1. 41-0002
CrV2O6.5
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.2530 4.2499 .0031 0 1 3
3.6330 3.6316 .0014 1 0 1
3.3760 3.3758 .0001 0 2 0
2.5010 2.5011 -.0001 1 2 0
2.4620 2.4621 -.0001 1 0 5
2.3440 2.3440 .0000 0 0 7
a= 3.724 b= 6.752 c=16.408
da= .001 db= .001 dc= .001
V= 412.5
2. 41-0090
SrCuV2O7
Triklin
Dexp Dcal d(D) h k l
7.2800 7.2844 -.0044 -1 0 1
4.2300 4.2253 .0047 1 1 1
3.7780 3.7732 .0048 1 0 3
3.6340 3.6314 .0026 0 0 4
3.6100 3.6064 .0036 -1 1 3
3.2770 3.2771 -.0001 2 -1 1
3.0340 3.0357 -.0017 -1 2 1
3.0150 3.0176 -.0026 0 1 4
2.9530 2.9520 .0010 -2 1 3
2.8970 2.8975 -.0005 -1 0 5
2.7450 2.7444 .0006 2 0 3
2.7100 2.7103 -.0003 -1 -2 3
A= 7.728 DA= .004
B= 6.630 DB= .003
C= 14.8701 DC= .0004
GAMMA= 95.11 DGAMMA= .01
BETA =100.003 DBETA = .006
ALPHA= 96.273 DALPHA= .002
V=741.8
3. 41-0091
Na3La8V3O21
Triklin
Dexp Dcal d(D) h k l
3.2780 3.2787 -.0007 3 0 0
3.2550 3.2524 .0026 -1 3 0
3.1640 3.1598 .0042 2 3 0
3.1560 3.1566 -.0006 -1 -3 1
3.0160 3.0165 -.0005 -3 1 0
2.9290 2.9292 -.0002 0 0 2
2.8542 2.8540 .0002 0 -1 2
2.7336 2.7349 -.0013 1 4 0
2.6217 2.6218 -.0001 -2 0 2
2.5523 2.5530 -.0007 2 4 0
2.4734 2.4733 .0001 -2 -2 2
2.4590 2.4590 -.0000 4 0 0
A= 9.99655 DA= .00008
B= 11.0413 DB= .0002
C= 5.8891 DC= .0004
GAMMA= 81.086 DGAMMA= .004
BETA = 95.506 DBETA = .007
ALPHA= 92.829 DALPHA= .006
V=638.6
4. 41-0092
NaCa{VO3}4
Triklin
Dexp Dcal d(D) h k l
4.9200 4.9189 .0011 -1 1 0
4.0900 4.0888 .0012 -1 2 0
3.6800 3.6795 .0005 1 -1 1
3.2900 3.2894 .0006 -1 3 0
2.9470 2.9474 -.0004 -1 2 2
2.6060 2.6059 .0001 1 3 1
2.4930 2.4928 .0002 1 -2 2
2.4300 2.4296 .0004 -1 0 3
2.3670 2.3673 -.0003 0 -1 3
2.2630 2.2632 -.0002 -2 3 0
2.2490 2.2491 -.0001 -1 -4 2
2.1800 2.1800 .0000 2 1 1
A= 5.4142 DA= .0001
B= 11.9539 DB= .0003
C= 7.4346 DC= .0001
GAMMA= 93.94218 DGAMMA= .00009
BETA =105.428 DBETA = .001
ALPHA= 92.5454 DALPHA= .0007
V=461.8
5. 41-0093
Na4Ca12{V2O7}7
Triklin
Dexp. Dcal. d(D) h k l
3.6200 3.6216 -.0016 1 -3 0
3.5800 3.5806 -.0006 0 -1 1
3.3700 3.3690 .0010 0 -4 0
3.3200 3.3196 .0004 2 0 0
3.1800 3.1795 .0005 2 -1 0
3.1400 3.1391 .0009 -1 0 1
3.0800 3.0793 .0007 -1 -4 0
3.0500 3.0508 -.0008 -2 -2 0
2.9800 2.9795 .0005 0 3 1
2.8540 2.8551 -.0011 1 3 1
2.8210 2.8223 -.0013 -1 -2 1
