== Соединения U (òîìà 25-27) == |
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1. 25-0016 Al2Fe2{UO2}2{PO4}4SO4{OH}2*20H2O Triklin
Dexp Dcal d(D) h k l 12.3000 12.2935 .0065 1 0 0 11.1000 11.1285 -.0285 -1 1 0 9.2000 9.1911 .0089 -1 0 1 8.6600 8.6256 .0344 1 1 0 8.4000 8.4235 -.0235 0 -1 1 7.6600 7.6476 .0124 1 0 1 7.2800 7.2868 -.0068 -1 2 1 6.2400 6.2340 .0060 -2 1 1 5.9100 5.9113 -.0013 0 -2 1 5.6400 5.6429 -.0029 0 0 2 5.5600 5.5642 -.0042 -2 2 0 5.0200 5.0158 .0042 0 -1 2
A= 13.107 DA= .005 B= 16.57 DB= .01 C= 11.833 DC= .001 GAMMA=107.46 DGAMMA= .01 BETA =104.00 DBETA = .07 ALPHA= 75.937 DALPHA= .009 V= 2337
2. 25-1469 BaU2O7*xH2O Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.5600 3.5573 .0027 -1 1 1 3.4100 3.4060 .0040 2 0 0 3.0900 3.0909 -.0009 2 1 0 2.4500 2.4528 -.0028 0 3 0 2.2700 2.2707 -.0007 3 0 0 2.1700 2.1697 .0003 3 1 0 2.1000 2.0999 .0001 -1 3 1 1.9800 1.9830 .0030 1 3 2 1.9480 1.9507 -.0027 -3 0 1 1.9080 1.9080 -.0000 3 2 2 1.7850 1.7847 .0003 -1 3 2 1.7230 1.7235 -.0005 -3 2 1
a= 7.2092 b= 7.358 c= 6.819 beta= 70.89 da=.0001 db=.004 dc= .004 dbeta=.04 V= 341.8
Triklin
Dexp Dcal d(D) h k l 3.5600 3.5588 .0012 0 1 1 3.4100 3.4089 .0011 1 0 1 3.0900 3.0920 -.0020 0 -1 1 2.4500 2.4486 .0014 2 0 1 2.2700 2.2688 .0012 0 0 2 2.1700 2.1727 -.0027 0 1 2 2.1000 2.0995 .0005 -1 2 0 1.9800 1.9794 .0006 2 -1 1 1.9480 1.9495 -.0015 0 -1 2 1.9080 1.9083 -.0003 -3 1 1 1.7850 1.7847 .0003 -3 -1 2 1.7230 1.7232 -.0002 1 2 2
A= 7.2253 DA= .0008 B= 5.0052 DB= .0005 C= 4.6951 DC= .0008 GAMMA= 76.10 DGAMMA= .01 BETA =102.57 DBETA = .03 ALPHA= 85.40 DALPHA= .01 V= 159.3
3. 26-1003 CaU2O7*11H2O Triklin
Dexp Dcal d(D) h k l 6.1820 6.1871 -.0051 -1 1 0 5.7410 5.7345 .0065 0 0 1 4.0820 4.0816 .0004 0 2 0 3.5050 3.5076 -.0026 -2 1 0 3.3670 3.3695 -.0025 2 0 0 3.2060 3.2045 .0015 0 -2 1 2.9390 2.9409 -.0019 -2 2 1 2.7200 2.7211 -.0011 0 3 0 2.4600 2.4590 .0010 -2 3 1 2.1820 2.1817 .0003 -3 0 1 2.0720 2.0723 -.0003 3 -1 1 2.0050 2.0055 -.0005 3 -2 1
A= 7.146 DA= .001 B= 8.623 DB= .001 C= 5.820 DC= .002 GAMMA=108.24 DGAMMA= .02 BETA = 98.69 DBETA = .01 ALPHA= 82.91 DALPHA= .01 V= 335.7
