1. 46-0061
Cr2V4O13
Triklin
Dexp Dcal d(D) h k l
7.0800 7.0887 -.0087 2 1 0
4.6500 4.6449 .0051 0 3 0
4.0800 4.0799 .0001 0 1 1
3.8900 3.8919 -.0019 0 -1 1
3.7700 3.7719 -.0019 3 3 0
3.7000 3.7012 -.0012 -2 0 1
3.6500 3.6505 -.0005 1 2 1
3.5900 3.5910 -.0010 -2 3 0
3.3900 3.3912 -.0012 2 2 1
3.3100 3.3092 .0008 -2 -2 1
3.2500 3.2496 .0004 -3 0 1
3.2500 3.2496 .0004 -3 0 1
3.0400 3.0387 .0013 3 2 1
A= 14.902 DA= .002
B= 14.289 DB= .001
C= 4.17471 DC= .00008
GAMMA= 78.189 DGAMMA= .006
BETA = 92.298 DBETA = .002
ALPHA= 85.649 DALPHA= .003
V=865.9
2. 46-0073
ErNb2O9
Triklin
Dexp Dcal d(D) h k l
7.7200 7.7269 -.0069 1 0 0
4.9300 4.9391 -.0091 1 1 1
4.6600 4.6513 .0087 -1 -1 1
4.5300 4.5301 -.0001 -1 0 1
3.8900 3.8834 .0066 1 2 0
3.6800 3.6817 -.0017 2 1 0
3.5400 3.5409 -.0009 -1 1 1
3.3400 3.3393 .0007 2 -2 2
3.9800 3.9767 .0033 1 -2 2
2.9700 2.9697 .0003 -1 0 2
2.9400 2.9420 -.0020 0 -3 2
2.8600 2.8603 -.0003 0 -1 3
A= 8.814 DA= .001
B= 9.3072 DB= .0003
C= 9.795 DC= .002
GAMMA= 95.820 DGAMMA= .007
BETA = 62.03 DBETA = .01
ALPHA=115.00 DALPHA= .02
V=638.9
3. 46-0074
TmVNb2O9
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7541 .0059 1 0 0
4.9300 4.9370 -.0070 1 1 1
4.6500 4.6594 -.0094 -1 -1 1
3.9000 3.9062 -.0062 0 -1 2
3.7100 3.7136 -.0036 1 -1 2
3.5200 3.5220 -.0020 2 1 1
3.5000 3.4972 .0028 1 1 2
3.3600 3.3608 -.0008 -1 2 0
3.1800 3.1789 .0011 -2 -1 1
3.0800 3.0757 .0043 0 -2 2
2.9800 2.9781 .0019 2 -1 2
2.9300 2.9297 .0003 2 2 0
A= 7.968 DA= .002
B= 7.9714 DB= .0001
C= 8.585 DC= .001
GAMMA= 85.13 DGAMMA= .02
BETA = 78.30 DBETA = .01
ALPHA= 96.61 DALPHA= .01
V=526.9
4. 46-0075
YbVNb2O3
Triklin
Dexp Dcal d(D) h k l
7.7700 7.7700 .0000 -1 1 0
4.9300 4.9269 .0031 -1 2 1
4.6400 4.6371 .0029 1 -2 1
4.5300 4.5296 .0004 -1 3 0
3.9100 3.9048 .0052 0 0 2
3.7000 3.6995 .0005 0 -3 1
3.5100 3.5125 -.0025 -2 1 1
3.5000 3.5058 -.0058 2 -2 1
3.3400 3.3418 -.0018 -1 0 2
3.1900 3.1887 .0013 1 -2 2
3.0700 3.0705 -.0005 1 -4 1
2.9500 2.9510 -.0010 1 3 2
A= 8.1897 DA= .0008
B= 14.5274 DB= .0002
C= 7.9626 DC= .0003
GAMMA=103.96 DGAMMA= .01
BETA = 85.45 DBETA = .01
ALPHA= 81.16 DALPHA= .02
V=901.9
5. 46-0076
LuVNb2O9
Triklin
Dexp Dcal d(D) h k l
7.7700 7.7705 -.0005 0 1 0
4.9300 4.9308 -.0008 0 -1 2
4.6400 4.6393 .0007 -1 -1 2
4.5300 4.5334 -.0034 -1 1 0
3.7100 3.7086 .0014 -1 -1 3
3.5100 3.5088 .0012 1 0 4
3.4900 3.4884 .0016 0 2 3
3.3500 3.3501 -.0001 -1 -2 2
3.1900 3.1893 .0007 0 -2 2
3.0600 3.0612 -.0012 0 0 5
2.9500 2.9506 -.0006 1 3 1
2.9200 2.9200 -.0000 -1 2 2
A= 8.487 DA= .001
