270. 35-0021
gamma-Ti{HPO4}2*2H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
11.5500 11.6009 -.0509 1 0 0
5.5600 5.5559 .0041 1 0 1
4.2900 4.2762 .0138 2 0 1
3.8600 3.8670 -.0070 3 0 0
3.4600 3.4611 -.0011 2 2 0
3.3000 3.2998 .0002 3 0 1
3.1700 3.1645 .0055 0 0 2
3.0500 3.0529 -.0029 1 0 2
2.7800 2.7780 .0020 2 0 2
2.5800 2.5763 .0037 2 3 0
2.5500 2.5514 -.0014 0 2 2
a=11.60 b= 8.63 c= 6.329
da= .01 db= .02 dc= .009
V= 633
271. 35-0162
BaLa2Ti4O12
Triklin
Dexp Dcal d(D) h k l
11.3000 11.1628 .1372 0 0 1
5.1000 5.0989 .0011 0 1 1
4.2200 4.2190 .0010 -2 -1 1
4.0300 4.0289 .0011 2 1 0
3.8600 3.8594 .0006 0 1 2
3.0800 3.0795 .0005 3 1 0
2.8400 2.8395 .0005 -3 -1 3
2.7200 2.7205 -.0005 -4 0 2
2.6300 2.6304 -.0004 -1 -2 3
2.2900 2.2884 .0016 -2 0 5
2.2100 2.2100 -.0000 2 -1 4
2.1000 2.0998 .0002 0 -3 1
A= 11.1547 DA= .0004
B= 6.3034 DB= .0004
C= 11.731 DC= .005
GAMMA= 88.62 DGAMMA= .01
BETA =105.44 DBETA = .02
ALPHA= 99.2291 DALPHA= .0007
V=784.5
272. 35-0163
BaLa2Ti3O10
Triklin
Dexp Dcal d(D) h k l
14.4000 14.3923 .0077 1 0 0
4.7400 4.7403 -.0003 -2 1 1
3.8400 3.8415 -.0015 -2 -1 1
3.4400 3.4397 .0003 -3 2 1
3.2100 3.2089 .0011 4 1 0
2.9800 2.9800 .0000 2 -2 1
2.8100 2.8106 -.0006 -2 1 2
2.7200 2.7213 -.0013 -5 0 1
2.7100 2.7098 .0002 4 1 1
2.3700 2.3701 -.0001 -4 2 2
2.2700 2.2700 -.0000 3 0 2
2.0400 2.0397 .0003 -3 -2 2
A= 14.7535 DA= .0001
B= 9.551 DB= .001
C= 5.763 DC= .001
GAMMA= 99.69 DGAMMA= .01
BETA =100.08 DBETA = .01
ALPHA= 77.42 DALPHA= .01
V= 773.2
273. 35-0164
BaLa2Ti2O8
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
4.3700 4.3608 .0092 0 0 2
3.7300 3.7203 .0097 0 3 0
3.1200 3.1231 -.0031 1 1 2
2.9500 2.9596 -.0096 1 3 0
2.7900 2.7902 -.0002 0 4 0
2.3500 2.3503 -.0003 0 4 2
2.2800 2.2801 -.0001 1 2 3
2.2400 2.2374 .0026 2 2 0
2.0300 2.0302 -.0002 1 5 0
1.7440 1.7443 -.0003 0 0 5
1.6430 1.6427 .0003 1 0 5
1.6150 1.6148 .0002 1 6 2
a= 4.884 b=11.16098 c= 8.7216
da= .005 db= .00004 dc= .0003
v= 475.5
274. 35-0228
BaPr2Ti4O12
Triklin
Dexp Dcal d(D) h k l
11.4000 11.2698 .1302 0 1 0
5.0900 5.0908 -.0008 1 0 0
4.2000 4.1998 .0002 -1 2 1
4.0200 4.0195 .0005 1 0 1
3.8300 3.8283 .0017 -1 2 0
3.0700 3.0707 -.0007 -1 2 3
2.8300 2.8309 -.0009 0 4 2
2.7200 2.7208 -.0008 0 -1 3
2.6200 2.6182 .0018 1 3 2
2.2800 2.2796 .0004 2 1 1
2.2000 2.2008 -.0008 1 -1 3
2.1000 2.0999 .0001 -2 4 2
A= 5.3105 DA= .0002
B= 11.969 DB= .001
C= 10.007 DC= .005
GAMMA= 96.850 DGAMMA= .004
BETA =106.48 DBETA = .02
ALPHA= 70.38 DALPHA= .04
V= 574.35
275. 35-0229
BaPrTi3O10
Triklin
Dexp Dcal d(D) h k l
14.4000 14.3938 .0062 0 0 1
4.7000 4.6995 .0005 0 -2 1
3.8200 3.8211 -.0011 1 1 0
3.4300 3.4304 -.0004 1 1 2
3.2000 3.2000 .0000 1 -1 2
2.9700 2.9703 -.0003 -1 -2 2
2.7900 2.7897 .0003 0 -1 5
2.7200 2.7206 -.0006 1 -2 2
2.3500 2.3500 .0000 0 -1 6
2.2600 2.2603 -.0003 -1 0 5
1.9400 1.9399 .0001 -2 -1 1
1.9180 1.9179 .0001 -1 3 4
A= 3.9523 DA= .0001
B= 9.9247 DB= .0001
C= 14.421 DC= .001
GAMMA= 81.985 DGAMMA= .003
BETA = 87.174 DBETA = .003
ALPHA= 91.648 DALPHA= .002
V= 559.01
