1. 33-0161
BaMg2{VO4}2
Triklin
Dexp. Dcal. d(D) h k l
4.4100 4.4090 .0010 -2 -1 0
3.8200 3.8204 -.0004 -1 -3 0
3.5100 3.5096 .0004 0 1 1
3.1900 3.1901 -.0001 1 -3 0
3.0980 3.0932 .0048 2 -2 0
2.8750 2.8752 -.0002 -1 2 1
2.8350 2.8349 .0001 0 -4 0
2.7650 2.7629 .0021 -2 -2 1
2.5150 2.5125 .0025 2 -1 1
2.4070 2.4060 .0010 -3 -1 1
2.2250 2.2235 .0015 -4 -1 0
2.1090 2.1090 -.0000 -4 -3 0
A= 8.9386 DA= .0003
B= 11.690 DB= .001
C= 3.6730 DC= .0008
GAMMA= 76.03 DGAMMA= .07
BETA = 94.83 DBETA = .05
ALPHA= 89.68 DALPHA= .05
V= 371.0
2. 33-0222
Vi4V6O21
Triklin
Dexp Dcal d(D) h k l
4.5700 4.5686 .0014 0 -3 1
4.2600 4.2582 .0018 1 0 1
3.0300 3.0293 .0007 0 -5 1
2.8660 2.8662 -.0002 -2 1 1
2.5660 2.5654 .0006 0 -6 1
2.5140 2.5134 .0006 1 -4 2
2.2280 2.2283 -.0003 -1 2 3
2.1038 2.1038 .0000 2 -5 1
1.9811 1.9811 .0000 2 -4 2
1.9569 1.9567 .0002 -2 2 3
1.9329 1.9329 -.0000 -2 -6 1
1.9061 1.9064 -.0003 1 -7 2
A= 5.99133 DA= .00004
B= 15.7206 DB= .0004
C= 7.5355 DC= .0001
GAMMA= 92.2018 DGAMMA= .0005
BETA = 99.432 DBETA = .001
ALPHA= 98.189 DALPHA= .003
V=691.8
3. 33-0318
Ca7V2Si2O16
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.9500 3.9488 .0012 0 0 3
2.8700 2.8704 -.0004 1 0 4
2.8300 2.8297 .0003 4 0 1
2.7600 2.7615 -.0015 0 1 2
2.7500 2.7516 -.0016 2 1 0
2.6900 2.6871 .0029 1 1 2
2.6400 2.6403 -.0003 2 0 4
a=11.6560 b= 3.1215 c=11.846
da= .0002 db= .0005 dc= .001
V= 431.0
4. 33-0382
CsVO3
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.3700 5.3863 -.0163 0 0 1
4.9000 4.9301 -.0301 1 0 1
4.2000 4.2024 -.0024 2 1 0
4.0400 4.0435 -.0035 2 0 1
3.7500 3.7510 -.0010 1 1 1
3.3200 3.3133 .0067 2 1 1
3.2600 3.2525 .0075 3 0 1
3.0600 3.0603 -.0003 4 0 0
2.8900 2.8901 -.0001 0 2 0
2.8400 2.8345 .0055 3 1 1
2.7000 2.7046 -.0046 4 1 0
2.6600 2.6608 -.0008 4 0 1
a=12.241 b= 5.780 c= 5.386
da= .007 db= .004 dc= .002
V= 381.1
5. 33-0383
Cs2V4O9
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
7.5600 7.5701 -.0101 2 1 0
7.4700 7.4464 .0236 1 2 0
4.1400 4.1403 -.0003 0 4 0
3.9100 3.9086 .0014 3 0 1
3.7600 3.7619 -.0019 1 3 1
3.3100 3.3123 -.0023 0 5 0
3.1500 3.1488 .0012 5 2 0
2.8600 2.8606 -.0006 3 5 0
2.6600 2.6609 -.0009 0 1 2
2.5100 2.5107 -.0007 6 0 1
2.4100 2.4091 .0009 3 1 2
2.2800 2.2795 .0005 2 7 0
a=17.022 b=16.561 c= 5.392
da= .006 db= .005 dc= .001
V=1520
6. 33-0383
Cs2V4O9
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
7.5600 7.5701 -.0101 2 1 0
7.4700 7.4464 .0236 1 2 0
4.1400 4.1403 -.0003 0 4 0
3.9100 3.9086 .0014 3 0 1
3.7600 3.7619 -.0019 1 3 1
3.3100 3.3123 -.0023 0 5 0
3.1500 3.1488 .0012 5 2 0
2.8600 2.8606 -.0006 3 5 0
2.6600 2.6609 -.0009 0 1 2
2.5100 2.5107 -.0007 6 0 1
2.4100 2.4091 .0009 3 1 2
2.2800 2.2795 .0005 2 7 0
a=17.022 b=16.561 c= 5.392
da= .006 db= .005 dc= .001
V=1520
7. 33-0728
