1. 15-0006
NaVO3*1.9H2O
Triklin
Dexp Dcal d(D) h k l
7.8600 7.8501 .0099 1 0 1
7.5300 7.5287 .0013 0 1 0
6.8100 6.8017 .0083 0 1 1
4.1600 4.1539 .0061 0 1 2
3.9300 3.9265 .0035 -1 2 0
3.7600 3.7644 -.0044 0 2 0
3.4000 3.4009 -.0009 0 2 2
3.3200 3.3179 .0021 1 -2 1
3.2900 3.2923 -.0023 1 2 2
3.0000 2.9991 .0009 0 -2 1
2.8800 2.8807 -.0007 3 -1 2
2.8100 2.8098 .0002 0 1 3
A= 9.531 DA= .006
B= 8.204 DB= .004
C= 9.23 DC= .01
GAMMA=100.20 DGAMMA= .05
BETA = 65.97 DBETA = .05
ALPHA= 75.36 DALPHA= .05
V= 604.9
2. 15-0051
NaVO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.8500 6.8608 -.0108 1 1 0
5.0000 5.0055 -.0055 0 1 2
4.7400 4.7447 -.0047 2 0 2
3.6100 3.6080 .0020 0 1 3
3.4400 3.4413 -.0013 3 0 2
3.2600 3.2602 -.0002 3 1 1
3.1800 3.1832 -.0032 -1 0 3
3.1500 3.1487 .0013 0 3 1
2.8500 2.8512 -.0012 0 3 2
2.7900 2.7898 .0002 0 1 4
2.6800 2.6797 .0003 3 2 0
2.5200 2.5199 .0001 -1 0 4
a=10.463 b=9.812 c=12.6903 beta=66.51
da=.004 db=.001 dc=.0002 dbeta=.01
V= 1195
Triklin
Dexp Dcal d(D) h k l
6.8500 6.8491 .0009 1 0 0
5.0000 4.9943 .0057 -1 1 1
4.7400 4.7387 .0013 -1 -1 1
3.6100 3.6070 .0030 -1 2 0
3.4400 3.4370 .0030 -2 1 0
3.2600 3.2610 -.0010 -1 2 1
3.1800 3.1815 -.0015 1 -2 1
3.1500 3.1485 .0015 -2 -1 1
2.8500 2.8479 .0021 0 -2 2
2.7900 2.7924 -.0024 1 -1 2
2.6800 2.6785 .0015 2 0 1
2.5200 2.5192 .0008 -2 0 3
2.4500 2.4515 -.0015 -3 0 2
2.1800 2.1802 -.0002 0 3 1
2.0900 2.0903 -.0003 1 -3 2
A= 7.684 DA= .001
B= 7.5744 DB= .0006
C= 7.9368 DC= .0006
GAMMA=100.36 DGAMMA= .01
BETA =113.28 DBETA = .08
ALPHA= 96.03 DALPHA= .02
V= 409.5
3. 15-102
Zn*Ni*V*O**OH
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
11.6000 11.6518 -.0518 1 0 0
7.1000 7.0954 .0046 1 2 0
5.8300 5.8259 .0041 2 0 0
4.6200 4.6205 -.0005 0 1 1
3.8800 3.8839 -.0039 3 0 0
2.6200 2.6174 .0026 4 3 0
2.5700 2.5710 -.0010 2 5 1
2.3900 2.3914 -.0014 0 0 2
1.9500 1.9496 .0004 3 7 1
1.5400 1.5405 -.0005 6 6 1
1.5200 1.5201 -.0001 7 3 1
1.5000 1.5002 -.0002 3 11 0
1.4700 1.4699 .0001 3 1 3
1.4200 1.4201 -.0001 4 11 0
a=11.652 b=17.8904 c= 4.783
da= .005 db= .0009 dc= .002
V= 997.0
4. 15-0247
V7O17*xH2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.1100 3.1110 -.0010 3 0 0
