== Соединения U (òîì 30) == |
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1. 30-0063 {NH4}8{UMo12O42}*7H2O Triklin
Dexp Dcal d(D) h k l 10.3000 10.3012 -.0012 -1 1 0 9.6900 9.6895 .0005 1 1 0 9.0900 9.0877 .0023 0 1 1 8.5600 8.5578 .0022 1 0 1 3.5800 3.5801 -.0001 0 -3 1 3.2500 3.2499 .0001 1 4 1 3.2000 3.2001 -.0001 -1 2 3 3.1400 3.1400 .0000 -1 0 3 3.1100 3.1101 -.0001 -5 1 0 3.0400 3.0402 -.0002 -4 1 2 2.9900 2.9899 .0001 -4 3 1 2.8800 2.8801 -.0001 -3 4 1
A= 15.8304 DA= .0002 B= 13.4341 DB= .0009 C= 10.1633 DC= .0003 GAMMA= 92.598 DGAMMA= .007 BETA = 86.956 DBETA = .006 ALPHA= 74.003 DALPHA= .002 V= 2070.7
2. 30-0196 Bi2UO6 Monoklin Grupa 3
Dexp Dcal d(D) h k l 9.7300 9.6993 .0307 1 0 0 4.8500 4.8497 .0003 2 0 0 3.4700 3.4616 .0084 0 1 0 3.2600 3.2602 -.0002 1 1 0 2.8030 2.8026 .0004 2 0 5 2.4260 2.4248 .0012 4 0 0 2.3610 2.3620 -.0010 -3 0 3 2.0300 2.0292 .0008 3 1 5 2.0040 2.0052 -.0012 0 0 7 1.9860 1.9860 -.0000 4 1 0 1.9520 1.9511 .0009 -3 1 3 1.9340 1.9339 .0001 4 1 4
a= 10.124 b= 3.4616 c=14.651 beta= 73.34 da=.002 db=.0004 dc=.003 dbeta=.02 V= 491.9
Monoklin Grupa 3
Dexp Dcal d(D) h k l 9.7300 9.7046 .0254 0 0 1 4.8500 4.8523 -.0023 0 0 2 3.4700 3.4683 .0017 -1 1 2 3.2600 3.2591 .0009 1 2 0 2.8030 2.8025 .0005 1 2 2 2.4260 2.4262 -.0002 0 0 4 2.3610 2.3618 -.0008 0 2 3 2.0300 2.0297 .0003 4 2 1 2.0040 2.0044 -.0004 -2 2 3 1.9860 1.9858 .0002 0 2 4 1.9520 1.9516 .0004 4 0 4 1.9340 1.9332 .0008 -4 1 2
a= 10.0354 b= 6.913 c= 9.950 beta= 77.242 da= .0005 db= .004 dc=.004 dbeta=.003 V= 673.2
3. 30-0379 Cs{UO2}2F5 Triklin
Dexp Dcal d(D) h k l 6.0600 6.0564 .0036 -1 1 0 4.3300 4.3300 -.0000 0 -1 2 4.0900 4.0897 .0003 1 -1 2 3.8300 3.8310 -.0010 2 -1 1 3.7500 3.7520 -.0020 -1 -1 2 3.7200 3.7197 .0003 2 0 2 3.5200 3.5217 -.0017 2 1 2 3.1200 3.1200 -.0000 0 -1 3 3.0800 3.0804 -.0004 1 -1 3 3.0200 3.0182 .0018 -1 -2 2 2.7970 2.7976 -.0006 -3 1 0 2.6370 2.6361 .0009 0 -2 3
A= 9.273 DA= .004 B= 8.723 DB= .006 C= 10.2754 DC= .0005 GAMMA= 85.29 DGAMMA= .05 BETA = 79.84 DBETA = .01 ALPHA= 87.97 DALPHA= .03 V= 815
4. 30-0623 Mn2{UO2}6{SO4}3{OH}10*16H2O Romb. Groupa 52
