1. 31-0076
{NH4}2V12O27*xH2O
Triklin
Dexp Dcal d(D) h k l
15.7000 15.7057 -.0057 0 0 1
7.8000 7.7904 .0096 0 1 0
5.7000 5.6947 .0053 0 -1 2
3.5200 3.5198 .0002 -1 1 4
3.1100 3.1102 -.0002 -1 2 3
2.9500 2.9500 .0000 -1 1 5
2.6600 2.6601 -.0001 1 -2 4
2.5500 2.5522 -.0022 -1 3 1
2.4200 2.4201 -.0001 1 3 0
2.3800 2.3800 .0000 0 2 5
2.2300 2.2301 -.0001 -2 3 3
1.9750 1.9764 -.0014 -2 0 8
A= 9.43 DA= .02
B= 7.854 DB= .002
C= 16.148 DC= .006
GAMMA= 96.52 DGAMMA= .02
BETA =103.059 DBETA = .004
ALPHA= 91.688 DALPHA= .003
V=1153
2. 31-0078
NH4V{SO4}2*6H2O
Triklin
Dexp Dcal d(D) h k l
6.6000 6.5980 .0020 1 0 0
5.2000 5.1994 .0006 -1 1 0
4.9800 4.9677 .0123 -1 0 1
4.7500 4.7509 -.0009 1 -1 1
4.3900 4.3866 .0034 -1 1 1
4.2000 4.2026 -.0026 0 2 1
3.6200 3.6198 .0002 -1 2 0
3.4300 3.4318 -.0018 0 2 2
3.2700 3.2694 .0006 -1 -2 1
3.2100 3.2142 -.0042 -1 -1 2
3.1600 3.1574 .0026 0 0 3
2.7720 2.7710 .0010 2 2 1
A= 6.7478 DA= .0004
B= 8.96002 DB= .00002
C= 9.7367 DC= .0001
GAMMA= 86.373 DGAMMA= .002
BETA = 78.127 DBETA = .004
ALPHA= 83.182 DALPHA= .003
V=571.7
3. 31-443
CoV10O28*27H2O
Triklin
Dexp Dcal d(D) h k l
11.1000 11.0954 .0046 1 0 0
9.8300 9.8372 -.0072 0 1 0
9.4100 9.4019 .0081 0 0 1
8.9300 8.9203 .0097 -1 1 0
8.1900 8.2133 -.0233 -1 1 1
7.3800 7.4034 -.0234 0 1 1
6.3300 6.3185 .0115 0 -1 1
4.2700 4.2795 -.0095 2 1 0
4.1500 4.1520 -.0020 -2 -1 1
4.0000 4.0036 -.0036 0 -1 2
3.9000 3.8992 .0008 -3 1 0
3.6300 3.6290 .0010 1 -1 2
A= 12.6092 DA= .0001
B= 10.817 DB= .008
C= 10.245 DC= .001
GAMMA=112.948 DGAMMA= .001
BETA =111.69 DBETA = .01
ALPHA= 73.83 DALPHA= .01
V= 1180.9
4. 31-0444
Co{VO3}2*4H2O
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
7.5600 7.5800 -.0200 0 0 1
3.8000 3.7900 .0100 0 0 2
3.1200 3.1196 .0004 1 1 1
3.0100 3.0111 -.0011 1 2 0
2.5780 2.5781 -.0001 0 4 1
a= 3.603 b=10.966 c= 7.580
da= .001 db= .003 dc= .001
v= 299.5
5. 31-0445
CoV10O28*30H2O
Triklin
Dexp Dcal d(D) h k l
11.1000 11.0988 .0012 1 0 0
9.8300 9.8339 -.0039 0 1 0
9.4100 9.4016 .0084 0 0 1
8.9300 8.9223 .0077 1 1 0
8.1900 8.2152 -.0252 -1 -1 1
7.3800 7.4021 -.0221 0 -1 1
6.3300 6.3173 .0127 0 1 1
4.2700 4.2794 -.0094 -2 1 0
4.1500 4.1518 -.0018 -2 1 1
