triklin
Dexp Dcal d(D) h k l 3.7600 3.7585 .0015 1 1 0 3.1300 3.1332 -.0032 0 1 1 3.0200 3.0226 -.0026 0 -1 1 2.8160 2.8155 .0005 1 0 1 2.6420 2.6410 .0010 0 2 0 1.8440 1.8437 .0003 -2 -1 1 1.8040 1.8042 -.0002 -2 1 0 1.6200 1.6201 -.0001 0 3 1 1.5900 1.5903 -.0003 -1 -3 1 1.5735 1.5737 -.0002 0 -3 1 1.5663 1.5666 -.0003 0 2 2 1.5120 1.5113 .0007 0 -2 2
A= 4.32298 DA= .00006 B= 5.44947 DB= .00003 C= 3.78761 DC= .00000 GAMMA= 75.93192 DGAMMA= .00134 BETA = 89.20845 DBETA = .00145 ALPHA= 87.70296 DALPHA= .00042 V=86.48
79. 24-0663 Li2W4O13 Triklin
Dexp Dcal d(D) h k l 5.9400 5.9409 -.0009 -1 1 1 5.7900 5.7758 .0142 1 -1 1 4.3900 4.3920 -.0020 2 0 0 4.1500 4.1477 .0023 -1 -1 1 3.8600 3.8664 -.0064 -1 2 0 3.7100 3.7122 -.0022 1 1 3 3.5900 3.5893 .0007 0 2 2 3.5200 3.5180 .0020 1 -2 1 3.4800 3.4812 -.0012 -1 2 2 3.3400 3.3423 -.0023 1 -1 3 3.2200 3.2183 .0017 2 -2 1 3.1300 3.1293 .0007 0 2 3
A= 9.384 DA= .001 B= 7.953 DB= .001 C= 12.40665 DC= .00006 GAMMA=104.27 DGAMMA= .01 BETA = 78.55 DBETA = .01 ALPHA= 78.811 DALPHA= .008 V=849.9
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80. 24-0664 Li2W2O7 Triklin
Dexp Dcal d(D) h k l 6.6500 6.6385 .0115 -1 1 0 6.5100 6.5272 -.0172 0 1 1 6.0400 6.0428 -.0028 2 0 0 4.8400 4.8347 .0053 2 0 1 4.5200 4.5183 .0017 -1 1 2 4.4700 4.4607 .0093 0 0 2 3.9500 3.9542 -.0042 -3 1 1 3.8900 3.8864 .0036 -3 1 0 3.7800 3.7814 -.0014 -3 0 1 3.5700 3.5707 -.0007 3 0 1 3.5500 3.5496 .0004 -2 2 1 3.5500 3.5496 .0004 -2 2 1
A= 12.5953 DA= .0006 B= 7.489 DB= .001 C= 9.551 DC= .002 GAMMA=105.783 DGAMMA= .007 BETA = 99.444 DBETA = .007 ALPHA= 69.52 DALPHA= .01 V=810.0
81. 24-0904 K4WO5 Triklin
Dexp Dcal d(D) h k l 5.6900 5.6974 -.0074 2 0 0 5.5400 5.5317 .0083 1 1 0 5.0400 5.0365 .0035 -2 0 2 4.8200 4.8181 .0019 -1 -1 2 4.7200 4.7178 .0022 0 1 2 4.4800 4.4853 -.0053 -2 -1 1 4.3000 4.2975 .0025 -1 0 4 4.1600 4.1610 -.0010 -1 1 2 4.0400 4.0383 .0017 1 -1 2 3.7600 3.7604 -.0004 -2 -1 3 3.5800 3.5811 -.0011 1 -1 3 3.3800 3.3798 .0002 1 1 4
