1. 29-0020
{Al,Cr}VO4*3H2O
Triklin
Dexp Dcal d(D) h k l
6.6100 6.6086 .0014 -1 1 0
5.8800 5.8818 -.0018 0 -1 1
3.9300 3.9301 -.0001 1 -1 2
3.8000 3.8007 -.0007 1 0 2
3.5900 3.5913 -.0013 2 0 1
3.2900 3.2921 -.0021 -1 2 1
2.9900 2.9874 .0026 -1 1 2
2.8700 2.8705 -.0005 -1 -1 2
2.7700 2.7703 -.0003 -1 3 0
2.6100 2.6110 -.0010 -2 -1 1
2.4900 2.4901 -.0001 3 -1 2
2.2670 2.2660 .0010 2 2 0
A= 8.083 DA= .001
B= 8.5265 DB= .0002
C= 8.214 DC= .002
GAMMA=113.65 DGAMMA= .01
BETA = 73.51 DBETA = .01
ALPHA=102.917 DALPHA= .006
V= 493.4
2. 29-0571
{Zn,Ni,Cu+2}8Al8V2+5Si50.35*27H2O
Rombik
Groupa 56
Dexp. Dcal. d(D) h k l
4.9100 4.9076 .0024 0 0 2
3.9100 3.9074 .0026 0 1 2
2.6100 2.6095 .0005 2 0 2
2.4200 2.4195 .0005 2 1 2
2.2800 2.2797 .0003 1 0 4
1.9900 1.9900 -.0000 1 3 1
1.6800 1.6798 .0002 3 1 3
1.5300 1.5302 -.0002 3 1 4
1.4200 1.4200 .0000 1 2 6
a= 6.1625 b= 6.4580 c= 9.8151
da= .0005 db= .0001 dc= .0001
V= 390.62
3. 30-0362
NaCs{VO3}2*H2O
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
8.3200 8.3161 .0039 1 1 0
4.8000 4.8185 -.0185 4 0 0
4.1600 4.1580 .0020 2 2 0
3.8600 3.8548 .0052 5 0 0
3.3900 3.3863 .0037 1 0 1
3.2200 3.2227 -.0027 0 1 1
3.0700 3.0728 -.0028 0 3 0
2.9300 2.9275 .0025 2 3 0
2.7300 2.7289 .0011 1 2 1
2.6500 2.6504 -.0004 2 2 1
a=19.27 b= 9.21827 c= 3.440
da= .05 db= .00002 dc= .001
V= 611
4. 30-0380
Cs0.125V0.125Mo0.875O3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.9100 8.8747 .0353 1 0 0
4.5000 4.4967 .0033 1 1 0
3.4200 3.4261 -.0061 0 1 1
3.3800 3.3866 -.0066 2 0 1
3.3800 3.3798 .0002 2 1 0
2.9900 2.9981 -.0081 -2 0 1
2.8400 2.8404 -.0004 2 1 1
2.6100 2.6079 .0021 0 2 0
2.5000 2.5021 -.0021 1 2 0
2.1300 2.1298 .0002 2 0 2
2.0800 2.0799 .0001 1 1 2
1.9800 1.9795 .0005 -1 1 2
a= 8.941 b= 5.216 c= 4.578 beta= 83.03
da=.004 db= .004 dc=.006 dbeta=.01
V= 211.9
Triklin
Dexp Dcal d(D) h k l
8.9100 8.9140 -.0040 0 1 0
4.5000 4.4991 .0009 -1 0 1
3.4200 3.4207 -.0007 0 -1 2
3.3800 3.3796 .0004 -1 -2 1
2.9900 2.9890 .0010 -1 2 1
2.8400 2.8396 .0004 2 1 1
2.6100 2.6098 .0002 -2 0 1
2.5000 2.4988 .0012 0 2 3
2.1300 2.1306 -.0006 -1 2 3
2.0800 2.0803 -.0003 2 1 3
1.9800 1.9802 -.0002 1 1 4
1.9300 1.9299 .0001 1 -3 2
A= 5.8705 DA= .0002
B= 9.4890 DB= .0009
C= 8.1764 DC= .001
GAMMA= 72.88 DGAMMA= .02
BETA = 84.23 DBETA = .01
ALPHA= 78.21 DALPHA= .02
V= 425.7
5. 30-0381
Cs0.25V0.25Mo0.75O3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.1300 9.1119 .0181 0 1 0
4.5400 4.5559 -.0159 0 2 0
3.9200 3.9216 -.0016 -2 1 2
3.6700 3.6738 -.0038 0 0 3
3.5800 3.5797 .0003 2 1 1
3.2700 3.2683 .0017 -2 1 3
3.1100 3.1119 -.0019 2 0 2
2.9100 2.9127 -.0027 -1 0 4
2.6400 2.6374 .0026 0 1 4
2.3400 2.3409 -.0009 0 3 3
2.1500 2.1500 .0000 1 2 4
2.1400 2.1392 .0008 1 4 1
2.0900 2.0899 .0001 4 2 0
2.0500 2.0502 -.0002 2 4 0
1.9900 1.9900 .0000 -5 0 2
a= 9.951 b= 9.112 c= 11.658 beta=109.0
da=.005 db= .005 dc=.001 dbeta=.1
V= 999
Triklin
Dexp Dcal d(D) h k l
9.1300 9.1364 -.0064 0 0 1
4.5400 4.5417 -.0017 0 -2 1
3.9200 3.9182 .0018 -1 -1 1
3.6700 3.6728 -.0028 -1 0 2
3.5800 3.5795 .0005 0 -2 2
3.2700 3.2719 -.0019 1 1 1
3.1100 3.1077 .0023 0 2 2
2.9100 2.9110 -.0010 0 3 1
2.6400 2.6399 .0001 1 1 2
2.3400 2.3406 -.0006 -2 0 1
2.1500 2.1504 -.0004 -1 -3 3
2.1400 2.1401 -.0001 -2 2 2
2.0900 2.0898 .0002 2 -2 1
2.0500 2.0501 -.0001 -2 1 3
1.9900 1.9895 .0005 -2 -1 3
A= 4.7435 DA= .0006
B= 9.883 DB= .002
C= 9.433 DC= .002
GAMMA= 99.21 DGAMMA= .01
BETA =101.98 DBETA = .02
ALPHA= 95.90 DALPHA= .02
V= 422.8
6. 30-0382
Cs0.40V0.40MoO.60O3
Triklin
Dexp Dcal d(D) h k l
9.0000 8.9984 .0016 1 0 1
3.7000 3.7024 -.0024 0 1 1
3.6100 3.6118 -.0018 0 -1 1
3.5000 3.4998 .0002 1 1 1
3.4700 3.4702 -.0002 1 1 0
3.3700 3.3698 .0002 -1 1 1
3.0900 3.0904 -.0004 3 0 2
2.9300 2.9326 -.0026 -1 0 6