B= 8.9440 DB= .0001
C= 15.9723 DC= .0001
GAMMA= 63.030 DGAMMA= .004
BETA = 79.432 DBETA = .002
ALPHA= 73.836 DALPHA= .002
V=1034
6. 46-0080
K2Zn{VO3}4
Triklin
Dexp. Dcal. d(D) h k l
5.8100 5.8102 -.0002 3 0 0
3.8900 3.8915 -.0015 -1 0 1
3.8000 3.8006 -.0006 -1 -2 0
3.7700 3.7697 .0003 0 -2 0
3.6600 3.6596 .0004 -2 -2 0
3.2900 3.2897 .0003 2 -2 0
3.1100 3.1104 -.0004 -4 -1 1
2.9700 2.9700 -.0000 3 -1 1
2.8300 2.8300 -.0000 -3 1 1
2.7100 2.7102 -.0002 2 -2 1
2.3900 2.3917 -.0017 5 -2 0
2.1800 2.1796 .0004 -8 -1 0
1.9050 1.9049 .0001 -3 0 2
1.8450 1.8452 -.0002 0 -4 1
1.8380 1.8383 -.0003 8 0 1
1.7730 1.7727 .0003 -5 0 2
A= 17.7413 DA= .0006
B= 7.796 DB= .001
C= 4.020 DC= .001
GAMMA= 80.44 DGAMMA= .02
BETA = 96.750 DBETA = .007
ALPHA=102.19 DALPHA= .02
V= 534.0
7. 46-0081
Rb2Zn{VO3}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.6700 3.6736 -.0036 -1 1 1
3.6300 3.6287 .0013 0 0 4
3.4400 3.4417 -.0017 -3 0 3
3.4200 3.4218 -.0018 -1 1 2
3.3200 3.3223 -.0023 2 0 3
3.2400 3.2401 -.0001 1 0 4
3.1300 3.1274 .0026 -2 1 2
3.0900 3.0903 -.0003 3 0 2
2.9600 2.9604 -.0004 -4 0 1
2.7300 2.7296 .0004 -3 1 2
2.7000 2.6993 .0007 3 0 3
2.5000 2.5002 -.0002 1 1 4
1.9370 1.9373 -.0003 1 2 0
1.7140 1.7136 .0004 3 2 1
a= 11.86 b= 3.9308 c= 14.97 beta= 104.2
da=.02 db=.0009 dc=.05 dbeta=.2
V= 676
8. 46-0082
Cs2Zn{VO3}4
Triklin
Dexp Dcal d(D) h k l
4.1000 4.0992 .0008 1 0 0
3.9000 3.8997 .0003 -1 1 1
3.7800 3.7802 -.0002 -1 -1 1
3.5300 3.5311 -.0011 -1 2 0
3.3900 3.3908 -.0008 -1 -2 1
3.3600 3.3606 -.0006 1 0 1
3.2200 3.2197 .0003 1 -1 1
3.1800 3.1825 -.0025 -1 0 2
3.0800 3.0798 .0002 -1 3 0
3.0400 3.0381 .0019 -1 -1 2
2.8000 2.8001 -.0001 0 5 1
2.7800 2.7796 .0004 -1 3 2
A= 4.190 DA= .002
B= 14.345 DB= .003
C= 8.108 DC= .005
GAMMA= 91.00 DGAMMA= .03
BETA =101.935 DBETA = .006
ALPHA= 81.85 DALPHA= .06
V=470.8
9. 46-0083
Ag2Zn{VO3}4
Triklin
Dexp Dcal d(D) h k l
7.3400 7.3652 -.0252 -1 0 1
3.7300 3.7265 .0035 0 1 1
3.6900 3.6911 -.0011 0 -1 1
3.2000 3.2032 -.0032 -1 1 1
3.1400 3.1423 -.0023 1 -1 1
3.0500 3.0542 -.0042 -2 -1 1
3.0200 3.0190 .0010 -1 1 2
2.9900 2.9805 .0095 0 -1 3
2.9800 2.9805 -.0005 0 -1 3
2.9500 2.9460 .0040 1 1 3
2.9200 2.9192 .0008 1 -1 2
2.8200 2.8221 -.0021 -2 0 4
A= 8.3486 DA= .0007
B= 3.9022 DB= .0008
C= 14.590 DC= .001
GAMMA= 79.442 DGAMMA= .002
BETA = 94.011 DBETA = .006
ALPHA= 89.65 DALPHA= .02
V=466.1
10. 46-0227
KV3Cu3O11
Monoklin
grupa 3
Dexp Dcal d(D) h k l
5.5000 5.5128 -.0128 1 1 0
3.5000 3.4995 .0005 1 1 1
3.4300 3.4307 -.0007 1 2 0
2.2400 2.2412 -.0012 3 1 1
