== Соединения W (томa 15-18) == |
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19. 15-0017 Y6WO12 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 6.4100 6.3881 .0219 1 0 1 6.2800 6.2849 -.0049 1 1 0 4.0700 4.0656 .0044 2 0 1 3.8500 3.8570 -.0070 1 2 1 3.7800 3.7811 -.0011 1 0 2 3.1100 3.1126 -.0026 2 2 1 3.0300 3.0331 -.0031 2 1 2 2.8200 2.8197 .0003 3 0 1 2.6300 2.6321 -.0021 -1 2 2 2.2740 2.2723 .0017 1 2 3 2.2470 2.2468 .0002 3 2 2 2.0880 2.0878 .0002 2 4 0
a= 8.526 b= 9.677 c=7.735 beta= 75.786 da= .001 db=.001 dc=.001 dbet= .008 V= 618.6
20. 15-0090 Ba5CaW2O12 Triklin
Dexp Dcal d(D) h k l 4.9000 4.8985 .0015 1 1 0 3.0700 3.0702 -.0002 3 1 0 2.9900 2.9871 .0029 0 1 1 2.6000 2.6013 -.0013 2 1 1 2.5400 2.5406 -.0006 -3 0 1 2.4300 2.4279 .0021 -2 -1 1 2.1600 2.1578 .0022 4 -1 1 2.1100 2.1101 -.0001 5 1 0 1.9300 1.9299 .0001 4 2 0 1.7600 1.7583 .0017 -3 -2 1 1.7200 1.7201 -.0001 6 -1 1 1.6200 1.6201 -.0001 -4 3 1
A= 12.369 DA= .003 B= 5.919 DB= .003 C= 3.317 DC= .005 GAMMA=100.46 DGAMMA= .02 BETA = 89.98 DBETA = .03 ALPHA= 85.00 DALPHA= .09 V= 237.9
21. 15-0176 Ba2WO5 Triklin
Dexp Dcal d(D) h k l 3.5000 3.4987 .0013 -2 -1 1 3.3200 3.3177 .0023 2 -1 1 3.1600 3.1612 -.0012 0 2 0 3.0700 3.0718 -.0018 -2 1 1 2.9700 2.9682 .0018 3 0 0 2.8400 2.8356 .0044 0 2 2 2.7200 2.7211 -.0011 0 0 4 2.6400 2.6417 -.0017 0 -2 2 2.4000 2.3986 .0014 -2 -1 3 2.2600 2.2598 .0002 4 0 2 2.2100 2.2100 .0000 1 1 5 2.1800 2.1796 .0004 2 1 5
A= 9.430 DA= .002 B= 6.520 DB= .002 C= 11.3211 DC= .0006 GAMMA= 76.63 DGAMMA= .03 BETA = 74.72 DBETA = .02 ALPHA= 82.11 DALPHA= .01 V=651.1
22. 15-0240 Ba3WO6 Rombik Groupa 19
Dexp. Dcal. d(D) h k l 3.0500 3.0587 -.0087 2 0 0 2.5800 2.5901 -.0101 2 1 0 2.1500 2.1524 -.0024 0 1 2 1.7600 1.7602 -.0002 2 1 2 1.6500 1.6460 .0040 1 2 2 1.5200 1.5198 .0002 0 1 3 1.4600 1.4591 .0009 4 1 0 1.3600 1.3610 -.0010 2 1 3 1.3100 1.3098 .0002 3 2 2 1.2700 1.2699 .0001 3 3 0 1.2300 1.2307 -.0007 2 3 2 1.2000 1.1998 .0002 0 0 4
a= 6.11743 b= 4.87 c= 4.799 da= .00005 db= .01 dc= .001 V= 142.9
23. 15-0437 Sc2W3O12 Triklin
Dexp Dcal d(D) h k l 6.5000 6.5023 -.0023 0 1 1 5.9200 5.9164 .0036 0 -1 1 4.6700 4.6664 .0036 -1 0 2 4.4600 4.4568 .0032 0 0 2 4.2200 4.2243 -.0043 -1 1 2 4.0200 4.0237 -.0037 0 2 1 3.9800 3.9886 -.0086 -1 -1 2 3.8400 3.8421 -.0021 2 0 0 3.6600 3.6554 .0046 -1 -2 1 3.5700 3.5749 -.0049 2 1 0 3.3600 3.3589 .0011 1 0 2 3.2800 3.2756 .0044 -1 2 2