4.0000 4.0032 -.0032 0 1 2
3.9000 3.9010 -.0010 3 1 0
3.6300 3.6290 .0010 1 1 2
A= 12.616 DA= .008
B= 10.815 DB= .002
C= 10.2460 DC= .0009
GAMMA= 67.04 DGAMMA= .01
BETA =111.705 DBETA = .003
ALPHA=106.1992 DALPHA= .0005
V= 1181.1
6. 31-0604
gamma-InVO4
Triklin
Dexp Dcal d(D) h k l
4.7000 4.6995 .0005 1 0 0
4.1900 4.1945 -.0045 0 1 1
3.8200 3.8185 .0015 0 -1 1
3.5500 3.5557 -.0057 -1 2 1
2.8490 2.8498 -.0008 1 2 0
2.6980 2.6979 .0001 -1 3 0
2.5290 2.5290 .0000 -2 0 1
2.1460 2.1457 .0003 2 1 0
2.1180 2.1185 -.0005 0 4 0
2.0080 2.0076 .0004 0 4 1
1.9180 1.9182 -.0002 1 3 1
1.7780 1.7778 .0002 -2 4 2
1.6180 1.6180 .0000 -3 0 2
1.5830 1.5831 -.0001 -3 -1 1
1.5122 1.5122 -.0000 1 3 2
1.4250 1.4249 .0001 2 4 0
A= 5.33469 DA= .00006
B= 8.9095 DB= .00037
C= 5.0451 DC= .0006
GAMMA=106.827 DGAMMA= .002
BETA =115.432 DBETA = .001
ALPHA= 77.202 DALPHA= .006
V=206.0
7. 31-0605
alfa-InVO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9300 3.9297 .0003 -2 1 1
3.5800 3.5813 -.0013 -2 1 2
3.3000 3.3019 -.0019 -2 0 3
2.9590 2.9593 -.0003 1 1 2
2.5570 2.5569 .0001 -2 2 2
2.4170 2.4187 -.0017 -3 0 4
2.2980 2.2992 -.0012 1 2 2
1.9770 1.9765 .0005 -2 2 4
1.9490 1.9489 .0001 1 3 1
1.7810 1.7820 -.0010 2 3 1
1.6640 1.6639 .0001 -2 0 6
a=10.03 b=6.3252 c= 10.13 beta=119.1
da=.04 db=.0008 dc=.01 dbeta=.1
V= 561.4
Triklin
Dexp Dcal d(D) h k l
3.9300 3.9301 -.0001 -1 1 1
3.5800 3.5803 -.0003 1 1 0
3.3000 3.2992 .0008 -1 -1 1
2.9590 2.9582 .0008 -1 2 1
2.5570 2.5581 -.0011 2 0 0
2.4170 2.4172 -.0002 -1 3 0
2.2980 2.2985 -.0005 0 3 0
1.9770 1.9781 -.0011 0 1 2
1.9490 1.9489 .0001 1 2 1
1.7810 1.7809 .0001 -3 2 0
1.6640 1.6640 .0000 -3 -1 1
A= 5.9098 DA= .0006
B= 7.324 DB= .001
C= 4.6181 DC= .0009
GAMMA=109.23 DGAMMA= .03
BETA =113.45 DBETA = .01
ALPHA= 86.271 DALPHA= .007
V= 172.7
8. 31-0606
beta-InVO4
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
4.2500 4.2423 .0077 3 0 0
3.4000 3.3978 .0022 0 3 0
3.2800 3.2828 -.0028 1 3 0
2.8490 2.8472 .0018 3 1 1
2.6980 2.6990 -.0010 4 2 0
2.6520 2.6520 -.0000 3 3 0
2.3260 2.3224 .0036 4 3 0
2.2650 2.2619 .0031 4 2 1
1.9330 1.9327 .0003 3 4 1
1.7490 1.7494 -.0004 3 2 2