2.1900 2.1904 -.0004 0 3 1
1.8180 1.8181 -.0001 -2 1 2
1.6750 1.6748 .0002 4 2 1
1.6070 1.6069 .0001 -3 1 2
1.2850 1.2850 .0000 3 4 2
a=8.03 b= 7.591 c= 4.383 beta= 86.48
da=.01 db=.001 dc=.003 dbeta=.01
V= 266.8
11. 46-0281
MgV6O16*9H2O
Triklin
Dexp Dcal d(D) h k l
10.5900 10.5807 .0093 1 0 0
6.1500 6.1752 -.0252 -1 1 0
5.5400 5.5245 .0155 1 0 2
5.2600 5.2903 -.0303 2 0 0
4.0500 4.0528 -.0028 2 -1 2
3.4900 3.4890 .0010 3 -1 2
3.4100 3.4073 .0027 -3 1 0
3.1000 3.0979 .0021 1 -1 3
2.9800 2.9781 .0019 1 2 0
2.9000 2.9004 -.0004 0 2 2
2.6900 2.6918 -.0018 -3 2 0
2.4500 2.4489 .0011 -2 2 2
A= 12.0681 DA= .0008
B= 6.725 DB= .001
C= 11.0549 DC= .0007
GAMMA= 99.54 DGAMMA= .01
BETA = 63.519 DBETA = .001
ALPHA= 88.17 DALPHA= .01
V=786.2
12. 46-0306
Li2VP3O10*4.4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.2000 9.2675 -.0675 0 0 1
5.9400 5.9524 -.0124 1 1 0
4.7100 4.7192 -.0092 1 1 1
4.6200 4.6337 -.0137 0 0 2
4.4100 4.4085 .0015 -1 0 2
3.9200 3.9303 -.0103 0 2 1
3.6600 3.6600 .0000 -1 2 1
3.4100 3.4054 .0046 -2 0 2
3.1000 3.0927 .0073 -1 2 2
2.9740 2.9762 -.0022 2 2 0
2.9100 2.9103 -.0003 0 1 3
2.8350 2.8320 .0030 1 2 2
a= 8.33 b= 8.68 c= 9.44 beta= 100.99
da=.01 db=.03 dc=.005 dbeta=.01
V= 670
Triklin
Dexp Dcal d(D) h k l
9.2000 9.2025 -.0025 0 0 1
5.9400 5.9419 -.0019 0 -1 1
4.7100 4.7135 -.0035 2 0 1
4.6200 4.6013 .0187 0 0 2
4.4100 4.4214 -.0114 -2 1 0
3.9200 3.9246 -.0046 2 0 2
3.6600 3.6652 -.0052 2 1 0
3.4100 3.4143 -.0043 2 1 2
3.1000 3.0980 .0020 -2 -1 1
2.9740 2.9741 -.0001 0 1 3
2.9100 2.9087 .0013 2 -1 3
2.8350 2.8351 -.0001 3 -2 1
A= 9.7808 DA= .0001
B= 8.646 DB= .003
C= 9.728 DC= .005
GAMMA=101.75 DGAMMA= .08
BETA = 71.85 DBETA = .03
ALPHA= 88.61 DALPHA= .09
V= 761.9
13. 46-0307
Na2VP3O10*4H2O
Triklin
Dexp Dcal d(D) h k l
9.4400 9.4349 .0051 1 0 0
5.6700 5.6699 .0001 1 1 1
4.7600 4.7608 -.0008 -1 -1 1
4.4700 4.4731 -.0031 1 0 2
4.2800 4.2752 .0048 0 2 0
3.8100 3.8115 -.0015 0 1 2
3.4700 3.4707 -.0007 2 1 2
3.3500 3.3545 -.0045 -2 1 1
3.2900 3.2898 .0002 3 0 1
3.1200 3.1216 -.0016 1 -2 2
3.1200 3.1216 -.0016 1 -2 2
2.8270 2.8283 -.0013 1 1 3
A= 9.893 DA= .002
B= 8.556 DB= .001
C= 9.071 DC= .002
GAMMA= 88.966 DGAMMA= .004
BETA = 72.571 DBETA = .004
ALPHA= 91.412 DALPHA= .005
V= 732.1
14. 46-0308
K2VP3O10*2.4H2O
Triklin
Dexp Dcal d(D) h k l
9.7000 9.6936 .0064 1 0 0
7.5300 7.5444 -.0144 -1 1 0
5.1900 5.1878 .0022 -1 1 1
4.7100 4.7059 .0041 1 1 1
4.2700 4.2687 .0013 2 1 0
3.5700 3.5692 .0008 0 3 0
3.4100 3.4083 .0017 -2 2 1
3.2700 3.2710 -.0010 0 0 2