2.8100 2.8088 .0012 0 -3 1
2.6950 2.6952 -.0002 0 -5 0
2.6280 2.6281 -.0001 1 -3 1
2.5200 2.5194 .0006 1 4 1
A= 6.694 DA= .002
B= 13.5302 DB= .0006
C= 3.8068 DC= .0009
GAMMA= 86.186 DGAMMA= .009
BETA = 83.55 DBETA = .02
ALPHA= 86.176 DALPHA= .008
V= 341.2
6. 41-0101
Na2Mn3V4O14
Triklin
Dexp Dcal d(D) h k l
6.4800 6.4843 -.0043 0 -1 1
3.2600 3.2600 .0000 0 -1 3
3.0600 3.0607 -.0007 -1 1 0
3.0200 3.0214 -.0014 -1 1 1
2.8600 2.8596 .0004 1 -1 1
2.7000 2.6977 .0023 -1 -1 1
2.5500 2.5506 -.0006 1 -2 1
2.5100 2.5099 .0001 0 3 1
2.3200 2.3182 .0018 1 -2 2
2.2800 2.2823 -.0023 -1 -1 3
2.2400 2.2411 -.0011 0 -2 4
2.1700 2.1711 -.0011 1 0 3
1.9950 1.9950 .0000 -1 -2 3
1.6860 1.6863 -.0003 0 -3 5
1.6310 1.6305 .0005 -1 -2 5
1.5950 1.5949 .0001 1 -2 5
A= 3.147 DA= .001
B= 8.023 DB= .004
C= 10.538 DC= .003
GAMMA=100.411 DGAMMA= .005
BETA = 96.726 DBETA = .001
ALPHA= 92.25 DALPHA= .05
V= 259.4
7. 41-0106
VOHPO484H2O
Triklin
Dexp Dcal d(D) h k l
7.4000 7.3984 .0016 0 0 1
6.5000 6.5030 -.0030 1 1 0
4.1900 4.1863 .0037 0 -2 1
4.0200 4.0189 .0011 -1 -2 1
3.8800 3.8812 -.0012 -2 -1 1
3.6900 3.6944 -.0044 -2 1 0
3.3600 3.3592 .0008 1 0 2
3.2500 3.2515 -.0015 2 2 0
3.1900 3.1945 -.0045 -1 -2 2
2.8600 2.8578 .0022 -2 2 0
2.8000 2.7981 .0019 -2 -2 2
2.6400 2.6406 -.0006 1 -3 1
A= 8.851 DA= .004
B= 8.856 DB= .001
C= 7.714 DC= .001
GAMMA= 81.67 DGAMMA= .01
BETA = 94.53 DBETA = .05
ALPHA=106.29 DALPHA= .03
V= 573.8
8. 41-0107
Cs4B2V12O35*8.3H2O
Rombik
Groupa 48
Dexp. Dcal. d(D) h k l
5.6000 5.6150 -.0150 0 1 1
4.8000 4.8018 -.0018 1 0 1
4.5000 4.4950 .0050 1 1 1
3.5300 3.5204 .0096 0 3 1
3.2400 3.2344 .0056 2 2 0
3.1210 3.1186 .0024 2 1 1
2.3680 2.3660 .0020 0 5 1
2.1410 2.1413 -.0003 1 4 2
1.9850 1.9832 .0018 1 1 3
1.9180 1.9194 -.0014 2 4 2
1.4350 1.4351 -.0001 3 7 1
1.4150 1.4150 .0000 5 3 0
1.3660 1.3662 -.0002 2 3 4
a= 7.501 b=12.781 c= 6.25052
da= .002 db= .004 dc= .0007
V= 599.2
Triklin
Dexp Dcal d(D) h k l
5.6000 5.6003 -.0003 -1 0 1
4.8000 4.8033 -.0033 0 1 1
4.5000 4.5019 -.0019 0 -1 1
3.5300 3.5292 .0008 -1 -1 1
3.2400 3.2402 -.0002 1 0 2
3.1210 3.1213 -.0003 -2 0 1
2.3680 2.3680 .0000 -2 2 1
2.1410 2.1411 -.0001 -3 1 1
1.9850 1.9849 .0001 -2 1 4
1.9180 1.9179 .0001 3 0 1
1.4350 1.4350 -.0000 -2 1 6
1.4150 1.4150 .0000 -4 -1 2
