1. 37-0076
Tm7V3O16
Triklin
Dexp. Dcal. d(D) h k l
5.7800 5.7527 .0273 0 -1 0
3.2000 3.1989 .0011 -3 0 1
3.0500 3.0500 .0000 3 -1 0
2.8780 2.8764 .0016 0 -2 0
2.6950 2.6952 -.0002 -2 -2 0
2.6240 2.6222 .0018 -1 -2 1
2.5760 2.5769 -.0009 0 -2 1
2.2060 2.2057 .0003 0 -1 2
2.1360 2.1360 .0000 -2 2 1
2.0920 2.0922 -.0002 1 -1 2
1.9380 1.9376 .0004 2 -1 2
1.9175 1.9176 -.0001 0 -3 0
A= 11.807 DA= .003
B= 5.8474 DB= .0005
C= 4.646 DC= .001
GAMMA= 82.446 DGAMMA= .003
BETA =100.09 DBETA = .05
ALPHA= 98.22 DALPHA= .02
V= 310.7
2. 37-0077
NdVO7
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.2660 3.2664 -.0004 5 1 0
3.1440 3.1420 .0020 2 1 1
3.1110 3.1144 -.0034 3 0 1
2.9190 2.9208 -.0018 3 1 1
2.7880 2.7869 .0011 6 1 0
2.7090 2.7107 -.0017 5 2 0
1.9700 1.9690 .0010 9 0 0
1.9160 1.9172 -.0012 9 1 0
1.8670 1.8668 .0002 7 2 1
a=17.721 b= 8.415 c= 3.665
da= .001 db= .003 dc= .003
V= 546.6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.2660 3.2652 .0008 2 1 0
3.1440 3.1443 -.0003 -2 0 2
3.1110 3.1085 .0025 1 1 2
2.9190 2.9181 .0009 -1 0 3
2.7880 2.7869 .0011 0 2 2
2.7090 2.7070 .0020 -1 1 3
1.9700 1.9703 -.0003 -3 2 2
1.9160 1.9160 .0000 -2 3 2
1.8670 1.8677 -.0007 0 2 4
a= 7.480 b=7.249 c=8.915 beta= 102.07
da=.002 db=.001 dc= .006 dbeta=.05
V= 472.7
3. 37-0078
La3VO7
Triklin
Dexp Dcal d(D) h k l
3.3300 3.3313 -.0013 0 1 1
3.1930 3.1919 .0011 0 -1 1
3.1820 3.1807 .0013 1 1 0
3.0510 3.0524 -.0014 1 -1 1
2.9830 2.9821 .0009 0 0 2
2.9590 2.9573 .0017 -2 0 1
2.8580 2.8585 -.0005 1 1 1
2.7550 2.7572 -.0022 -1 -1 1
2.1260 2.1257 .0003 -3 0 1
2.0150 2.0149 .0001 2 -1 2
2.0050 2.0054 -.0004 -3 1 1
1.9880 1.9880 -.0000 0 0 3
1.9530 1.9527 .0003 -1 2 0
A= 6.9381 DA= .0001
B= 3.94298 DB= .00001
C= 5.97066 DC= .00003
GAMMA= 98.8472 DGAMMA= .0009
BETA = 89.762 DBETA = .001
ALPHA= 87.4010 DALPHA= .0003
V=161.2
4. 37-079
Eu3VO7
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.1100 3.1095 .0005 0 2 0
2.7000 2.6975 .0025 2 0 0
1.9300 1.9298 .0002 0 1 1
1.7990 1.7983 .0007 3 0 0
1.7270 1.7276 -.0006 3 1 0
1.6220 1.6220 -.0000 2 0 1
a= 5.395 b= 6.22 c= 2.030
da= .001 db= .02 dc= .001
V=68.1
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
3.1100 3.1095 .0005 0 2 0