LaVO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8700 3.8695 .0005 -1 0 2
2.7470 2.7461 .0009 2 1 0
2.2510 2.2506 .0004 2 2 0
1.9520 1.9519 .0001 0 3 3
1.8950 1.8958 -.0008 3 0 3
1.7510 1.7506 .0004 -1 0 6
1.7050 1.7050 .0000 -2 0 5
1.5970 1.5970 -.0000 0 1 7
1.3850 1.3858 -.0008 -1 3 6
1.3610 1.3607 .0003 0 5 0
1.3060 1.3058 .0002 -4 1 3
1.2390 1.2392 -.0002 -4 2 3
a= 6.073 b= 6.8036 c= 11.635 beta= 81.26
da=.001 db=.0001 dc=.003 dbeta=.02
V= 475.2
Triklin
Dexp Dcal d(D) h k l
3.8700 3.8701 -.0001 0 -2 1
2.7470 2.7488 -.0018 0 -4 1
2.2510 2.2517 -.0007 1 3 1
1.9520 1.9526 -.0006 1 1 2
1.8950 1.8951 -.0001 1 2 2
1.7510 1.7514 -.0004 1 6 0
1.7050 1.7048 .0002 1 6 1
1.5970 1.5969 .0001 0 -8 1
1.3850 1.3851 -.0001 0 5 3
1.3610 1.3608 .0002 0 -5 3
1.3060 1.3061 -.0001 1 5 3
1.2390 1.2392 -.0002 1 -6 3
A= 2.8609 DA= .0001
B= 13.665 DB= .001
C= 4.818 DC= .003
GAMMA= 91.317 DGAMMA= .007
BETA = 81.42 DBETA = .02
ALPHA= 89.05 DALPHA= .04
V= 186.2
33-836
Ñì. ñîåäèíåíèÿ U
8. 33-0852
Lu7V3O16
Triklin
Dexp Dcal d(D) h k l
5.7020 5.7093 -.0073 1 0 1
5.1060 5.1088 -.0028 1 2 0
4.2340 4.2356 -.0016 1 -2 1
3.5010 3.5004 .0006 -1 -2 1
3.3970 3.3975 -.0005 1 4 1
3.3470 3.3448 .0022 2 0 1
3.1640 3.1634 .0006 2 -1 1
3.0210 3.0205 .0005 -1 3 1
2.9960 2.9974 -.0014 -2 1 0
2.8550 2.8547 .0003 2 0 2
2.6690 2.6693 -.0003 2 3 2
2.5978 2.5978 -.0000 -1 5 0
A= 6.8088 DA= .0007
B= 15.239 DB= .002
C= 7.139 DC= .004
GAMMA= 81.48 DGAMMA= .02
BETA = 67.787 DBETA = .009
ALPHA= 83.51 DALPHA= .02
V=677.1
9. 33-1055
K6S6V2O26
Triklin
Dexp Dcal d(D) h k l
6.5800 6.5795 .0005 1 0 0
5.5400 5.5675 -.0275 1 1 1
5.1900 5.1962 -.0062 -1 -1 1
4.7700 4.7674 .0026 1 0 2
7.1300 7.1580 -.0280 0 -1 1
4.5200 4.5200 -.0000 -1 1 0
4.1400 4.1251 .0149 0 2 0
3.9000 3.9009 -.0009 -1 1 1
3.5960 3.5982 -.0022 0 -1 3
3.4320 3.4333 -.0013 2 1 1
3.3440 3.3470 -.0030 2 0 1
3.3050 3.3046 .0004 1 1 3
A= 7.006 DA= .006
B= 8.692 DB= .007
C= 11.46 DC= .01
GAMMA= 73.65 DGAMMA= .03
BETA = 80.21 DBETA = .02
ALPHA= 95.22 DALPHA= .01
V= 652.8
10. 33-1056
K4V2S4O19
Triklin
Dexp Dcal d(D) h k l
7.4200 7.4002 .0198 1 1 0
6.3700 6.3677 .0023 0 1 1
5.6000 5.6078 -.0078 0 -1 1
5.1600 5.1544 .0056 0 2 0
4.8640 4.8667 -.0027 -1 0 1
4.6080 4.6085 -.0005 -1 -1 1
4.0510 4.0475 .0035 2 1 0
3.8370 3.8387 -.0017 2 0 0
3.7290 3.7305 -.0015 2 2 1
3.6450 3.6446 .0004 0 0 2
3.5960 3.5965 -.0005 1 3 0
3.5500 3.5493 .0007 1 0 2
A= 8.3460 DA= .0002
B= 11.1239 DB= .0002
C= 7.5727 DC= .0006
GAMMA= 69.260 DGAMMA= .007
BETA = 76.252 DBETA = .008
ALPHA= 78.118 DALPHA= .007
V=633.2
11. 33-1136
beta-Rb0.3V2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.0900 7.0865 .0035 1 0 1
4.6300 4.6345 -.0045 1 2 1
4.0800 4.0841 -.0041 0 3 0
3.4000 3.4038 -.0038 2 1 2
3.0700 3.0672 .0028 2 2 2
2.8200 2.8210 -.0010 4 0 0
2.7000 2.7012 -.0012 -3 1 2
2.4500 2.4505 -.0005 0 5 0
