1. 42-0093
BaCs2V4O12
Rombik
Grupa 16
Dexp Dcal d(D) h k l
4.0200 4.0181 .0019 2 1 0
3.8100 3.8056 .0044 -2 1 1
3.5400 3.5421 -.0021 2 0 2
3.3000 3.2995 .0005 -1 0 3
3.1700 3.1720 -.0020 1 0 3
3.0800 3.0797 .0003 2 1 2
2.9800 2.9810 -.0010 0 2 1
2.6300 2.6276 .0024 4 0 0
2.5500 2.5491 .0009 0 0 4
2.4200 2.4213 -.0013 4 1 0
2.3400 2.3401 -.0001 2 2 2
a= 10.534 b= 6.234 c= 10.219 beta= 93.849210
da=.005 db=.009 dc=.004 dbeta=.07
V= 670
Triklin
Dexp Dcal d(D) h k l
4.0200 4.0206 -.0006 0 0 1
3.8100 3.8112 -.0012 0 -2 1
3.5400 3.5403 -.0003 1 1 0
3.3000 3.2992 .0008 -1 4 0
3.1700 3.1701 -.0001 1 -2 1
3.0800 3.0800 .0000 1 -3 1
2.9800 2.9796 .0004 0 7 1
2.6300 2.6305 -.0005 -1 8 0
2.5500 2.5501 -.0001 1 7 1
2.4200 2.4198 .0002 1 -8 1
2.3400 2.3399 .0001 -1 1 1
A= 3.79808 DA= .00001
B= 29.03 DB= .01
C= 4.2501 DC= .0005
GAMMA= 92.428 DGAMMA= .005
BETA = 71.441 DBETA = .003
ALPHA= 87.29 DALPHA= .01
V= 442.8
2. 42-0094
BaRb2V4O12
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
7.4200 7.4153 .0047 3 0 0
4.0500 4.0454 .0046 5 1 0
3.2800 3.2814 -.0014 5 2 0
3.2400 3.2394 .0006 0 3 0
3.1100 3.1102 -.0002 2 3 0
3.0200 3.0206 -.0006 7 1 0
2.5000 2.5007 -.0007 4 2 1
2.3700 2.3696 .0004 5 2 1
a=22.2460 b= 9.7182 c= 3.4254
da= .0003 db= .0004 dc= .0001
V= 740.54
3. 42-0107
LaVNb2O9
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9275 .0025 -2 1 0
4.8200 4.8204 -.0004 2 0 0
4.3500 4.3521 -.0021 0 3 0
3.7100 3.7092 .0008 -2 3 0
3.6200 3.6212 -.0012 1 0 1
3.5100 3.5111 -.0011 1 -1 1
3.3900 3.3895 .0005 0 2 1
3.3500 3.3485 .0015 -1 4 0
3.2000 3.1991 .0009 1 -2 1
3.0900 3.0897 .0003 2 0 1
3.0700 3.0710 -.0010 -2 4 0
2.9500 2.9501 -.0001 -3 3 0
A= 9.953 DA= .003
B= 13.480 DB= .005
C= 3.8143 DC= .0002
GAMMA=103.84 DGAMMA= .02
BETA = 86.922 DBETA = .002
ALPHA= 86.814 DALPHA= .007
V=494.9
4. 42-0108
Nb2VYO9
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9274 .0026 -2 1 0
3.7100 3.7095 .0005 -2 3 0
3.5100 3.5106 -.0006 0 4 0
3.3400 3.3381 .0019 -3 1 0
3.0900 3.0908 -.0008 0 1 1
2.9600 2.9595 .0005 -1 -1 1
2.8700 2.8690 .0010 0 2 1
2.6900 2.6901 -.0001 2 0 1
2.6600 2.6604 -.0004 -2 1 1
2.5100 2.5108 -.0008 -4 1 0
2.4800 2.4796 .0004 4 0 0
2.4200 2.4201 -.0001 2 2 1
A= 10.0455 DA= .0002