1.3660 1.3660 .0000 1 -4 1
A= 6.4974 DA= .0002
B= 5.6826 DB= .0001
C= 8.8821 DC= .0004
GAMMA=103.4855 DGAMMA= .0002
BETA =103.082 DBETA = .004
ALPHA= 83.100 DALPHA= .007
V= 309.8
9. 41-0108
Cs4B2V12O35*2.3H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
7.8000 7.7656 .0344 0 0 1
7.1000 7.1573 -.0573 1 0 1
3.9700 3.9654 .0046 4 0 1
3.5800 3.5787 .0013 2 0 2
3.4000 3.4006 -.0006 2 1 0
3.3100 3.3094 .0006 0 1 1
2.4100 2.4104 -.0004 6 0 2
a=18.448 b= 3.658 c= 7.766
da= .009 db= .002 dc= .008
V= 524
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
7.8000 7.7930 .0070 1 1 0
7.1000 7.1022 -.0022 1 0 1
3.9700 3.9700 .0000 0 2 1
3.5800 3.5812 -.0012 1 1 2
3.4000 3.3992 .0008 4 0 1
3.3100 3.3092 .0008 2 1 2
2.4100 2.4102 -.0002 6 1 0
a=14.9938 b= 9.12192 c= 8.0643
da= .0008 db= .00007 dc= .0003
V=1102.97
10. 41-0109
Cs4B2V12O35*H2O
Triklin
Dexp Dcal d(D) h k l
8.0000 8.0056 -.0056 1 0 0
4.0600 4.0548 .0052 -1 1 1
3.6600 3.6591 .0009 1 -1 1
3.5200 3.5242 -.0042 -1 -1 2
2.8000 2.7998 .0002 0 2 0
2.7880 2.7879 .0001 1 2 2
2.7060 2.7055 .0005 3 1 0
2.5780 2.5770 .0010 3 0 1
2.4490 2.4500 -.0010 2 -1 2
2.2810 2.2803 .0007 -1 -1 4
2.2700 2.2699 .0001 3 2 1
2.2100 2.2095 .0005 1 2 4
A= 8.310 DA= .001
B= 5.923 DB= .004
C= 11.153 DC= .004
GAMMA= 74.53 DGAMMA= .01
BETA = 88.45 DBETA = .02
ALPHA= 78.81 DALPHA= .03
V= 518.7
11. 41-0140
VO{ReO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
6.4300 6.4277 .0023 0 0 1
4.7600 4.7652 -.0052 0 -2 1
4.1700 4.1672 .0028 -1 1 0
3.9900 3.9873 .0027 1 -1 1
3.7900 3.7940 -.0040 0 -3 1
3.4800 3.4762 .0038 0 4 0
3.2500 3.2519 -.0019 1 -3 1
3.1700 3.1700 -.0000 -1 0 1
3.0800 3.0824 -.0024 0 -4 1
2.9400 2.9387 .0013 0 -2 2
2.7800 2.7809 -.0009 0 5 0
2.6000 2.5995 .0005 1 2 2
A= 4.373 DA= .001
B= 14.04 DB= .01
C= 6.6460 DC= .0003
GAMMA= 97.96 DGAMMA= .05
BETA = 75.319 DBETA = .007
ALPHA= 93.07 DALPHA= .01
V= 390.9
12. 41-0141
VO{ReO4}2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.6600 5.6459 .0141 0 2 1
5.1100 5.1106 -.0006 0 2 2
4.6600 4.6605 -.0005 1 0 1
4.1600 4.1653 -.0053 0 0 5
3.8400 3.8432 -.0032 0 3 1
3.4700 3.4710 -.0010 0 0 6
2.8800 2.8839 -.0039 0 1 7
2.6000 2.5959 .0041 0 3 6
2.4000 2.3980 .0020 0 4 5
2.2800 2.2814 -.0014 1 3 6
2.2000 2.2016 -.0016 2 2 1