2.7000 2.6975 .0025 2 0 0
1.9300 1.9298 .0002 0 1 2
1.7990 1.7983 .0007 3 0 0
1.7270 1.7276 -.0006 3 1 0
1.6220 1.6220 -.0000 2 0 2
a= 5.395 b= 6.219 c= 4.060
da= .001 db= .003 dc= .001
v= 136.2
5. 37-0093
V2Te2O9
Triklin
Dexp Dcal d(D) h k l
4.8500 4.8589 -.0089 -1 2 0
4.3200 4.3215 -.0015 2 0 0
3.7000 3.6916 .0084 0 3 0
3.5000 3.5071 -.0071 -1 3 0
3.2900 3.2928 -.0028 1 3 0
3.1000 3.1013 -.0013 1 0 1
3.0500 3.0502 -.0002 0 -1 1
2.8500 2.8494 .0006 -3 1 0
2.7400 2.7402 -.0002 2 0 1
2.6300 2.6294 .0006 1 2 1
2.4600 2.4598 .0002 1 -3 1
2.4300 2.4294 .0006 -2 4 0
A= 8.7787 DA= .0002
B= 11.1322 DB= .0002
C= 3.1778 DC= .0002
GAMMA= 95.398 DGAMMA= .004
BETA = 81.232 DBETA = .003
ALPHA= 92.991 DALPHA= .003
V=304.8
6. 37-0094
KV3Te3O14
Triklin
Dexp Dcal d(D) h k l
6.1000 6.1185 -.0185 0 1 1
5.5300 5.5237 .0063 0 -1 1
4.0900 4.0851 .0049 1 1 0
3.8300 3.8324 -.0024 1 0 1
3.7000 3.7011 -.0011 0 0 2
3.4700 3.4697 .0003 -1 -1 1
3.3100 3.3125 -.0025 1 2 0
3.1400 3.1394 .0006 1 2 1
3.1100 3.1093 .0007 0 3 0
3.0600 3.0592 .0008 0 2 2
2.9800 2.9802 -.0002 0 3 1
2.8500 2.8497 .0003 1 1 2
A= 4.411 DA= .002
B= 9.4030 DB= .0008
C= 7.4483 DC= .0006
GAMMA= 85.96 DGAMMA= .03
BETA = 87.85 DBETA = .01
ALPHA= 83.866 DALPHA= .008
V=306.7
7. 37-0105
Cs2V4O11
Triklin
Dexp Dcal d(D) h k l
6.1680 6.1627 .0053 0 1 0
4.9280 4.9263 .0017 -1 0 1
3.5240 3.5242 -.0002 0 -1 2
2.8490 2.8476 .0014 -1 -1 2
2.7978 2.7984 -.0006 1 -2 2
2.6110 2.6115 -.0005 3 -1 1
2.4660 2.4660 .0000 3 0 1
2.4580 2.4584 -.0004 3 0 0
2.4170 2.4184 -.0014 2 -1 3
2.2980 2.2968 .0012 2 0 3
2.2200 2.2201 -.0001 -2 -1 2
2.1880 2.1882 -.0002 1 -3 1
A= 7.897 DA= .001
B= 6.5854 DB= .0004
C= 8.005 DC= .001
GAMMA=108.63 DGAMMA= .04
BETA = 76.947 DBETA = .003
ALPHA=102.57 DALPHA= .02
V= 379.5
8. 37-0164
Cs4V2O7
Triklin
Dexp Dcal d(D) h k l
6.1940 6.2120 -.0180 2 0 0
5.4850 5.4920 -.0070 -1 0 1
4.4530 4.4612 -.0082 -2 1 0
4.3410 4.3382 .0028 0 2 0
4.2710 4.2633 .0077 3 1 0
4.1640 4.1673 -.0033 2 1 1
3.5700 3.5738 -.0038 3 2 0
3.5480 3.5472 .0008 -1 -2 1
3.4090 3.4085 .0005 3 1 1
3.3070 3.3062 .0008 3 0 1
3.2780 3.2774 .0006 -1 2 1
3.2480 3.2471 .0009 4 1 0
A= 13.028 DA= .001
B= 9.095 DB= .004
C= 5.959 DC= .002
GAMMA= 72.82 DGAMMA= .02