2.8800 2.8806 -.0006 -2 1 1
2.8200 2.8215 -.0015 3 2 0
2.7200 2.7205 -.0005 2 4 0
2.6600 2.6598 .0002 0 4 1
2.2800 2.2791 .0009 3 4 0
1.7960 1.7959 .0001 2 4 2
1.5590 1.5591 -.0001 5 0 2
1.5270 1.5271 -.0001 -1 8 1
1.4690 1.4689 .0001 6 3 0
1.4060 1.4060 .0000 1 3 3
1.2730 1.2739 -.0009 -2 3 3
1.1640 1.1640 .0000 -5 8 1
a= 9.475 b=13.394 c=4.4447 beta=80.08
da=.002 db=.002 dc=.0002 dbeta=.01
V= 555.6
Triklin
Dexp Dcal d(D) h k l
3.1100 3.1100 .0000 0 1 0
2.8800 2.8790 .0010 0 0 4
2.8200 2.8196 .0004 0 -1 2
2.7200 2.7210 -.0010 -1 -1 1
2.6600 2.6600 -.0000 0 1 2
2.2800 2.2792 .0008 -1 0 3
1.7960 1.7961 -.0001 -1 1 0
1.5590 1.5589 .0001 2 1 2
1.5270 1.5270 .0000 0 2 1
1.4690 1.4690 -.0000 2 0 0
1.4060 1.4060 -.0000 -1 0 7
1.2730 1.2730 .0000 0 1 8
1.1640 1.1640 .0000 1 -1 8
A= 3.2295 DA= .0008
B= 3.4226 DB= .0005
C= 11.5469 DC= .0001
GAMMA= 65.63 DGAMMA= .01
BETA = 88.7003 DBETA = .0006
ALPHA= 93.100 DALPHA= .002
V= 115.9
5. 15-279
Fe6+3KAl3V6+4{V20+5O76}*30H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.2000 10.2001 -.0001 -1 0 1
5.8100 5.8179 -.0079 3 0 0
3.4500 3.4492 .0008 -2 1 1
2.9300 2.9324 -.0024 4 1 0
2.7700 2.7699 .0001 6 0 2
2.6200 2.6186 .0014 5 1 0
2.4900 2.4934 -.0034 7 0 0
2.0800 2.0799 .0001 6 0 5
1.9800 1.9800 .0000 0 2 0
1.9420 1.9416 .0004 2 1 6
1.8280 1.8279 .0001 4 0 7
1.8030 1.8030 -.0000 4 2 0
a=17.54 b=3.9600 c=13.54 beta=84.44
da=.01 db=.0001 dc=.01 dbeta=.05
V= 935.8
Triklin
Dexp Dcal d(D) h k l
10.2000 10.0947 .1053 0 0 1
5.8100 5.8114 -.0014 1 0 1
3.4500 3.4500 -.0000 -2 1 0
2.9300 2.9314 -.0014 2 -1 2
2.7700 2.7700 .0000 1 1 2
2.6200 2.6200 -.0000 0 1 3
2.4900 2.4899 .0001 -2 0 3
2.0800 2.0799 .0001 0 2 2
1.9800 1.9798 .0002 -3 2 1
1.9420 1.9419 .0001 0 -1 5
1.8280 1.8280 -.0000 -1 -1 5
1.8030 1.8030 -.0000 3 -1 4
A= 7.6020 DA= .0001
B= 5.0913 DB= .0004
C= 10.162 DC= .001
GAMMA=108.17 DGAMMA= .03
BETA = 89.22 DBETA = .02
ALPHA= 96.46 DALPHA= .02
V= 371.2
6. 15-0435
Pb5GeV2O12
Triklin
Dexp Dcal d(D) h k l
8.6700 8.6599 .0101 1 1 0
6.3700 6.3757 -.0057 -1 1 0
4.4600 4.4575 .0025 0 2 0
4.3300 4.3299 .0001 2 2 0
4.1300 4.1300 .0000 -1 0 1
3.6800 3.6761 .0039 3 2 0
3.3900 3.3913 -.0013 -3 1 0
3.2900 3.2931 -.0031 4 1 0