a= 4.782 b=11.73 c=20.83
da= .003 db= .01 dc= .01
V=1168
Triklin
Dexp Dcal d(D) h k l
5.6600 5.6581 .0019 0 1 0
5.1100 5.1057 .0043 0 -1 2
4.6600 4.6574 .0026 1 -1 1
4.1600 4.1582 .0018 1 0 3
3.8400 3.8372 .0028 1 -1 3
3.4700 3.4729 -.0029 -1 0 5
2.8800 2.8791 .0009 -1 2 0
2.6000 2.5997 .0003 -1 2 3
2.4000 2.3996 .0004 0 -2 5
2.2800 2.2800 .0000 -1 2 5
2.2000 2.2004 -.0004 1 2 2
2.1300 2.1307 -.0007 2 -1 6
A= 6.2510 DA= .0001
B= 5.8927 DB= .0006
C= 19.725 DC= .002
GAMMA=105.35 DGAMMA= .01
BETA = 95.86 DBETA = .01
ALPHA= 93.556 DALPHA= .003
V= 694.0
13. 41 - 0146
Bi8V2O17
Rombik
Groupa 50
Dexp. Dcal. d(D) h k l
3.3000 3.2981 .0019 0 0 3
3.0100 3.0146 -.0046 1 1 2
2.7400 2.7397 .0003 2 1 2
1.9810 1.9814 -.0004 5 1 0
1.8950 1.8956 -.0006 6 0 0
1.6910 1.6904 .0006 6 1 1
1.6470 1.6470 .0000 2 2 3
1.6230 1.6228 .0002 4 2 1
1.5610 1.5611 -.0001 4 2 2
a=11.374 b= 4.0340 c= 9.894
da= .002 db= .0001 dc= .009
V= 453.9
14. 41-0433
GdVTa2O9
Triklin
Dexp Dcal d(D) h k l
7.7100 7.7108 -.0008 1 0 0
4.9300 4.9291 .0009 -1 1 1
4.7100 4.7076 .0024 -1 -1 1
3.6900 3.6895 .0005 0 2 2
3.5700 3.5700 .0000 2 1 0
3.4800 3.4841 -.0041 -1 -1 2
3.3300 3.3296 .0004 -2 0 1
3.2400 3.2373 .0027 0 3 1
3.1900 3.1867 .0033 1 -1 3
3.0500 3.0503 -.0003 1 3 1
2.8500 2.8513 -.0013 2 -2 2
2.6800 2.6806 -.0006 -1 -1 3
A= 7.978 DA= .003
B= 10.037 DB= .005
C= 10.49 DC= .01
GAMMA= 90.33 DGAMMA= .03
BETA = 75.19 DBETA = .03
ALPHA= 86.23 DALPHA= .07
V= 810.3
15. 41-0434
DyVTa2O9
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9299 .0001 -1 1 0
4.6800 4.6783 .0017 0 1 1
3.7100 3.7105 -.0005 0 -1 1
3.4800 3.4790 .0010 1 -1 1
2.9500 2.9485 .0015 1 1 1
2.6600 2.6613 -.0013 -2 2 1
2.6200 2.6201 -.0001 0 -1 2
2.5200 2.5197 .0003 -2 2 2
2.4700 2.4708 -.0008 1 -1 2
2.0800 2.0795 .0005 -3 2 1
2.0500 2.0496 .0004 2 0 2
2.0100 2.0106 -.0006 2 1 1
A= 6.5138 DA= .0008
B= 5.9290 DB= .0009
C= 7.667 DC= .001
GAMMA=118.78 DGAMMA= .04
BETA =107.50 DBETA = .03
ALPHA= 69.75 DALPHA= .01
V= 240.3
16. 41-0435
HoVTa2O9
Triklin
Dexp Dcal d(D) h k l
7.7300 7.7397 -.0097 0 1 0
4.9300 4.9369 -.0069 0 -1 2
4.6700 4.6610 .0090 1 0 0
3.6900 3.6927 -.0027 1 -1 1
3.5900 3.5970 -.0070 0 -2 2
3.4900 3.4961 -.0061 0 -1 3
3.3400 3.3408 -.0008 -1 1 1
3.0500 3.0521 -.0021 -1 -2 2
2.9300 2.9294 .0006 1 2 1