1.6420 1.6414 .0006 2 6 0
1.5900 1.5908 -.0008 8 0 0
1.5170 1.5172 -.0002 6 4 1
a=12.727 b=10.193 c= 4.146
da= .006 db= .001 dc= .003
V= 537.9
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
4.2500 4.2538 -.0038 0 1 1
3.4000 3.4010 -.0010 2 1 1
3.2800 3.2838 -.0038 -3 0 1
2.8490 2.8479 .0011 3 2 0
2.6980 2.6999 -.0019 -4 0 1
2.6520 2.6508 .0012 0 3 0
2.3260 2.3262 -.0002 1 1 2
2.2650 2.2647 .0003 -5 0 1
1.9330 1.9331 -.0001 -3 2 2
1.7490 1.7490 -.0000 7 0 0
1.6420 1.6420 -.0000 0 1 3
1.5900 1.5905 -.0005 0 5 0
1.5170 1.5166 .0004 -4 0 3
a=12.273 b=7.952 c=5.0468 beta=93.97
da=.002 db=.004 dc=.0007 dbet=.01
V=491.4
9. 31-0810
SrMg2{VO4}2
Triklin
Dexp Dcal d(D) h k l
3.8200 3.8206 -.0006 3 2 0
3.4980 3.4987 -.0007 2 3 0
3.1600 3.1596 .0004 3 3 0
3.0640 3.0643 -.0003 4 2 0
2.8630 2.8629 .0001 -1 -1 1
2.8140 2.8137 .0003 -1 0 1
2.7460 2.7457 .0003 4 3 0
2.5120 2.5119 .0001 5 2 0
2.3890 2.3890 .0000 3 -1 1
2.3580 2.3581 -.0001 3 2 1
2.2000 2.2000 -.0000 -3 -3 1
2.0890 2.0891 -.0001 -4 -1 1
A= 12.71903 DA= .00006
B= 10.8630 DB= .0006
C= 3.00593 DC= .00001
GAMMA= 70.983 DGAMMA= .003
BETA = 85.861 DBETA = .001
ALPHA= 95.565 DALPHA= .00179
V=388.4
10. 31-0848
Mn4V2O9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.0800 6.0729 .0071 1 1 0
5.5200 5.5170 .0030 -1 0 1
4.4800 4.4717 .0083 1 1 1
3.4370 3.4322 .0048 0 2 1
3.1130 3.1175 -.0045 3 0 0
2.8570 2.8532 .0038 -3 0 1
2.4890 2.4897 -.0007 -1 2 2
2.4600 2.4572 .0028 3 2 0
2.3970 2.3973 -.0003 -1 3 1
2.1790 2.1796 -.0006 2 3 1
1.8360 1.8360 -.0000 2 4 0
1.7910 1.7913 -.0003 5 0 1
1.7570 1.7567 .0003 4 3 0
1.7480 1.7478 .0002 5 1 1
1.4980 1.4983 -.0003 -5 3 1
a= 9.355 b= 7.985 c= 6.72 beta=91.32
da= .001 db= .005 dc= .02 dbeta=.03
V= 502
Triklin
Dexp Dcal d(D) h k l
6.0800 6.0793 .0007 -1 1 0
5.5200 5.5245 -.0045 0 1 1
4.4800 4.4812 -.0012 0 -1 1
3.4370 3.4386 -.0016 -1 0 2
3.1130 3.1128 .0002 -2 -1 1
2.8570 2.8569 .0001 -3 0 1
2.4890 2.4890 .0000 -2 -1 2
2.4600 2.4606 -.0006 -3 0 2
2.3970 2.3970 -.0000 -1 3 0
2.1790 2.1787 .0003 -4 0 1
1.8360 1.8361 -.0001 -4 3 2
1.7910 1.7910 .0000 4 -2 1
1.7570 1.7569 .0001 -2 2 4
1.7480 1.7480 .0000 -5 1 0
1.4980 1.4980 -.0000 3 2 3