3.2100 3.2085 .0015 0 3 1
3.0600 3.0608 -.0008 -2 -2 1
3.0100 3.0111 -.0011 -2 3 0
2.9450 2.9441 .0009 1 3 1
A= 9.764 DA= .001
B= 10.775 DB= .002
C= 6.571 DC= .005
GAMMA= 95.60 DGAMMA= .01
BETA = 94.336 DBETA = .005
ALPHA= 86.45 DALPHA= .05
V= 685.0
15. 46-0309
RbVP3O10*2.1H2O
Triklin
Dexp Dcal d(D) h k l
9.4900 9.4833 .0067 1 0 0
4.7700 4.7727 -.0027 -1 0 1
4.1100 4.1052 .0048 1 -2 1
3.8800 3.8751 .0049 -1 -2 1
3.6600 3.6604 -.0004 -2 2 0
3.5500 3.5569 -.0069 2 3 0
3.3400 3.3396 .0004 -1 3 1
3.1800 3.1804 -.0004 0 0 2
3.1600 3.1611 -.0011 3 0 0
3.0700 3.0699 .0001 2 1 2
3.0200 3.0202 -.0002 -2 2 1
2.9400 2.9425 -.0025 3 -1 1
A= 9.944 DA= .004
B= 14.06 DB= .01
C= 6.654 DC= .003
GAMMA= 79.51 DGAMMA= .04
BETA = 74.54 DBETA = .02
ALPHA= 80.25 DALPHA= .04
V= 874.3
16. 46-0310
Cs2VP3O10*2.5H2O
Triklin
Dexp Dcal d(D) h k l
10.0200 10.0554 -.0354 0 0 1
4.9000 4.9014 -.0014 -1 -1 1
3.9800 3.9765 .0035 0 -2 1
3.7500 3.7491 .0009 -1 -2 1
3.6900 3.6871 .0029 -1 2 0
3.3500 3.3518 -.0018 0 0 3
3.2300 3.2294 .0006 1 2 3
3.1200 3.1211 -.0011 -2 -1 1
3.0300 3.0292 .0008 0 -2 2
2.9580 2.9564 .0016 -1 -2 2
2.9100 2.9126 -.0026 0 -3 1
2.8350 2.8349 .0001 0 4 2
A= 6.7117 DA= .0002
B= 11.65096 DB= .00006
C= 11.0715 DC= .0001
GAMMA= 78.183 DGAMMA= .001
BETA = 89.330 DBETA = .003
ALPHA= 65.683 DALPHA= .001
V=769.2
17. 46-0311
LiVP2O7
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.5600 6.5580 .0020 1 1 0
5.0900 5.0914 -.0014 1 0 2
4.0700 4.0678 .0022 2 0 2
3.9100 3.9075 .0025 -1 0 2
3.4400 3.4402 -.0002 1 2 2
3.2700 3.2677 .0023 1 1 3
3.2100 3.2058 .0042 2 0 3
3.0300 3.0319 -.0019 2 1 3
3.0000 2.9960 .0040 -1 2 2
2.9710 2.9698 .0012 0 3 1
2.9070 2.9059 .0011 1 3 1
2.5450 2.5457 -.0007 2 0 4
a= 9.691 b= 9.333 c=10.481 beta= 71.99
da=.001 db= .001 dc=.005 dbeta=.05
V= 901.5
Triklin
Dexp Dcal d(D) h k l
6.5600 6.5469 .0131 0 1 0
5.0900 5.0917 -.0017 0 -1 2
4.0700 4.0685 .0015 -1 0 1
3.9100 3.9091 .0009 0 -1 3
3.4400 3.4386 .0014 1 -1 1
3.2700 3.2734 -.0034 0 2 0
3.2100 3.2157 -.0057 0 1 3
3.0300 3.0310 -.0010 -1 -2 1
3.0000 3.0002 -.0002 1 1 3
2.9710 2.9696 .0014 -1 -1 3
2.9070 2.9049 .0021 1 2 1
2.5450 2.5458 -.0008 0 -2 4
A= 4.731 DA= .003
B= 6.886 DB= .003
C= 12.856 DC= .00171
GAMMA= 76.67 DGAMMA= .02
BETA = 83.67 DBETA = .01
ALPHA=100.41 DALPHA= .02
V= 395.8
18. 46-0313
RbVP2O7
Triklin
Dexp Dcal d(D) h k l
4.1700 4.1710 -.0010 0 0 1
3.9400 3.9381 .0019 3 0 0
3.8500 3.8511 -.0011 -1 0 1
3.6600 3.6572 .0028 0 -1 1
3.5900 3.5865 .0035 -1 -1 1
3.4100 3.4076 .0024 1 -1 1
3.0900 3.0897 .0003 -2 2 0