2.8100 2.8091 .0009 0 1 5
2.7500 2.7489 .0011 -2 0 5
2.5800 2.5800 .0000 -1 1 5
2.5100 2.5100 .0000 -2 -1 3
2.3900 2.3895 .0005 0 -1 6
2.3400 2.3400 .0000 -2 -1 4
2.3300 2.3300 .0000 0 1 7
A= 9.3429 DA= .0005
B= 3.7309 DB= .0007
C= 20.230 DC= .005
GAMMA= 88.14 DGAMMA= .04
BETA = 78.91 DBETA = .02
ALPHA= 85.81 DALPHA= .01
V= 690.0
7. 30-0383
Cs0.50V0.50Mo0.50O3
Triklin
Dexp Dcal d(D) h k l
4.6700 4.6706 -.0006 1 1 1
4.2200 4.2185 .0015 2 0 1
3.8600 3.8580 .0020 1 -1 1
3.6200 3.6191 .0009 0 2 0
3.5200 3.5199 .0001 2 -1 1
3.3800 3.3764 .0036 3 0 1
3.2900 3.2892 .0008 1 2 1
3.1600 3.1593 .0007 -4 1 0
2.9200 2.9214 -.0014 -4 1 1
2.8200 2.8209 -.0009 0 0 2
2.7800 2.7796 .0004 -2 1 2
2.7200 2.7204 -.0004 1 -2 1
2.5600 2.5594 .0006 -2 0 2
2.2100 2.2098 .0002 5 1 0
2.1300 2.1302 -.0002 4 2 0
A= 12.92 DA= .05
B= 7.898 DB= .001
C= 5.98028 DC= .00005
GAMMA=104.29 DGAMMA= .05
BETA = 94.0 DBETA = .1
ALPHA= 70.65 DALPHA= .01
V= 557.9
8. 30-0387
omega-CsV2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.5200 3.5204 -.0004 -2 1 1
3.2700 3.2688 .0012 3 0 0
3.2000 3.2023 -.0023 -1 0 2
3.0100 3.0109 -.0009 0 3 0
2.7700 2.7692 .0008 0 3 1
2.5600 2.5600 .0000 3 2 1
2.4600 2.4599 .0001 2 3 1
2.2700 2.2693 .0007 -3 0 2
2.1700 2.1708 -.0008 -4 1 1
2.0300 2.0300 .0000 -2 0 3
1.7390 1.7390 .0000 1 1 4
a= 9.8738 b= 9.033 c= 7.103 beta= 83.30
da=.0009 db=.003 dc=.001 dbeta=.04
V= 629.2
9. 30-0388
kappa-CsV3O7.5
Triklin
Dexp Dcal d(D) h k l
4.1000 4.1015 -.0015 2 1 0
4.0000 4.0007 -.0007 2 1 1
3.8000 3.7980 .0020 0 -1 1
3.6700 3.6677 .0023 -1 -1 1
3.5400 3.5390 .0010 1 -1 1
3.2900 3.2915 -.0015 -3 0 1
3.2200 3.2200 -.0000 3 1 1
3.0700 3.0730 -.0030 2 -1 1
2.9200 2.9196 .0004 -3 1 0
2.7300 2.7305 -.0005 1 2 1
2.6800 2.6796 .0004 4 0 1
2.5700 2.5695 .0005 -1 2 1
A= 11.455 DA= .001
B= 5.5177 DB= .0003
C= 7.506 DC= .006
GAMMA= 82.52 DGAMMA= .01
BETA = 85.592 DBETA = .009
ALPHA= 74.06 DALPHA= .02
V=452.6
10. 30-0389
CsV3O8
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
4.1200 4.1107 .0093 1 1 0
4.0800 4.0800 .0000 2 0 0
3.6800 3.6801 -.0001 -2 0 2
3.5600 3.5567 .0033 1 1 1
3.3200 3.3188 .0012 0 1 2
3.2400 3.2396 .0004 -1 0 3
3.0900 3.0873 .0027 0 0 3
2.9400 2.9400 .0000 -2 0 3
2.7200 2.7200 .0000 3 0 0
2.5900 2.5900 .0000 0 1 3
a= 8.5842 b= 4.7587 c= 9.7435 beta= 108.082
da=.0001 db=.0007 dc=.0004 dbet=.004
V=378.7
11. 30-0390
beta-CsV6O15
Monoklin
GRUPA 7,13
Dexp. Dcal. d(D) h k l
4.1000 4.1100 -.0100 0 3 0
3.4200 3.4148 .0052 2 1 0
3.0900 3.0902 -.0002 -1 2 1
2.8300 2.8280 .0020 1 4 0
2.6900 2.6893 .0007 -2 1 1
2.4800 2.4791 .0009 2 1 1
2.3700 2.3692 .0008 3 0 0
1.9800 1.9800 .0000 1 5 1
a= 7.13 b= 12.330 c= 3.9450 beta= 94.89
da= .02 db=.005 dc=.0001 dbet=.02
V=345.9
12. 30-0391
Cs2V4O11
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
3.6200 3.6190 .0010 1 1 1
2.8400 2.8370 .0030 0 1 2
2.8300 2.8265 .0035 0 3 0
2.6800 2.6779 .0021 2 0 0
2.5000 2.4997 .0003 1 3 0
2.3500 2.3509 -.0009 2 1 1
2.2300 2.2314 -.0014 1 2 2
1.9430 1.9440 -.0010 2 3 0
1.7470 1.7470 .0000 3 1 0
1.6780 1.6778 .0002 3 1 1
a= 5.3558 b= 8.479 c= 6.021
da= .0005 db= .002 dc= .005
V= 273.4
13. 30-0393
Cs4V2O7
Monoklin
Grupa 3
Dexp. Dcal. d(D) h k l
3.9800 3.9769 .0031 1 0 1
3.3600 3.3637 -.0037 0 1 3
3.3000 3.3019 -.0019 0 2 0
3.1200 3.1199 .0001 1 1 2
2.8800 2.8770 .0030 0 2 2
2.5400 2.5404 -.0004 1 2 1
2.3600 2.3602 -.0002 1 1 4
2.2100 2.2100 .0000 0 1 5
1.9180 1.9180 .0000 0 3 3
1.9040 1.9040 .0000 2 1 2
a= 4.0738 b=6.6037 c=11.818 beta=82.852
da=.0002 db=.0003 dc=.001 dbet=.001
V=315.5
14. 30-0394
CsV6O14*4H2O
Triklin
Dexp Dcal d(D) h k l
3.5600 3.5612 -.0012 0 1 1
3.4500 3.4488 .0012 0 -1 1
3.2200 3.2207 -.0007 -1 1 1
3.0900 3.0916 -.0016 -1 2 1
2.7800 2.7788 .0012 1 -2 1
2.4800 2.4791 .0009 -1 5 1