BETA = 92.64 DBETA = .05
ALPHA= 87.80 DALPHA= .07
V=671.9
9. 37-0165
CsVO3
Triklin
Dexp Dcal d(D) h k l
5.3920 5.3915 .0005 0 1 1
5.0500 5.0480 .0020 -1 1 1
4.9280 4.9348 -.0068 0 -1 1
4.1990 4.2031 -.0041 -1 2 0
4.0510 4.0499 .0011 -1 -1 1
3.7600 3.7639 -.0039 -1 2 1
3.6570 3.6547 .0023 -2 1 1
3.3190 3.3206 -.0016 2 1 0
3.2670 3.2686 -.0016 2 -1 1
3.0620 3.0607 .0013 1 2 1
2.8940 2.8937 .0003 -1 3 0
2.8400 2.8389 .0011 2 -2 1
A= 8.38587 DA= .00008
B= 8.7801 DB= .0005
C= 6.5652 DC= .0003
GAMMA=105.3771 DGAMMA= .0008
BETA = 96.115 DBETA = .001
ALPHA= 83.360 DALPHA= .001
V=461.2
10. 37-0166
Cs2V6O16
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
5.8670 5.8754 -.0084 1 1 0
4.4260 4.4359 -.0099 -1 0 1
4.2500 4.2540 -.0040 0 2 0
4.0580 4.0618 -.0038 2 0 0
3.9340 3.9334 .0006 -1 1 1
3.7600 3.7685 -.0085 1 2 0
3.6690 3.6715 -.0025 1 1 1
3.3020 3.3058 -.0038 -2 0 1
3.2270 3.2325 -.0055 0 2 1
3.0790 3.0814 -.0024 -2 1 1
3.0040 3.0069 -.0029 2 0 1
2.9440 2.9408 .0032 1 2 1
a= 8.161 b= 8.51 c= 5.00 beta= 95.53
da=.005 db=.01 dc=.01 dbet=.02
V=344.5
11. 37-0168
KFeV2O7
Triklin
Dexp Dcal d(D) h k l
8.7100 8.7056 .0044 1 0 0
7.0400 7.0484 -.0084 0 1 1
6.3500 6.3508 -.0008 0 -1 1
5.0000 4.9984 .0016 0 -2 1
4.4800 4.4783 .0017 0 3 1
4.3100 4.3111 -.0011 -1 -2 1
3.9400 3.9380 .0020 2 0 1
3.6800 3.6820 -.0020 2 -1 1
3.6200 3.6199 .0001 -1 -3 1
3.5000 3.5005 -.0005 0 -1 2
3.3400 3.3394 .0006 1 -1 2
3.1600 3.1603 -.0003 1 3 2
A= 8.80 DA= .01
B= 15.467 DB= .006
C= 7.538 DC= .006
GAMMA= 84.10 DGAMMA= .05
BETA = 83.27 DBETA = .09
ALPHA= 81.82 DALPHA= .05
V=1005
12. 37-0169
KAlV2O7
Triklin
Dexp Dcal d(D) h k l
8.7500 8.7551 -.0051 1 0 0
6.9600 6.9608 -.0008 0 1 0
6.3100 6.3118 -.0018 0 -1 1
4.5000 4.5073 -.0073 -1 1 1
3.8300 3.8330 -.0030 1 1 1
3.6000 3.6000 .0000 2 1 0
3.4800 3.4804 -.0004 0 2 0
3.4000 3.4001 -.0001 -2 -1 2
3.1100 3.1116 -.0016 -1 -2 2
3.0100 3.0101 -.0001 -3 0 1
2.9400 2.9393 .0007 -1 -1 3
2.6100 2.6103 -.0003 -2 2 1
2.2200 2.2199 .0001 3 -2 1
2.1400 2.1399 .0001 -4 -1 2
2.0800 2.0797 .0003 0 3 1
A= 9.072 DA= .001
B= 7.2833 DB= .0003
C= 8.919 DC= .002
GAMMA= 89.33 DGAMMA= .01
BETA =104.73 DBETA = .01
ALPHA=106.71 DALPHA= .05
V= 544.7
13. 37-0175
K2V6O16