2.3600 2.3587 .0013 0 5 1
2.3100 2.3084 .0016 -4 0 2
2.0000 2.0001 -.0001 2 4 3
1.9660 1.9666 -.0006 -2 1 4
a= 11.30 b=12.25242 c= 8.715 beta= 86.763550
da=.01 db=.00003 dc=.002 dbeta=.05
V= 1205
Triklin
Dexp Dcal d(D) h k l
7.0900 7.0929 -.0029 1 0 0
4.6300 4.6278 .0022 0 0 1
4.0800 4.0830 -.0030 0 3 0
3.4000 3.3998 .0002 0 2 1
3.0700 3.0693 .0007 -2 0 1
2.8200 2.8227 -.0027 1 2 1
2.7000 2.6993 .0007 2 -1 1
2.4500 2.4498 .0002 0 5 0
2.3600 2.3593 .0007 0 4 1
2.3100 2.3089 .0011 1 -5 1
2.2000 2.2001 -.0001 0 1 2
2.0000 2.0009 -.0009 1 -6 1
A= 7.2998 DA= .0004
B= 12.6566 DB= .0004
C= 4.7524 DC= .0005
GAMMA= 99.92 DGAMMA= .02
BETA = 97.63 DBETA = .01
ALPHA= 99.173 DALPHA= .009
V= 421.2
12. 33-1137
gamma-Rb0.9V2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1200 4.1189 .0011 2 1 2
3.8100 3.8125 -.0025 3 1 1
3.5500 3.5470 .0030 2 2 1
3.4300 3.4333 -.0033 1 0 3
3.2200 3.2201 -.0001 0 2 2
3.1200 3.1203 -.0003 3 0 3
3.0400 3.0411 -.0011 -3 1 1
2.8100 2.8084 .0016 1 3 0
2.7600 2.7623 -.0023 1 3 1
2.5100 2.5097 .0003 3 0 4
2.4100 2.4100 .0000 -2 3 1
2.3400 2.3402 -.0002 4 0 4
a= 12.744 b=8.673 c=10.361 beta= 68.11
da=.006 db=.003 dc=.001 dbeta=.06
V= 1063
Triklin
Dexp Dcal d(D) h k l
4.1200 4.1172 .0028 0 0 1
3.8100 3.8114 -.0014 -1 0 1
3.5500 3.5498 .0002 -1 1 1
3.4300 3.4309 -.0009 1 -2 1
3.2200 3.2212 -.0012 -2 3 0
3.1200 3.1178 .0022 0 2 1
3.0400 3.0426 -.0026 -2 1 1
2.8100 2.8105 -.0005 2 1 1
2.7600 2.7606 -.0006 -2 2 1
2.5100 2.5087 .0013 -3 1 1
2.4100 2.4103 -.0003 -4 1 0
2.3400 2.3397 .0003 -4 2 0
A= 9.65 DA= .01
B= 11.444 DB= .005
C= 4.155 DC= .002
GAMMA=100.241 DGAMMA= .009
BETA = 90.03 DBETA = .09
ALPHA= 97.64 DALPHA= .02
V= 447.3
13. 33-1138
delta-Rb0.42V2O5
Triklin
Dexp Dcal d(D) h k l
3.4700 3.4706 -.0006 0 1 1
3.3300 3.3290 .0010 0 -1 1
3.2100 3.2093 .0007 -2 1 0
2.6300 2.6298 .0002 2 1 1
2.4100 2.4102 -.0002 0 -1 3
1.9280 1.9279 .0001 -2 1 5
1.8260 1.8262 -.0002 2 1 4
1.7950 1.7949 .0001 -6 0 1
1.7440 1.7441 -.0001 0 -1 5
1.7290 1.7292 -.0002 -6 1 1
1.6900 1.6899 .0001 3 -1 4
1.6680 1.6679 .0001 -2 1 6
A= 10.9684 DA= .0003
B= 3.6631 DB= .0001
C= 10.7124 DC= .0004
GAMMA=100.221 DGAMMA= .002
BETA =104.472 DBETA = .004
ALPHA= 83.790 DALPHA= .001
V=409.2
14. 33-1302
Na3V3O8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.8300 6.8282 .0018 1 1 0
5.0300 5.0390 -.0090 0 0 2
4.8700 4.8833 -.0133 2 0 1
3.8600 3.8621 -.0021 -1 2 1
3.7800 3.7782 .0018 -1 0 2
3.0200 3.0211 -.0011 1 2 3
2.9740 2.9752 -.0012 3 0 0
2.8660 2.8646 .0014 3 1 0
2.7850 2.7849 .0001 3 1 3
2.7370 2.7378 -.0008 2 3 2
2.5410 2.5409 .0001 1 4 0
2.0810 2.0809 .0001 0 4 3
1.9400 1.9397 .0003 4 0 5
a= 9.774 b= 10.602 c= 11.0358 beta=65.945
da=.007 db=.002 dc= .0003 dbeta=.001
V= 1044
Triklin
Dexp Dcal d(D) h k l
6.8300 6.8370 -.0070 1 0 0
5.0300 5.0247 .0053 -1 1 0