2.4300 2.4306 -.0006 -2 2 1
2.1900 2.1896 .0004 2 -2 1
2.1300 2.1301 -.0001 -1 8 0
2.0700 2.0694 .0006 0 -7 1
1.9640 1.9635 .0005 -3 -2 1
1.7220 1.7221 -.0001 0 11 0
A= 6.7970 DA= .0005
B= 19.235 DB= .003
C= 3.5888 DC= .0004
GAMMA= 81.38 DGAMMA= .02
BETA = 94.22 DBETA = .01
ALPHA= 85.65 DALPHA= .01
V=461.0
15. 30-0570
GaInV2O8
Triklin
Dexp Dcal d(D) h k l
4.7900 4.7927 -.0027 0 1 1
4.2900 4.2893 .0007 -1 1 1
3.8900 3.8900 .0000 0 -1 1
3.5900 3.5889 .0011 1 -1 1
3.2900 3.2890 .0010 -2 1 1
2.9300 2.9303 -.0003 2 -1 1
2.8600 2.8545 .0055 3 0 0
2.7200 2.7203 -.0003 -1 1 2
2.5600 2.5613 -.0013 -3 0 1
2.4300 2.4301 -.0001 2 2 1
2.3400 2.3405 -.0005 3 -1 1
2.1400 2.1409 -.0009 4 0 0
A= 8.586 DA= .001
B= 6.615 DB= .004
C= 5.825 DC= .002
GAMMA= 94.09 DGAMMA= .02
BETA = 91.356 DBETA = .003
ALPHA= 77.98 DALPHA= .03
V= 322.7
16. 30-0667
FeVO4
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
5.6300 5.6363 -.0063 1 1 0
4.4000 4.3954 .0046 4 0 0
3.2400 3.2434 -.0034 1 0 1
2.8900 2.8859 .0041 0 1 1
2.7400 2.7419 -.0019 2 1 1
2.5100 2.5116 -.0016 7 0 0
2.1900 2.1911 -.0011 6 0 1
1.8300 1.8292 .0008 8 0 1
1.7000 1.7000 -.0000 0 3 1
a=17.58 b= 5.950 c= 3.300
da= .01 db= .007 dc= .005
v= 345.2
17. 30-0695
Pb6BVO10
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.1100 6.1361 -.0261 2 0 1
3.8700 3.8599 .0101 1 1 1
3.5600 3.5641 -.0041 4 0 1
3.4000 3.3926 .0074 1 0 3
3.3300 3.3281 .0019 0 1 2
3.1300 3.1327 -.0027 3 1 1
2.8490 2.8495 -.0005 4 1 0
2.6670 2.6680 -.0010 1 1 3
2.2760 2.2752 .0008 6 0 2
2.1220 2.1215 .0005 7 0 1
1.9370 1.9367 .0003 7 1 0
1.8800 1.8802 -.0002 0 1 5
1.6920 1.6924 -.0004 7 1 3
1.6100 1.6100 -.0000 6 0 5
a=15.167 b= 4.319 c=10.442
da= .007 db= .004 dc= .005
V= 684.1
18. 30-0696
Pb10B3VO17
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
7.0200 6.9739 .0461 0 0 1
5.8400 5.8602 -.0202 1 0 0
3.8700 3.8722 -.0022 0 2 1
3.1000 3.1039 -.0039 0 3 0
2.9310 2.9301 .0009 2 0 0
2.8400 2.8357 .0043 0 3 1
2.5220 2.5198 .0022 1 2 2
1.9610 1.9600 .0010 1 2 3
1.4710 1.4714 -.0004 1 3 4
1.4630 1.4631 -.0001 3 4 1
a= 5.860 b= 9.312 c= 6.974
da= .005 db= .008 dc= .009
V= 380.5
19. 30-0703
Pb5Ge6V18O62
Triklin
Dexp Dcal d(D) h k l
5.5400 5.5499 -.0099 0 1 1
4.9200 4.9224 -.0024 1 1 0
4.3500 4.3459 .0041 0 -1 1
3.6000 3.5965 .0035 1 -1 1
3.4500 3.4486 .0014 0 2 0
3.2900 3.2887 .0013 -1 2 0
3.2200 3.2206 -.0006 -2 1 2
3.1000 3.1041 -.0041 -2 0 2
3.0000 3.0026 -.0026 2 0 1
2.8700 2.8685 .0015 1 2 1
2.7300 2.7291 .0009 2 -1 1
2.5300 2.5337 -.0037 -3 1 0
A= 8.44 DA= .01
B= 7.25057 DB= .00007
C= 7.492 DC= .00149
GAMMA=101.53 DGAMMA= .04
BETA =110.99 DBETA = .03
ALPHA= 73.092 DALPHA= .007
V= 407.2
20. 30-0704
Pb6GeV4O18
Triklin
Dexp Dcal d(D) h k l
4.9200 4.9238 -.0038 0 1 1
4.5600 4.5602 -.0002 -1 0 1
4.4800 4.4835 -.0035 0 -1 1
4.2700 4.2724 -.0024 -1 -1 1
3.9700 3.9685 .0015 -1 2 1
3.8300 3.8236 .0064 0 -2 1
3.4300 3.4298 .0002 1 -1 1
3.1600 3.1603 -.0003 -2 -1 1
3.0700 3.0713 -.0013 1 -2 1
3.0200 3.0194 .0006 2 3 0
2.8400 2.8397 .0003 1 4 1
2.7900 2.7907 -.0007 1 5 0
A= 7.255 DA= .003
B= 14.661 DB= .008
C= 5.128 DC= .002
GAMMA= 84.90 DGAMMA= .05
BETA =102.04 DBETA = .01
ALPHA= 82.564 DALPHA= .007
V=527.9
21. 30-0705
Pb15Ge4V6O38
Triklin
Dexp Dcal d(D) h k l
4.4200 4.4193 .0007 2 0 1
4.2100 4.2095 .0005 0 1 1
3.7200 3.7207 -.0007 2 -1 1
3.3300 3.3307 -.0007 3 -1 1
3.1200 3.1193 .0007 -1 2 0
3.0400 3.0390 .0010 -3 -1 1
3.0100 3.0135 -.0035 4 1 0
2.9300 2.9307 -.0007 4 -1 1
2.2200 2.2192 .0008 -7 1 0
2.2000 2.1997 .0003 4 2 0
2.0900 2.0904 -.0004 -6 2 1
2.0400 2.0399 .0001 0 3 0
A= 15.782 DA= .001
B= 6.2477 DB= .0003
C= 5.5796 DC= .0008
GAMMA=101.357 DGAMMA= .001
BETA = 93.24 DBETA = .01
ALPHA= 86.9332 DALPHA= .0006
V=538.1
22. 30-0706
Pb17Ge2O26