3.1900 3.1878 .0022 -2 2 0
3.1300 3.1286 .0014 4 0 0
2.9900 2.9900 .0000 2 -1 1
2.9700 2.9717 -.0017 0 3 0
A= 13.4004 DA= .0001
B= 9.5066 DB= .0001
C= 4.2620 DC= .0001
GAMMA= 70.535 DGAMMA= .001
BETA =100.361 DBETA = .003
ALPHA= 98.965 DALPHA= .001
V= 500.9
7. 15-0455
VO0.53
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.7960 7.8844 -.0981 1 0 0
3.8900 3.8897 .0003 2 1 1
2.2830 2.2839 -.0009 -2 0 2
2.6660 2.6663 -.0003 3 1 2
2.1480 2.1477 .0003 4 0 1
2.0730 2.0729 .0001 1 4 1
2.0190 2.0197 -.0007 -2 2 2
1.8980 1.8975 .0005 0 0 4
1.8030 1.8034 -.0004 -2 0 3
1.7940 1.7937 .0003 4 2 0
1.4700 1.4699 .0001 1 5 3
1.4630 1.4628 .0002 5 3 1
a= 8.7489 b=8.6516 c=8.422 beta=64.31
da=.0006 db=.0004 dc=.003 dbeta=.01
V= 574.5
Triklin
Dexp Dcal d(D) h k l
7.7960 7.7974 -.0014 1 0 0
3.8900 3.8894 .0006 0 1 1
2.2830 2.2829 .0001 -2 -1 1
2.6660 2.6664 -.0004 0 2 0
2.1480 2.1480 .0000 3 0 2
2.0730 2.0729 .0001 -1 -1 2
2.0190 2.0185 .0005 -2 1 2
1.8980 1.8987 -.0007 3 -2 2
1.8030 1.8038 -.0008 0 0 3
1.7940 1.7944 -.0004 2 -3 1
1.4700 1.4696 .0004 -2 -2 2
1.4630 1.4630 .0000 0 -2 3
A= 8.4760 DA= .0004
B= 5.6354 DB= .0004
C= 5.5756 DC= .0008
GAMMA=108.6878 DGAMMA= .0009
BETA = 76.319 DBETA = .001
ALPHA= 91.908 DALPHA= .002
V= 244.8
15-0609
Ca-U-VO4*H2O
Cì. ñîåäèíåíèÿ U.
8. 15-0625
Pb5SiV2O12
Triklin
Dexp. Dcal. d(D) h k l
5.3400 5.3344 .0056 -2 -1 0
4.3100 4.3153 -.0053 1 -2 0
4.1900 4.1856 .0044 -3 -1 0
4.1100 4.1155 -.0055 2 -2 0
3.6600 3.6543 .0057 1 -1 1
3.4700 3.4689 .0011 -2 -2 0
3.3800 3.3787 .0013 -1 -1 1
3.2700 3.2687 .0013 5 -1 0
3.0900 3.0920 -.0020 2 -2 1
3.0400 3.0403 -.0003 0 -2 1
2.9800 2.9802 -.0002 4 -1 1
2.9600 2.9597 .0003 3 -2 1
A= 16.778 DA= .001
B= 8.82068 DB= .00009
C= 3.753 DC= .002
GAMMA=103.22 DGAMMA= .03
BETA = 81.92 DBETA = .08
ALPHA=101.51 DALPHA= .02
V= 527.2
9. 16-0127
ÑuV2O6
Triklin
Dexp Dcal d(D) h k l
4.2600 4.2561 .0039 0 1 0
3.3200 3.3153 .0047 0 -1 2
3.2100 3.2111 -.0011 1 -1 2
3.0300 3.0300 .0000 -1 0 1
3.0100 3.0073 .0027 1 0 2
2.8100 2.8083 .0017 0 0 3
2.6400 2.6389 .0011 1 -1 3
2.3200 2.3208 -.0008 1 -2 1
2.2700 2.2715 -.0015 1 -2 2
2.1400 2.1399 .0001 1 -1 4
2.0100 2.0098 .0002 -1 -1 2
1.7620 1.7629 -.0009 0 1 4