4.8700 4.8821 -.0121 1 0 1
3.8600 3.8608 -.0008 1 1 0
3.7800 3.7845 -.0045 -1 1 1
3.0200 3.0195 .0005 2 -1 1
2.9740 2.9763 -.0023 -1 -1 1
2.8660 2.8661 -.0001 -1 2 0
2.7850 2.7845 .0005 -2 1 1
2.7370 2.7369 .0001 0 1 2
2.5410 2.5409 .0001 1 -1 2
2.0810 2.0810 .0000 -3 1 1
A= 7.164 DA= .001
B= 5.819 DB= .001
C= 5.956 DC= .004
GAMMA=104.27 DGAMMA= .06
BETA = 81.55 DBETA = .05
ALPHA= 85.08 DALPHA= .03
V= 236.1
15. 33-1359
SrV2O5
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.5340 3.5318 .0022 0 1 1
3.2930 3.2979 -.0049 2 0 3
3.0930 3.0893 .0037 3 0 0
2.8310 2.8290 .0020 3 0 2
2.7520 2.7509 .0011 1 1 3
2.6510 2.6550 -.0040 2 1 2
2.3450 2.3472 -.0022 0 0 6
2.1960 2.2009 -.0049 4 0 2
2.0830 2.0814 .0016 3 0 5
2.0100 2.0091 .0009 2 1 5
1.8690 1.8689 .0001 3 0 6
1.7250 1.7240 .0010 5 0 3
a= 9.268 b= 3.6484 c=14.083
da= .002 db= .0001 dc= .005
V= 476.2
Triklin
Dexp Dcal d(D) h k l
3.5340 3.5362 -.0022 0 1 1
3.2930 3.2917 .0013 -1 0 1
3.0930 3.0924 .0006 0 -1 1
2.8310 2.8314 -.0004 -1 2 1
2.7520 2.7532 -.0012 1 -1 1
2.6510 2.6550 -.0040 -1 -1 1
2.3450 2.3447 .0003 2 1 0
2.1960 2.1988 -.0028 1 2 1
2.0830 2.0814 .0016 0 3 1
2.0100 2.0107 -.0007 -2 3 1
1.8690 1.8680 .0010 -3 2 0
1.7250 1.7256 -.0006 -2 1 2
A= 5.8869 DA= .0007
B= 7.193 DB= .004
C= 3.869 DC= .001
GAMMA=108.111 DGAMMA= .007
BETA = 99.37 DBETA = .03
ALPHA= 78.622 DALPHA= .001
V= 151.7
16. 33-1442
V{PO3}3
Triklin
Dexp. Dcal. d(D) h k l
5.4300 5.4319 -.0019 -1 -1 0
5.2500 5.2519 -.0019 1 -1 0
4.6500 4.6610 -.0110 -2 -1 0
3.8500 3.8620 -.0120 -3 -1 0
3.7500 3.7521 -.0021 4 0 0
3.6700 3.6728 -.0028 3 -1 0
3.5700 3.5678 .0022 -1 0 1
3.4200 3.4218 -.0018 -1 -1 1
3.2700 3.2737 -.0037 -2 0 1
3.1800 3.1787 .0013 -2 -1 1
3.0700 3.0658 .0042 4 -1 0
3.0000 3.0017 -.0017 5 0 0
A= 15.034 DA= .004
B= 5.890 DB= .003
C= 3.822 DC= .003
GAMMA= 87.58 DGAMMA= .04
BETA = 88.37 DBETA = .01
ALPHA=103.777 DALPHA= .009
V= 328.1
17. 33-1443
VO{PO3}2
Triklin
Dexp Dcal d(D) h k l
6.0300 6.0264 .0036 1 0 0
4.7600 4.7557 .0043 1 2 1
4.2400 4.2419 -.0019 -1 0 1
3.9400 3.9437 -.0037 1 1 2
3.8400 3.8427 -.0027 -1 -1 1
3.6500 3.6502 -.0002 0 3 1
3.2600 3.2607 -.0007 1 3 0
3.2100 3.2076 .0024 2 1 1
3.0600 3.0602 -.0002 2 0 1
3.0300 3.0317 -.0017 2 1 0
2.9030 2.9018 .0012 -1 0 2
2.6100 2.6096 .0004 -1 -3 1
A= 6.433 DA= .002
B= 11.4719 DB= .0003
C= 8.399 DC= .001
GAMMA= 74.69 DGAMMA= .04
BETA = 71.78 DBETA = .03
ALPHA= 67.62 DALPHA= .03099
V=536.7
18. 33-1961
C12H30O9P3V
Geksagon
Grupa 143
Dexp. Dcal. d(D) h k l
11.3000 11.4841 -.1841 0 0 1
5.7500 5.7420 .0080 0 0 2
4.4600 4.4569 .0031 2 0 1
4.0000 4.0032 -.0032 1 1 2
3.5600 3.5594 .0006 1 0 3
a=11.168 c= 11.484
da=.009 dc=.005
V=1240.5
19. 33-1962
C12H37-xN3O19V2-xW4+x*H2O
Triklin
Dexp Dcal d(D) h k l
9.3000 9.2856 .0144 0 1 1
8.8000 8.7987 .0013 1 1 1
8.4000 8.4053 -.0053 -1 1 0