3.0600 3.0562 .0038 4 2 0
3.0200 3.0218 -.0018 3 2 1
2.9830 2.9818 .0012 -2 1 1
2.9510 2.9536 -.0026 4 0 0
2.8540 2.8572 -.0032 -2 -2 1
A= 12.83008 DA= .00009
B= 9.9179 DB= .0002
C= 4.21970 DC= .00001
GAMMA= 67.37404 DGAMMA= .00005
BETA = 83.4137 DBETA = .0001
ALPHA= 82.2279 DALPHA= .0003
V=490.2
19. 46-0314
CsVP2O7
Triklin
Dexp Dcal d(D) h k l
4.9800 4.9794 .0006 1 0 1
3.9900 3.9899 .0001 2 -1 1
3.7000 3.6995 .0005 1 -2 1
3.4800 3.4797 .0003 2 -2 1
3.1500 3.1490 .0010 3 1 1
3.1100 3.1098 .0002 3 -2 1
3.0500 3.0492 .0008 -4 1 1
3.0300 3.0307 -.0007 -4 3 0
2.9910 2.9914 -.0004 1 -3 1
2.9830 2.9843 -.0013 -2 -2 1
2.6610 2.6613 -.0003 5 0 0
2.4760 2.4763 -.0003 -2 -3 1
A= 14.0513 DA= .0005
B= 12.4281 DB= .0005
C= 5.5234 DC= .0005
GAMMA=108.701 DGAMMA= .006
BETA = 94.76 DBETA = .01
ALPHA= 79.025 DALPHA= .003
V= 896.7
20. 46-0350
KVOF{SO4}*3H2O
Triklin
Dexp Dcal d(D) h k l
6.0800 6.0746 .0054 0 1 1
5.1800 5.1791 .0009 0 -1 1
4.8500 4.8465 .0035 -1 -1 1
4.6600 4.6615 -.0015 0 2 0
4.5000 4.5029 -.0029 -2 1 1
3.7700 3.7671 .0029 1 2 0
3.5100 3.5062 .0038 2 1 0
3.1100 3.1077 .0023 0 3 0
3.0900 3.0904 -.0004 -1 3 0
2.9800 2.9808 -.0008 -2 3 1
2.9310 2.9325 -.0015 -2 -1 2
2.8720 2.8716 .0004 -3 2 1
A= 9.259 DA= .005
B= 9.821 DB= .001
C= 7.903 DC= .004
GAMMA=105.75 DGAMMA= .07
BETA =116.88 DBETA = .07
ALPHA= 74.68 DALPHA= .03
V= 608.5
21. 46-0351
RbVOF{SO4}*3H2O
Triklin
Dexp Dcal d(D) h k l
6.2200 6.2122 .0078 1 0 0
5.2600 5.2535 .0065 -1 1 0
5.1100 5.1167 -.0067 1 0 1
4.9300 4.9234 .0066 -1 1 1
4.5900 4.5754 .0146 1 -1 1
3.8700 3.8622 .0078 1 0 2
3.7900 3.7847 .0053 -1 -1 1
3.5500 3.5508 -.0008 1 1 1
3.1300 3.1296 .0004 0 1 3
3.1000 3.1021 -.0021 -2 0 1
3.0400 3.0424 -.0024 1 -2 1
2.9800 2.9822 -.0022 1 0 3
A= 6.5578 DA= .0008
B= 6.5706 DB= .0009
C= 11.095 DC= .003
GAMMA=107.014 DGAMMA= .002
BETA = 97.77 DBETA = .01
ALPHA= 89.14 DALPHA= .01
V=453.0
22. 46-0352
NH4VOF{SO4}*3H2O
Triklin
Dexp Dcal d(D) h k l
6.2500 6.2505 -.0005 1 0 1
5.2900 5.2918 -.0018 -1 0 2
4.9300 4.9257 .0043 1 -1 1
4.5900 4.5915 -.0015 -1 -1 1
3.8700 3.8667 .0033 0 2 0
3.8000 3.8017 -.0017 1 1 3
3.5300 3.5326 -.0026 -1 2 1
3.1400 3.1391 .0009 1 2 2
2.9900 2.9909 -.0009 2 1 1
2.9540 2.9545 -.0005 0 -2 3
2.9180 2.9175 .0005 -2 0 3
2.8670 2.8665 .0005 2 0 3
A= 6.8492 DA= .0003
B= 7.857 DB= .004
C= 16.58 DC= .01
GAMMA= 95.47 DGAMMA= .08
BETA = 91.94 DBETA = .01
ALPHA= 81.26 DALPHA= .08
V=879.4
23. 46-0687
AlVMoO7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.3800 6.3555 .0245 2 0 0
4.4900 4.4964 -.0064 0 1 0