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
7.6200 7.6240 -.0040 0 1 0
5.6400 5.6203 .0197 1 1 0
3.2000 3.2001 -.0001 2 0 1
2.8500 2.8501 -.0001 1 2 1
2.8100 2.8102 -.0002 2 2 0
a= 8.318 b= 7.624 c= 5.01
da= .001 db= .001 dc= .001
V= 317.7
14. 37-0176
NaV3O8*xH2O
Rombik
Groupa 60
Dexp. Dcal. d(D) h k l
8.0300 8.0400 -.0100 0 0 2
3.4300 3.4309 -.0009 1 1 0
3.1100 3.1092 .0008 2 0 2
2.8900 2.8896 .0004 1 1 3
2.3200 2.3203 -.0003 2 1 3
1.8000 1.8000 .0000 1 2 3
a= 6.743 b= 3.98530 c=16.080
da= .001 db= .00001 dc= .001
Vv= 432.12
15. 37-0177
CaV6O16*xH2O
Rombik
Grupa 19
Dexp. Dcal. d(D) h k l
7.8500 7.8700 -.0200 0 0 1
3.4400 3.4355 .0045 2 1 1
3.1000 3.1005 -.0005 3 0 1
2.9100 2.9099 .0001 0 2 0
2.3200 2.3202 -.0002 4 1 0
1.8000 1.7999 .0001 5 0 2
a=10.120 b= 5.8198 c= 7.870
da= .001 db= .001 dc= .001
V= 463.5
16. 37-0180
K2Ca{VO3}4
Triklin
Dexp Dcal d(D) h k l
4.3100 4.3126 -.0026 0 1 2
4.2600 4.2601 -.0001 0 -1 2
4.1400 4.1414 -.0014 0 -3 1
3.8800 3.8812 -.0012 -1 3 0
3.7600 3.7595 .0005 0 -2 2
3.3300 3.3298 .0002 1 3 2
3.2700 3.2687 .0013 0 -4 1
3.1900 3.1899 .0001 3 1 0
3.1200 3.1200 .0000 -2 0 2
2.9600 2.9601 -.0001 1 -3 2
2.8900 2.8903 -.0003 1 5 0
2.8100 2.8096 .0004 0 4 2
A= 9.60388 DA= .00012
B= 14.51556 DB= .00100
C= 9.02888 DC= .00024
GAMMA= 77.18940 DGAMMA= .00456
BETA = 85.16428 DBETA = .00267
ALPHA= 87.75205 DALPHA= .00167
V=1222
17. 37-0181
K2CaV2O7
Triklin
Dexp Dcal d(D) h k l
4.3500 4.3525 -.0025 1 0 1
3.7200 3.7181 .0019 2 -1 1
3.7000 3.7000 -.0000 -3 1 0
3.4900 3.4884 .0016 2 1 1
3.2900 3.2917 -.0017 2 -2 1
3.1200 3.1210 -.0010 -3 2 0
3.1100 3.1094 .0006 3 -1 1
3.0700 3.0703 -.0003 -1 -3 1
3.0100 3.0136 -.0036 3 1 1
2.8700 2.8696 .0004 -3 0 1
2.8300 2.8288 .0012 3 -2 1
2.6900 2.6888 .0012 3 2 1
A= 12.362 DA= .002
B= 11.248 DB= .003
C= 4.5824 DC= .0008
GAMMA= 84.98 DGAMMA= .01
BETA = 85.078 DBETA = .002
ALPHA=100.93 DALPHA= .01
V=619.6
18. 37-0182
KCaVO4
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
4.2000 4.2032 -.0032 0 0 4
4.0900 4.0875 .0025 1 1 0
3.8200 3.8245 -.0045 0 2 1
3.0400 3.0362 .0038 1 2 0
2.9900 2.9879 .0021 1 2 1
2.8700 2.8697 .0003 0 2 4
2.8500 2.8557 -.0057 1 2 2
2.0800 2.0798 .0002 2 0 4
2.0700 2.0708 -.0008 1 1 7