A= 8.257 DA= .001 B= 8.639 DB= .002 C= 9.609 DC= .009 GAMMA= 89.056 DGAMMA= .008 BETA =111.30 DBETA = .01 ALPHA= 85.317 DALPHA= .002 V=635.9
24. 15-0447 Y2W3O12 Triklin
Dexp Dcal d(D) h k l 6.7500 6.7397 .0103 -1 1 1 6.2300 6.2400 -.0100 1 -1 1 4.7400 4.7402 -.0002 2 0 0 4.6200 4.6204 -.0004 -2 2 0 4.3700 4.3684 .0016 0 1 2 4.2500 4.2519 -.0019 -2 2 1 4.1900 4.1874 .0026 -2 0 1 4.1100 4.1069 .0031 1 0 2 4.0600 4.0651 -.0051 0 -1 2 3.8100 3.8087 .0013 -1 2 2 3.7500 3.7486 .0014 0 3 0 3.7200 3.7250 -.0050 0 2 2
A= 10.3035 DA= .0006 B= 12.2879 DB= .0002 C= 9.1313 DC= .0001 GAMMA=113.0620 DGAMMA= .0005 BETA = 92.012 DBETA = .005 ALPHA= 83.755 DALPHA= .004 V=1057.4
25. 15-0473 Y6W3O15 Monoklin Grupa 3
Dexp Dcal d(D) h k l 4.4600 4.4610 -.0010 2 1 0 4.2200 4.2178 .0022 -2 0 2 3.7200 3.7220 -.0020 0 2 0 3.4000 3.4053 -.0053 -1 2 1 3.0600 3.0587 .0013 -2 1 3 2.7900 2.7908 -.0008 -2 2 2 2.6500 2.6521 -.0021 3 0 3 2.6300 2.6304 -.0004 -3 1 3 2.5000 2.4983 .0017 3 1 3 2.4790 2.4813 -.0023 0 3 0 2.2630 2.2626 .0004 -2 0 5 2.2360 2.2375 -.0015 -2 3 1
a= 11.1640 b= 7.444 c= 12.0820 beta= 93.354 da= .0009 db= .001 dc=.0002 dbet= .004 V= 1002.3
Triklin
Dexp Dcal d(D) h k l 4.4600 4.4675 -.0075 0 -1 2 4.2200 4.2121 .0079 0 1 2 3.7200 3.7221 -.0021 -2 1 0 3.4000 3.4009 -.0009 2 -1 2 3.0600 3.0589 .0011 2 0 2 2.7900 2.7884 .0016 1 1 3 2.6500 2.6503 -.0003 2 1 0 2.6300 2.6309 -.0009 -2 3 0 2.5000 2.4981 .0019 3 -1 1 2.4790 2.4776 .0014 2 1 2 2.2630 2.2638 -.0008 2 0 4 2.2360 2.2375 -.0015 2 1 3
A= 7.6126 DA= .0005 B= 8.438 DB= .002 C= 10.8874 DC= .0006 GAMMA=117.158 DGAMMA= .004 BETA = 77.9395 DBETA = .0002 ALPHA= 98.61 DALPHA= .01 V=607.6
26. 15-0494 Na2W4O13 Monoklin Grupa 4, 11
Dexp Dcal d(D) h k l 8.1100 8.0658 .0442 -1 0 1 6.1200 6.1061 .0139 1 1 0 5.4600 5.4544 .0056 -1 1 1 4.0600 4.0658 -.0058 1 1 2 3.7800 3.7755 .0045 2 0 2 3.6200 3.6224 -.0024 -1 0 3 3.4820 3.4770 .0050 1 0 3 3.1480 3.1473 .0007 1 1 3 3.0550 3.0531 .0019 2 2 0 2.8780 2.8813 -.0033 -3 1 2 2.7280 2.7272 .0008 -2 2 2 2.7280 2.7272 .0008 -2 2 2 2.5900 2.5891 .0009 -1 2 3
a= 10.820 b= 7.404 c= 11.2926 beta= 93.774 da= .001 db=.001 dc=.0003 dbet=.004 V= 902.7