4.2400 4.2390 .0010 1 1 0
4.1100 4.1142 -.0042 1 1 1
4.0900 4.0882 .0018 3 0 1
4.0200 4.0235 -.0035 0 1 2
3.8900 3.8952 -.0052 -3 0 2
3.8500 3.8559 -.0059 -1 1 2
3.7700 3.7765 -.0065 3 0 2
3.6700 3.6707 -.0007 2 1 0
3.4900 3.4859 .0041 -1 1 3
3.4000 3.3990 .0010 3 0 3
a= 12.72 b=4.496 c=18.04 beta= 92.3
da=.02 db=.009 dc=.04 dbeta=.3
V= 1031
Triklin
Dexp Dcal d(D) h k l
6.3800 6.3916 -.0116 -1 -1 1
4.4900 4.4850 .0050 -1 1 0
4.2400 4.2467 -.0067 -1 -1 2
4.1100 4.1149 -.0049 0 2 0
4.0900 4.0922 -.0022 0 -1 2
4.0200 4.0208 -.0008 0 -2 1
3.8900 3.8927 -.0027 -1 0 2
3.8500 3.8472 .0028 -2 -1 1
3.7700 3.7730 -.0030 2 1 0
3.6700 3.6652 .0048 -1 -2 2
3.4900 3.4873 .0027 0 1 2
3.4000 3.3996 .0004 -2 0 1
A= 7.8327 DA= .0007
B= 9.376 DB= .003
C= 8.9264 DC= .0009
GAMMA= 63.516 DGAMMA= .006
BETA =105.51 DBETA = .05
ALPHA=106.73 DALPHA= .03
V=554.7
24. 46-0691
Fe2Cr2V2Mo3O20
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7500 4.7429 .0071 2 1 0
4.5700 4.5541 .0159 2 1 1
4.3400 4.3368 .0032 1 2 0
4.2600 4.2749 -.0149 0 0 3
4.1400 4.1491 -.0091 1 2 1
3.8900 3.8944 -.0044 0 1 3
3.8000 3.8020 -.0020 0 2 2
3.6500 3.6473 .0027 1 2 2
3.4000 3.4002 -.0002 -2 2 1
3.3600 3.3594 .0006 3 1 1
3.2900 3.2929 -.0029 2 1 3
3.2100 3.2062 .0038 0 0 4
a= 11.01 b= 9.443 c= 12.87 beta= 85.32
da=.02 db=.003 dc=.01 dbeta=.06
V= 1333
Triklin
Dexp Dcal d(D) h k l
4.7500 4.7612 -.0112 2 0 0
4.5700 4.5702 -.0002 2 2 0
4.3400 4.3446 -.0046 1 3 0
4.2600 4.2577 .0023 0 0 1
4.1400 4.1491 -.0091 0 -1 1
3.8900 3.8808 .0092 1 0 1
3.8000 3.7980 .0020 2 3 0
3.6500 3.6538 -.0038 1 -1 1
3.4000 3.4008 -.0008 -1 3 0
3.3600 3.3611 -.0011 1 2 1
3.2900 3.2876 .0024 2 -2 0
3.2100 3.2084 .0016 -1 -3 1
A= 10.091 DA= .006
B= 13.18 DB= .01
C= 4.28 DC= .001
GAMMA= 70.68 DGAMMA= .02
BETA = 92.164 DBETA = .006
ALPHA= 95.854 DALPHA= .006
V=534.9
25. 46-0720
K2Mn{VO3}4
Triklin
Dexp Dcal d(D) h k l
5.8500 5.8509 -.0009 -1 1 1
5.4700 5.4695 .0005 1 0 0
3.9400 3.9390 .0010 -1 -1 1
3.8200 3.8182 .0018 1 -1 1
3.6800 3.6805 -.0005 -1 1 3
3.3300 3.3288 .0012 0 2 3
3.1100 3.1096 .0004 0 3 2
3.0000 3.0000 -.0000 -2 1 1
2.8700 2.8692 .0008 -1 -2 1
2.7500 2.7485 .0015 0 -2 2
2.7100 2.7115 -.0015 0 -1 3
2.2100 2.2099 .0001 -1 -3 1
1.9620 1.9617 .0003 -3 1 1
1.8550 1.8549 .0001 2 1 3
1.8520 1.8521 -.0001 0 5 1
A= 6.060 DA= .001
B= 10.162 DB= .003
C= 11.588 DC= .009
GAMMA=110.25 DGAMMA= .02
BETA =113.053 DBETA = .005
ALPHA= 61.10 DALPHA= .03
V= 563.8
26. 46-0721
Rb2Mn{VO3}4
Triklin
Dexp Dcal d(D) h k l
5.8700 5.8608 .0092 -1 0 1
4.0500 4.0551 -.0051 0 1 1