7.9000 7.8984 .0016 1 -1 1
6.3800 6.3853 -.0053 -1 1 1
4.6400 4.6389 .0011 1 0 3
3.6400 3.6403 -.0003 -1 3 1
3.4900 3.4919 -.0019 -1 1 3
3.4600 3.4599 .0001 2 3 0
3.4100 3.4098 .0002 -3 0 1
3.2600 3.2601 -.0001 1 3 3
3.1800 3.1785 .0015 -1 2 3
A= 12.954 DA= .004
B= 12.500 DB= .004
C= 14.006 DC= .003
GAMMA= 85.48 DGAMMA= .02
BETA = 66.26 DBETA = .02
ALPHA= 83.99 DALPHA= .04
V=2061
20. 33-1963
C12H37-xN3O19V2-xW4+x*H2O
Triklin
Dexp Dcal d(D) h k l
9.3000 9.2888 .0112 0 2 0
8.7000 8.7086 -.0086 0 1 1
8.4000 8.4042 -.0042 1 0 0
7.9000 7.8993 .0007 0 -1 1
6.3400 6.3405 -.0005 -1 2 0
3.4700 3.4699 .0001 -2 3 2
3.4300 3.4301 -.0001 1 -4 1
3.4100 3.4097 .0003 2 0 1
3.0500 3.0500 -.0000 0 6 1
2.9810 2.9810 .0000 0 -1 3
2.9080 2.9080 .0000 -3 -1 1
2.4570 2.4570 -.0000 3 0 1
A= 8.97735 DA= .00003
B= 18.7797 DB= .0002
C= 9.94044 DC= .00007
GAMMA= 94.680 DGAMMA= .001
BETA =110.504 DBETA = .003
ALPHA= 81.823 DALPHA= .001
V= 1552.9
21. 34-0022
CsxV2O5
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
8.1900 8.1743 .0157 0 1 0
4.0900 4.0871 .0029 0 2 0
3.6920 3.6910 .0010 2 2 0
3.3260 3.3273 -.0013 3 2 0
3.2430 3.2411 .0019 3 1 1
3.1000 3.1021 -.0021 4 0 1
3.0180 3.0202 -.0022 0 2 1
2.9590 2.9615 -.0025 4 2 0
2.7220 2.7248 -.0028 0 3 0
2.5990 2.5973 .0017 2 3 0
2.4680 2.4710 -.0030 4 2 1
2.2220 2.2225 -.0005 1 0 2
a=17.19 b= 8.1742 c= 4.482677
da= .02 db= .0003 dc= .000002
V= 629.8
22. 34-0592
beta-Cs0.34V2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1200 4.1186 .0014 2 1 0
3.4300 3.4312 -.0012 -2 2 1
3.0900 3.0892 .0008 -1 0 3
2.9800 2.9799 .0001 -1 1 3
2.8400 2.8387 .0013 -2 3 1
2.6900 2.6911 -.0011 1 4 0
2.4700 2.4698 .0002 1 2 3
2.3800 2.3808 -.0008 2 4 0
2.3400 2.3406 -.0006 -1 0 4
2.2600 2.2600 .0000 0 5 0
2.2200 2.2189 .0011 1 3 3
2.1900 2.1896 .0004 1 5 0
a= 9.008 b= 11.2998 c= 9.387 beta= 100.89
da=.003 db=.0004 dc=.002 dbeta=.01
V= 938.3
triklin
Dexp Dcal d(D) h k l
4.1200 4.1198 .0002 1 0 1
3.4300 3.4248 .0052 1 1 1
3.0900 3.0897 .0003 1 0 2
2.9800 2.9794 .0006 0 0 3
2.8400 2.8409 -.0009 1 -1 1
2.6900 2.6910 -.0010 0 1 3
2.4700 2.4697 .0003 -1 1 3
2.3800 2.3804 -.0004 1 -1 2
2.3400 2.3399 .0001 0 2 0
2.2600 2.2611 -.0011 1 2 0
2.2200 2.2199 .0001 1 2 1
2.1900 2.1892 .0008 0 -2 1
A= 5.2595 DA= .0008
B= 4.7660 DB= .0007
C= 9.165 DC= .001
GAMMA= 82.67 DGAMMA= .01
BETA = 99.91 DBETA = .02
ALPHA= 83.36 DALPHA= .01
V=222.0
23. 34-0604
gamma-Cs0.97V2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1800 4.1802 -.0002 -2 1 1
3.6100 3.6099 .0001 -3 1 1
3.4000 3.3997 .0003 2 3 0
3.3100 3.3132 -.0032 4 2 0
3.0300 3.0308 -.0008 -1 3 1
2.8000 2.8000 .0000 -4 2 1
2.6400 2.6402 -.0002 -1 1 2
2.3000 2.3005 -.0005 4 1 2
2.1700 2.1704 -.0004 5 0 2
2.0400 2.0399 .0001 -5 1 2
1.9500 1.9500 -.0000 -1 4 2
1.9320 1.9318 .0002 -3 5 1
a= 16.454 b= 11.203 c=5.557 beta= 87.37