A= 3.92856 DA= .00005
B= 4.7525 DB= .0004
C= 8.9584 DC= .0008
GAMMA=114.340 DGAMMA= .005
BETA = 73.116 DBETA = .006
ALPHA=106.30060 DALPHA= .00005
V= 143.3
10. 16-0132
beta-{Nb,V}2O5
Triklin
Dexp Dcal d(D) h k l
5.0700 5.0740 -.0040 -1 0 1
3.7700 3.7705 -.0005 -1 1 1
3.5600 3.5570 .0030 1 -1 1
3.4000 3.3987 .0013 0 0 2
3.1100 3.1101 -.0001 -2 -2 1
2.9000 2.8993 .0007 -1 2 0
2.7180 2.7183 -.0003 -1 2 1
2.5000 2.5001 -.0001 2 -1 1
2.4430 2.4429 .0001 -3 -1 1
2.3360 2.3360 -.0000 2 2 2
2.1510 2.1512 -.0002 1 -2 2
2.0730 2.0731 -.0001 2 -1 2
A= 7.7054 DA= .0005
B= 8.524 DB= .001
C= 6.820 DC= .001
GAMMA= 65.073 DGAMMA= .003
BETA = 94.476 DBETA = .005
ALPHA= 90.625 DALPHA= .002
V= 404.9
11. 16-0417
Cu2V2O7
Triklin
Dexp Dcal d(D) h k l
5.1300 5.1353 -.0053 -1 0 1
4.9400 4.9386 .0014 0 1 0
4.0900 4.0900 .0000 -1 1 0
3.2500 3.2500 .0000 -2 -1 1
3.1900 3.1909 -.0009 0 1 1
3.0700 3.0710 -.0010 -1 1 1
2.5700 2.5678 .0022 1 -1 2
2.4700 2.4693 .0007 0 2 0
2.2000 2.1997 .0003 -3 -1 2
2.0900 2.0912 -.0012 2 -1 2
2.0500 2.0493 .0007 0 -1 3
1.8560 1.8556 .0004 4 0 0
A= 7.676 DA= .006
B= 5.3545 DB= .0007
C= 6.3581 DC= .0007
GAMMA= 83.77 DGAMMA= .03
BETA =104.768 DBETA = .001
ALPHA=112.73 DALPHA= .01
V= 233.1
12. 16-0418
Cu5V2O10
Triklin
Dexp Dcal d(D) h k l
4.7900 4.7930 -.0030 0 -1 1
3.8300 3.8255 .0045 0 -3 1
3.2300 3.2310 -.0010 1 0 0
3.0900 3.0917 -.0017 -1 2 0
3.0300 3.0277 .0023 1 2 0
2.7900 2.7889 .0011 -1 2 1
2.7600 2.7639 -.0039 0 6 1
2.6900 2.6879 .0021 -1 -2 1
2.6000 2.5994 .0006 1 0 1
2.5400 2.5425 -.0025 -1 -3 1
2.4600 2.4581 .0019 0 7 1
2.4000 2.4004 -.0004 1 -3 1
A= 3.25140 DA= .00009
B= 19.07 DB= .02
C= 5.076 DC= .005
GAMMA= 92.37 DGAMMA= .01
BETA = 96.1201 DBETA = .0008
ALPHA= 86.09 DALPHA= .07
V= 312.1
13. 16-0419
Cu3+2V2O8
Triklin
Dexp Dcal d(D) h k l
5.9500 5.9493 .0007 0 0 1
4.6600 4.6581 .0019 0 -2 1
4.2200 4.2200 .0000 1 -2 1
3.9700 3.9728 -.0028 -1 3 0
3.1300 3.1296 .0004 1 -4 1
3.1000 3.1040 -.0040 -1 -2 1
3.0400 3.0382 .0018 -1 3 1
2.9100 2.9093 .0007 0 -1 2
2.8000 2.7988 .0012 2 0 1
2.7000 2.6998 .0002 2 1 1
2.6200 2.6213 -.0013 2 1 0
2.5600 2.5615 -.0015 0 6 0
A= 5.721 DA= .001
B= 15.4830 DB= .0001
C= 6.221 DC= .001