Dexp. Dcal. d(D) h k l 8.5200 8.5334 -.0134 2 0 0 7.1500 7.1632 -.0132 0 0 2 6.2200 6.2176 .0024 0 1 1 5.4900 5.4864 .0036 2 0 2 4.2900 4.2947 -.0047 2 1 2 4.1900 4.1971 -.0071 3 1 1 3.9300 3.9270 .0030 0 1 3 3.6700 3.6657 .0043 4 0 2 3.5800 3.5816 -.0016 0 0 4 3.4500 3.4507 -.0007 0 2 0 3.3200 3.3204 -.0004 5 0 1 3.1100 3.1088 .0012 0 2 2
a=17.067 b= 6.901 c=14.33 da= .009 db= .007 dc= .01 V=1687
Triklin
Dexp. Dcal. d(D) h k l 8.5200 8.5200 .0000 1 -1 0 7.1500 7.1588 -.0088 2 0 0 6.2200 6.2202 -.0002 -2 -1 0 5.4900 5.4801 .0099 0 1 1 4.2900 4.2831 .0069 3 -1 0 4.1900 4.1896 .0004 2 0 1 3.9300 3.9277 .0023 -3 0 1 3.6700 3.6714 -.0014 0 -2 1 3.5800 3.5794 .0006 4 0 0 3.4500 3.4486 .0014 1 -2 1 3.3200 3.3222 -.0022 -1 3 1 3.1100 3.1101 -.0001 -4 -2 0
A= 14.464 DA= .001 B= 11.34 DB= .002 C= 5.832 DC= .002 GAMMA= 87.40 DGAMMA= .01 BETA = 97.19 DBETA = .02 ALPHA= 80.213 DALPHA= .001 V= 933.1
5. 30-1008 KUO2{NO3}2 Romb Groupa 17
Dexp. Dcal. d(D) h k l 7.6300 7.6209 .0091 0 0 1 6.4400 6.4469 -.0069 1 0 1 5.9900 5.9714 .0186 0 3 0 4.7500 4.7359 .0141 2 0 1 4.2500 4.2481 .0019 2 3 0 3.9300 3.9316 -.0016 3 1 0 3.7100 3.7106 -.0006 2 3 1 3.3100 3.3102 -.0002 3 2 1 2.6100 2.6102 -.0002 0 5 2 2.3500 2.3502 -.0002 0 6 2 2.1500 2.1501 -.0001 5 3 1
a=12.0895 b=17.914 c= 7.621 da= .0004 db= .008 dc= .003 V=1650
Triklin
Dexp Dcal d(D) h k l 7.6300 7.6258 .0042 1 0 0 6.4400 6.4496 -.0096 0 1 0 5.9900 5.9849 .0051 0 0 1 4.7500 4.7560 -.0060 0 -1 1 4.2500 4.2535 -.0035 -1 1 0 3.9300 3.9297 .0003 2 1 0 3.7100 3.7081 .0019 1 -1 1 3.3100 3.3100 .0000 2 0 1 2.6100 2.6101 -.0001 2 2 1 2.3500 2.3501 -.0001 2 1 2 2.1500 2.1499 .0001 0 3 0
A= 8.125 DA= .001 B= 6.9372 DB= .0005 C= 6.053 DC= .003 GAMMA= 70.107 DGAMMA= .001 BETA = 89.37 DBETA = .03 ALPHA= 97.87 DALPHA= .05 V= 317.22
6. 30-1254 Na2U2O5Cl4 Triklin
Dexp Dcal d(D) h k l 8.1900 8.1810 .0090 0 1 1 7.9800 7.9756 .0044 0 -1 1 7.7400 7.7216 .0184 1 0 0 7.4300 7.4313 -.0013 -1 1 0 6.6100 6.6076 .0024 0 2 0 5.7100 5.6892 .0208 -1 2 0 4.8600 4.8663 -.0063 -1 1 2 4.8100 4.8020 .0080 0 1 2 4.7200 4.7179 .0021 0 -1 2 4.2600 4.2588 .0012 -1 3 0 4.0800 4.0835 -.0035 0 3 1 3.8400 3.8423 -.0023 -2 2 1