da=.004 db=.001 dc=.001 dbeta=.04
V= 1023
Triklin
Dexp Dcal d(D) h k l
4.1800 4.1783 .0017 -1 0 1
3.6100 3.6086 .0014 0 1 1
3.4000 3.4007 -.0007 0 -1 1
3.3100 3.3079 .0021 -2 1 1
3.0300 3.0296 .0004 0 2 0
2.8000 2.8012 -.0012 -2 -1 1
2.6400 2.6411 -.0011 -1 2 1
2.3000 2.2996 .0004 -1 -2 1
2.1700 2.1701 -.0001 -1 0 2
2.0400 2.0399 .0001 2 2 1
1.9500 1.9500 -.0000 4 0 1
1.9320 1.9320 .0000 -3 0 2
A= 9.874 DA= .002
B= 6.202 DB= .0010
C= 4.36879 DC= .00004
GAMMA=101.78 DGAMMA= .06
BETA =100.469 DBETA = .002
ALPHA= 84.41 DALPHA= .02
V=257.0
24. 34-0619
gamma-cs0.68V2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.0000 3.9992 .0008 2 1 0
3.5800 3.5784 .0016 1 0 2
3.2300 3.2293 .0007 3 0 1
2.9300 2.9272 .0028 2 2 0
2.5800 2.5791 .0009 1 2 2
2.3400 2.3400 .0000 2 0 3
2.2600 2.2593 .0007 4 1 0
2.1400 2.1404 -.0004 -3 2 1
2.0800 2.0797 .0003 3 1 3
2.0000 1.9996 .0004 4 2 0
1.9350 1.9355 -.0005 4 2 2
1.8600 1.8602 -.0002 0 4 0
a=9.862 b=7.441 c= 7.188 beta= 74.09
da=.005 db=.001 dc=.0008 dbeta=.03
V= 507.3
25. 34-0777
NH4V{SO4}2*3H2O
Triklin
Dexp Dcal d(D) h k l
9.2800 9.2877 -.0077 0 0 1
5.6200 5.6171 .0029 1 -1 1
4.5400 4.5417 -.0017 0 -2 1
4.3400 4.3398 .0002 -1 -1 1
4.0800 4.0784 .0016 1 2 0
3.8900 3.8838 .0062 1 -1 2
3.6900 3.6920 -.0020 -1 2 2
3.5100 3.5113 -.0013 -2 2 0
3.4400 3.4418 -.0018 1 -3 1
3.3600 3.3597 .0003 -2 1 1
3.0100 3.0110 -.0010 1 0 3
2.9720 2.9721 -.0001 1 3 2
2.7820 2.7827 -.0007 0 3 3
2.4930 2.4929 .0001 2 -4 1
2.4000 2.3994 .0006 -1 4 3
A= 7.47333 DA= .00008
B= 12.6138 DB= .0005
C= 9.6036 DC= .0004
GAMMA=103.842 DGAMMA= .001
BETA = 84.717 DBETA = .002
ALPHA= 77.990 DALPHA= .001
V=850.1
26. 34-0867
NH4V{SO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
8.6100 8.6084 .0016 0 1 0
5.5500 5.5531 -.0031 -1 -1 2
5.1600 5.1618 -.0018 0 -1 2
4.2600 4.2612 -.0012 -1 1 1
3.7600 3.7611 -.0011 -1 -2 3
3.4400 3.4385 .0015 0 2 1
3.4100 3.4089 .0011 2 0 0
3.3600 3.3598 .0002 -1 1 2
3.2900 3.2915 -.0015 -1 2 0
3.0700 3.0695 .0005 0 -3 2
2.8830 2.8834 -.0004 -2 -3 1
2.8210 2.8208 .0002 -1 -1 4
2.5770 2.5768 .0002 -1 -4 2
2.4970 2.4969 .0001 -2 -4 3
2.2150 2.2151 -.0001 1 4 0
A= 7.868 DA= .002
B= 10.376 DB= .001
C= 11.702 DC= .004
GAMMA= 65.15 DGAMMA= .02
BETA =116.62 DBETA = .03
ALPHA=121.13 DALPHA= .05
V= 708.7
27. 34-0882
{NH4}3VOF5
Triklin
Dexp Dcal d(D) h k l
5.1800 5.1815 -.0015 1 1 0
4.5700 4.5736 -.0036 0 1 1
4.4400 4.4401 -.0001 0 -1 1
3.4800 3.4795 .0005 1 -2 1
3.1800 3.1796 .0004 0 -2 1
3.1400 3.1360 .0040 3 -1 1
2.7400 2.7413 -.0013 -2 -1 1
2.6900 2.6871 .0029 -1 -2 1
2.5800 2.5787 .0013 3 1 0
2.4900 2.4909 -.0009 -3 2 1
2.4700 2.4693 .0007 2 2 1
2.3400 2.3407 -.0007 2 1 2
A= 10.202 DA= .008
B= 8.644 DB= .001
C= 5.565 DC= .001
GAMMA=111.98 DGAMMA= .05
BETA = 78.37 DBETA = .02
ALPHA= 92.67 DALPHA= .01
V= 445.6
28.