3.8000 3.8021 -.0021 0 -1 1
3.6900 3.6906 -.0006 1 -1 1
3.3400 3.3406 -.0006 0 -1 2
3.1500 3.1509 -.0009 1 1 0
3.0000 2.9999 .0001 2 0 2
2.9100 2.9108 -.0008 -2 1 1
2.7800 2.7785 .0015 0 1 4
2.7000 2.7006 -.0006 -1 1 4
2.4700 2.4691 .0009 -1 -1 3
2.2900 2.2896 .0004 -2 1 4
A= 6.7962 DA= .0009
B= 4.252 DB= .001
C= 13.679 DC= .003
GAMMA=104.06 DGAMMA= .01
BETA = 89.92 DBETA = .01
ALPHA= 83.55 DALPHA= .01
V= 380.9
27. 46-0722
Cs2Mn{VO3}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.5300 3.5313 -.0013 4 0 1
3.4900 3.4894 .0006 -4 0 1
3.3800 3.3780 .0020 1 2 1
3.3500 3.3485 .0015 4 1 1
3.2300 3.2343 -.0043 7 0 0
3.0300 3.0300 .0000 -5 1 1
2.8300 2.8301 -.0001 8 0 0
2.7800 2.7764 .0036 5 3 0
2.5900 2.5890 .0010 -3 3 1
2.4900 2.4911 -.0011 4 3 1
2.2700 2.2704 -.0004 9 2 0
2.2000 2.1999 .0001 2 0 2
1.9700 1.9699 .0001 -8 3 1
1.9000 1.9016 -.0016 1 5 1
1.7700 1.7696 .0004 11 2 1
a= 22.6 b= 10.544 c= 4.47486 beta= 89.29
da=.1 db=.006 dc=.00006 dbeta=.01
V= 1068
Triklin
Dexp Dcal d(D) h k l
3.5300 3.5280 .0020 1 0 1
3.4900 3.4933 -.0033 0 1 1
3.3800 3.3775 .0025 0 -1 1
3.3500 3.3508 -.0008 1 1 1
3.2300 3.2332 -.0032 3 1 0
3.0300 3.0286 .0014 2 0 1
2.8300 2.8292 .0008 1 2 1
2.7800 2.7794 .0006 2 -1 1
2.5900 2.5877 .0023 2 3 0
2.4900 2.4897 .0003 -3 0 1
2.2700 2.2710 -.0010 3 2 1
2.2000 2.2009 -.0009 -1 -3 1
1.9700 1.9698 .0002 4 2 1
1.9000 1.8963 .0037 1 4 1
1.7700 1.7699 .0001 -5 0 1
A= 10.148 DA= .001
B= 8.625 DB= .005
C= 3.751 DC= .001
GAMMA= 85.00 DGAMMA= .08
BETA = 89.04 DBETA = .02
ALPHA= 87.30 DALPHA= .02
V=327.1
28. 46-0892
LaV18O48H3*19.5H2O
Geksagon
Grupa 143
Dexp. Dcal. d(D) h k l
12.9000 13.1104 -.2104 0 0 1
4.2600 4.2609 -.0009 2 1 1
3.4400 3.4412 -.0012 2 2 0
2.9600 2.9592 .0008 1 1 4
2.5600 2.5609 -.0009 1 0 5
1.9160 1.9147 .0013 3 0 6
1.7990 1.8006 -.0016 6 1 1
1.5200 1.5199 .0001 4 1 7
a= 13.765 c= 13.1104
da= .008 dc= .0004
V= 2484
29. 46-0914
C37VOF3Cl0.32
Tetragon
Groupa 134
Dexp. Dcal. d(D) h k l
3.6600 3.6699 -.0099 1 1 0
2.9600 2.9565 .0035 1 0 1
1.8360 1.8350 .0010 2 2 0
1.6340 1.6346 -.0006 2 2 1
a= 5.190 c= 3.60
da= .008 dc= .01
v= 96.9
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
3.6600 3.6605 -.0005 0 2 0
2.9600 2.9595 .0005 1 2 0
1.8360 1.8360 .0000 0 0 2
1.6340 1.6340 .0000 3 1 0
a= 5.029 b= 7.321 c= 3.672
da= .001 db= .001 dc= .001
V= 135.19
30. 46-924
RbV2F6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
5.9900 5.9989 -.0089 1 2 0
3.6600 3.6620 -.0020 4 1 0
3.2900 3.2935 -.0035 4 2 0
3.1500 3.1532 -.0032 0 0 1