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.6600 3.6574 .0026 4 0 0
3.3100 3.3113 -.0013 1 0 1
3.1400 3.1339 .0061 4 1 0
3.0400 3.0396 .0004 0 2 0
2.9300 2.9259 .0041 5 0 0
2.8100 2.8069 .0031 2 2 0
2.0900 2.0899 .0001 7 0 0
1.9000 1.9020 -.0020 6 2 0
1.7400 1.7406 -.0006 0 3 1
1.6400 1.6393 .0007 3 3 1
a=14.630 b= 6.079 c= 3.399
da= .009 db= .001 dc= .005
V= 302.3
23. 30-707
Pb19GeV4O31
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.0300 7.0545 -.0245 0 0 2
3.1200 3.1215 -.0015 -1 1 1
3.0800 3.0810 -.0010 1 1 1
2.9900 2.9887 .0013 3 0 0
2.8200 2.8218 -.0018 0 0 5
2.6300 2.6278 .0022 1 0 5
2.2400 2.2393 .0007 -3 1 1
2.0100 2.0069 .0031 -2 1 5
1.9700 1.9700 -.0000 -4 0 4
1.9200 1.9186 .0014 -1 1 6
1.8700 1.8714 -.0014 4 1 0
1.7000 1.6998 .0002 0 2 0
a=9.00 b=3.4000 c= 14.16 beta= 94.92
da=.01 db= .0002 dc=.01 dbeta=.09
V= 432
Triklin
Dexp Dcal d(D) h k l
7.0300 7.0280 .0020 1 0 0
3.1200 3.1183 .0017 1 1 1
3.0800 3.0785 .0015 -1 -1 1
2.9900 2.9899 .0001 2 0 2
2.8200 2.8199 .0001 -2 1 1
2.6300 2.6286 .0014 1 -1 3
2.2400 2.2396 .0004 -3 0 1
2.0100 2.0094 .0006 0 2 1
1.9700 1.9712 -.0012 1 -2 2
1.9200 1.9188 .0012 -2 -1 3
1.8700 1.8699 .0001 3 1 0
1.7000 1.7005 -.0005 -2 -1 4
A= 7.2280 DA= .0004
B= 4.225 DB= .001
C= 10.003 DC= .002
GAMMA=102.67 DGAMMA= .01
BETA = 84.886 DBETA = .001
ALPHA= 92.30 DALPHA= .03
V= 296.8
24. 30-0735
Pb10V2SiO17
Triklin
Dexp Dcal d(D) h k l
3.3000 3.3018 -.0018 0 0 1
3.1600 3.1604 -.0004 0 -2 1
3.0700 3.0693 .0007 1 0 0
3.0100 3.0080 .0020 -1 1 0
2.8700 2.8707 -.0007 1 2 0
2.8500 2.8528 -.0028 -1 2 0
2.8000 2.7993 .0007 1 -1 1
2.2600 2.2617 -.0017 0 7 0
2.0100 2.0101 -.0001 1 6 0
1.9800 1.9790 .0010 0 8 0
1.9300 1.9296 .0004 -1 -1 1
1.8500 1.8501 -.0001 -1 -3 1
A= 3.290 DA= .001
B= 15.916 DB= .007
C= 3.5563 DC= .0005
GAMMA= 91.63 DGAMMA= .07
BETA = 68.912 DBETA = .004
ALPHA= 95.89 DALPHA= .03
V= 172.8
25. 30-0736
Pb15Si4V6O38
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.3900 4.3926 -.0026 1 0 1
4.1900 4.1909 -.0009 1 2 0
3.7100 3.7141 -.0041 2 0 1
3.4200 3.4241 -.0041 2 1 1
3.3100 3.3013 .0087 4 0 0
3.0200 3.0171 .0029 -2 2 1
2.9200 2.9182 .0018 3 1 1
2.2200 2.2178 .0022 5 0 1
2.0800 2.0814 -.0014 -2 2 2
2.0300 2.0290 .0010 3 0 2
1.9700 1.9701 -.0001 6 2 0
1.9000 1.8990 .0010 2 4 1
a= 13.29 b= 8.839 c= 4.873 beta= 96.35
da=.03 db=.005 dc=.0004 dbeta=.08
V= 568.8
Triklin
Dexp Dcal d(D) h k l
4.3900 4.3933 -.0033 0 1 1
4.1900 4.1882 .0018 0 -1 1
3.7100 3.7107 -.0007 1 1 0
3.4200 3.4165 .0035 -1 1 0
3.3100 3.3102 -.0002 1 2 0
3.0200 3.0196 .0004 1 2 1
2.9200 2.9191 .0009 -1 2 0
2.2200 2.2200 -.0000 -1 -3 1
2.0800 2.0804 -.0004 -1 4 0
2.0300 2.0299 .0001 0 5 1
1.9700 1.9700 .0000 -1 -4 1
1.9000 1.9001 -.0001 2 1 1
A= 3.87781 DA= .00005
B= 11.069 DB= .003
C= 4.776 DC= .001
GAMMA= 81.37 DGAMMA= .02
BETA = 78.03 DBETA = .01
ALPHA= 84.55 DALPHA= .02
V= 197.8
26. 30-0774
ksi-LiV15O35.5
Triklin
Dexp Dcal d(D) h k l
13.7000 13.7000 .0000 -1 1 0
10.5000 10.5000 .0000 1 1 0
7.2000 7.2000 .0000 -1 -1 1
6.5000 6.5000 .0000 0 -2 1
5.0000 5.0000 .0000 -2 -2 1
4.5000 4.5000 .0000 -2 4 0
3.7200 3.7189 .0011 -2 5 0
3.4700 3.4717 -.0017 -3 1 2
3.4300 3.4327 -.0027 2 -5 1
3.0900 3.0917 -.0017 1 2 2
3.0200 3.0188 .0012 2 5 0
2.7400 2.7400 .0000 -5 5 0
A= 16.27498 DA= .00000
B= 19.18178 DB= .00002
C= 8.02360 DC= .00000
GAMMA=103.44930 DGAMMA= .00001
BETA =101.82770 DBETA = .00001
ALPHA= 96.79557 DALPHA= .00001
V= 2348.1
27. 30-0802
MgV2O6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.0800 6.0806 -.0006 0 1 0
5.0300 5.0309 -.0009 1 0 2
4.1600 4.1605 -.0005 -1 0 2
3.1200 3.1182 .0018 4 1 1
3.0400 3.0403 -.0003 0 2 0
2.5400 2.5401 -.0001 3 2 0
2.3300 2.3314 -.0014 4 2 1
2.1600 2.1604 -.0004 6 1 0
2.0800 2.0802 -.0002 -2 0 4
1.9400 1.9391 .0009 2 3 1
1.7400 1.7401 -.0001 8 1 2