2.8600 2.8594 .0006 -1 -1 3
2.6800 2.6795 .0005 1 -2 2
2.6500 2.6496 .0004 -1 -2 3
A= 4.727 DA= .001
B= 8.158 DB= .002
C= 10.6471 DC= .0009
GAMMA= 80.543 DGAMMA= .008
BETA = 90.99 DBETA = .05
ALPHA=105.84 DALPHA= .09
V= 389.6
17. 41-0435
HoVTa2O9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.7300 7.7378 -.0078 2 0 0
4.9300 4.9314 -.0014 1 0 3
4.6700 4.6663 .0037 2 0 3
3.6900 3.6939 -.0039 1 0 4
3.5900 3.5939 -.0039 1 1 0
3.4900 3.4908 -.0008 -4 0 1
3.3400 3.3377 .0023 2 1 1
3.0500 3.0536 -.0036 -4 0 2
2.9300 2.9274 .0026 -2 0 4
2.8600 2.8604 -.0004 -5 0 1
2.6800 2.6794 .0006 6 0 2
2.6500 2.6504 -.0004 -4 0 3
a= 16.13 b=3.695 c= 14.80 beta= 73.57
da= .01 db=.001 dc=.02 dbeta=.09
V= 846
Triklin
Dexp Dcal d(D) h k l
7.7300 7.7302 -.0002 0 1 0
4.9300 4.9323 -.0023 0 -1 2
4.6700 4.6674 .0026 1 0 0
3.6900 3.6939 -.0039 1 -1 1
3.5900 3.5923 -.0023 0 -2 2
3.4900 3.4936 -.0036 0 -1 3
3.3400 3.3415 -.0016 -1 1 1
3.0500 3.0517 -.0017 -1 -2 2
2.9300 2.9297 .0003 1 2 1
2.8600 2.8597 .0003 -1 -1 3
2.6800 2.6780 .0020 0 -3 1
2.6500 2.6488 .0012 -1 -2 3
A= 4.734 DA= .006
B= 8.15 DB= .01
C= 10.641 DC= .005
GAMMA= 80.511 DGAMMA= .001
BETA = 90.99 DBETA = .06
ALPHA=105.81 DALPHA= .01
V=389.5
18. 41-0436
ErVIa2O9
Triklin
Dexp Dcal d(D) h k l
7.7500 7.7588 -.0088 1 0 0
4.9100 4.9074 .0026 -1 1 1
4.6600 4.6581 .0019 1 -1 1
3.6900 3.6922 -.0022 1 1 1
3.4800 3.4867 -.0067 -1 0 2
3.3300 3.3262 .0038 0 1 2
3.2400 3.2385 .0015 0 -1 2
3.0500 3.0501 -.0001 -2 2 0
2.8500 2.8523 -.0023 -2 1 2
2.6800 2.6812 -.0012 2 1 1
2.6500 2.6483 .0017 -3 1 1
2.4800 2.4815 -.0015 1 2 1
A= 8.3387 DA= .0009
B= 6.7785 DB= .0005
C= 7.6963 DC= .0009
GAMMA=111.43 DGAMMA= .04
BETA = 92.59 DBETA = .01
ALPHA= 87.460 DALPHA= .005
V= 404.4
19. 41-0437
TmVTa2O9
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7583 .0017 1 0 0
4.9300 4.9330 -.0030 1 1 1
4.6600 4.6575 .0025 -1 -1 1
3.8900 3.8919 -.0019 -1 2 0
3.7000 3.6991 .0009 2 0 1
3.5000 3.4989 .0011 -2 0 1
3.3400 3.3393 .0007 -1 -2 1
3.3100 3.3104 -.0004 2 1 1
2.9800 2.9798 .0002 -1 2 2
2.9000 2.9017 -.0017 -2 0 2
2.8700 2.8699 .0001 -1 0 3
2.8100 2.8093 .0007 -2 1 2
A= 7.8090 DA= .0001
B= 8.6087 DB= .0004
C= 9.597 DC= .001
GAMMA= 94.67 DGAMMA= .01
BETA = 85.481 DBETA = .008
ALPHA= 89.55 DALPHA= .01