B= 14.2310 DB= .0005
C= 3.19633 DC= .00005
GAMMA= 99.124 DGAMMA= .003
BETA = 89.4527 DBETA = .0009
ALPHA= 92.1159 DALPHA= .0006
V=450.9
5. 42-1063
Al80V20
Tetragon
Groupa 106,135
Dexp. Dcal. d(D) h k l
4.0020 4.0024 -.0004 2 1 0
2.2384 2.2374 .0010 4 0 0
2.1335 2.1334 .0001 3 2 1
1.5438 1.5440 -.0002 5 2 1
1.3142 1.3142 -.0000 2 1 3
1.1424 1.1424 .0000 4 2 3
a= 8.949 c=4.174
da= .005 dc=.003
V= 334.3
6. 42-1064
Al80V20
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9767 3.9771 -.0004 1 1 1
2.6071 2.6076 -.0005 3 0 0
2.4458 2.4456 .0002 2 1 2
2.2249 2.2247 .0002 -1 1 3
2.1241 2.1242 -.0001 3 0 2
1.8868 1.8867 .0001 3 2 1
1.7952 1.7953 -.0001 4 1 1
1.7074 1.7074 .0000 -2 0 4
1.6535 1.6533 .0002 4 1 2
1.3095 1.3096 -.0001 4 1 4
1.2740 1.2740 -.0000 0 4 3
1.2516 1.2516 .0000 6 1 1
a= 7.824 b=5.9169 c=7.5230 beta= 91.078
da=.001 db=.0009 dc=.0007 dbeta=.004
V= 348.2
7. 43-0091
La4V8O10
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.3100 4.3069 .0031 3 0 2
4.1100 4.1125 -.0025 1 0 3
3.4700 3.4781 -.0081 1 1 1
3.2900 3.2906 -.0006 2 1 1
3.0800 3.0775 .0025 5 0 2
2.8000 2.8046 -.0046 3 1 2
2.7500 2.7488 .0012 1 1 3
2.6600 2.6621 -.0021 6 0 2
2.5400 2.5378 .0022 0 0 5
2.4100 2.4101 -.0001 6 0 3
2.0900 2.0920 -.0020 0 1 5
2.0200 2.0187 .0013 6 1 3
a=17.596 b= 3.696 c=12.689
da= .003 db= .003 dc= .002
V= 825
Triklin
Dexp Dcal d(D) h k l
4.3100 4.3093 .0007 1 1 1
4.1100 4.1114 -.0014 -1 1 1
3.4700 3.4727 -.0027 -1 -1 1
3.2900 3.2899 .0001 -1 1 2
3.0800 3.0786 .0014 0 2 1
2.8000 2.7999 .0001 2 1 1
2.7500 2.7500 -.0000 -2 1 0
2.6600 2.6602 -.0002 -1 -1 2
2.5400 2.5403 -.0003 -1 2 2
2.4100 2.4102 -.0002 0 2 3
2.0900 2.0900 .0000 -1 -1 3
2.0200 2.0198 .0002 -2 0 3
A= 6.2787 DA= .0005
B= 6.16829 DB= .00004
C= 8.6999 DC= .0009
GAMMA= 88.298 DGAMMA= .009
BETA = 86.720 DBETA = .008
ALPHA= 72.1574 DALPHA= .0009
V=320.1
8. 43-0107
NaFe18V15Ox*xH2O
Rombik
Groupa 61
Dexp. Dcal. d(D) h k l
4.1640 4.1361 .0279 0 2 0
3.1600 3.1614 -.0014 0 2 3
2.6700 2.6689 .0011 2 1 0
2.5100 2.5088 .0012 2 1 2
2.4500 2.4513 -.0013 0 0 6
2.4000 2.3972 .0028 0 2 5
2.2100 2.2110 -.0010 1 3 3
2.1600 2.1599 .0001 2 1 4
1.9700 1.9714 -.0014 2 3 0
1.7000 1.6998 .0002 3 2 1
1.6800 1.6800 -.0000 0 2 8