A= 11.76430 DA= .00004 B= 5.73266 DB= .00001 C= 17.91021 DC= .00007 GAMMA= 76.8096 DGAMMA= .0002 BETA = 96.0505 DBETA = .0003 ALPHA= 91.6819 DALPHA= .0002 V=1169.5
82. 24-0956 Na5{W6O21H}810.5H2O Triklin
Dexp Dcal d(D) h k l 12.2000 12.2035 -.0035 0 0 1 11.0000 10.9880 .0120 1 0 0 9.7000 9.7460 -.0460 0 -2 1 9.2000 9.1834 .0166 -1 2 0 8.8300 8.8292 .0008 -1 0 1 8.2600 8.2751 -.0151 -1 -1 1 7.9300 7.9325 -.0025 1 -1 1 7.5900 7.5803 .0097 0 -3 1 7.3100 7.3297 -.0197 -1 3 0 6.2200 6.2212 -.0012 0 3 1 6.2200 6.2212 -.0012 0 3 1 5.9100 5.9046 .0054 -1 4 0
A= 11.293 DA= .001 B= 25.560 DB= .004 C= 12.555 DC= .004 GAMMA=100.44 DGAMMA= .09 BETA = 96.13 DBETA = .04 ALPHA=100.772 DALPHA= .002 V=3460.4
83. 24-1147 C8F12Na2O10W Monoklin Grupa 14
Dexp Dcal d(D) h k l 12.4000 12.4021 -.0021 0 0 2 10.9000 10.9012 -.0012 1 0 2 4.2400 4.2406 -.0006 1 0 6 3.5400 3.5404 -.0004 1 1 5 2.3700 2.3702 -.0002 0 2 3
a= 15.6200 b= 4.948 c=25.4700 beta=76.862 da=.0003 db=.001 dc=.0001 dbet=.002 V= 1917.1
84. 25-0045 {NH4}10W12O41 Triklin
Dexp Dcal d(D) h k l 10.1000 10.0885 .0115 1 0 0 8.4100 8.4200 -.0100 1 1 1 7.3000 7.2921 .0079 -1 -1 1 6.5200 6.5140 .0060 -1 1 1 6.3700 6.3746 -.0046 0 0 2 5.9300 5.9318 -.0018 1 2 0 5.1200 5.1142 .0058 -2 0 1 5.0400 5.0442 -.0042 2 0 0 4.8300 4.8290 .0010 -1 -2 1 4.7000 4.6958 .0042 0 -1 2 4.3700 4.3683 .0017 -1 2 1 4.2100 4.2100 -.0000 2 2 2
A= 11.31 DA= .01 B= 12.69 DB= .01 C= 13.968 DC= .009 GAMMA= 66.55 DGAMMA= .07 BETA = 93.58 DBETA = .07 ALPHA= 69.78 DALPHA= .05 V= 1678.4
85. 25-0191 Ce2W2O9 Triklin
Dexp Dcal d(D) h k l 5.9000 5.8992 .0008 1 1 0 4.9600 4.9645 -.0045 1 1 1 4.4600 4.4647 -.0047 1 -1 1 3.5630 3.5590 .0040 2 1 0 3.3520 3.3516 .0004 0 2 0 3.2970 3.2887 .0083 2 0 2 3.1820 3.1835 -.0015 -1 -2 1 3.0160 3.0172 -.0012 -1 1 1 2.9490 2.9496 -.0006 2 2 0 2.8230 2.8237 -.0007 0 1 2 2.7890 2.7882 .0008 0 -2 2 2.6470 2.6465 .0005 1 -2 2
A= 7.8933 DA= .0003 B= 7.19376 DB= .00005 C= 7.8877 DC= .0005 GAMMA= 74.130 DGAMMA= .002 BETA = 66.086 DBETA = .003 ALPHA= 96.157 DALPHA= .004 V=381.5
86. 25-0192 Ce4W9O33 Triklin