2.0500 2.0490 .0010 0 2 7
a= 4.787 b= 7.85492 c=16.813
da= .002 db= .00009 dc= .009
V= 632.1
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
4.2000 4.2001 -.0001 -1 1 1
4.0900 4.0900 -.0000 0 2 0
3.8200 3.8154 .0046 1 1 1
3.0400 3.0398 .0002 -1 0 2
2.9900 2.9937 -.0037 0 1 2
2.8700 2.8695 .0005 -2 1 1
2.8500 2.8495 .0005 -1 1 2
2.0800 2.0800 .0000 0 3 2
2.0700 2.0700 .0000 -3 1 1
2.0500 2.0500 .0000 -1 1 3
a= 6.5633 b= 8.1800 c= 6.485 beta= 97.217
da=.0006 db=.0008 dc=.001 dbet=.006
V=345.4
19. 37-0183
K4Ca{VO4}2
Momnoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1200 4.1194 .0006 2 1 0
4.0100 4.0097 .0003 -2 0 1
3.1200 3.1200 .0000 1 2 1
2.9900 2.9885 .0015 -2 0 2
2.9500 2.9499 .0001 -3 0 1
2.8600 2.8564 .0036 1 1 3
2.7600 2.7625 -.0025 2 1 3
2.7300 2.7331 -.0031 -2 1 2
2.6800 2.6796 .0004 -1 0 3
2.4700 2.4699 .0001 3 2 1
2.4200 2.4188 .0012 3 2 0
2.1500 2.1502 -.0002 5 0 2
2.0600 2.0597 .0003 4 2 0
1.9300 1.9301 -.0001 -1 3 2
1.7900 1.7902 -.0002 -3 3 1
a= 10.900 b= 6.7572 c=9.456 beta= 72.45
da=.002 db=.0008 dc=.009 dbeta=.01
V= 664.1
20. 37-0234
alfa-ZrHVO0.5{PO4}2*3.1H2O
Triklin
Dexp Dcal d(D) h k l
9.7500 9.7577 -.0077 0 0 1
4.8700 4.8733 -.0033 0 -2 1
4.7900 4.7899 .0001 1 1 0
4.5900 4.5920 -.0020 1 0 1
4.4300 4.4262 .0038 -1 1 0
4.1300 4.1306 -.0006 1 1 1
3.8800 3.8815 -.0015 -1 1 1
3.7300 3.7299 .0001 -1 -2 1
3.3200 3.3197 .0003 0 -1 3
3.0700 3.0699 .0001 0 -3 2
2.6500 2.6499 .0001 1 3 1
A= 5.2182 DA= .0009
B= 10.192 DB= .001
C= 10.0170 DC= .0006
GAMMA= 84.42 DGAMMA= .01
BETA = 91.05 DBETA = .03
ALPHA=103.07 DALPHA= .02
V= 516.5
21. 37-0263
La8V2O17
Triklin
Dexp Dcal d(D) h k l
4.1250 4.1197 .0053 0 1 0
3.7790 3.7792 -.0002 0 -1 2
3.7080 3.7076 .0004 1 -1 2
3.3460 3.3441 .0019 1 1 0
3.3090 3.3081 .0009 -1 -1 1
3.2860 3.2888 -.0028 1 -1 3
3.2270 3.2259 .0011 1 0 4
3.1910 3.1939 -.0029 1 1 1
3.0440 3.0459 -.0019 -2 1 0
3.0060 3.0065 -.0005 2 0 3
2.9880 2.9868 .0012 2 -1 2
2.8540 2.8544 -.0004 1 -1 4
A= 7.572 DA= .003
B= 4.2484 DB= .0004
C= 13.99 DC= .01
GAMMA=101.579 DGAMMA= .009
BETA = 83.36 DBETA = .07
ALPHA= 99.314 DALPHA= .007
V=434.6
22. 37-0724
CsVO{SO4}2
Triklin
Dexp Dcal d(D) h k l
5.7540 5.7558 -.0018 -1 0 1
4.1070 4.1064 .0006 1 2 0