1.5400 1.5401 -.0001 2 0 8
a= 5.639 b= 8.27 c=14.708
da= .001 db= .01 dc= .001
V= 686
9. 43-0614
H2VP3O10*3H2O
Triklin
Dexp Dcal d(D) h k l
10.1500 10.1368 .0132 1 0 0
9.8100 9.8160 -.0060 1 1 0
7.5100 7.5181 -.0081 1 0 1
7.0900 7.0989 -.0089 0 1 1
5.9500 5.9492 .0008 1 2 0
5.1100 5.1092 .0008 0 -2 1
5.0300 5.0294 .0006 -2 -1 1
4.8700 4.8705 -.0005 -1 -1 2
4.5300 4.5287 .0013 1 1 2
3.6700 3.6702 -.0002 3 2 0
3.0500 3.0501 -.0001 2 -2 1
2.8800 2.8800 .0000 -2 2 1
2.8400 2.8399 .0001 3 -1 1
A= 11.261 DA= .002
B= 12.079 DB= .003
C= 10.789 DC= .006
GAMMA= 64.30 DGAMMA= .01
BETA = 91.15 DBETA = .03
ALPHA= 97.83 DALPHA= .04
V= 1308.7
10. 43-0615
H2VP3O10*1.5H2O
Triklin
Dexp Dcal d(D) h k l
8.9800 8.9844 -.0044 1 0 0
8.0300 8.0290 .0010 0 1 1
7.1100 7.1010 .0090 0 -1 1
5.7800 5.7843 -.0043 -1 2 0
5.3600 5.3596 .0004 0 2 1
4.7200 4.7188 .0012 0 1 2
4.4000 4.3994 .0006 -2 1 1
3.7000 3.6996 .0004 2 -2 1
3.5500 3.5505 -.0005 0 -2 2
3.2700 3.2704 -.0004 0 3 2
2.9100 2.9101 -.0001 3 -1 1
2.6300 2.6300 -.0000 -3 -1 1
2.5900 2.5900 .0000 1 4 0
1.9800 1.9800 .0000 0 6 1
A= 9.443 DA= .001
B= 12.5086 DB= .0004
C= 9.868 DC= .002
GAMMA=107.71 DGAMMA= .01
BETA = 95.26 DBETA = .01
ALPHA= 81.6142 DALPHA= .00000
V= 1097
11. 43-1427
NH4VO{SO4}
Triklin
Dexp Dcal d(D) h k l
8.3500 8.3467 .0033 0 0 1
6.0300 6.0283 .0017 1 0 0
4.3600 4.3538 .0062 0 -2 1
4.2200 4.2167 .0033 1 -1 1
3.8300 3.8304 -.0004 -1 -2 1
3.6200 3.6246 -.0046 1 2 1
3.4200 3.4157 .0043 -1 0 2
3.3000 3.3069 -.0069 0 -2 2
3.2900 3.2900 .0000 1 -2 1
3.1300 3.1325 -.0025 -1 2 1
3.0400 3.0393 .0007 2 1 0
2.8700 2.8724 -.0024 -2 -1 1
A= 6.131 DA= .001
B= 9.873 DB= .001
C= 8.3795 DC= .0002
GAMMA= 79.51 DGAMMA= .01
BETA = 90.37 DBETA = .03
ALPHA= 95.05 DALPHA= .04
V=497.1
12. 43-1428
NH4{VO2}{SO4}*2H2O
Triklin
Dexp Dcal d(D) h k l
7.2300 7.2222 .0078 1 0 1
6.2400 6.2353 .0047 -1 1 0
5.4700 5.4683 .0017 1 -1 2
5.1100 5.1114 -.0014 1 1 0
4.7400 4.7476 -.0076 1 1 1
4.4500 4.4503 -.0003 -1 1 1
4.1400 4.1333 .0067 -1 2 0
3.6300 3.6305 -.0005 2 0 0
3.4900 3.4927 -.0027 2 -2 1
3.3600 3.3607 -.0007 2 -1 3
3.1900 3.1910 -.0010 2 1 1
3.1400 3.1395 .0005 2 1 0
A= 8.1778 DA= .0009
B= 9.593 DB= .002
C= 11.712 DC= .001
GAMMA=108.79 DGAMMA= .01