A= 9.058 DA= .003
B= 7.466 DB= .002
C= 7.2552 DC= .0001
GAMMA=104.62 DGAMMA= .03
BETA =105.01 DBETA = .02
ALPHA= 75.041 DALPHA= .007
V= 448.7
11. 31-0920
Ni2V2PbO8
Triklin
Dexp Dcal d(D) h k l
6.1000 6.0990 .0010 -1 0 1
4.9400 4.9403 -.0003 0 1 1
4.6600 4.6677 -.0077 0 -1 1
4.5200 4.5207 -.0007 -1 1 1
4.3300 4.3343 -.0043 -1 -1 1
3.7600 3.7617 -.0017 -2 -1 1
3.5900 3.5865 .0035 3 1 1
3.4400 3.4392 .0008 3 -1 1
3.2200 3.2237 -.0037 0 1 2
3.0700 3.0678 .0022 1 -1 2
2.9760 2.9757 .0003 1 2 1
2.8400 2.8394 .0006 1 -2 1
2.7370 2.7374 -.0004 -4 1 1
2.4960 2.4958 .0002 3 -2 1
2.3740 2.3744 -.0004 5 0 2
A= 14.19 DA= .09
B= 6.441 DB= .002
C= 7.286 DC= .009
GAMMA= 88.8 DGAMMA= .1
BETA = 82.4 DBETA = .2
ALPHA= 86.60 DALPHA= .04
V= 659
12. 31-0921
alfa-Ni3{VO4}2
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
4.1400 4.1427 -.0027 0 1 0
3.8200 3.8139 .0061 2 1 0
3.1700 3.1754 -.0054 2 1 1
2.8700 2.8665 .0035 0 0 2
2.7900 2.7908 -.0008 7 0 0
2.7500 2.7505 -.0005 2 0 2
2.5100 2.5093 .0007 7 0 1
2.4700 2.4721 -.0021 4 0 2
2.0600 2.0598 .0002 1 2 0
2.0000 1.9996 .0004 7 0 2
a=19.536 b= 4.143 c= 5.733
da= .007 db= .001 dc= .001
V=464.0
13. 31-0922
Ni{VO3}2*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.1900 8.2493 -.0593 1 1 0
7.0300 7.0655 -.0355 0 1 1
5.9900 5.9871 .0029 1 1 1
5.7200 5.7017 .0183 2 0 0
4.7700 4.7598 .0102 2 0 1
4.1100 4.1130 -.0030 0 1 2
3.7400 3.7410 -.0010 -2 2 1
3.6200 3.6222 -.0022 3 1 0
3.4500 3.4517 -.0017 1 3 1
2.9880 2.9871 .0009 0 4 0
2.9210 2.9205 .0005 0 0 3
2.8580 2.8586 -.0006 3 0 2
2.5780 2.5786 -.0006 3 2 2
2.3800 2.3799 .0001 4 0 2
1.8240 1.8232 .0008 -2 3 4
1.8240 1.8240 .0000 1 5 3
a=11.4038 b=11.948 c=8.762 beta=90.5
da=.00032 db=.008 dc=.003 dbeta=.1
V= 1193.8
Triklin
Dexp Dcal d(D) h k l
8.1900 8.2028 -.0128 1 0 0
7.0300 7.0193 .0107 0 1 0
5.9900 5.9798 .0102 -1 0 1
5.7200 5.7155 .0045 0 1 1
4.7700 4.7686 .0014 1 1 0
4.1100 4.1144 -.0044 1 1 1
3.7400 3.7389 .0011 0 0 2
3.6200 3.6184 .0016 -1 2 1
3.4500 3.4517 -.0017 0 2 1
2.9880 2.9899 -.0019 -2 0 2
2.9210 2.9203 .0007 2 1 1
2.8580 2.8577 .0003 0 2 2
2.5780 2.5782 -.0002 -3 2 1
2.3800 2.3795 .0005 -3 0 2
1.8240 1.8240 .0000 4 -2 1