GAMMA= 96.86 DGAMMA= .04
BETA = 73.05 DBETA = .06
ALPHA= 90.88 DALPHA= .01
V= 523.2
14. 16-0609
NaAl8V10O38*30H2O
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7970 .0030 1 0 0
6.7000 6.6997 .0003 0 1 1
5.4500 5.4429 .0071 0 -1 1
4.9400 4.9421 -.0021 0 2 1
4.1400 4.1410 -.0010 -2 0 1
3.7800 3.7815 -.0015 -2 1 1
3.3200 3.3223 -.0023 -2 0 2
2.9500 2.9503 -.0003 -1 -2 2
2.6500 2.6505 -.0005 3 1 0
2.4800 2.4795 .0005 -2 0 3
2.2670 2.2672 -.0002 0 5 1
2.2120 2.2125 -.0005 0 -1 3
A= 8.491 DA= .001
B= 11.47315 DB= .00005
C= 7.7684 DC= .0007
GAMMA= 82.748 DGAMMA= .001
BETA =110.442 DBETA = .006
ALPHA= 80.474 DALPHA= .004
V= 685.3
15. 17-307
FeVC4
Triklin
Dexp Dcal d(D) h k l
3.4800 3.4784 .0016 0 4 0
2.8300 2.8298 .0002 -1 5 0
2.7700 2.7681 .0019 3 0 0
2.4200 2.4206 -.0006 2 4 0
2.4000 2.3995 .0005 3 2 0
2.2420 2.2421 -.0001 -2 6 0
2.1190 2.1192 -.0002 -4 2 0
1.9910 1.9913 -.0003 4 1 0
1.9150 1.9150 .0000 0 0 2
1.8230 1.8230 -.0000 4 -1 1
1.7410 1.7410 -.0000 -2 2 2
1.7040 1.7040 .0000 0 -4 2
A= 8.51340 DA= .00008
B= 14.258 DB= .005
C= 3.8356 DC= .0002
GAMMA=102.449 DGAMMA= .003
BETA = 92.3248 DBETA = .0002
ALPHA= 91.545 DALPHA= .008
V= 454.15
16. 17-585
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.4000 6.3930 .0070 0 0 4
3.7100 3.7119 -.0019 1 1 0
3.7100 3.7067 .0033 -1 1 1
3.6400 3.6409 -.0009 1 1 1
3.2000 3.1965 .0035 0 0 8
3.0700 3.0693 .0007 -3 0 1
3.0100 3.0094 .0006 -3 0 3
2.8900 2.8908 -.0008 -1 1 6
2.8300 2.8296 .0004 -2 0 8
2.7300 2.7286 .0014 3 0 3
2.5900 2.5906 -.0006 3 0 4
2.4200 2.4188 .0012 -3 1 3
2.3400 2.3408 -.0008 -1 0 11
a= 9.21405 b=4.065 c= 25.883 beta= 98.885
da=.0003 db=.002 dc=.008 dbeta= .009
V= 957.8
Triklin
Dexp Dcal d(D) h k l
6.4000 6.3974 .0026 -1 1 0
3.7100 3.7107 -.0007 0 2 0
3.6400 3.6429 -.0029 2 2 0
3.2000 3.1987 .0013 -2 2 0
3.0700 3.0726 -.0026 4 2 0
3.0100 3.0114 -.0014 1 1 1
2.8900 2.8898 .0002 -2 0 1
2.8300 2.8253 .0047 6 0 0
2.7300 2.7303 -.0003 1 -1 1
2.5900 2.5922 -.0022 4 1 1
2.4200 2.4217 -.0017 7 0 0
2.3400 2.3379 .0021 4 2 1
A= 17.259 DA= .008
B= 7.590 DB= .002
C= 3.1508 DC= .0001
GAMMA= 79.51 DGAMMA= .02
BETA = 86.19 DBETA = .03
ALPHA= 83.34 DALPHA= .02
V= 402.7
17. 18-0040
{Ti,Al8,Mo,V}