Triklin Na2W4O13
Dexp Dcal d(D) h k l 8.1100 8.1176 -.0076 1 0 0 6.1200 6.1138 .0062 1 1 0 5.4600 5.4564 .0036 1 1 1 4.0600 4.0588 .0012 2 0 0 3.7800 3.7835 -.0035 -1 1 1 3.6200 3.6208 -.0008 1 1 2 3.4820 3.4842 -.0022 0 2 0 3.1480 3.1468 .0012 2 -1 1 3.0550 3.0569 -.0019 2 2 0 2.8780 2.8789 -.0009 -1 -1 2 2.7280 2.7282 -.0002 2 2 2 2.5900 2.5892 .0008 1 0 3
A= 8.800 DA= .004 B= 7.2694 DB= .0001 C= 7.839 DC= .004 GAMMA= 73.72 DMMA= .01 BETA = 72.56 DBETA = .05 ALPHA= 82.47 DALPHA= .03 V=458.7
27. 15-0709 K2W4O13 Triklin
Dexp Dcal d(D) h k l 6.3200 6.3102 .0098 -1 1 0 3.8140 3.8161 -.0021 -1 0 2 3.6300 3.6274 .0026 0 -1 2 3.2580 3.2577 .0003 0 2 0 3.1560 3.1551 .0009 -2 2 0 2.9950 2.9938 .0011 -2 1 2 2.7690 2.7644 .0046 -1 2 2 2.6340 2.6323 .0017 -2 2 2 2.4330 2.4329 .0001 -3 1 0 2.3070 2.3101 -.0031 -2 -1 2 2.1100 2.1120 -.0020 -2 3 2 2.0270 2.0283 -.0013 0 2 3
A= 7.474 DA= .002 B= 7.363 DB= .002 C= 8.415 DC= .001 GAMMA=117.423 DGAMMA= .005 BETA = 99.15 DBETA = .02 ALPHA= 89.795 DALPHA= .007 V=405.2 |
28. 16-0660 Ba2MgWO6 Triklin
Dexp Dcal d(D) h k l 4.6300 4.6395 -.0095 1 1 0 2.8400 2.8398 .0002 1 2 0 2.4200 2.4204 -.0004 -1 -2 1 2.3200 2.3197 .0003 2 2 0 2.0100 2.0111 -.0011 0 2 2 1.8440 1.8448 -.0008 1 3 1 1.6420 1.6419 .0001 0 3 2 1.5470 1.5470 .0000 -1 2 3 1.4230 1.4231 -.0001 0 -1 3 1.3610 1.3611 -.0001 -1 4 1 1.2740 1.2737 .0003 -4 2 2 1.2290 1.2291 -.0001 -2 4 1
A= 6.343 DA= .001 B= 5.9108 DB= .0006 C= 5.1127 DC= .0001 GAMMA= 79.482 DGAMMA= .003 BETA =111.83 DBETA = .01 ALPHA= 83.246 DALPHA= .003 V= 171.3
29. 17-0261 WCl2 Triklin
Dexp Dcal d(D) h k l 6.9400 6.9283 .0117 0 1 0 5.6300 5.6300 .0000 1 0 0 3.4700 3.4703 -.0003 0 -1 2 2.8800 2.8816 -.0016 1 0 2 2.6100 2.6105 -.0005 -2 -1 2 2.5200 2.5209 -.0009 2 0 1 2.3700 2.3694 .0006 2 2 1 2.3200 2.3206 -.0006 -2 1 0 2.2000 2.2003 -.0003 -2 -3 2 2.0900 2.0902 -.0002 0 3 1 2.0500 2.0503 -.0003 -3 -2 1 2.0000 2.0003 -.0003 -1 -3 3
A= 6.216 DA= .002 B= 7.726 DB= .003 C= 7.5005 DC= .0006 GAMMA= 65.84 DGAMMA= .01 BETA =102.08 DBETA = .03 ALPHA=104.49 DALPHA= .04 V= 315.9
30. 17-0262 WBr2 Rombik Groupa 16
Dexp. Dcal. d(D) h k l 7.3100 7.3362 -.0262 1 1 0 5.9100 5.9032 .0068 0 1 1 3.6300 3.6316 -.0016 3 0 0 2.7200 2.7218 -.0018 3 2 1 2.6400 2.6385 .0015 2 3 1 2.4800 2.4808 -.0008 0 4 0 2.4600 2.4576 .0024 0 3 2 2.4200 2.4189 .0011 1 4 0 2.3000 2.2975 .0025 1 4 1 2.1800 2.1789 .0011 5 0 0 2.1500 2.1521 -.0021 1 2 3 2.0900 2.0889 .0011 5 0 1