A= 8.2515 DA= .0001 B= 13.6169 DB= .0001 C= 10.63035 DC= .00001 GAMMA=103.8778 DGAMMA= .0006 BETA =106.2316 DBETA = .0007 ALPHA= 84.7577 DALPHA= .0002 V= 1113.0
7. 30-1255 NaUV3O10 Monoklin Grupa 3
Dexp Dcal d(D) h k l 5.9200 5.9196 .0004 1 1 1 5.6200 5.6188 .0012 2 0 1 5.4000 5.4008 -.0008 2 0 0 3.6000 3.6005 -.0005 3 0 0 3.4100 3.4097 .0003 -2 1 2 3.2200 3.2208 -.0008 -1 0 4 2.9910 2.9947 -.0037 -3 1 1 2.9500 2.9490 .0010 1 2 3 2.7060 2.7059 .0001 -1 2 3 2.4270 2.4267 .0003 -3 1 3 2.2550 2.2551 -.0001 5 0 2 2.2550 2.2556 -.0006 3 1 6
a= 11.276 b= 7.2593 c= 15.4087 beta= 73.32 da=.005 db=.0003 dc=.0005 dbeta= .02 V= 1208.2
Triklin
Dexp Dcal d(D) h k l 5.9200 5.9189 .0011 0 1 1 5.6200 5.6197 .0003 0 -1 1 5.4000 5.4107 -.0107 1 0 0 3.6000 3.6017 -.0017 -1 2 0 3.4100 3.4123 -.0023 1 -2 1 3.2200 3.2208 -.0008 1 1 2 2.9910 2.9904 .0006 -1 0 2 2.9500 2.9501 -.0001 -1 1 2 2.7060 2.7054 .0006 2 0 0 2.4270 2.4269 .0001 -2 0 1 2.2550 2.2548 .0002 -1 1 3 2.2140 2.2142 -.0002 0 -2 3
A= 5.631 DA= .002 B= 8.2581 DB= .0009 C= 8.38574 DC= .00006 GAMMA=101.10 DGAMMA= .01 BETA = 78.623 DBETA = .007 ALPHA= 89.324 DALPHA= .006 V= 374.7
8. 30-1256 NaV7UO21 Triklin
Dexp Dcal d(D) h k l 9.7200 9.7176 .0024 1 0 0 7.3400 7.3431 -.0031 1 1 0 5.9600 5.9680 -.0080 -1 0 1 4.7800 4.7819 -.0019 -2 -1 1 4.3000 4.2959 .0041 0 2 0 3.6300 3.6284 .0016 -1 2 0 3.3900 3.3912 -.0012 0 -1 2 3.2200 3.2195 .0005 -3 -2 1 3.0700 3.0678 .0022 -2 -3 1 3.0000 3.0027 -.0027 0 -3 1 2.9260 2.9244 .0016 -1 2 1 2.9000 2.9000 .0000 -2 2 0
A= 10.514 DA= .002 B= 9.607 DB= .005 C= 7.1458 DC= .0007 GAMMA= 70.98 DGAMMA= .01 BETA =108.118 DBETA = .005 ALPHA=113.1230 DALPHA= .0001 V= 613.6
9. 30-1257 Na2UO2Cl4 Triklin
Dexp Dcal d(D) h k l 9.2900 9.2850 .0050 1 0 0 8.5800 8.5839 -.0039 0 0 1 6.9200 6.9421 -.0221 0 -2 1 6.3400 6.3479 -.0079 1 2 0 6.2000 6.1997 .0003 1 1 1 6.0400 6.0335 .0065 1 -2 1 5.7200 5.7227 -.0027 -1 -1 1 5.1900 5.1828 .0072 -1 -2 1 4.7500 4.7495 .0005 -1 3 0 4.4400 4.4412 -.0012 -2 1 0 4.2500 4.2501 -.0001 0 3 1 4.0800 4.0796 .0004 1 3 1