276. 35-0887
TiCl4*2OP{NCs}3
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7644 -.0044 0 1 1
7.5000 7.4857 .0143 0 -1 1
4.5100 4.5038 .0062 2 0 0
4.3500 4.3548 -.0048 1 0 2
4.1700 4.1687 .0013 2 1 1
4.0200 4.0214 -.0014 2 0 1
3.8800 3.8822 -.0022 0 2 2
3.8500 3.8430 .0070 1 -1 2
3.7700 3.7707 -.0007 1 2 2
3.6700 3.6704 -.0004 -2 1 1
3.5900 3.5909 -.0009 -2 -1 2
3.5400 3.5365 .0035 -2 0 2
A= 9.44372 DA= .00000
B= 11.74913 DB= .00004
C= 10.40674 DC= .00001
GAMMA= 73.0603 DGAMMA= .0002
BETA = 93.91815 DBETA = .00008
ALPHA= 89.14151 DALPHA= .00001
V=1101.2
277. 35-0983
TiF3
Triklin
Dexp Dcal d(D) h k l
4.2300 4.2278 .0022 0 1 1
3.8400 3.8400 -.0000 0 -1 1
3.5700 3.5703 -.0003 1 1 0
3.1100 3.1106 -.0006 1 -1 1
2.7100 2.7099 .0001 0 1 3
2.3100 2.3102 -.0002 -2 -1 1
2.0800 2.0800 -.0000 2 0 3
1.9200 1.9200 -.0000 0 -2 2
1.8000 1.8004 -.0004 0 1 5
1.7200 1.7196 .0004 0 2 4
1.6200 1.6199 .0001 -3 1 2
1.5700 1.5699 .0001 3 -1 2
A= 5.616 DA= .001
B= 4.4947 DB= .0005
C= 9.3918 DC= .0006
GAMMA= 87.36 DGAMMA= .01
BETA = 89.79 DBETA = .02
ALPHA= 82.92 DALPHA= .01
V= 235.0
278. 35-0984
TiF4
Triklin
Dexp Dcal d(D) h k l
8.5000 8.5360 -.0360 0 1 0
6.0000 5.9998 .0002 1 0 1
4.0000 3.9999 .0001 0 2 1
3.7900 3.7902 -.0002 2 0 1
3.6800 3.6796 .0004 1 0 2
3.0900 3.0907 -.0007 2 2 1
2.6800 2.6802 -.0002 3 0 0
2.3500 2.3497 .0003 -1 0 3
2.2200 2.2200 .0000 2 2 3
2.0100 2.0101 -.0001 4 0 0
1.8900 1.8904 -.0004 1 2 4
1.7200 1.7201 -.0001 0 3 4
A= 8.176 DA= .001
B= 8.694 DB= .004
C= 7.8857 DC= .0003
GAMMA= 83.43 DGAMMA= .03
BETA = 80.932 DBETA = .009
ALPHA= 80.363 DALPHA= .007
V= 543.4
279. 35-1751
C3H9O3Ti
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
8.5000 8.5106 -.0106 1 0 1
5.2100 5.2133 -.0033 1 1 0
4.8700 4.8454 .0246 1 0 2
3.7850 3.7829 .0021 1 1 2
3.6250 3.6211 .0039 0 1 2
3.2300 3.2296 .0004 1 0 3
2.9600 2.9597 .0003 3 1 2
2.5640 2.5637 .0003 4 0 0
a= 11.030 b= 6.054 c= 9.7200 beta= 68.382
da= .001 db=.001 dc=.0001 dbet=.007
V= 603.4
280. 35-1778
C10H14O5Ti
Triklin
Dexp Dcal d(D) h k l
19.3200 19.3360 -.0160 0 0 1
9.8900 9.9292 -.0392 0 1 0
9.1000 9.0998 .0002 2 0 1
7.0100 7.0067 .0033 2 -1 1
5.8800 5.8853 -.0053 2 -1 3
5.6300 5.6235 .0065 -2 -1 1
5.4800 5.4829 -.0029 -2 1 1
5.2100 5.2086 .0014 2 0 4
5.0000 5.0054 -.0054 3 1 1
4.5200 4.5199 .0001 2 -2 1
4.4100 4.4084 .0016 4 0 3
3.8400 3.8474 -.0074 -2 1 3
A= 18.26 DA= .01
B= 10.0454 DB= .0003
C= 21.445 DC= .006
GAMMA= 94.688 DGAMMA= .009
BETA = 65.39 DBETA = .03
ALPHA= 98.64 DALPHA= .01
V=3536.5
281. 35-1989
C12H30O9P3Ti
Tetragon
Groupa 103,124
Dexp. Dcal. d(D) h k l
11.3000 11.3757 -.0757 1 0 0
5.7100 5.6878 .0222 2 0 0
4.4400 4.4455 -.0055 2 1 1
3.9800 3.9745 .0055 1 1 2
3.5600 3.5633 -.0033 2 0 2
a= 11.38 c= 9.14
da= .01 dc= .06
V=1183
282. 35-1993
C12H30O9P3Ti
Tetragon
Groupa 86
Dexp. Dcal. d(D) h k l
12.6000 12.7603 -.1603 1 1 0
11.2000 11.2164 -.0164 0 0 2
6.1500 6.1368 .0132 2 2 1
4.7400 4.7631 -.0231 2 0 4
3.9300 3.9213 .0087 2 1 5
3.4500 3.4504 -.0004 4 1 4
a= 18.05 c= 22.43
da= .02 dc= .05
v=7305