34-0988
NaFe3V4O15
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1500 4.1516 -.0016 -1 1 1
3.8300 3.8359 -.0059 -2 0 1
3.2900 3.2931 -.0031 0 2 0
3.2400 3.2382 .0018 3 0 0
3.1500 3.1494 .0006 1 0 2
3.1200 3.1188 .0012 1 2 0
2.8600 2.8612 -.0012 -3 0 1
2.8400 2.8413 -.0013 1 1 2
2.6900 2.6924 -.0024 3 1 1
2.4300 2.4287 .0013 4 0 0
2.1600 2.1598 .0002 -3 2 1
2.1400 2.1402 -.0002 -3 1 2
a= 9.722 b= 6.586 c=6.576 beta= 87.8
da=.006 db=.005 dc=.001 dbet= .01
V= 420.7
Triklin
Dexp Dcal d(D) h k l
4.1500 4.1502 -.0002 0 -1 1
3.8300 3.8298 .0002 -1 2 1
3.2900 3.2888 .0012 1 -2 1
3.2400 3.2398 .0002 1 -3 0
3.1500 3.1498 .0002 -2 3 0
3.1200 3.1208 -.0008 2 -2 1
2.8600 2.8592 .0008 -2 3 1
2.8400 2.8405 -.0005 -3 2 1
2.6900 2.6896 .0004 2 2 1
2.4300 2.4311 -.0011 -1 0 2
2.1600 2.1604 -.0004 0 3 2
2.1400 2.1405 -.0005 1 -2 2
A= 10.66 DA= .01
B= 9.876 DB= .003
C= 5.229 DC= .003
GAMMA=111.46 DGAMMA= .01
BETA = 88.43 DBETA = .09
ALPHA= 80.74 DALPHA= .01
V= 503.5
29. 34-1014
Cd{Oh}{VO4}3
Triklin
Dexp Dcal d(D) h k l
4.8700 4.8809 -.0109 0 1 1
4.6700 4.6792 -.0092 -1 0 1
3.9200 3.9233 -.0033 0 -1 1
3.3000 3.3039 -.0039 1 0 1
3.1600 3.1593 .0007 1 2 0
2.8500 2.8489 .0011 -1 0 2
2.8000 2.7994 .0006 -1 1 2
2.7900 2.7937 -.0037 -2 0 1
2.6700 2.6672 .0028 2 0 0
2.5700 2.5697 .0003 -2 1 1
2.5100 2.5098 .0002 -1 -1 2
2.3400 2.3396 .0004 -2 0 2
A= 5.67554 DA= .00000
B= 7.2763 DB= .0001
C= 5.9031 DC= .0009
GAMMA= 85.91 DGAMMA= .01
BETA =108.34 DBETA = .01
ALPHA= 79.1722 DALPHA= .0005
V=225.1
30. 34-1017
NaFeV2O7
Triklin
Dexp Dcal d(D) h k l
8.4400 8.4508 -.0108 1 0 0
6.9900 6.9953 -.0053 0 1 1
6.1300 6.1272 .0028 0 -1 1
4.5600 4.5614 -.0014 -1 1 1
4.1700 4.1684 .0016 1 1 2
3.8200 3.8209 -.0009 1 2 2
3.4400 3.4403 -.0003 2 3 1
3.3900 3.3901 -.0001 0 -3 1
2.9900 2.9911 -.0011 -1 -1 2
2.9800 2.9787 .0013 0 4 1
2.9700 2.9710 -.0010 3 2 1
2.9600 2.9580 .0020 -2 -2 1
2.7700 2.7697 .0003 3 0 2
2.4300 2.4302 -.0002 3 4 1
2.4200 2.4199 .0001 3 1 3
A= 9.234 DA= .006
B= 12.616 DB= .003
C= 8.416 DC= .005
GAMMA= 76.80 DGAMMA= .02
BETA = 68.06 DBETA = .04
ALPHA= 77.49 DALPHA= .03
V= 876.0
31. 34-1069
VO{As}3}2
Triklin
Dexp Dcal d(D) h k l
6.1200 6.1202 -.0002 0 1 1
4.3300 4.3293 .0007 0 -1 1
4.1800 4.1780 .0020 -1 0 1
3.7100 3.7061 .0039 -1 -1 1
3.1600 3.1589 .0011 0 2 0
3.0600 3.0601 -.0001 0 2 2
2.9700 2.9692 .0008 -1 0 2
2.8800 2.8799 .0001 2 2 3
2.6500 2.6512 -.0012 -1 -1 2
2.5400 2.5401 -.0001 0 2 3
2.4600 2.4602 -.0002 2 3 1
2.4000 2.4000 .0000 1 2 4
A= 7.035 DA= .005
B= 8.059 DB= .006
C= 9.850 DC= .003
GAMMA= 56.61 DGAMMA= .04
BETA = 62.09 DBETA = .05
ALPHA= 59.24 DALPHA= .03
V=386.9
32. 34-1210
VOAsO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.1800 4.1800 .0000 0 1 0
3.4900 3.4864 .0036 1 1 1
3.1600 3.1599 .0001 2 0 2
3.0600 3.0590 .0010 3 1 0
2.5200 2.5207 -.0007 2 1 2