A= 9.5354 DA= .00031 B= 17.444 DB= .003 C= 9.095 DC= .003 GAMMA= 91.51 DGAMMA= .01 BETA = 76.9656 DBETA = .0009 ALPHA=104.33 DALPHA= .01 V= 1427.3 |
10. 30-1261 Na0.75V0.75U0.25O3 Triklin
Dexp Dcal d(D) h k l 12.0000 12.0129 -.0129 0 1 0 6.1700 6.1715 -.0015 0 -1 2 5.9700 5.9690 .0010 -1 0 2 5.5800 5.5773 .0027 -1 2 0 5.0100 5.0115 -.0015 1 -1 2 4.8900 4.8905 -.0005 2 -1 1 3.9800 3.9814 -.0014 -2 -1 3 3.6000 3.6013 -.0013 0 2 2 3.4500 3.4498 .0002 -1 3 1 3.2800 3.2786 .0014 -2 -3 3 3.2600 3.2601 -.0001 1 2 2 3.1800 3.1804 -.0004 1 3 1
A= 12.735 DA= .007 B= 12.833 DB= .001 C= 12.965 DC= .001 GAMMA= 88.962 DGAMMA= .004 BETA =105.89 DBETA = .02 ALPHA=110.058 DALPHA= .002 V= 1907.7
11. 30-1312 Sr3U2O9 Triklin
Dexp Dcal d(D) h k l 6.4300 6.4358 -.0058 -1 1 0 5.5900 5.5975 -.0075 0 1 1 5.5200 5.5172 .0028 0 -1 1 4.5300 4.5323 -.0023 -1 0 1 3.9600 3.9601 -.0001 0 -2 1 3.3700 3.3703 -.0003 1 2 1 3.3300 3.3294 .0006 2 0 1 3.2200 3.2194 .0006 1 0 2 2.8000 2.7988 .0012 0 2 2 2.7590 2.7586 .0004 0 -2 2 2.5000 2.5010 -.0010 -1 -3 1 2.3860 2.3855 .0005 1 -4 1
A= 7.2959 DA= .0007 B= 10.166 DB= .003 C= 6.783 DC= .002 GAMMA=102.43 DGAMMA= .02 BETA = 81.44 DBETA = .04 ALPHA= 90.98 DALPHA= .01 V= 485.7
12. 30-1389 UO2Cl Triklin
Dexp Dcal d(D) h k l 2.9600 2.9603 -.0003 1 -1 1 2.5600 2.5597 .0003 -1 2 1 1.9270 1.9272 -.0002 1 1 3 1.7860 1.7859 .0001 2 -1 2 1.7430 1.7429 .0001 -1 3 2 1.6840 1.6841 -.0001 -1 -2 1 1.6090 1.6094 -.0004 3 0 0 1.5600 1.5599 .0001 -1 3 3 1.3060 1.3060 .0000 3 1 3 1.2720 1.2720 -.0000 3 2 2 1.1720 1.1720 -.0000 0 3 5 1.1260 1.1260 .0000 4 1 2
A= 4.9861 DA= .0002 B= 5.468 DB= .001 C= 6.1441 DC= .0005 GAMMA=101.58 DGAMMA= .02 BETA = 86.56 DBETA = .01 ALPHA= 67.441 DALPHA= .003 V= 149.78
13. 30-1390 U3O12P2 Triklin
Dexp Dcal d(D) h k l 7.9900 7.9769 .0131 -1 0 1 6.0400 6.0422 -.0022 -1 1 1 5.2300 5.2329 -.0029 1 -1 1 5.1200 5.1195 .0005 -2 1 1 4.7500 4.7501 -.0001 2 -1 1 4.5700 4.5681 .0019 -1 0 2 4.5100 4.5042 .0058 0 1 2 4.3400 4.3431 -.0031 1 1 2 4.1900 4.1921 -.0021 -3 1 1 3.9300 3.9307 -.0007 2 1 2 3.8300 3.8294 .0006 4 0 1 3.5000 3.4993 .0007 0 2 0