3.9620 3.9610 .0010 -1 0 2
3.7290 3.7280 .0010 -1 1 2
3.5200 3.5180 .0020 -1 -1 2
3.4090 3.4063 .0027 -2 0 1
3.2620 3.2643 -.0023 -2 -1 1
3.1040 3.1038 .0002 -2 1 1
2.8980 2.8989 -.0009 -1 0 3
2.7340 2.7344 -.0004 -2 1 2
2.6410 2.6410 .0000 -1 -3 1
2.4910 2.4912 -.0002 2 -2 1
A= 7.496 DA= .002
B= 9.203 DB= .003
C= 9.814 DC= .006
GAMMA= 80.35 DGAMMA= .04
BETA = 86.08 DBETA = .03
ALPHA= 78.18 DALPHA= .04
V=652.9
23. 37-0733
RbVO{SO4}
Triklin
Dexp Dcal d(D) h k l
6.0420 6.0449 -.0029 0 1 0
4.6850 4.6837 .0013 0 -1 2
4.3830 4.3821 .0009 1 -1 2
4.2420 4.2467 -.0047 1 1 2
3.8830 3.8817 .0013 0 -1 3
3.7700 3.7752 -.0052 1 -1 3
3.4480 3.4440 .0040 0 1 4
3.1930 3.1930 .0000 2 1 1
3.0580 3.0579 .0001 -1 1 4
2.8260 2.8273 -.0013 1 1 5
2.7800 2.7780 .0020 2 -1 4
2.6560 2.6561 -.0001 3 0 1
A= 8.004 DA= .001
B= 6.0842 DB= .0003
C= 16.2853 DC= .0002
GAMMA= 95.384 DGAMMA= .002
BETA = 80.570 DBETA = .005
ALPHA= 87.266 DALPHA= .004
V=777.2
24. 37-0751
KVO2SO4*3H2O
Triklin
Dexp Dcal d(D) h k l
6.1900 6.1794 .0106 0 1 1
5.2500 5.2502 -.0002 -1 0 1
4.9300 4.9287 .0013 0 -1 1
3.8670 3.8652 .0018 2 2 0
3.7950 3.7957 -.0007 -2 0 1
3.5340 3.5327 .0013 0 1 2
3.1600 3.1615 -.0015 1 -2 1
3.1150 3.1166 -.0016 1 3 1
3.0620 3.0631 -.0011 -3 1 0
3.0220 3.0206 .0014 1 -1 2
2.9730 2.9731 -.0001 3 -1 1
2.9220 2.9228 -.0008 3 0 2
A= 11.773 DA= .003
B= 9.437 DB= .005
C= 7.635 DC= .002
GAMMA= 71.29297 DGAMMA= .03
BETA = 70.05 DBETA = .04
ALPHA= 71.81 DALPHA= .04
V=734.9
25. 37-0781
KVO2SeO4
Triklin
Dexp Dcal d(D) h k l
6.6800 6.6837 -.0037 0 1 1
5.9100 5.9095 .0005 1 0 0
5.1300 5.1215 .0085 0 -1 1
4.4300 4.4296 .0004 -1 2 0
3.8700 3.8699 .0001 1 -1 1
3.5300 3.5372 -.0072 -1 3 1
3.3500 3.3496 .0004 0 0 2
3.1800 3.1778 .0022 -1 2 2
2.9550 2.9548 .0002 2 0 0
2.8370 2.8368 .0002 -2 2 1
2.8020 2.8022 -.0002 1 0 2
2.6980 2.6985 -.0005 1 2 2
A= 6.0535 DA= .0003
B= 11.953 DB= .002
C= 7.0920 DC= .0009
GAMMA=101.30 DGAMMA= .02
BETA = 98.64 DBETA = .02
ALPHA= 71.608 DALPHA= .001
V= 475.4
26. 37-0782
CsVO2SeO4*4H2O
Triklin
Dexp Dcal d(D) h k l
5.5100 5.5060 .0040 0 3 0
5.2300 5.2225 .0075 -1 3 0
5.0600 5.0596 .0004 -2 2 0
4.0200 4.0198 .0002 0 2 1
3.9000 3.8982 .0018 3 0 0
3.6300 3.6303 -.0003 -1 3 1
3.3800 3.3793 .0007 -2 3 1