2.3900 2.3906 -.0006 4 0 2
2.2500 2.2496 .0004 -4 1 2
2.0900 2.0900 .0000 0 2 0
2.0000 2.0014 -.0014 -1 2 1
1.8810 1.8812 -.0002 3 1 3
1.7440 1.7432 .0008 2 2 2
1.6200 1.6200 -.0000 -7 0 3
a=13.549 b=4.1800 c= 7.63654 beta=96.34
da=.003 db=.0005 dc=.00001 dbeta=.05
V= 429.8
Triklin
Dexp Dcal d(D) h k l
4.1800 4.1803 -.0003 0 1 1
3.4900 3.4888 .0012 0 -1 1
3.1600 3.1585 .0015 -1 0 1
3.0600 3.0562 .0038 0 2 0
2.5200 2.5177 .0023 -2 2 0
2.3900 2.3910 -.0010 0 -2 1
2.2500 2.2519 -.0019 -2 1 1
2.0900 2.0902 -.0002 0 2 2
2.0000 1.9987 .0013 -1 0 2
1.8810 1.8810 -.0000 2 -3 1
1.7440 1.7444 -.0004 0 -2 2
1.6200 1.6201 -.0001 2 2 2
A= 5.832 DA= .009
B= 6.6238 DB= .0007
C= 5.036 DC= .002
GAMMA=110.16 DGAMMA= .02
BETA = 77.19 DBETA = .04
ALPHA= 84.730 DALPHA= .004
V= 175.0
33. 34-1227
CaMgO7
Triklin
Dexp Dcal d(D) h k l
4.8900 4.8886 .0014 1 1 0
4.2800 4.2804 -.0004 -1 1 1
3.5780 3.5806 -.0026 -1 -1 1
3.2810 3.2802 .0008 0 2 0
3.1770 3.1760 .0010 -2 0 1
3.1220 3.1223 -.0003 -1 2 0
3.0700 3.0702 -.0002 1 2 1
3.0190 3.0190 .0000 -1 1 2
2.9800 2.9804 -.0004 -1 2 1
2.7890 2.7887 .0003 0 -2 1
2.7640 2.7639 .0001 0 2 2
2.6670 2.6671 -.0001 3 0 0
A= 8.320 DA= .004
B= 6.7146 DB= .0003
C= 7.860 DC= .003
GAMMA= 91.26 DGAMMA= .04
BETA = 74.73 DBETA = .02
ALPHA= 78.55 DALPHA= .01
V= 413.8
34. 34-1385
K2V10O26
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.6000 6.5977 .0023 1 1 1
6.0000 5.9921 .0079 0 0 2
5.8800 5.8758 .0042 1 0 2
3.4000 3.4027 -.0027 3 0 0
3.2300 3.2293 .0007 0 3 0
3.1700 3.1714 -.0014 3 1 2
2.8100 2.8115 -.0015 2 1 4
2.7300 2.7289 .0011 2 3 0
2.6100 2.6093 .0007 3 0 4
2.5100 2.5113 -.0013 0 3 3
2.3800 2.3803 -.0003 3 3 1
2.0100 2.0101 -.0001 -1 2 5
1.9700 1.9689 .0011 -4 2 2
a=10.57 b=9.688 c=12.41 beta=75.0
da=.01 db=.005 dc=.003 dbeta=.1
V= 1227
Triklin
Dexp Dcal d(D) h k l
6.6000 6.6002 -.0002 1 0 0
6.0000 6.0024 -.0024 0 1 0
5.8800 5.8799 .0001 -1 0 1
3.4000 3.3999 .0001 -2 0 1
3.2300 3.2295 .0005 -1 2 1
3.1700 3.1720 -.0020 -2 1 2
2.8100 2.8099 .0001 0 -1 2
2.7300 2.7305 -.0005 -1 -1 2
2.6100 2.6102 -.0002 1 2 1
2.5100 2.5110 -.0010 2 1 1
2.3800 2.3798 .0002 0 2 3
2.0100 2.0099 .0001 1 2 3
1.9700 1.9699 .0001 3 0 1
A= 7.134 DA= .001
B= 6.6199 DB= .0009
C= 8.670 DC= .002
GAMMA=105.26 DGAMMA= .02
BETA =110.87 DBETA = .03
ALPHA= 66.322 DALPHA= .003
V= 346.9
35. 34-1652
C15H30N3SW6V
Triklin
Dexp Dcal d(D) h k l
8.6500 8.6545 -.0045 1 0 0
7.8100 7.8170 -.0070 -1 1 0
6.8900 6.8912 -.0012 1 1 1
6.3700 6.3652 .0048 0 2 0
5.0600 5.0608 -.0008 1 0 2
4.8700 4.8680 .0020 2 -1 1
4.3000 4.3005 -.0005 0 1 2
4.0600 4.0583 .0017 0 -1 2
3.9500 3.9510 -.0010 1 -2 2
3.6600 3.6596 .0004 2 2 1
3.3200 3.3202 -.0002 2 2 0
A= 10.026 DA= .001
B= 12.928 DB= .003
C= 10.125 DC= .001
GAMMA= 98.50 DGAMMA= .04
BETA = 61.24 DBETA = .02
ALPHA= 89.44 DALPHA= .03
V=1132