V=641.7
20. 41-0438
LuVTa2O9
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7671 -.0071 -1 0 1
4.9300 4.9325 -.0025 1 1 1
4.6300 4.6297 .0003 -1 -1 1
3.9000 3.9009 -.0009 1 1 2
3.7100 3.7104 -.0004 0 -1 2
3.4900 3.4885 .0015 0 0 3
3.3400 3.3377 .0023 -3 0 1
3.0500 3.0512 -.0012 -2 0 3
2.9900 2.9904 -.0004 1 2 0
2.8700 2.8702 -.0002 3 1 1
2.8000 2.7996 .0004 -1 2 2
2.6400 2.6399 .0001 -3 -1 2
A= 10.220 DA= .003
B= 6.284 DB= .001
C= 10.6820 DC= .0005
GAMMA= 89.34 DGAMMA= .03
BETA = 96.73 DBETA = .01
ALPHA= 80.730 DALPHA= .001
V= 672.1
21. 41-0492
NH4V3O8*0.5H2O
Triklin
Dexp Dcal d(D) h k l
7.8932 7.8933 -.0001 0 1 1
5.7487 5.7385 .0102 1 1 0
4.9786 4.9824 -.0038 0 -1 1
4.4356 4.4389 -.0033 0 2 0
4.2668 4.2664 .0004 -1 -1 1
3.8969 3.8997 -.0028 -1 2 2
3.6156 3.6110 .0046 2 1 0
3.5587 3.5619 -.0032 2 0 1
3.2522 3.2523 -.0001 -1 3 1
3.2291 3.2282 .0009 -2 2 2
3.0353 3.0362 -.0009 -1 -2 1
2.9190 2.9190 .0000 0 2 3
A= 8.5516 DA= .0001
B= 10.0238 DB= .0001
C= 9.0511 DC= .0004
GAMMA=100.83 DGAMMA= .01
BETA =100.013 DBETA = .007
ALPHA= 63.211 DALPHA= .001
V=676.7
22. 41-0498
CeVTa2O9
Triklin
Dexp Dcal d(D) h k l
5.3400 5.3462 -.0062 0 1 0
4.9400 4.9430 -.0030 1 0 1
4.8400 4.8337 .0063 0 -1 2
4.7100 4.7111 -.0011 -1 0 1
3.6700 3.6714 -.0014 1 -1 4
3.3000 3.3019 -.0019 -1 0 4
3.0500 3.0506 -.0006 1 1 1
2.9500 2.9492 .0008 1 1 2
2.8500 2.8492 .0008 0 -1 6
2.7500 2.7502 -.0002 0 0 7
2.6200 2.6204 -.0004 0 2 1
2.5600 2.5602 -.0002 1 -1 7
A= 5.4914 DA= .0007
B= 5.8815 DB= .0001
C= 19.506 DC= .003
GAMMA=114.27 DGAMMA= .02
BETA = 81.85 DBETA = .01
ALPHA= 97.3337 DALPHA= .0001
V= 566.8
23. 41-0499
PrVTa2O9
Triklin
Dexp Dcal d(D) h k l
5.3200 5.3249 -.0049 0 1 1
4.9200 4.9201 -.0001 1 0 0
4.8000 4.7896 .0104 0 -1 1
4.6700 4.6700 .0000 1 0 1
3.6300 3.6285 .0015 -1 0 2
3.3000 3.2941 .0059 1 1 0
3.0500 3.0500 -.0000 1 1 2
2.9500 2.9470 .0030 -1 0 3
2.8000 2.8003 -.0003 0 2 1
2.7200 2.7204 -.0004 -1 -1 2
2.6200 2.6232 -.0032 1 -2 1
2.5800 2.5781 .0019 -1 2 2
A= 5.0961 DA= .0001
B= 5.813 DB= .001
C= 11.836 DC= .009
GAMMA=104.43 DGAMMA= .02
BETA = 87.36 DBETA = .02
ALPHA= 83.112 DALPHA= .008
V= 336.1
24. 41-0500
SmVTa2O9
Triklin
Dexp Dcal d(D) h k l
5.3400 5.3417 -.0017 -1 1 0
4.9500 4.9573 -.0073 1 1 1
4.7600 4.7569 .0031 -1 0 1