3.2800 3.2812 -.0012 -1 5 0
3.1800 3.1794 .0006 -1 4 1
3.0320 3.0322 -.0002 -2 5 0
2.9250 2.9236 .0014 4 0 0
2.6910 2.6921 -.0011 -4 1 1
A= 11.9718 DA= .0009
B= 16.677 DB= .005
C= 4.552 DC= .001
GAMMA= 97.36 DGAMMA= .02
BETA =100.40 DBETA = .01
ALPHA= 85.79 DALPHA= .01
V=885.9
27. 37-0783
KVO2SeO4*4H2O
Triklin
Dexp Dcal d(D) h k l
5.3300 5.3234 .0066 1 2 0
4.9900 4.9859 .0041 2 0 0
3.9100 3.9113 -.0013 2 2 0
3.8700 3.8664 .0036 1 3 0
3.6000 3.5994 .0006 0 -1 1
3.2100 3.2112 -.0012 -3 1 0
3.1400 3.1422 -.0022 0 4 0
3.0600 3.0596 .0004 2 0 1
2.9940 2.9945 -.0005 -1 4 0
2.9250 2.9253 -.0003 -1 2 1
2.8000 2.8004 -.0004 2 -2 1
2.6560 2.6549 .0011 -2 4 0
A= 9.9906 DA= .0005
B= 12.588 DB= .002
C= 3.7074 DC= .0007
GAMMA= 90.04 DGAMMA= .04
BETA = 86.49126 DBETA = .00003
ALPHA= 93.20 DALPHA= .01
V=464.9
28. 37-0894
La3VO7
Triklin
Dexp Dcal d(D) h k l
9.5960 9.5795 .0165 1 0 0
9.0170 9.0151 .0019 0 1 0
7.6580 7.6583 -.0003 -1 0 2
6.9810 6.9800 .0010 0 -1 2
4.5140 4.5140 .0000 -2 0 2
3.7650 3.7650 .0000 -2 1 5
3.6700 3.6700 -.0000 1 0 6
3.3296 3.3297 -.0001 -1 -2 2
3.1931 3.1932 -.0001 3 0 0
3.1817 3.1817 .0000 -3 0 1
3.0512 3.0510 -.0000 -1 3 4
2.9833 2.9833 .0000 -3 3 1
A= 10.801 DA= .001
B= 10.1873 DB= .0004
C= 24.3781 DC= .0008
GAMMA=117.442 DGAMMA= .001
BETA = 94.757 DBETA = .002
ALPHA= 83.92 DALPHA= .01
V=2366
29. 37-0894
La3VO7
Triklin
Dexp Dcal d(D) h k l
9.5960 9.5795 .0165 1 0 0
9.0170 9.0151 .0019 0 1 0
7.6580 7.6583 -.0003 -1 0 2
6.9810 6.9800 .0010 0 -1 2
4.5140 4.5140 .0000 -2 0 2
3.7650 3.7650 .0000 -2 1 5
3.6700 3.6700 -.0000 1 0 6
3.3296 3.3297 -.0001 -1 -2 2
3.1931 3.1932 -.0001 3 0 0
3.1817 3.1817 .0000 -3 0 1
3.0512 3.0510 -.0002 -1 3 4
2.9833 2.9833 .0000 -3 3 1
A= 10.801 DA= .001
B= 10.1873 DB= .0004
C= 24.3781 DC= .0008
GAMMA=117.442 DGAMMA= .001
BETA = 94.757 DBETA = .002
ALPHA= 83.92 DALPHA= .01
V=2366
30. 37-0895
La1.42V0.58O3.58
Triklin
Dexp Dcal d(D) h k l
7.6290 7.6193 .0097 0 -1 1
5.7000 5.7040 -.0040 1 -1 0
3.8243 3.8246 -.0003 2 -1 1
3.6632 3.6638 -.0006 1 -2 1
3.3457 3.3442 .0015 3 0 1
3.2994 3.2989 .0005 -2 -3 1
3.1935 3.1914 .0021 -1 1 2
3.1768 3.1797 -.0029 0 -1 3
3.1544 3.1559 -.0015 -3 -1 2
3.0717 3.0692 .0025 -1 -2 3