A= 8.6698 DA= .0002
B= 7.488 DB= .004
C= 7.800 DC= .004
GAMMA=106.98 DGAMMA= .04
BETA =102.00 DBETA = .05
ALPHA= 75.74 DALPHA= .03
V= 464.3
14. 31-0923
Ni3V10O28824H2O
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
12.0000 12.0033 -.0033 0 1 0
11.1000 11.0518 .0482 0 0 1
9.3100 9.3392 -.0292 1 1 0
8.9300 8.8695 .0605 1 0 1
8.1900 8.1304 .0596 0 1 1
7.3800 7.4332 -.0532 2 0 0
6.3300 6.3196 .0104 2 1 0
5.4700 5.4860 -.0160 2 1 1
4.7500 4.7558 -.0058 1 1 2
4.3100 4.3014 .0086 2 2 1
3.8700 3.8636 .0064 1 3 0
3.2400 3.2408 -.0008 0 3 2
3.1600 3.1598 .0002 4 2 0
2.9600 2.9565 .0035 3 0 3
2.8850 2.8861 -.0011 5 1 0
2.0320 2.0326 -.0006 0 4 4
a=14.87 b=12.00 c=11.05
da= .01 db= .04 dc= .01
V=1972
31-1434
Ñì. ñîåäèíåíèÿ U
15. 31-1985
C10H10Cl4N6V
Triklin
Dexp Dcal d(D) h k l
5.0000 5.0065 -.0065 0 0 1
4.7000 4.6982 .0018 -1 -1 1
4.3500 4.3531 -.0031 0 -2 1
3.9700 3.9769 -.0069 -1 1 1
3.6500 3.6473 .0027 -1 -3 1
3.4200 3.4222 -.0022 2 2 0
3.2100 3.2081 .0019 1 2 1
2.9800 2.9785 .0015 -2 1 1
2.7100 2.7112 -.0012 2 0 1
2.5600 2.5607 -.0007 -1 -2 2
2.4400 2.4405 -.0005 -1 -3 2
2.3300 2.3300 -.0000 -3 -3 1
A= 7.583 DA= .001
B= 13.43 DB= .01
C= 5.22320 DC= .00004
GAMMA= 78.26 DGAMMA= .02
BETA =103.06 DBETA = .02
ALPHA=102.49 DALPHA= .06
V= 499.2
16. 32-0143
Cd2{OH4}4x{V2O7}1-x*zH2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5100 5.5161 -.0061 1 1 0
4.2500 4.2497 .0003 2 1 0
3.8400 3.8386 .0014 -2 0 2
3.6600 3.6595 .0005 3 0 1
3.1400 3.1396 .0004 0 2 0
3.0100 3.0105 -.0005 0 2 1
2.8300 2.8289 .0011 3 1 2
2.7600 2.7605 -.0005 -4 0 1
2.6800 2.6804 -.0004 2 2 1
2.6400 2.6412 -.0012 1 2 2
2.4300 2.4302 -.0002 -2 2 2
2.3700 2.3698 .0002 -3 1 3
a=11.5527 b= 6.279 c=10.614 beta=87.96
da=.0008 db=.002 dc=.008 dbeta=.02
V= 769.5
Triklin
Dexp Dcal d(D) h k l
5.5100 5.5131 -.0031 0 0 1
4.2500 4.2527 -.0027 -1 -1 1
3.8400 3.8365 .0035 0 -2 1
3.6600 3.6577 .0023 -1 -2 1
3.1400 3.1395 .0005 -1 2 0
3.0100 3.0088 .0012 -2 -1 1
2.8300 2.8292 .0008 1 -1 2
2.7600 2.7608 -.0008 0 3 0
2.6800 2.6805 -.0005 3 1 1
2.6400 2.6410 -.0010 0 -2 2
2.4300 2.4293 .0007 0 1 2
2.3700 2.3707 -.0007 -1 0 2
A= 8.326 DA= .008
B= 9.137 DB= .002