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4. 27-0821 Na4UO5 Monoklin Grupa 4.7
Dexp Dcal d(D) h k l 5.3800 5.3783 .0017 1 1 1 3.9500 3.9487 .0013 2 1 1 3.7700 3.7692 .0008 0 2 0 2.9400 2.9376 .0024 2 0 3 2.7300 2.7300 -.0000 3 1 0 2.7000 2.6974 .0026 0 1 3 2.3000 2.3013 -.0013 1 0 4 2.2100 2.2091 .0009 2 3 1 1.9600 1.9597 .0003 3 3 1 1.9100 1.9095 .0005 2 3 3 1.7600 1.7627 -.0027 5 1 3 1.7400 1.7429 -.0029 1 4 2 1.7100 1.7100 -.0000 4 2 4
a= 9.394 b= 7.538 c= 9.266 beta= 69.27 da=.005 db=.003 dc=.003 dbeta=.06 V= 614
Triklin
Dexp Dcal d(D) h k l 5.3800 5.3904 -.0104 1 0 0 3.9500 3.9450 .0050 0 1 1 3.7700 3.7695 .0005 0 -1 1 2.9400 2.9405 -.0005 1 -1 1 2.7300 2.7317 -.0017 1 0 2 2.7000 2.6952 .0048 2 0 0 2.3000 2.3014 -.0014 -2 0 1 2.2100 2.2107 -.0007 2 1 2 1.9600 1.9599 .0001 -1 2 1 1.9100 1.9095 .0005 1 0 3 1.7600 1.7599 .0001 3 2 1 1.7400 1.7400 .0000 3 2 0
A= 5.747 DA= .002 B= 5.462 DB= .003 C= 5.867 DC= .002 GAMMA= 71.92 DGAMMA= .05 BETA = 79.33 DBETA = .03 ALPHA= 84.26 DALPHA= .03 V= 171.9
5. 27-0938 UO3*SiO2*H2O Triklin
Dexp Dcal d(D) h k l 11.6000 11.6116 -.0116 1 0 0 7.3000 7.2973 .0027 0 1 1 6.1900 6.1950 -.0050 0 -1 1 5.7900 5.7827 .0073 1 2 1 5.2400 5.2395 .0005 -1 -1 1 4.9900 4.9899 .0001 2 1 1 4.5600 4.5570 .0030 -2 2 0 4.2600 4.2581 .0019 -2 0 1 3.8800 3.8818 -.0018 -2 2 1 3.6700 3.6701 -.0001 -1 4 0 3.5400 3.5407 -.0007 3 2 1 3.5000 3.5002 -.0002 -1 4 1
A= 11.795 DA= .002 B= 16.186 DB= .0063 C= 7.6526 DC= .0002 GAMMA= 84.87 DGAMMA= .01 BETA = 80.37 DBETA = .01 ALPHA= 77.15 DALPHA= .03 V= 1402
6. 27-1730 C9H15LiO8U*xH2O Triklin
Dexp Dcal d(D) h k l 7.9300 7.9520 -.0220 1 0 0 5.6600 5.6587 .0013 0 1 1 5.4500 5.4595 -.0095 0 -1 1 3.9800 3.9760 .0040 2 0 0 3.9200 3.9183 .0017 -2 0 1 3.6100 3.6124 -.0024 -1 1 2 3.2200 3.2199 .0001 -1 -1 3 2.9900 2.9917 -.0017 -2 1 0 2.9000 2.9003 -.0003 -2 0 3 2.8000 2.7986 .0014 2 -1 1 2.7300 2.7297 .0003 0 -2 2 2.6700 2.6703 -.0003 1 -1 3
A= 8.449 DA= .005 B= 6.788 DB= .002 C= 11.0648 DC= .0001 GAMMA= 71.91 DGAMMA= .01 BETA = 97.748 DBETA = .007 ALPHA= 90.192 DALPHA= .003 V= 597.3
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