4.7100 4.7065 .0035 0 2 0
3.6100 3.6123 -.0023 2 1 1
3.3000 3.2981 .0019 -2 1 0
3.0500 3.0502 -.0002 0 -2 2
2.9500 2.9522 -.0022 -1 2 1
2.8000 2.7996 .0004 1 3 1
2.7000 2.7000 .0000 2 -2 1
2.6200 2.6198 .0002 3 1 1
2.5700 2.5693 .0007 0 2 2
A= 8.129 DA= .001
B= 9.853 DB= .001
C= 7.0635 DC= .0004
GAMMA= 76.15 DGAMMA= .03
BETA = 82.24 DBETA = .06
ALPHA= 98.01 DALPHA= .02
V=535.4
25. 41-0644
Cs2{HBV6O18}83.65H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6000 5.5945 .0055 1 0 1
4.8000 4.8080 -.0080 1 1 0
4.5000 4.4925 .0075 1 1 1
3.5300 3.5286 .0014 0 0 2
3.2400 3.2420 -.0020 2 0 1
3.1210 3.1213 -.0003 2 0 0
2.3680 2.3672 .0008 0 3 1
2.1410 2.1407 .0003 2 1 3
1.9850 1.9860 -.0010 2 3 1
1.9180 1.9209 -.0029 2 2 3
1.4350 1.4347 .0003 -4 0 1
1.4150 1.4149 .0001 -1 5 1
1.3660 1.3662 -.0002 -3 0 3
a= 6.5521 b= 7.5382 c= 7.41 beta= 72.31
da=.0009 db=.0006 dc=.01 dbeta=.03
V= 348.6
26. 41-0653
NH4VOF3
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
6.9000 6.8815 .0185 1 0 1
5.8000 5.7926 .0074 2 0 0
4.8000 4.7963 .0037 2 0 1
4.2700 4.2770 -.0070 0 0 2
3.8100 3.8200 -.0100 0 1 0
3.5100 3.5197 -.0097 3 0 1
3.4300 3.4407 -.0107 2 0 2
3.3500 3.3399 .0101 1 1 1
3.1800 3.1890 -.0090 2 1 0
2.9000 2.8963 .0037 4 0 0
2.8500 2.8491 .0009 0 1 2
2.7700 2.7666 .0034 1 1 2
a=11.58 b= 3.820 c= 8.554
da= .01 db= .004 dc= .007
V= 378
Triklin
Dexp Dcal d(D) h k l
6.9000 6.8951 .0049 1 0 0
5.8000 5.7933 .0067 0 1 1
4.8000 4.8005 -.0005 0 -1 1
4.2700 4.2732 -.0032 0 2 0
3.8100 3.8125 -.0025 1 2 0
3.5100 3.5117 -.0017 -1 2 1
3.4300 3.4296 .0004 -2 0 1
3.3500 3.3498 .0002 1 2 1
3.1800 3.1797 .0003 -2 1 1
2.9000 2.9000 -.0000 0 -1 2
2.8500 2.8488 .0012 0 3 0
2.7700 2.7702 -.0002 1 -2 1
A= 7.1347 DA= .0003
B= 8.7229 DB= .0001
C= 6.9298 DC= .0002
GAMMA= 86.691 DGAMMA= .002
BETA =103.699 DBETA = .005
ALPHA= 80.0709 DALPHA= .0001
V=410.8
27. 41-0654
{NH4}3VOF5
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
5.2300 5.2131 .0169 2 0 1
4.5600 4.5551 .0049 2 1 0
4.4700 4.4768 -.0068 4 0 0
3.2100 3.2060 .0040 0 0 2
2.7100 2.7103 -.0003 1 1 2
2.6100 2.6065 .0035 4 0 2
2.3600 2.3591 .0009 2 2 1
2.3000 2.3031 -.0031 7 1 0
2.2400 2.2384 .0016 8 0 0
2.0000 1.9996 .0004 7 0 2
1.9000 1.9003 -.0003 9 0 1
1.8640 1.8624 .0016 9 1 0