BETA = 64.98 DBETA = .01
ALPHA=111.27 DALPHA= .02
V=760.6
13 43-1429
NH4{VO2}{SO4}*3H2O
Triklin
Dexp Dcal d(D) h k l
7.9600 7.9659 -.0059 1 0 0
6.3300 6.3315 -.0015 -1 1 1
5.3300 5.3314 -.0014 -1 -1 1
4.9700 4.9644 .0056 1 -1 1
4.5900 4.5953 -.0053 1 2 0
4.1000 4.1004 -.0004 -1 3 1
3.9200 3.9173 .0027 -1 1 2
3.7900 3.7892 .0008 1 2 1
3.6000 3.6002 -.0002 1 -3 1
3.5400 3.5408 -.0008 -2 -1 1
3.1800 3.1807 -.0007 -1 -2 2
3.0700 3.0675 .0025 -2 -2 1
A= 8.4731 DA= .0008
B= 13.843 DB= .007
C= 8.1521 DC= .0004
GAMMA=104.99 DGAMMA= .03
BETA =104.13 DBETA = .05
ALPHA= 84.93 DALPHA= .04
V= 895.4
14. 43-1430
{NH4}2V2O2{SO4}3
Triklin
Dexp Dcal d(D) h k l
7.6900 7.6941 -.0041 0 0 1
5.8300 5.8418 -.0118 0 -2 1
4.5300 4.5303 -.0003 -1 0 1
4.3200 4.3220 -.0020 -1 1 1
3.9800 3.9783 .0017 1 0 1
3.8500 3.8470 .0030 0 0 2
3.6900 3.6872 .0028 1 -2 1
3.2700 3.2692 .0008 -1 -1 2
3.1600 3.1576 .0024 0 5 0
3.0400 3.0416 -.0016 0 -5 1
2.9340 2.9347 -.0007 -1 4 1
2.7750 2.7761 -.0011 1 1 2
A= 5.1122 DA= .0005
B= 15.8904 DB= .0009
C= 7.8154 DC= .0002
GAMMA= 91.47 DGAMMA= .01
BETA = 97.893 DBETA = .008
ALPHA= 96.084 DALPHA= .002
V=624.7
15. 44-0015
Al6V10{OH}12O28*29H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.2130 9.2203 -.0073 2 0 0
5.7680 5.7673 .0007 3 0 1
4.1220 4.1165 .0055 -4 0 1
3.9760 3.9743 .0017 3 1 1
3.7450 3.7485 -.0035 -1 0 3
3.4770 3.4778 -.0008 4 1 1
3.1680 3.1671 .0009 4 -1 2
2.9250 2.9250 -.0000 -2 1 3
2.6150 2.6144 .0006 1 1 4
2.3660 2.3661 -.0001 -2 -2 2
2.0830 2.0834 -.0004 4 2 3
2.0130 2.0135 -.0005 1 -2 4
1.9320 1.9326 -.0006 9 1 1
1.8290 1.8291 -.0001 10 0 2
1.6140 1.6142 -.0002 -4 2 5
A= 18.5985 DA= .0005
B= 5.4771 DB= .0006
C= 11.900 DC= .001
GAMMA= 89.938 DGAMMA= .009
BETA = 82.5372 DBETA = .0005
ALPHA= 89.95 DALPHA= .01
V=1202
Triklin
Dexp Dcal d(D) h k l
9.2130 9.2169 -.0039 0 0 1
5.7680 5.7677 .0003 0 -2 1
4.1220 4.1228 -.0008 1 -2 2
3.9760 3.9759 .0001 0 -3 1
3.7450 3.7431 .0019 1 -3 1
3.4770 3.4736 .0034 -2 1 0
3.1680 3.1677 .0003 1 -1 3
2.9250 2.9249 .0001 1 -3 3
2.6150 2.6149 .0001 2 -1 3
2.3660 2.3661 -.0001 0 -5 2
2.0830 2.0828 .0002 0 4 2
2.0130 2.0129 .0001 -1 4 2
1.9320 1.9322 -.0002 0 -1 5
1.8290 1.8293 -.0003 2 -6 1
1.6140 1.6141 -.0001 4 0 3