Dexp Dcal d(D) h k l 8.3600 8.4024 -.0424 0 1 0 6.0500 6.0588 -.0088 -1 -1 1 5.2600 5.2463 .0137 0 -1 2 4.6700 4.6707 -.0007 -1 1 0 4.4400 4.4376 .0024 -1 -1 2 3.9500 3.9472 .0028 1 -1 2 3.8200 3.8264 -.0064 -1 1 1 3.6200 3.6189 .0011 0 1 2 3.5500 3.5567 -.0067 0 -1 3 3.4900 3.4904 -.0004 -2 -1 1 3.4200 3.4218 -.0018 1 2 1 3.3900 3.3862 .0038 0 2 1
A= 7.2351 DA= .0001 B= 9.6706 DB= .0002 C= 10.69945 DC= .00005 GAMMA= 72.240 DGAMMA= .003 BETA = 93.9958 DBETA = .0006 ALPHA=114.2209 DALPHA= .0008 V=649.3
87. 27-0313 MnWB Triklin
Dexp Dcal d(D) h k l 2.8150 2.8148 .0002 -4 1 0 2.7610 2.7627 -.0017 4 1 0 2.4550 2.4542 .0008 6 0 0 2.1190 2.1189 .0001 -1 2 0 2.0740 2.0736 .0004 2 0 2 1.9960 1.9977 -.0017 2 1 2 1.9710 1.9717 -.0007 -3 2 0 1.8310 1.8321 -.0011 4 2 0 1.7850 1.7838 .0012 1 -2 1 1.5760 1.5755 .0005 -4 2 2 1.5380 1.5376 .0004 -9 1 0 1.3930 1.3928 .0002 2 3 0
A= 14.7620 DA= .0001 B= 4.3426 DB= .0002 C= 4.4860 DC= .0001 GAMMA= 91.772 DGAMMA= .001 BETA = 93.905 DBETA = .001 ALPHA= 79.615 DALPHA= .004 V=282.2
88. 27-0562 Rb2WO4 Triklin
Dexp Dcal d(D) h k l 5.6810 5.6824 -.0014 0 1 1 4.6870 4.6869 .0001 -1 0 1 4.1540 4.1524 .0016 0 -1 1 3.7580 3.7580 -.0000 1 -1 1 3.4920 3.4925 -.0005 -2 0 1 3.3520 3.3574 -.0054 -1 2 0 3.2800 3.2795 .0005 -2 -1 1 3.1000 3.0982 .0018 2 2 2 2.9510 2.9509 .0001 1 0 2 2.8390 2.8379 .0011 2 3 0 2.6870 2.6856 .0014 -3 0 1 2.6590 2.6597 -.0007 4 1 0
A= 11.294 DA= .009 B= 9.556 DB= .008 C= 6.541 DC= .002 GAMMA= 63.57 DGAMMA= .02 BETA = 70.63 DBETA = .02 ALPHA= 65.29 DALPHA= .01 V= 564.9
89. 27-1314 Tl2WO2S2 Triklin
Dexp Dcal d(D) h k l 4.4800 4.4811 -.0011 -1 1 1 4.3900 4.3886 .0014 -1 -1 1 4.1700 4.1703 -.0003 -2 0 1 3.7100 3.7106 -.0006 -2 1 1 3.4800 3.4814 -.0014 0 2 1 3.3600 3.3588 .0012 -1 2 1 3.2100 3.2104 -.0004 -3 0 1 2.8900 2.8904 -.0004 0 3 0 2.8400 2.8398 .0002 3 2 0 2.6900 2.6903 -.0003 -1 3 0 2.5800 2.5798 .0002 -2 0 2 2.4400 2.4400 .0000 2 -2 1 2.3400 2.3396 .0004 -2 3 1
A= 10.4901 DA= .0008 B= 8.757 DB= .002 C= 5.35957 DC= .00002 GAMMA= 83.778 DGAMMA= .002 BETA =103.84 DBETA = .02 ALPHA= 86.577 DALPHA= .007 V= 473.4 |
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