A= 16.06726 DA= .00002 B= 7.21678 DB= .00001 C= 10.14370 DC= .00001 GAMMA= 97.40497 DGAMMA= .00003 BETA = 84.98336 DBETA = .00007 ALPHA= 78.74713 DALPHA= .00001 V= 1136.26
14. 30-1397 UXeF11 Triklin
Dexp Dcal d(D) h k l 9.7000 9.6891 .0109 0 1 0 5.7600 5.7692 -.0092 0 -1 2 4.7800 4.7830 -.0030 1 0 0 4.5300 4.5386 -.0086 -1 -1 1 4.1600 4.1654 -.0054 0 -1 3 4.0600 4.0574 .0026 -1 1 0 3.9000 3.8992 .0008 -1 1 1 3.6400 3.6419 -.0019 0 2 2 3.4900 3.4890 .0010 -1 -2 2 3.2100 3.2083 .0017 0 -1 4 3.0200 3.0195 .0005 0 2 3 2.9300 2.9294 .0006 -1 -3 1
A= 4.872 DA= .003 B= 9.920 DB= .009 C= 13.175 DC= .004 GAMMA= 80.57 DGAMMA= .06 BETA = 96.98 DBETA = .04 ALPHA= 99.04 DALPHA= .04 V= 617.4
15. 30-1399 UO2CO3*2H2O Triklin
Dexp Dcal d(D) h k l 7.6700 7.6728 -.0028 0 1 0 6.3000 6.2777 .0223 1 -1 1 4.9500 4.9409 .0091 0 -1 2 4.9100 4.9089 .0011 1 0 2 4.4400 4.4416 -.0016 1 1 0 4.2200 4.2158 .0042 -1 2 0 3.9500 3.9524 -.0024 -1 2 1 3.7200 3.7197 .0003 1 -1 3 3.5650 3.5642 .0008 2 0 1 3.4200 3.4210 -.0010 2 -2 1 3.3100 3.3110 -.0010 0 -2 2 3.1830 3.1828 .0002 0 0 4 2.9640 2.9647 -.0007 1 0 4 2.8530 2.8527 .0003 -2 1 3 2.7310 2.7301 .0009 -1 3 1 2.6220 2.6226 -.0006 -2 3 1
A= 8.1206 DA= .0002 B= 8.48626 DB= .00005 C= 12.7514 DC= .0002 GAMMA=115.282 DGAMMA= .002 BETA = 86.946 DBETA = .001 ALPHA= 92.20 DALPHA= .01 V= 793.4
16. 30-1400 UOF4 Monoklin Grupa 3
Dexp Dcal d(D) h k l 5.0300 5.0243 .0057 1 1 0 3.9900 3.9944 -.0044 0 1 1 3.7800 3.7802 -.0002 -2 0 1 3.4100 3.4102 -.0002 2 1 0 3.2700 3.2735 -.0035 1 1 1 2.7500 2.7516 -.0016 -3 0 1 2.5300 2.5299 .0001 -3 1 1 2.3700 2.3687 .0013 0 1 2 2.1200 2.1167 .0033 3 0 1 2.0100 2.0107 -.0007 3 1 1 1.9200 1.9192 .0008 4 1 0 1.8900 1.8901 -.0001 -4 0 2
a= 8.463 b= 6.4341 c= 5.361 beta= 108.12 da=.001 db=.0004 dc=.002 dbeta= .06 V= 277.4
Triklin
Dexp Dcal d(D) h k l 5.0300 5.0231 .0069 0 0 1 3.9900 3.9878 .0022 0 -2 1 3.7800 3.7802 -.0002 1 0 0 3.4100 3.4095 .0005 1 2 0 3.2700 3.2721 -.0021 -1 2 0 2.7500 2.7475 .0025 -1 -1 1 2.5300 2.5296 .0004 -1 4 0 2.3700 2.3729 -.0029 0 6 0 2.1200 2.1179 .0021 1 -2 2 2.0100 2.0097 .0003 1 6 1 1.9200 1.9205 -.0005 -1 -1 2 1.8900 1.8901 -.0001 2 0 0