1.6600 1.6598 .0002 7 2 0
1.5200 1.5202 -.0002 0 4 0
1.4300 1.4300 .0000 2 0 7
a= 14.56 b= 6.0806 c= 10.07 beta= 72.3
da=.03 db=.0001 dc=.01 dbeta=.1
V= 849.3
28. 30-0948
K2Mg2V10O28
Triklin
Dexp Dcal d(D) h k l
9.5100 9.4928 .0172 1 0 0
6.7800 6.7965 -.0165 -1 1 0
6.2400 6.2383 .0017 -1 0 1
5.6800 5.6779 .0021 0 1 1
5.4200 5.4198 .0002 0 0 2
4.7300 4.7302 -.0002 0 -1 2
4.3000 4.3002 -.0002 2 0 2
3.9200 3.9201 -.0001 -2 0 1
3.8000 3.7984 .0016 -1 2 0
3.6700 3.6706 -.0006 0 2 0
3.5200 3.5199 .0001 3 -1 1
3.3000 3.3002 -.0002 -1 2 1
A= 10.6702 DA= .0004
B= 7.935 DB= .004
C= 11.848 DC= .008
GAMMA=110.49 DGAMMA= .02
BETA = 67.887 DBETA = .006
ALPHA=105.57 DALPHA= .03
V=860.3
29. 30-0986
KNaV2O6
Triklin
Dexp Dcal d(D) h k l
3.7100 3.7044 .0056 1 2 0
3.5700 3.5732 -.0032 0 1 2
3.2600 3.2603 -.0003 0 -1 2
3.2100 3.2075 .0025 1 0 2
3.1000 3.0980 .0020 1 1 2
2.8500 2.8507 -.0007 -1 -1 2
2.7880 2.7895 -.0015 1 3 0
2.7480 2.7470 .0010 0 -2 2
2.5440 2.5434 .0006 -2 3 0
2.4670 2.4703 -.0033 2 0 2
2.4520 2.4522 -.0002 0 4 1
2.4060 2.4072 -.0012 2 -1 2
A= 6.711 DA= .006
B= 10.126 DB= .001
C= 7.328 DC= .006
GAMMA= 98.79 DGAMMA= .09
BETA = 90.19 DBETA = .07
ALPHA= 81.94 DALPHA= .01
V=487.2
30. 30-0987
Na3K{VO3}4
GRUPA 3
Dexp. Dcal. d(D) h k l
5.0600 5.0428 .0172 1 1 0
4.9000 4.9143 -.0143 0 0 2
3.6900 3.6933 -.0033 0 3 0
3.5300 3.5333 -.0033 -1 0 2
3.2700 3.2762 -.0062 0 0 3
3.2000 3.2000 -.0000 1 2 2
3.1400 3.1417 -.0017 0 1 3
2.8200 2.8200 .0000 0 2 3
2.8000 2.8000 .0000 2 0 1
2.7700 2.7700 .0000 0 4 0
a= 5.695 b= 11.08000 c= 9.88 beta= 83.99
da=.005 db=.000046 dc=.01 dbet= .01
V=619.7
Triklin
Dexp Dcal d(D) h k l
5.0600 5.0566 .0034 1 0 0
4.9000 4.9034 -.0034 0 1 1
3.6900 3.6893 .0007 0 -1 1
3.5300 3.5292 .0008 1 2 1
3.2700 3.2699 .0001 0 2 1
3.2000 3.2003 -.0003 1 -1 1
3.1400 3.1400 -.0000 -1 0 1
2.8200 2.8204 -.0004 1 2 2
2.8000 2.8004 -.0004 -1 -1 1
2.7700 2.7696 .0004 0 1 2
A= 5.821 DA= .001
B= 7.411 DB= .002
C= 6.282 DC= .002
GAMMA= 69.30 DGAMMA= .02
BETA = 62.68 DBETA = .01
ALPHA= 66.56 DALPHA= .02
V= 216.00
31. 30-0988
NaK{VO3}4*H2O
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
7.8000 7.7822 .0178 0 1 0
7.1500 7.1433 .0067 1 1 0
6.0000 6.0008 -.0008 3 0 0
4.7800 4.7521 .0279 3 1 0
3.8100 3.8033 .0067 1 2 0
3.5800 3.5716 .0084 2 2 0
3.4200 3.4124 .0076 2 1 1
2.1400 2.1419 -.0019 2 3 1
3.0000 3.0004 -.0004 6 0 0
2.0000 2.0003 -.0003 9 0 0
a=18.00 b= 7.78 c= 4.19
da= .02 db= .01 dc= .01
v= 587
32. 30-1009
K2V2Mo3O15
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.6100 3.6146 -.0046 4 1 0
3.2500 3.2437 .0063 1 1 1
3.2300 3.2437 -.0137 1 1 1
3.0200 3.0185 .0015 1 2 0
2.6430 2.6426 .0004 5 0 1
2.5310 2.5277 .0033 4 2 0
2.3590 2.3609 -.0019 7 1 0
2.2110 2.2132 -.0022 6 1 1
2.0230 2.0216 .0014 7 1 1
1.9460 1.9456 .0004 1 0 2
1.8930 1.8926 .0004 9 1 0
1.7910 1.7910 -.0000 10 0 0
1.5310 1.5311 -.0001 0 4 0
a=17.910 b= 6.125 c= 3.914
da= .006 db= .003 dc= .003
V=429.4
33. 30-1011
K2V8O6
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
9.5000 9.4755 .0245 1 0 1
4.7300 4.7378 -.0078 2 0 2
4.5900 4.5796 .0104 0 0 4
3.5300 3.5287 .0013 2 0 4
3.4000 3.4008 -.0008 1 1 0
3.1600 3.1585 .0015 3 0 3
3.0000 3.0024 -.0024 2 1 0
2.8700 2.8736 -.0036 3 0 4
2.6500 2.6496 .0004 4 0 2
2.5600 2.5582 .0018 0 1 5
2.3700 2.3689 .0011 4 0 4
1.9100 1.9104 -.0004 2 0 9
a=11.072 b= 3.5736 c=18.32
da= .009 db= .0008 dc= .02
v= 725
34. 30-1012
K3{VO4}
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
5.2900 5.3016 -.0116 1 0 2
4.5400 4.5356 .0044 2 0 2
3.7600 3.7707 -.0107 3 0 2
3.5600 3.5589 .0011 0 1 1
3.2200 3.2219 -.0019 2 1 1
3.1200 3.1253 -.0053 0 1 2
2.8300 2.8292 .0008 0 0 4
2.2400 2.2386 .0014 1 0 5
1.8800 1.8793 .0007 7 0 3
1.8300 1.8304 -.0004 2 0 6
1.7200 1.7205 -.0005 7 0 4