C= 5.8539 DC= .0006
GAMMA= 70.09 DGAMMA= .05
BETA = 77.662 DBETA = .003
ALPHA= 99.86 DALPHA= .02
V=394.3
17. 32-0446
H2VP3O10
Triklin
Dexp Dcal d(D) h k l
6.9400 6.9405 -.0005 1 0 0
5.7200 5.7031 .0169 1 1 0
5.5700 5.5779 -.0079 -1 0 1
5.3500 5.3576 -.0076 -1 1 1
4.7900 4.7893 .0007 1 0 1
4.7000 4.6935 .0065 0 2 0
4.3700 4.3793 -.0093 -1 -1 1
4.0900 4.0908 -.0008 0 1 2
3.7700 3.7683 .0017 -1 1 2
3.6800 3.6818 -.0018 0 2 2
3.5900 3.5865 .0035 -1 0 2
3.4800 3.4808 -.0008 0 -2 1
A= 7.022 DA= .001
B= 10.06 DB= .01
C= 8.281 DC= .003
GAMMA= 90.64 DGAMMA= .05
BETA = 98.39 DBETA = .03
ALPHA= 69.08 DALPHA= .08
V=540.2
18. 32-0615
LuV4O8
Rombik
Groupa 54
Dexp. Dcal. d(D) h k l
5.0400 5.0557 -.0157 1 0 2
4.8520 4.8542 -.0022 0 1 2
4.5700 4.5722 -.0022 2 1 0
4.4160 4.4132 .0028 1 1 2
3.8990 3.8973 .0017 2 0 2
3.5810 3.5793 .0017 2 1 2
3.4390 3.4402 -.0012 2 2 0
3.3720 3.3710 .0010 1 2 2
3.0100 3.0102 -.0002 3 0 2
2.9500 2.9525 -.0025 2 2 2
2.7760 2.7758 .0002 1 0 4
2.6700 2.6708 -.0008 0 3 2
a=10.597 b= 9.046 c=11.505
da= .001 db= .003 dc= .002
V=1103
19. 32-0868
k3VCl6
Triklin
Dexp. Dcal. d(D) h k l
6.0000 6.0011 -.0011 -2 -1 0
3.6500 3.6512 -.0012 -3 -2 0
3.5200 3.5221 -.0021 0 0 1
3.1100 3.1135 -.0035 -2 -3 0
2.9700 2.9707 -.0007 0 -3 0
2.9000 2.8993 .0007 -3 -3 0
2.7700 2.7714 -.0014 3 1 1
2.6800 2.6796 .0004 1 -3 0
2.6400 2.6397 .0003 -3 -1 1
2.5800 2.5796 .0004 -2 -2 1
2.4900 2.4918 -.0018 -5 -2 0
2.3800 2.3794 .0006 4 2 1
A= 12.744 DA= .007
B= 9.576 DB= .002
C= 3.5619 DC= .0008
GAMMA= 70.17 DGAMMA= .01
BETA = 88.11 DBETA = .08
ALPHA= 81.49 DALPHA= .07
V= 404.3
20. 32-0968
Rb3VCl6
Triklin
Dexp Dcal d(D) h k l
4.3900 4.3914 -.0014 -1 3 0
3.7300 3.7296 .0004 3 0 0
3.6100 3.6079 .0021 -3 2 0
3.2500 3.2507 -.0007 0 4 0
3.0700 3.0704 -.0004 1 1 1
2.8100 2.8117 -.0017 -4 2 0
2.7900 2.7901 -.0001 1 -3 1
2.7400 2.7401 -.0001 -1 -2 1
2.6400 2.6391 .0009 -4 3 0
2.5800 2.5793 .0007 -2 -1 1
2.5300 2.5295 .0005 0 3 1
2.5100 2.5105 -.0005 -2 2 1
A= 11.643 DA= .001
B= 13.4217 DB= .0003
C= 3.3173 DC= .0001
GAMMA=103.861 DGAMMA= .007
BETA = 80.684 DBETA = .007
ALPHA= 95.867 DALPHA= .005
V=495.5
21. 32-0970
Rb2VCl4
Triklin
Dexp Dcal d(D) h k l