3.0900 3.0880 .0020 1 0 1
3.0000 2.9994 .0006 2 4 0
2.6100 2.6096 .0004 0 5 0
2.3700 2.3698 .0002 6 2 0
2.0000 1.9996 .0004 3 6 0
1.9800 1.9797 .0003 6 0 1
1.8500 1.8503 -.0003 1 7 0
1.8200 1.8200 .0000 5 4 1
a=15.26 b=13.048 c= 3.153
da= .01 db= .001 dc= .001
V= 627.9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9900 5.9991 -.0091 0 0 1
3.6600 3.6555 .0045 1 1 1
3.2900 3.2867 .0033 3 0 0
3.1500 3.1544 -.0044 2 1 1
3.0900 3.0891 .0009 3 0 1
3.0000 3.0008 -.0008 1 0 2
2.6100 2.6105 -.0005 3 1 1
2.3700 2.3697 .0003 1 2 0
2.0000 1.9997 .0003 0 0 3
1.9800 1.9800 -.0000 -4 1 1
1.8500 1.8505 -.0005 0 1 3
1.8200 1.8196 .0004 2 1 3
a= 9.98 b= 4.882 c= 6.071 beta= 81.2
da=.04 db= 2.928 dc= .02 dbeta=.1
V= 292.3
31. 46-0971
Na2Ie6O28
Tetragon
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
7.0500 7.0517 -.0017 1 0 0
3.5200 3.5259 -.0059 2 0 0
3.4100 3.4101 -.0001 1 1 2
3.1100 3.1160 -.0060 0 0 3
2.9900 2.9882 .0018 2 1 1
2.4100 2.4090 .0010 2 2 1
2.3500 2.3506 -.0006 3 0 0
1.8700 1.8696 .0004 0 0 5
a= 7.0517 c= 9.35
da= .0003 dc= .01
V= 464.8
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
7.0500 7.0486 .0014 0 0 1
3.5200 3.5243 -.0043 0 0 2
3.4100 3.4120 -.0020 1 0 1
3.1100 3.1094 .0006 0 1 2
2.9900 2.9906 -.0006 0 2 1
2.4100 2.4098 .0002 0 2 2
2.3500 2.3495 .0005 0 0 3
1.8700 1.8699 .0001 2 1 0
a= 3.899 b= 6.6051 c= 7.0486
da= .002 db= .0003 dc= .0003
V=181.5
32. 46-1004
Nb2V2O9
Triklin
Dexp Dcal d(D) h k l
6.8800 6.8896 -.0096 1 1 0
6.5200 6.5118 .0082 -1 0 1
5.0200 5.0141 .0059 -1 -1 2
4.1500 4.1505 -.0005 0 -2 1
4.0700 4.0693 .0007 0 1 3
4.0400 4.0415 -.0015 2 1 0
3.8500 3.8486 .0014 0 -2 2
3.8100 3.8084 .0016 -1 -2 2
3.7400 3.7435 -.0035 0 0 4
3.6900 3.6908 -.0008 2 1 2
3.5700 3.5686 .0014 1 0 4
3.4100 3.4120 -.0020 0 -2 3
A= 8.216 DA= .005
B= 8.845 DB= .003
C= 15.171 DC= .001
GAMMA= 71.82 DGAMMA= .02
BETA = 83.96 DBETA = .03
ALPHA= 94.75 DALPHA= .03
V=1036
33. 46-1021
BiVS3
Geksagon
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
11.2500 11.2838 -.0338 0 0 1
5.6300 5.6312 -.0012 1 0 1
3.7590 3.7613 -.0023 0 0 3
2.8200 2.8209 -.0009 0 0 4
2.2560 2.2568 -.0008 0 0 5
1.8810 1.8806 .0004 0 0 6
1.6080 1.6080 .0000 4 0 1
1.4105 1.4105 .0000 0 0 8
a= 7.504 c= 11.284
da=.002 dc= .002
V= 550.2
34. 46-1024
BiVSe3
Tetragon
Groupa 85,118,129
Dexp. Dcal. d(D) h k l
11.9800 11.9109 .0691 0 0 1
5.9650 5.9554 .0096 0 0 2
3.9710 3.9703 .0007 0 0 3
2.9740 2.9721 .0019 1 0 3
2.3820 2.3822 -.0002 0 0 5
1.4860 1.4861 -.0001 2 0 6
a= 4.483 c= 11.911
da= .004 dc= .004
V= 239.3