a=15.177 b= 3.749 c=11.317
da= .005 db= .003 dc= .003
V=644.1
35. 30-1097
gamma-RbV4O10.26
Triklin
Dexp Dcal d(D) h k l
5.6000 5.5853 .0147 0 1 1
5.3000 5.3006 -.0006 0 -1 1
4.9000 4.9066 -.0066 1 0 1
4.2000 4.2007 -.0007 1 1 1
3.6800 3.6833 -.0033 0 0 2
3.4000 3.4009 -.0009 -2 -1 1
3.0600 3.0613 -.0013 -2 0 2
3.0100 3.0129 -.0029 2 -1 1
2.8700 2.8668 .0032 1 -1 2
2.7700 2.7701 -.0001 2 2 0
2.7000 2.6993 .0007 -3 0 1
2.6500 2.6503 -.0003 0 -2 2
A= 8.200 DA= .002
B= 8.086 DB= .006
C= 7.5649 DC= .0001
GAMMA= 93.53 DGAMMA= .02
BETA =102.81 DBETA = .01
ALPHA= 86.30 DALPHA= .02
V=489.1
36. 30-1098
RbV6O15
Monok
Grupa 3
Dexp Dcal d(D) h k l
4.1000 4.1016 -.0016 -1 1 1
3.3500 3.3505 -.0005 3 0 0
3.0800 3.0807 -.0007 -3 0 2
2.8300 2.8304 -.0004 -2 1 3
2.6700 2.6688 .0012 3 1 1
2.4900 2.4897 .0003 -4 0 1
2.3700 2.3713 -.0013 -1 0 6
2.3200 2.3203 -.0003 0 2 1
2.2100 2.2096 .0004 -3 1 4
2.0200 2.0194 .0006 1 0 7
1.9600 1.9590 .0010 -2 2 3
1.8760 1.8756 .0004 -1 1 7
a=10.057 b=4.7011 c=14.534 beta= 91.86
da=.002 db=.0009 dc=.005 dbeta=.03
V= 686.7
Triklin
Dexp Dcal d(D) h k l
4.1000 4.1002 -.0002 -1 1 0
3.3500 3.3500 -.0000 -1 -1 2
3.0800 3.0800 -.0000 -2 1 0
2.8300 2.8298 .0002 -2 0 2
2.6700 2.6703 -.0003 -2 -1 2
2.4900 2.4919 -.0019 2 -1 4
2.3700 2.3701 -.0001 -3 1 0
2.3200 2.3181 .0019 -1 2 0
2.2100 2.2093 .0007 1 0 5
2.0200 2.0183 .0017 3 2 0
1.9600 1.9601 -.0001 1 2 3
1.8760 1.8754 .0006 0 2 3
A= 9.388 DA= .001
B= 5.0699 DB= .0003
C= 11.272 DC= .001
GAMMA= 85.999 DGAMMA= .002
BETA = 68.430 DBETA = .008
ALPHA= 97.482 DALPHA= .007
V= 490.6
37. 30-1099
RbV6O14*4H2O
rombik
Grupa 16
Dexp. Dcal. d(D) h k l
3.5600 3.5636 -.0036 3 0 3
3.4500 3.4492 .0008 4 0 0
3.2200 3.2193 .0007 0 1 0
3.1100 3.1126 -.0026 3 0 4
2.7900 2.7956 -.0056 0 1 3
2.4800 2.4784 .0016 5 0 3
2.2100 2.2091 .0009 2 1 5
2.1300 2.1292 .0008 6 0 3
2.0900 2.0896 .0004 1 0 8
1.9700 1.9710 -.0010 7 0 0
1.8590 1.8598 -.0008 6 1 1
1.7250 1.7246 .0004 8 0 0
a=13.7969 b= 3.219 c=16.912
da= .0007 db= .001 dc= .001
V= 751.2
Triklin
Dexp Dcal d(D) h k l
3.5600 3.5605 -.0005 0 1 1
3.4500 3.4500 -.0000 1 1 1
3.2200 3.2200 .0000 -1 -1 1
3.1100 3.1110 -.0010 2 1 0
2.7900 2.7907 -.0007 2 1 1
2.4800 2.4804 -.0004 0 1 2
2.2100 2.2095 .0005 2 -1 1
2.1300 2.1297 .0003 -3 -1 1
2.0900 2.0910 -.0010 1 2 1
1.9700 1.9702 -.0002 2 2 1
1.8590 1.8593 -.0003 -1 0 3
1.7250 1.7250 .0000 2 2 2
A= 7.342 DA= .005
B= 4.3700 DB= .0007
C= 5.7676 DC= .0001
GAMMA= 76.52 DGAMMA= .01
BETA = 90.009 DBETA = .008
ALPHA= 85.108 DALPHA= .006
V= 179.2
38. 30-1255
NaUV3O10
Triklin
Dexp Dcal d(D) h k l
5.9200 5.9211 -.0011 0 1 1
5.6200 5.6145 .0055 1 0 0
5.4000 5.3958 .0042 0 -1 1
3.6000 3.5961 .0039 -1 -1 1
3.4100 3.4091 .0009 1 1 1
3.2200 3.2209 -.0009 -1 0 3
2.9910 2.9926 -.0016 -2 1 0
2.9500 2.9464 .0036 -2 1 2
2.7060 2.7092 -.0032 -2 0 2
2.4270 2.4272 -.0002 -2 0 3
2.2550 2.2563 -.0013 0 3 0
2.2140 2.2139 .0001 -2 3 2
A= 6.215 DA= .002
B= 7.3660 DB= .0003
C= 10.623 DC= .001
GAMMA=112.547 DGAMMA= .003
BETA =105.17 DBETA = .01
ALPHA= 79.0582 DALPHA= .0001
V= 431.3
Ñì. òàêæå "Ñîåäèíåíèÿ U"
30-1256
Cì." Ñîåäèíåíèÿ U "
39. 30-1259
NaVO3
Triklin
Dexp Dcal d(D) h k l
6.8900 6.8868 .0032 0 1 0
4.9300 4.9279 .0021 0 -1 2
4.7100 4.7058 .0042 1 1 1
3.6200 3.6180 .0020 0 -1 3
3.4300 3.4287 .0013 1 0 3
3.2700 3.2678 .0022 1 -1 3
3.1600 3.1602 -.0002 2 0 2
2.8500 2.8497 .0003 2 -1 2
2.7900 2.7900 .0000 -2 0 2
2.6700 2.6702 -.0002 1 0 4
2.2900 2.2901 -.0001 -2 -2 3
2.1400 2.1400 -.0000 0 3 1
A= 7.1956 DA= .0005
B= 7.210 DB= .002
C= 11.3348 DC= .0006
GAMMA= 80.88 DGAMMA= .01
BETA = 84.639 DBETA = .007
ALPHA=103.54 DALPHA= .03
V= 559.2
40. 30-1260
beta-NaVO3
Triklin
Dexp Dcal d(D) h k l
7.1000 7.0995 .0005 1 0 0
5.0500 5.0500 .0000 0 1 1
3.5500 3.5497 .0003 2 0 0