a=10.894 b= 9.923 c= 7.344 da= .002 db= .005 dc= .002 v= 793.9
31. 17-0615 Na2O*xWO3*xH2O Triklin
Dexp Dcal d(D) h k l 5.9600 5.9538 .0062 -1 0 1 3.7800 3.7808 -.0008 -1 -2 1 3.7400 3.7389 .0011 -1 0 2 3.6700 3.6747 -.0047 0 -2 1 3.4400 3.4405 -.0005 0 -1 2 3.2900 3.2911 -.0011 0 2 1 3.1000 3.0987 .0013 -1 -2 2 2.9700 2.9708 -.0008 -2 -2 1 2.5690 2.5667 .0023 2 1 1 2.3560 2.3559 .0001 -3 -1 1 2.0950 2.0944 .0006 -3 1 1 1.9760 1.9755 .0005 0 -4 1
A= 7.1102 DA= .0001 B= 8.2011 DB= .0002 C= 7.8164 DC= .0003 GAMMA= 76.898 DGAMMA= .001 BETA =112.200 DBETA = .002 ALPHA=101.7022 DALPHA= .0009 V=407.5
32. 17-0616 Na2{WO3*0.5H2O}x Triklin
Dexp Dcal d(D) h k l 6.4000 6.4011 -.0011 1 2 0 4.9500 4.9529 -.0029 1 3 0 3.9000 3.9017 -.0017 0 -3 1 3.6900 3.6888 .0012 2 2 1 3.6800 3.6808 -.0008 2 3 0 3.6700 3.6715 -.0015 0 5 0 3.3200 3.3190 .0010 2 3 1 3.1800 3.1799 .0001 3 -2 1 2.6740 2.6740 -.0000 1 0 2 2.4630 2.4626 .0004 -3 6 0 2.1110 2.1112 -.0002 5 -1 1 2.0420 2.0418 .0002 3 4 2
A= 10.6934 DA= .0007 B= 18.54922 DB= .00006 C= 5.3483 DC= .0003 GAMMA= 98.097 DGAMMA= .005 BETA = 75.8770 DBETA = .0009 ALPHA= 90.423 DALPHA= .002 V=1018.1
33. 18-0072 2Al2O3.5WO3 Triklin
Dexp Dcal d(D) h k l 6.2700 6.2778 -.0078 1 -1 1 5.7000 5.7017 -.0017 0 2 0 4.5100 4.5113 -.0013 0 2 2 4.4900 4.4884 .0016 2 1 1 4.2800 4.2788 .0012 2 -1 1 4.0500 4.0488 .0012 -2 1 1 3.8600 3.8585 .0015 1 1 3 3.8500 3.8511 -.0011 1 0 3 3.8000 3.8012 -.0012 0 3 0 3.6900 3.6907 -.0007 -2 2 0 3.6700 3.6717 -.0017 2 2 0 3.5100 3.5093 .0007 -2 2 1
A= 9.77939 DA= .00002 B= 11.59484 DB= .00001 C= 12.08852 DC= .00000 GAMMA= 88.55956 DGAMMA= .00003 BETA = 80.35153 DBETA = .00009 ALPHA= 79.58574 DALPHA= .00001 V=1329.3
34. 18-1416 WNCl3 Triklin
Dexp Dcal d(D) h k l 8.3400 8.3426 -.0026 1 1 0 6.3200 6.3199 .0001 0 1 1 5.6800 5.6797 .0003 0 -1 1 5.0400 5.0393 .0007 0 2 1 4.7200 4.7155 .0045 2 0 0 4.3900 4.3867 .0033 0 3 0 4.0400 4.0291 .0109 2 0 1 3.6200 3.6205 -.0005 -2 -1 1 3.2800 3.2786 .0014 1 4 0 3.1200 3.1203 -.0003 0 4 1 2.9200 2.9206 -.0006 2 1 2 2.7800 2.7809 -.0009 3 3 0