3.0449 3.0454 -.0005 0 -3 1
2.8586 2.8588 -.0002 3 3 0
A= 11.788 DA= .006
B= 10.0370 DB= .0002
C= 9.624 DC= .007
GAMMA= 65.56 DGAMMA= .01
BETA = 97.59 DBETA = .03
ALPHA=110.85 DALPHA= .05
V=969.4
31. 37-1019
Yb7V3O16
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
5.7300 5.7182 .0118 0 2 0
3.1760 3.1753 .0007 -2 0 2
3.0330 3.0330 .0000 -1 2 2
2.8630 2.8626 .0004 2 0 2
2.6800 2.6814 -.0014 1 4 0
2.6080 2.6071 .0009 -1 4 1
2.5600 2.5622 -.0022 -3 0 2
2.1930 2.1932 -.0002 1 5 0
2.1260 2.1265 -.0005 -3 3 2
2.0800 2.0815 -.0015 -3 1 3
1.9282 1.9261 .0021 -4 2 2
1.9076 1.9081 -.0005 -3 4 2
a= 8.38 b= 11.4364 c= 7.097 beta= 112.76
da=.03 db=.0004 dc=.006 dbet=.04
V=613.8
Triklin
Dexp Dcal d(D) h k l
5.7300 5.7236 .0064 -1 1 0
3.1760 3.1762 -.0002 1 1 2
3.0330 3.0325 .0005 3 0 1
2.8630 2.8618 .0012 -2 2 0
2.6800 2.6801 -.0001 1 -2 1
2.6080 2.6097 -.0017 3 -1 1
2.5600 2.5587 .0013 3 2 1
2.1930 2.1928 .0002 1 0 3
2.1260 2.1259 .0001 -5 1 2
2.0800 2.0795 .0005 -5 -1 2
1.9282 1.9283 -.0001 4 3 0
1.9076 1.9078 -.0002 0 3 3
A= 11.8627 DA= .0004
B= 7.287 DB= .001
C= 7.500 DC= .003
GAMMA= 86.881 DGAMMA= .005
BETA =104.25 DBETA = .01
ALPHA= 77.44 DALPHA= .05
V= 609.3
32. 37-1065
K2VO{SO4}2
Triklin
Dexp Dcal d(D) h k l
6.4920 6.4940 -.0020 -1 1 0
5.2580 5.2417 .0163 -1 1 1
4.3240 4.3185 .0055 -1 -1 1
4.2380 4.2343 .0037 -1 2 0
3.7230 3.7262 -.0032 -2 1 0
3.5840 3.5874 -.0034 0 0 2
3.3760 3.3723 .0037 -1 1 2
2.2510 2.2519 -.0009 -2 3 2
3.2500 3.2470 .0030 -2 2 0
3.0790 3.0779 .0011 2 -1 1
2.8720 2.8719 .0001 -1 2 2
2.8280 2.8288 -.0008 -2 0 2
A= 7.676 DA= .003
B= 8.896 DB= .001
C= 7.314 DC= .002
GAMMA=106.62 DGAMMA= .03
BETA =101.16 DBETA = .04
ALPHA= 87.87 DALPHA= .01
V= 469.9
33. 37-1066
K2{VO}2{SO4}3
Triklin
Dexp Dcal d(D) h k l
7.3750 7.3626 .0124 0 1 1
6.9700 6.9652 .0048 1 0 1
5.9220 5.9222 -.0002 0 -1 1
4.5060 4.5048 .0012 1 0 2
4.0220 4.0225 -.0005 0 -2 1
3.8670 3.8652 .0018 -1 2 1
3.5070 3.5056 .0014 -2 1 0
3.1820 3.1821 -.0001 1 -2 2
3.1380 3.1418 -.0038 -2 2 0
3.0040 3.0039 .0001 0 3 2
2.8760 2.8764 -.0004 0 1 3
2.7500 2.7489 .0011 -2 2 1
A= 7.730 DA= .001
B= 10.586 DB= .004
C= 9.355 DC= .005
GAMMA= 94.07 DGAMMA= .08
BETA = 67.50 DBETA = .04
ALPHA= 79.97 DALPHA= .04
V= 688.3