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
2.5500 2.5528 -.0028 0 2 0
2.4800 2.4802 -.0002 -1 1 3
2.3600 2.3589 .0011 2 1 0
2.3010 2.3015 -.0005 1 2 0
2.2400 2.2399 .0001 0 0 4
2.1940 2.1944 -.0004 2 1 1
1.7200 1.7193 .0007 2 1 3
1.7000 1.6991 .0009 -1 1 5
1.4700 1.4701 -.0001 -3 1 4
1.4500 1.4500 .0000 -1 1 6
1.3300 1.3299 .0001 4 0 0
1.3000 1.3002 -.0002 -4 1 2
a= 5.413 b=5.106 c=9.117 beta= 100.636
da=.001 db=.004 dc=.003 dbeta=.004
V= 247.6
Dexp Dcal d(D) h k l
2.5500 2.5490 .0010 0 1 1
2.4800 2.4799 .0001 1 1 1
2.3600 2.3606 -.0006 0 -1 1
2.3010 2.2989 .0021 0 2 0
2.2400 2.2401 -.0001 1 -1 1
2.1940 2.1949 -.0009 2 1 1
1.7200 1.7211 -.0011 -3 -1 1
1.7000 1.7015 -.0015 -3 1 1
1.4700 1.4699 .0001 -4 -1 1
1.4500 1.4501 -.0001 -3 -2 1
1.3300 1.3297 .0003 -2 0 2
1.3000 1.2996 .0004 -5 0 1
A= 7.469 DA= .001
B= 4.6373 DB= .0002
C= 2.90841 DC= .00016
GAMMA= 84.326 DGAMMA= .007
BETA = 87.13 DBETA = .02
ALPHA= 84.878 DALPHA= .009
V= 99.7
18. 18-0041
{Ti,Al8,Mo,V}
Triklin
Dexp Dcal d(D) h k l
2.6400 2.6403 -.0003 1 0 0
2.3300 2.3303 -.0003 0 1 1
2.2190 2.2191 -.0001 -1 0 1
1.7100 1.7106 -.0006 -1 0 2
1.4600 1.4600 -.0000 2 1 0
1.3300 1.3297 .0003 0 2 1
1.2660 1.2658 .0002 -1 1 2
1.2370 1.2370 -.0000 -2 0 1
1.2200 1.2199 .0001 0 -2 3
1.1650 1.1651 -.0001 0 2 2
1.1130 1.1131 -.0001 1 -2 1
1.0610 1.0609 .0001 2 -1 1
A= 2.92615 DA= .00004
B= 3.2527 DB= .0002
C= 5.1330 DC= .0009
GAMMA= 65.56884 DGAMMA= .00007
BETA = 86.69 DBETA = .01
ALPHA= 98.655 DALPHA= .007
V= 43.6
19. 18-0074
AlVO4
Triklin
Dexp Dcal d(D) h k l
8.5800 8.5741 .0059 1 0 0
6.2100 6.2153 -.0053 0 1 1
6.0500 6.0653 -.0153 0 -1 1
5.7600 5.7693 -.0093 -1 -1 1
5.2000 5.1925 .0075 -1 0 2
4.9400 4.9449 -.0049 -1 1 1
4.3300 4.3322 -.0022 -2 0 1
4.2900 4.2870 .0030 2 0 0
3.7300 3.7281 .0019 2 0 1
3.6800 3.6799 .0001 0 0 3
3.6600 3.6571 .0029 1 2 0
3.5900 3.5926 -.0026 2 1 1
A= 8.95667 DA= .00005
B= 7.528 DB= .001
C= 11.3209 DC= .0007
GAMMA= 78.98 DGAMMA= .01
BETA =102.72 DBETA = .01
ALPHA= 90.968 DALPHA= .006
V= 730.5
20. 18-138
VCxOz
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
2.3870 2.3870 .0000 0 0 1
2.0700 2.0689 .0011 1 2 0
1.4640 1.4641 -.0001 1 4 0
1.2490 1.2488 .0002 1 5 0