a=17.907 b= 5.291 c= 6.412
da= .001 db= .002 dc= .003
V= 607.5
Triklin
Dexp Dcal d(D) h k l
5.2300 5.2259 .0041 1 0 1
4.5600 4.5615 -.0015 0 1 1
4.4700 4.4668 .0032 0 -1 1
3.2100 3.2078 .0022 2 1 1
2.7100 2.7093 .0007 0 0 2
2.6100 2.6130 -.0030 2 0 2
2.3600 2.3604 -.0004 -2 1 0
2.3000 2.3000 .0000 2 -1 2
2.2400 2.2409 -.0009 2 3 2
2.0000 1.9997 .0003 -2 2 0
1.9000 1.9004 -.0004 -2 1 1
1.8640 1.8636 .0004 1 4 2
A= 6.424 DA= .003
B= 8.634 DB= .004
C= 6.233 DC= .003
GAMMA= 70.89 DGAMMA= .01
BETA = 60.41 DBETA = .03
ALPHA= 79.61 DALPHA= .01
V= 284.0
28. 41-0655
{NH4}3VOF5
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
5.3500 5.3572 -.0072 0 3 0
4.6500 4.6524 -.0024 1 3 0
3.2200 3.2143 .0057 0 5 0
2.3900 2.3897 .0003 1 1 1
2.0400 2.0406 -.0006 2 3 1
1.9640 1.9644 -.0004 1 8 0
1.8640 1.8640 -.0000 5 1 0
1.7570 1.7567 .0003 3 4 1
a= 9.383 b=16.07 c= 2.5009
da= .001 db= .01 dc= .0008
V=377.1
29. 41-0656
{NH4}3VOF5
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
5.3000 5.3048 -.0048 1 1 0
4.6000 4.5917 .0083 1 0 1
3.2800 3.2792 .0008 1 2 0
2.0500 2.0502 -.0002 2 3 0
1.8300 1.8301 -.0001 0 1 3
1.7600 1.7600 .0000 1 4 0
a= 7.813 b= 7.226 c= 5.675
da= .001 db= .002 dc= .001
V= 320.4
30. 41-0674
Na4VO{SO4}3
Triklin
Dexp Dcal d(D) h k l
6.7600 6.7633 -.0033 0 1 1
5.4200 5.4180 .0020 2 1 0
5.3700 5.3714 -.0014 -2 -1 1
4.3100 4.3112 -.0012 2 2 0
4.1400 4.1378 .0022 2 1 1
3.8500 3.8498 .0002 -3 -1 1
3.6600 3.6574 .0026 1 0 2
3.4300 3.4264 .0036 3 2 0
3.2700 3.2705 -.0005 -3 0 2
3.2300 3.2288 .0012 1 3 0
3.0700 3.0679 .0021 3 1 1
2.9600 2.9633 -.0033 3 2 1
A= 11.6034 DA= .0006
B= 9.753 DB= .001
C= 9.5196 DC= .0003
GAMMA= 67.330 DGAMMA= .006
BETA =108.509 DBETA = .006
ALPHA= 90.695 DALPHA= .003
V=935.2
31. 41-0675
K3V2O2{SO4}4
Triklin
Dexp Dcal d(D) h k l
8.9700 8.9763 -.0063 0 1 1
7.8300 7.8282 .0018 -1 1 0
6.3000 6.3001 -.0001 0 -1 1
4.4100 4.4104 -.0004 1 1 2
4.3000 4.3023 -.0023 -1 2 2
4.0400 4.0435 -.0035 1 -2 1
3.9800 3.9800 .0000 2 -1 1
3.8300 3.8297 .0003 1 2 2
3.5600 3.5594 .0006 -2 -1 1
3.3500 3.3498 .0002 2 1 2
3.2400 3.2405 -.0005 2 2 0
3.1600 3.1603 -.0003 1 3 0
A= 9.529 DA= .003
B= 11.698 DB= .002
C= 10.553 DC= .00301
GAMMA=101.38 DGAMMA= .06
BETA = 93.41 DBETA = .04
ALPHA= 69.79 DALPHA= .01
V= 1082.2