3.2400 3.2398 .0002 1 2 1
3.0200 3.0193 .0007 1 -1 1
2.9700 2.9689 .0011 -1 2 0
2.5300 2.5297 .0003 -2 1 2
2.3300 2.3293 .0007 1 -2 1
2.2600 2.2609 -.0009 -1 3 1
1.9700 1.9700 .0000 -4 -1 1
1.8900 1.8900 -.0000 2 0 2
1.8300 1.8298 .0002 -3 2 2
A= 7.8825 DA= .0001
B= 8.045 DB= .002
C= 6.0157 DC= .0004
GAMMA= 74.630 DGAMMA= .007
BETA =108.10 DBETA = .01
ALPHA= 83.219 DALPHA= .009
V= 341.2
30-1261
Ñì. ñîåäèíåíèÿ U
41. 30-1313
SrV2O6
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
3.6300 3.6321 -.0021 -1 1 1
3.3100 3.3126 -.0026 0 1 2
3.0500 3.0536 -.0036 -1 0 3
2.3520 2.3554 -.0034 0 0 4
2.1870 2.1871 -.0001 1 2 0
2.0870 2.0882 -.0012 0 2 2
1.9010 1.9023 -.0013 1 1 4
1.8830 1.8830 .0000 -2 2 1
1.8280 1.8280 .0000 3 1 1
1.8080 1.8080 .0000 3 0 2
a= 6.4692 b=4.6591 c=9.59 beta= 100.88
da=.0001 db=.0001 dc=.03 dbet=.08
V=283.5
42. 30-1315
Sr2V2O7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.4600 3.4608 -.0008 2 1 0
3.1800 3.1798 .0002 -1 0 3
2.9860 2.9845 .0015 2 0 2
2.8380 2.8389 -.0009 3 0 0
2.7280 2.7296 -.0016 -1 2 1
2.5190 2.5177 .0013 -2 1 3
2.3780 2.3765 .0015 1 2 2
2.2410 2.2420 -.0010 0 1 4
2.1300 2.1292 .0008 4 0 0
2.0040 2.0043 -.0003 4 1 0
a= .008 b= 5.939 c= 9.794 beta= 98.57
da=.001 db=.002 dc=.003 dbeta=.06
V= 495.4
43. 30-1324
beta-TlGaV2O8
Triklin
Dexp Dcal d(D) h k l
5.1600 5.1617 -.0017 -1 1 1
3.9400 3.9411 -.0011 0 -1 1
3.8400 3.8382 .0018 1 -1 1
3.6500 3.6491 .0009 0 0 2
3.5100 3.5094 .0006 -2 0 1
3.1700 3.1741 -.0041 0 2 1
3.0100 3.0097 .0003 -1 2 0
2.8700 2.8677 .0023 0 2 2
2.8100 2.8104 -.0004 2 0 2
2.5700 2.5699 .0001 1 2 2
2.5200 2.5207 -.0007 -1 1 3
2.4600 2.4600 -.0000 1 1 3
A= 8.478 DA= .001
B= 6.520 DB= .003
C= 7.848 DC= .002
GAMMA=102.99 DGAMMA= .04
BETA = 91.85 DBETA = .01
ALPHA= 68.65 DALPHA= .02
V= 393.1
44. 30-1327
alfa-TlInV2O8
Triklin
Dexp Dcal d(D) h k l
4.7400 4.7407 -.0007 1 0 0
4.2300 4.2278 .0022 -1 1 0
3.8600 3.8597 .0003 -1 1 1
3.5500 3.5500 .0000 1 1 0
2.8600 2.8600 .0000 1 1 2
2.8500 2.8501 -.0001 1 -1 2
2.6800 2.6799 .0001 0 1 3
2.5500 2.5501 -.0001 -1 2 2
2.3800 2.3800 .0000 0 -2 2
2.2700 2.2700 .0000 2 -1 1
A= 4.8221 DA= .0004
B= 6.7685 DB= .0004
C= 8.2992 DC= .0003
GAMMA=100.231 DGAMMA= .008
BETA = 89.10 DBETA = .01
ALPHA= 80.934 DALPHA= .001
V= 262.97
45. 30-1328
beta-TlInV2O8
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.2200 4.2280 -.0080 1 0 0
3.9800 3.9785 .0015 0 2 0
3.8800 3.8609 .0191 1 0 1
2.9300 2.9350 -.0050 0 1 3
2.9300 2.9322 -.0022 1 1 2
2.5500 2.5541 -.0041 0 3 1
2.0000 1.9999 .0001 1 1 4
2.0000 1.9972 .0028 2 1 1
a= 4.228 b= 7.957 c= 9.473
da= .001 db= .001 dc= .001
V= 318.7
46. 30-1329
gamma-TlInV2O8
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.6800 4.6822 -.0022 1 1 0
4.2400 4.2401 -.0001 0 0 3
3.3200 3.3217 -.0017 0 2 1
3.1400 3.1429 -.0029 1 1 3
3.0300 3.0296 .0004 1 2 0
2.9000 2.8974 .0026 2 1 0
2.8900 2.8868 .0032 0 1 4
2.5500 2.5513 -.0013 2 0 3
2.1200 2.1201 -.0001 0 0 6
a= 6.3886 b= 6.882 c=12.720
da= .0003 db= .002 dc= .001
v= 559.3
47. 30-1334
TlV3O9
Triklin
Dexp Dcal d(D) h k l
4.2700 4.2675 .0025 -1 0 1
3.9600 3.9620 -.0020 1 -2 1
3.9000 3.9009 -.0009 -1 -1 1
3.6700 3.6687 .0013 2 -2 1
3.5600 3.5605 -.0005 -3 2 0
3.1800 3.1807 -.0007 -1 -2 1
3.0600 3.0601 -.0001 0 2 1
2.9000 2.8994 .0006 0 -3 1
2.8800 2.8776 .0024 3 1 0
2.5800 2.5803 -.0003 4 0 0
2.4600 2.4590 .0010 4 -3 1
2.3600 2.3601 -.0001 1 -2 2
A= 11.3820 DA= .0005
B= 10.6421 DB= .0003
C= 4.85314 DC= .00002
GAMMA=114.92 DGAMMA= .02
BETA = 83.59 DBETA = .02
ALPHA=102.8990 DALPHA= .0001
V=520.7
48. 30-1335
Tl2V6O16
Triklin
Dexp Dcal d(D) h k l
7.5800 7.5832 -.0032 1 1 0
6.7800 6.7790 .0010 0 1 1
5.3200 5.3195 .0005 0 -1 1
4.9800 4.9801 -.0001 -1 -1 1
4.1500 4.1494 .0006 -2 -1 1
3.9600 3.9614 -.0014 2 -1 1