1.1940 1.1939 .0001 2 2 0
a= 2.532 b= 7.178 c= 2.387
da= .001 db= .001 dc= .001
v= 43.38
21. 18-0463
ýòà-{Cu0.95V2O5}
Triklin
Dexp Dcal d(D) h k l
8.3000 8.3014 -.0014 1 0 0
5.5900 5.5914 -.0014 -1 1 1
4.1000 4.0996 .0004 -1 -1 1
3.9300 3.9328 -.0028 2 0 1
3.4800 3.4796 .0004 -1 2 1
3.3500 3.3505 -.0005 -1 2 0
2.8370 2.8358 .0012 0 -1 3
2.7690 2.7671 .0019 3 0 0
2.7220 2.7198 .0022 -3 1 0
2.5830 2.5833 -.0003 1 0 4
2.5260 2.5262 -.0002 2 2 1
2.5060 2.5066 -.0006 3 0 2
A= 8.409 DA= .002
B= 7.2350 DB= .0008
C= 11.21 DC= .01
GAMMA= 98.78 DGAMMA= .02
BETA = 90.03 DBETA = .06
ALPHA= 72.916 DALPHA= .004
V= 643.8
22. 18-0850
MoV2O7.5
Triklin
Dexp Dcal d(D) h k l
5.9000 5.8998 .0002 -1 1 0
4.1500 4.1491 .0009 1 -2 0
3.5000 3.4986 .0014 -1 1 1
3.4000 3.3986 .0014 -1 -1 1
2.9570 2.9571 -.0001 1 -3 1
2.6720 2.6723 -.0003 0 -1 2
2.0780 2.0777 .0003 3 -2 1
1.9710 1.9707 .0003 3 0 0
1.9510 1.9503 .0007 -1 2 2
1.8220 1.8226 -.0006 -3 2 1
1.8050 1.8053 -.0003 1 2 2
1.7820 1.7821 -.0001 0 -1 3
A= 6.4061 DA= .0001
B= 9.2623 DB= .0003
C= 5.42387 DC= .00001
GAMMA=112.457 DGAMMA= .001
BETA = 80.74883 DBETA = .00008
ALPHA=107.2706 DALPHA= .0008
V= 283.63
23. 18-1330
Te2V2O9
Triklin
Dexp Dcal d(D) h k l
4.8500 4.8517 -.0017 -1 0 1
4.3200 4.3214 -.0014 0 1 2
3.7000 3.7002 -.0002 -1 0 2
3.5000 3.5004 -.0004 -1 1 1
3.2900 3.2891 .0009 0 1 3
3.1100 3.1075 .0025 2 1 0
3.0500 3.0501 -.0001 2 1 2
2.8500 2.8496 .0004 0 2 2
2.7420 2.7419 .0001 -2 0 1
2.6320 2.6327 -.0007 2 2 2
2.4680 2.4684 -.0004 -2 -1 2
2.4310 2.4311 -.0001 -2 1 0
A= 6.4807 DA= .0005
B= 6.835 DB= .002
C= 11.487 DC= .002
GAMMA= 70.494 DGAMMA= .006
BETA = 76.10 DBETA = .02
ALPHA= 82.70 DALPHA= .02
V= 465
24. 18-1453
V3O7
Triklin
Dexp Dcal d(D) h k l
11.3000 11.3006 -.0006 1 0 0
5.4900 5.4871 .0029 -2 1 0
4.6100 4.6057 .0043 0 -1 2
4.5300 4.5387 -.0087 -1 0 2
4.1100 4.1121 -.0021 -2 2 0
3.6600 3.6586 .0014 2 1 1
3.5900 3.5855 .0045 2 -1 2
3.5200 3.5225 -.0025 3 -1 1
3.2700 3.2721 -.0021 2 -2 2
3.1500 3.1498 .0002 -1 3 0
3.0560 3.0554 .0006 -1 2 2
3.0200 3.0191 .0009 2 -3 1
A= 11.736 DA= .003
B= 9.637 DB= .009
C= 9.645 DC= .006
GAMMA=103.96 DGAMMA= .02
BETA = 94.13 DBETA = .06
ALPHA=101.33 DALPHA= .07
V= 1030