A= 3.84400 DA= .00009 B= 14.293 DB= .004 C= 5.112 DC= .002 GAMMA= 86.488 DGAMMA= .004 BETA = 79.947 DBETA = .001 ALPHA= 85.849 DALPHA= .005 V= 275.45
17. 30-1401 UO2F2*{OH}x*{OH}x*H2O Triklin
Dexp Dcal d(D) h k l 6.7100 6.7103 -.0003 -1 2 0 5.9400 5.9478 -.0078 0 0 1 5.8500 5.8564 -.0064 1 2 0 5.7500 5.7497 .0003 0 4 0 5.3300 5.3314 -.0014 0 -2 1 5.1300 5.1303 -.0003 -1 0 1 4.9800 4.9784 .0016 1 3 0 4.6500 4.6496 .0004 0 3 1 4.6000 4.5998 .0002 0 5 0 4.2500 4.2517 -.0017 1 4 0 4.1100 4.1083 .0017 -1 -3 1 3.8800 3.8788 .0012 1 2 1
A= 7.6427 DA= .0002 B= 23.2567 DB= .0004 C= 6.0529 DC= .0001 GAMMA= 98.454 DGAMMA= .005 BETA =100.625 DBETA = .003 ALPHA= 89.691 DALPHA= .001 V= 1045.8
18. 30-1404 UO2{NO3}2*2H2O Romb Groupa 26,28,51
Dexp. Dcal. d(D) h k l 6.5100 6.5105 -.0005 0 2 0 5.0900 5.0780 .0120 1 0 0 4.6900 4.6931 -.0031 1 0 1 4.3400 4.3403 -.0003 0 3 0 3.7500 3.7485 .0015 1 1 2 2.9900 2.9900 -.0000 0 1 4
a= 5.078 b=13.021 c=12.288 da= .001 db= .001 dc= .001 V= 812.5
19. 30-1408 UO2SO4*3H2O Triklin
Dexp Dcal d(D) h k l 10.8000 10.7782 .0218 -1 0 1 8.1700 8.1828 -.0128 -1 1 0 7.9500 7.9453 .0047 -1 0 2 7.7400 7.7507 -.0107 1 -1 1 7.5300 7.5249 .0051 -1 -1 2 6.0700 6.0680 .0020 2 0 0 5.9300 5.9314 -.0014 -1 -1 3 5.4900 5.4873 .0027 -1 -2 2 5.3900 5.3891 .0009 -2 0 2 5.3500 5.3473 .0027 -2 -1 2 5.2500 5.2477 .0023 1 -1 3 5.2300 5.2283 .0017 -2 1 0
A= 12.290 DA= .001 B= 12.457 DB= .002 C= 19.858 DC= .002 GAMMA= 83.124 DGAMMA= .007 BETA = 97.34 DBETA = .01 ALPHA=103.328 DALPHA= .008 V= 2922
20. 30-1409 beta-UO2SO4*H2O Triklin
Dexp Dcal d(D) h k l 7.5000 7.5075 -.0075 1 1 0 7.0300 7.0159 .0141 0 -1 1 6.8600 6.8624 -.0024 -1 -1 1 5.4300 5.4447 -.0147 1 1 1 5.0600 5.0658 -.0058 0 0 2 4.7900 4.7884 .0016 0 2 0 4.5800 4.5821 -.0021 -1 -2 1 4.3600 4.3562 .0038 0 -2 1 4.1700 4.1703 -.0003 -1 1 2 3.8800 3.8753 .0047 -2 0 2 3.8200 3.8234 -.0034 -1 2 0 3.6700 3.6718 -.0018 -2 1 0
A= 9.50192 DA= .00001 B= 9.9385 DB= .0001 C= 10.54853 DC= .00003 GAMMA= 74.52720 DGAMMA= .00003 BETA =106.1446 DBETA = .0001 ALPHA= 95.1115 DALPHA= .0002 V= 922.07 |
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