A= 7.1993 DA= .0007
B= 12.107 DB= .002
C= 10.0026 DC= .0004
GAMMA= 99.40 DGAMMA= .03
BETA = 80.252 DBETA = .008
ALPHA=111.88 DALPHA= .01
V= 792.6
16. 44-0350
K2Ni{VO3}4
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
5.7500 5.7496 .0004 0 2 0
3.7400 3.7394 .0006 2 1 0
3.6500 3.6500 -.0000 1 1 1
3.2600 3.2581 .0019 2 2 0
2.9400 2.9393 .0007 2 1 1
2.8100 2.8078 .0022 0 3 1
2.6900 2.6876 .0024 2 2 1
2.3800 2.3820 -.0020 2 3 1
1.9400 1.9401 -.0001 -1 0 2
1.9400 1.9412 -.0012 0 2 2
1.8200 1.8201 -.0001 3 4 1
a= 7.9648 b= 11.4992 c= 4.1539 beta= 83.18
da=.0007 db=.0005 dc=.0004 dbeta=.05
V= 377.8
17. 44 - 0351
LiK2{VO3}3
Rombik
Groupa 46,74
Dexp. Dcal. d(D) h k l
7.5600 7.5943 -.0343 2 0 0
5.9100 5.9274 -.0174 1 0 1
4.5100 4.5405 -.0305 1 1 0
3.4700 3.4672 .0028 3 1 0
2.5600 2.5604 -.0004 5 1 0
2.3800 2.3790 .0010 0 2 0
1.9900 1.9898 .0002 6 0 2
a=15.188690 b= 4.758067 c= 6.437848
da= .008721 db= .001933 dc= .002169
v= 465.3
18. 44-400
Li1.11V3O7.89
Geksagon
Groupa 169,170,178,179
Dexp. Dcal. d(D) h k l
6.3120 6.4059 -.0939 1 0 0
3.8020 3.7829 .0191 1 0 1
3.2140 3.2029 .0111 2 0 0
2.8950 2.9035 -.0085 1 1 1
2.1350 2.1353 -.0003 3 0 0
a= 7.40 c= 4.69
da=.01 dc= .03
v= 222.1
Rombik
Groupa 21,35,38,65
Dexp. Dcal. d(D) h k l
6.3120 6.3205 -.0085 0 2 0
3.8020 3.8015 .0005 0 1 1
3.2140 3.2140 .0000 1 0 0
2.8950 2.8957 -.0007 0 3 1
2.1350 2.1350 .0000 0 5 1
a= 3.214 b=12.641 c= 3.986
da= .001 db= .001 dc= .001
V= 161.9
19. 44-0636
CeNb2VO9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.9300 4.9285 .0015 2 1 0
4.8600 4.8579 .0021 0 2 1
3.7000 3.6996 .0004 -2 0 2
3.5100 3.5097 .0003 -2 1 2
3.3500 3.3500 .0000 0 0 3
3.0700 3.0698 .0002 2 3 0
2.8700 2.8692 .0008 3 1 2
2.7500 2.7503 -.0003 4 0 0
2.6900 2.6904 -.0004 1 4 0
2.6000 2.5998 .0002 1 4 1
2.4800 2.4803 -.0003 3 0 3
2.4200 2.4201 -.0001 -1 3 3
a= 11.001 b= 11.098 c=10.0501 beta= 89.670
da=.003 db=.001 dc=.0002 dbeta=.001
V= 1227.1
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9298 .0002 1 -1 1
4.8600 4.8622 -.0022 1 1 0
3.7000 3.6986 .0014 3 0 0
3.5100 3.5099 .0001 2 1 1
3.3500 3.3506 -.0006 2 -1 2
3.0700 3.0708 -.0008 -3 1 1
2.8700 2.8692 .0008 3 -1 2
2.7500 2.7500 -.0000 -3 -1 1
2.6900 2.6896 .0004 0 1 3