A= 9.62255 DA= .00000 B= 13.49157 DB= .00000 C= 6.80725 DC= .00000 GAMMA= 79.73351 DGAMMA= .00002 BETA = 83.52422 DBETA = .00001 ALPHA= 81.45367 DALPHA= .00001 V=856.4
35. 18-1419 WO3*2H2O Triklin
Dexp Dcal d(D) h k l 6.8000 6.8004 -.0004 1 0 0 3.6700 3.6660 .0040 0 0 1 3.3700 3.3673 .0027 0 -2 1 3.2100 3.2084 .0016 1 0 1 3.0000 2.9978 .0022 0 -3 1 2.5800 2.5792 .0008 1 3 1 2.5100 2.5104 -.0004 -2 0 1 2.4300 2.4302 -.0002 2 -1 1 2.2700 2.2692 .0008 0 6 0 2.0700 2.0716 -.0016 -2 3 1 1.9400 1.9401 -.0001 -3 0 1 1.8500 1.8507 -.0007 0 6 1
A= 6.8432 DA= .0002 B= 13.765 DB= .005 C= 3.6845 DC= .0008 GAMMA= 83.65 DGAMMA= .02 BETA = 91.4223 DBETA = .0007 ALPHA= 95.70724 DALPHA= .00003 V= 343.2
36. 18-1481 Y2W5O14{OH}8 Triklin
Dexp Dcal d(D) h k l 6.7300 6.7295 .0005 0 1 1 4.9300 4.9324 -.0024 -1 0 1 4.6500 4.6494 .0006 0 -1 1 4.3700 4.3673 .0027 -1 1 0 3.8000 3.8017 -.0017 0 0 2 3.6400 3.6427 -.0027 1 2 2 3.3600 3.3647 -.0047 0 2 2 3.2500 3.2532 -.0032 2 2 0 3.0400 3.0404 -.0004 1 3 1 2.8600 2.8595 .0005 -1 -1 2 2.7700 2.7704 -.0004 -2 1 0 2.6400 2.6389 .0011 -1 2 2
A= 7.6541 DA= .0004 B= 9.140 DB= .002 C= 8.3660 DC= .0005 GAMMA= 64.228 DGAMMA= .004 BETA = 76.342 DBETA = .007 ALPHA= 65.65 DALPHA= .01 V=478.9
37. 18-1914 C10H10Br4N2W Triklin
Dexp Dcal d(D) h k l 6.5900 6.5833 .0067 0 1 1 6.2900 6.2898 .0002 0 -1 1 5.2700 5.2733 -.0033 -1 1 1 2.7000 2.6998 .0002 -1 -2 2 4.2000 4.2009 -.0009 1 1 2 4.0300 4.0339 -.0039 2 -1 2 3.8400 3.8408 -.0009 -1 2 1 3.7800 3.7770 .0030 2 -2 1 3.6900 3.6964 -.0064 1 2 1 3.2000 3.1985 .0015 1 2 2 2.8400 2.8395 .0005 2 2 2 2.6200 2.6201 -.0001 -3 2 1
A= 10.7364 DA= .003 B= 9.113 DB= .005 C= 9.974 DC= .005 GAMMA=102.93 DGAMMA= .02 BETA = 69.56 DBETA = .03 ALPHA= 92.095 DALPHA= .007 V-890.2
38. 18-1917 C10H10Cl4N2W Triklin
Dexp. Dcal. d(D) h k l 6.4300 6.4300 .0000 -1 -1 0 6.1000 6.0992 .0008 0 0 1 5.1400 5.1400 .0000 3 0 0 4.1300 4.1337 -.0037 1 -1 1 3.9100 3.9100 .0000 -3 -1 0 3.8200 3.8257 -.0057 4 -1 0 3.6900 3.6987 -.0087 -4 1 1 3.6400 3.6411 -.0011 -2 -1 1 3.2600 3.2604 -.0004 -1 1 2 3.2000 3.1962 .0038 -3 -1 1 3.1200 3.1158 .0042 2 2 1 2.7900 2.7869 .0031 -4 -1 1
A= 16.153 DA= .002 B= 8.5869 DB= .0008 C= 6.527 DC= .002 GAMMA=106.15 DGAMMA= .02 BETA =101.24 DBETA = .02 ALPHA= 70.11 DALPHA= .03 V= 812.6 |
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