3.7800 3.7813 -.0013 -1 0 2
3.6600 3.6596 .0004 -3 0 1
3.5000 3.5012 -.0012 2 1 2
3.4100 3.4085 .0015 2 0 2
3.3600 3.3591 .0009 -3 -1 1
3.1900 3.1898 .0002 -1 2 2
A= 12.597 DA= .001
B= 9.122 DB= .003
C= 8.247 DC= .00211
GAMMA= 83.41 DGAMMA= .01
BETA = 87.01 DBETA = .01
ALPHA= 75.94 DALPHA= .02
V= 914.9
49. 30-1336
Tl2V8O23
Triklin
Dexp Dcal d(D) h k l
5.3500 5.3411 .0089 -1 1 0
4.9700 4.9538 .0162 0 1 1
4.1600 4.1709 -.0109 0 -1 1
3.6600 3.6685 -.0085 -2 0 1
3.5100 3.5101 -.0001 2 0 1
3.4200 3.4180 .0020 -1 0 2
3.3700 3.3699 .0001 0 1 2
3.1700 3.1703 -.0003 2 -1 1
3.0100 3.0105 -.0005 2 1 0
2.9300 2.9306 -.0006 -1 2 0
2.8700 2.8686 .0014 0 -1 2
2.7800 2.7794 .0006 1 -1 2
A= 8.51538 DA= .00009
B= 6.0104 DB= .0008
C= 7.493 DC= .001
GAMMA=104.82 DGAMMA= .03
BETA = 95.67 DBETA = .02
ALPHA= 78.805 DALPHA= .005
V=364.4
50. 30-1337
Tl3VO4
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
5.0500 5.0583 .0083 0 1 0
3.8100 3.8166 .0066 2 1 0
3.3900 3.3849 -.0051 0 1 2
3.0400 3.0368 -.0032 0 0 3
2.9400 2.9383 -.0017 1 0 3
2.5500 2.5499 -.0001 3 1 2
2.3300 2.3262 -.0038 5 0 0
2.1200 2.1207 .0007 2 0 4
2.1200 2.1183 -.0017 3 2 0
1.9400 1.9397 -.0003 4 1 3
1.9400 1.9385 -.0015 6 0 0
1.8000 1.8001 .0001 1 0 5
a= 11.631210 b=5.06 c=9.110
da=.009 db=.01 dc=.002
V= 536.0
Triklin
Dexp Dcal d(D) h k l
5.0500 5.0521 -.0021 0 0 1
3.8100 3.8103 -.0003 0 -2 1
3.3900 3.3898 .0002 -1 -1 1
3.0400 3.0403 -.0003 2 -2 1
2.9400 2.9400 .0000 1 -3 1
2.5500 2.5499 .0001 2 -3 1
2.3300 2.3300 -.0000 2 0 2
2.1200 2.1200 .0000 -2 -2 1
1.9400 1.9400 .0000 0 2 2
1.8000 1.8000 .0000 2 -1 3
A= 6.935 DA= .001
B= 9.094 DB= .001
C= 5.6027 DC= .0001
GAMMA=104.67 DGAMMA= .01
BETA = 70.025 DBETA = .002
ALPHA=110.049 DALPHA= .008
V= 308.2
51. 30-1418
VCl3*6H2O
Triklin
Dexp Dcal d(D) h k l
6.3700 6.3761 -.0061 0 1 1
5.9100 5.9220 -.0120 1 1 0
5.6400 5.6391 .0009 0 -1 1
4.6800 4.6840 -.0040 0 3 1
4.4000 4.4009 -.0009 -1 2 1
4.0900 4.0868 .0032 -1 -1 1
3.3500 3.3501 -.0001 1 4 0
3.2200 3.2182 .0018 1 4 1
3.1100 3.1092 .0008 -2 3 0
2.9830 2.9833 -.0003 2 1 1
2.8340 2.8342 -.0002 -2 3 1
2.7010 2.7012 -.0002 2 3 0
A= 6.800 DA= .001
B= 17.447 DB= .002
C= 6.5020 DC= .0006
GAMMA= 98.562 DGAMMA= .008
BETA = 87.46 DBETA = .02
ALPHA= 79.84 DALPHA= .01
V= 748.8
52. 30-1419
VH{SO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
7.0100 6.9755 .0345 0 1 1
5.4600 5.4795 -.0195 -1 0 1
4.8800 4.8732 .0068 0 -1 1
4.7300 4.7274 .0026 -1 1 1
4.4800 4.4784 .0016 0 0 2
4.0000 3.9986 .0014 1 -1 1
3.7000 3.6950 .0050 -1 1 2
3.6400 3.6403 -.0003 0 2 0
3.4900 3.4877 .0023 0 2 2
3.4400 3.4392 .0008 2 0 1
3.3200 3.3205 -.0005 1 2 2
3.2600 3.2631 -.0031 -1 2 1
A= 7.327 DA= .003
B= 7.831 DB= .005
C= 9.614 DC= .007
GAMMA= 83.24 DGAMMA= .07
BETA = 84.32 DBETA = .05
ALPHA= 68.97 DALPHA= .02
V= 510.4
53. 30-1431
gamma-VOSO4
triklin
Dexp Dcal d(D) h k l
10.1000 10.1010 -.0010 1 0 0
6.7500 6.7488 .0012 1 1 0
6.5900 6.5928 -.0028 -1 0 1
5.9600 5.9569 .0031 -1 1 0
5.0900 5.0877 .0023 -1 1 1
4.7300 4.7355 -.0055 0 0 2
4.3600 4.3633 -.0033 2 1 1
4.1900 4.1913 -.0013 1 1 2
4.1300 4.1341 -.0041 -1 0 2
3.9100 3.9112 -.0012 0 -1 2
3.6400 3.6378 .0022 2 0 2
3.5900 3.5869 .0031 0 -2 1
A= 10.25 DA= .01
B= 8.218 DB= .006
C= 9.59 DC= .01
GAMMA= 82.01 DGAMMA= .06
BETA = 83.49 DBETA = .09
ALPHA= 83.13 DALPHA= .08
V= 790.1
54. 30-1494
Zn{Zn0.5V1.5}O4
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
4.8600 4.8545 .0055 2 1 0
3.4800 3.4707 .0093 0 1 1
2.9700 2.9687 .0013 1 2 1
2.8400 2.8370 .0030 1 4 0
2.6300 2.6336 -.0036 3 3 0
2.5400 2.5396 .0004 3 0 1
2.4300 2.4272 .0028 4 2 0
2.3300 2.3319 -.0019 3 2 1
2.1000 2.1014 -.0014 2 4 1
2.1000 2.0973 .0027 5 1 0
1.9300 1.9297 .0003 1 6 0
a=10.657 b=11.773 c= 3.6321
da= .007 db= .003 dc= .0005
v= 455.7