2.6000 2.6000 .0000 1 2 1
2.4800 2.4804 -.0004 3 0 3
2.4200 2.4200 .0000 -3 -1 2
A= 11.2845 DA= .0007
B= 5.91920 DB= .00003
C= 9.3224 DC= .0005
GAMMA= 99.2547 DGAMMA= .0003
BETA = 84.604 DBETA = .001
ALPHA= 93.036 DALPHA= .002
V=611.7
20. 44-0637
PrNb2VO9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.9300 4.9305 -.0005 -2 1 1
4.8500 4.8534 -.0034 -3 0 1
3.6600 3.6606 -.0006 0 1 2
3.5800 3.5806 -.0006 -2 1 2
3.5100 3.5101 -.0001 -1 2 1
2.9300 2.9289 .0011 3 0 2
2.8700 2.8699 .0001 -1 2 2
2.7400 2.7419 -.0019 3 1 2
2.7000 2.6996 .0004 5 0 1
2.6000 2.5994 .0006 0 3 0
2.4800 2.4804 -.0004 0 3 1
2.4300 2.4297 .0003 4 1 2
a=15.75 b= 7.7982 c=8.492 beta= 102.46
da=.03 db=.0004 dc=.002 dbeta=.08
V= 1018
21. 44-0638
NdNb2VO9
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9287 .0013 -1 2 1
4.8200 4.8204 -.0004 -1 -1 2
3.7100 3.7068 .0032 1 2 3
3.6500 3.6500 -.0000 2 0 2
3.5700 3.5716 -.0016 2 2 1
3.5400 3.5397 .0003 -2 0 2
3.5000 3.4996 .0004 -2 2 0
3.4700 3.4724 -.0024 0 1 4
3.3400 3.3396 .0004 -1 -2 3
3.1600 3.1595 .0005 -1 1 4
3.0600 3.0605 -.0005 -1 4 1
2.9100 2.9099 .0001 0 -4 2
A= 8.3901 DA= .0002
B= 13.510 DB= .003
C= 14.0703 DC= .0004
GAMMA= 87.783 DGAMMA= .005
BETA = 87.79 DBETA = .01
ALPHA= 83.95 DALPHA= .03
V=1587
22. 44-0639
SmNb2VO9
44-0639
Grupa 3
Dexp Dcal d(D) h k l
4.9300 4.8985 .0315 1 2 0
4.7500 4.7537 -.0037 2 1 0
3.6900 3.6895 .0005 0 3 0
3.6000 3.6022 -.0022 -1 2 1
3.5100 3.5093 .0007 3 0 0
3.3400 3.3397 .0003 3 0 1
3.1300 3.1292 .0008 0 3 1
3.0200 3.0213 -.0013 2 3 0
2.8600 2.8594 .0006 3 2 1
2.7000 2.7004 -.0004 -1 0 2
2.5600 2.5606 -.0006 4 1 0
2.4800 2.4791 .0009 -3 2 1
a= 10.767 b= 11.068 c=6.041 beta= 77.905
da=.004 db=.001 dc=.001 dbeta=.003
V= 703.9
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9299 .0001 -1 0 1
4.7500 4.7391 .0109 0 1 1
3.6900 3.6854 .0046 0 -1 1
3.6000 3.6044 -.0044 -1 1 0
3.5100 3.5095 .0005 -1 1 1
3.3400 3.3425 -.0025 2 0 0
3.1300 3.1274 .0026 -2 0 1
3.0200 3.0217 -.0017 -1 0 2
2.8600 2.8588 .0012 1 -1 1
2.7000 2.7009 -.0009 0 2 0
2.5600 2.5602 -.0002 -1 -1 2
2.4800 2.4799 .0001 -2 1 1
A= 7.192 DA= .001
B= 5.952 DB= .004
C= 6.56 DC= .01
GAMMA= 69.59 DGAMMA= .01
BETA = 92.33 DBETA = .09
ALPHA= 77.33 DALPHA= .09
V=254