6.7000 6.7024 -.0024 1 0 0
3.7100 3.7174 -.0074 1 1 1
3.4500 3.4509 -.0009 -1 -1 1
3.1700 3.1728 -.0028 -2 0 1
2.8100 2.8118 -.0018 -2 -1 1
2.3900 2.3907 -.0007 2 1 2
2.2000 2.1992 .0008 -3 0 1
2.0800 2.0781 .0019 0 2 1
2.0400 2.0397 .0003 2 2 0
1.9400 1.9398 .0002 -3 -1 2
1.8600 1.8596 .0004 0 0 4
1.8000 1.8001 -.0001 0 1 4
A= 6.9999 DA= .0004
B= 4.357 DB= .003
C= 7.5353 DC= .0006
GAMMA= 74.164 DGAMMA= .007
BETA = 93.311 DBETA = .007
ALPHA= 82.66 DALPHA= .01
V= 218.2
22. 32-1027
AgTlV2O6
Triklin
Dexp Dcal d(D) h k l
5.2400 5.2381 .0019 1 -1 1
5.1400 5.1402 -.0002 0 1 1
4.8600 4.8596 .0004 0 -1 1
4.2300 4.2292 .0008 2 -1 1
3.8200 3.8220 -.0020 1 1 2
3.6700 3.6698 .0002 -2 0 1
3.3100 3.3115 -.0015 1 -1 3
3.2400 3.2389 .0011 2 -1 3
3.1800 3.1794 .0006 0 1 3
3.1500 3.1507 -.0007 3 -1 1
2.9000 2.8998 .0002 3 0 3
2.0000 2.0000 .0000 -2 -2 1
A= 9.93892 DA= .00009
B= 5.8211 DB= .0003
C= 11.9272 DC= .0006
GAMMA=105.3907 DGAMMA= .0004
BETA = 68.174 DBETA = .004
ALPHA= 92.0934 DALPHA= .0003
V=616
23. 32-1055
Na2CaV2O7
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
4.3300 4.3189 .0111 3 0 0
3.3600 3.3655 -.0055 3 2 0
3.3100 3.3076 .0024 1 2 1
3.2400 3.2392 .0008 4 0 0
3.1300 3.1334 -.0034 2 3 0
2.9700 2.9742 -.0042 3 1 1
2.7900 2.7864 .0036 0 3 1
2.5200 2.5191 .0009 5 1 0
2.1900 2.1872 .0028 1 0 2
2.1900 2.1908 -.0008 5 1 1
2.1600 2.1595 .0005 6 0 0
a=12.956840 b=10.739990 c= 4.438033
da= .002317 db= .001400 dc= .001182
V= 617.6
24. 32-1196
Na3VCl6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
3.0900 3.0903 -.0003 0 5 0
2.9500 2.9511 -.0011 0 5 1
2.6500 2.6493 .0007 1 1 0
2.2600 2.2603 -.0003 0 5 3
2.1500 2.1549 -.0049 0 7 1
2.0900 2.0905 -.0005 0 4 4
1.8800 1.8783 .0017 1 5 2
1.8000 1.8004 -.0004 0 8 2
1.6700 1.6688 .0012 0 8 3
1.6000 1.5990 .0010 1 0 5
1.4600 1.4605 -.0005 0 5 6
1.2800 1.2800 .0000 2 2 2
1.1700 1.1701 -.0001 1 9 5
a= 2.6891 b=15.451 c= 9.944
da= .0001 db= .002 dc= .004
V= 413.2
Triklin
Dexp Dcal d(D) h k l
3.0900 3.0889 .0011 1 1 1
2.9500 2.9497 .0003 0 -1 1
2.6500 2.6506 -.0006 -1 -1 1
2.2600 2.2600 .0000 0 -2 1
2.1500 2.1506 -.0006 -1 -2 1
2.0900 2.0902 -.0002 -2 1 1
1.8800 1.8795 .0005 -2 -2 1
1.8000 1.8003 -.0003 2 3 1
1.6700 1.6702 -.0002 1 -3 1
1.6000 1.6000 .0000 0 4 0
1.4600 1.4600 .0000 -2 0 2
1.2800 1.2800 .0000 0 5 0
1.1700 1.1700 .0000 1 1 3
A= 6.70 DA= .01
B= 6.506 DB= .003
C= 3.521 DC= .001
GAMMA= 80.85 DGAMMA= .07
BETA = 81.87 DBETA = .09
ALPHA= 83.97 DALPHA= .05
V= 149.5
25. 32-1379
TiV4O10
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
3.2400 3.2395 .0005 2 0 1
2.6800 2.6818 -.0018 2 2 0
2.5000 2.5014 -.0014 1 3 0
2.4300 2.4323 -.0023 0 0 3
2.2000 2.2003 -.0003 3 1 1
2.1500 2.1457 .0043 2 3 0
2.0000 1.9995 .0005 0 4 0
1.8500 1.8495 .0005 2 3 2
1.7000 1.7015 -.0015 2 4 1
1.6600 1.6597 .0003 0 2 4
1.6100 1.6091 .0009 2 3 3
1.4400 1.4406 -.0006 3 3 3
1.3600 1.3599 .0001 5 2 0
a= 7.2306 b= 7.9982 c= 7.298
da= .0004 db= .0003 dc= .001
V= 422.0
26. 32-1978
C26H16N6S2V
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
8.5400 8.5537 -.0137 1 0 1
7.8000 7.7849 .0151 0 1 1
7.0800 7.1033 -.0233 1 1 1
6.4000 6.3751 .0249 0 2 0
5.7900 5.7953 -.0053 2 1 1
5.0000 4.9865 .0135 3 0 1
4.5900 4.5861 .0039 0 1 2
3.7500 3.7460 .0040 3 0 2
3.2500 3.2531 -.0031 4 0 2
3.1600 3.1611 -.0011 1 3 2
2.0200 2.0200 -.0000 2 6 1
a=17.358 b=12.750 c= 9.83
da= .007 db= .002 dc= .02
V=2176
27. 32-1979
C22H20N6S2V
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.2100 8.1817 .0283 1 0 1
7.6100 7.6156 -.0056 1 1 0
5.9200 5.9297 -.0097 -2 1 1
5.4000 5.3959 .0041 0 1 2
4.6400 4.6360 .0040 2 1 1
4.5000 4.5030 -.0030 0 2 0
4.3400 4.3415 -.0015 -3 0 3
4.0200 4.0204 -.0004 0 1 3
3.8300 3.8344 -.0044 1 0 3
3.6800 3.6791 .0009 -4 0 3
3.5800 3.5802 -.0002 -3 0 4
a= 15.843 b= 9.006 c= 14.968 beta=115.8
da=.0083 db=.009 dc=.002 dbeta=.1
V= 1923
Triklin
Dexp Dcal d(D) h k l
8.2100 8.2020 .0080 0 1 1
7.6100 7.6069 .0031 0 -1 1
5.9200 5.9280 -.0080 1 0 0
5.4000 5.3969 .0031 -1 1 0
4.6400 4.6398 .0002 1 -1 1
4.5000 4.5011 -.0011 0 1 2
4.3400 4.3404 -.0004 0 -3 1
4.0200 4.0199 .0001 1 -2 1
3.8300 3.8295 .0005 1 3 1
3.6800 3.6802 -.0002 0 4 1
3.5800 3.5797 .0003 -1 0 2
A= 5.949 DA= .002
B= 15.588 DB= .001
C= 9.2060 DC= .0002
GAMMA= 85.372 DGAMMA= .001
BETA = 88.069 DBETA = .007
ALPHA= 84.950 DALPHA= .008
V= 847.4