205. 32-0206
Ce2Ti4{SO4}11
Triklin
Dexp Dcal d(D) h k l
13.7000 13.7042 -.0042 1 0 0
7.6200 7.6159 .0041 0 1 0
6.5100 6.5157 -.0057 2 0 1
6.2800 6.2815 -.0015 0 -1 1
5.6600 5.6662 -.0062 1 1 2
5.4500 5.4421 .0079 2 1 0
4.2900 4.2925 -.0025 -1 0 3
4.1500 4.1522 -.0022 3 1 0
3.7400 3.7410 -.0010 0 -1 3
3.6100 3.6101 -.0001 2 2 1
3.4400 3.4400 .0000 0 1 4
3.2000 3.1997 .0003 -1 1 4
A= 13.98 DA= .01
B= 7.815 DB= .002
C= 14.55 DC= .05
GAMMA= 81.36 DGAMMA= .04
BETA = 80.99 DBETA = .09
ALPHA= 79.18 DALPHA= .06
V= 1530.5
206. 32-0207
Ce2{SSO4}3{TiOH}2{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
9.1200 9.1186 .0014 0 0 1
8.5600 8.5601 -.0001 1 1 0
5.6100 5.6071 .0029 0 -2 1
5.1000 5.0990 .0010 0 2 1
4.6000 4.6009 -.0009 -1 -1 2
4.3100 4.3202 -.0102 -1 2 1
4.1900 4.1898 .0002 -1 -2 2
3.7400 3.7414 -.0014 1 0 2
3.3800 3.3813 -.0013 1 4 0
3.2800 3.2793 .0007 -2 2 1
3.2300 3.2297 .0003 -3 -1 1
3.0600 3.0600 .0000 2 4 0
A= 9.737 DA= .002
B= 13.806 DB= .003
C= 9.509 DC= .002
GAMMA= 73.287 DGAMMA= .009
BETA =105.49 DBETA = .01
ALPHA= 99.73 DALPHA= .04
V= 1174.0
207. 32-0494
La2Ti4{SO4}11
Triklin
Dexp Dcal d(D) h k l
13.7000 13.7031 -.0031 1 0 0
7.5600 7.5638 -.0038 -1 1 0
6.1600 6.1614 -.0014 -1 1 1
5.6300 5.6343 -.0043 -2 0 1
4.5200 4.5212 -.0012 0 1 2
4.2900 4.2897 .0003 -2 -2 1
3.7530 3.7532 -.0002 0 2 2
3.6170 3.6150 .0020 0 3 0
3.4360 3.4352 .0008 0 -2 2
3.2000 3.1992 .0008 4 0 1
3.0880 3.0883 -.0003 1 1 3
2.9360 2.9357 .0003 -4 1 1
A= 14.2371 DA= .0003
B= 11.309 DB= .003
C= 9.588 DC= .004
GAMMA= 74.327 DGAMMA= .001
BETA = 90.06 DBETA = .02
ALPHA= 85.10 DALPHA= .03
V= 1480.4
208. 32-0685
Nd2Ti4O4{SO4}7
Rombik
Groupa 26, 28, 51
Dexp. Dcal. d(D) h k l
4.4400 4.4433 -.0033 1 0 0
3.6600 3.6545 .0055 1 2 0
3.6000 3.5977 .0023 1 0 1
3.1400 3.1390 .0010 1 2 1
2.5700 2.5699 .0001 0 5 0
2.0990 2.0997 -.0007 2 2 0
2.0620 2.0617 .0003 2 1 1
1.9840 1.9842 -.0002 1 4 2
a= 4.443 b=12.8495 c= 6.13
da= .001 db= .0009 dc= .01
V= 350.0
209. 32-0686
Nd2Ti4{SO4}11
Triklin
Dexp Dcal d(D) h k l
13.7000 13.7519 -.0519 0 1 0
7.5600 7.5605 -.0005 1 0 0
5.6000 5.5977 .0023 1 0 1
4.5700 4.5699 .0001 1 2 0
4.4500 4.4482 .0018 -1 -2 1
4.2700 4.2662 .0038 0 0 2
3.7400 3.7436 -.0036 0 -3 2
3.6100 3.6057 .0043 0 3 1
3.4400 3.4401 -.0001 2 1 0
3.1900 3.1885 .0015 1 -4 2
3.0900 3.0890 .0010 2 1 1
2.9280 2.9316 -.0036 2 -3 2
A= 7.800 DA= .006
B= 14.89361 DB= .00003
C= 8.973 DC= .003
GAMMA=104.19 DGAMMA= .01
BETA = 86.84 DBETA = .04
ALPHA=107.99 DALPHA= .03
V= 961.0
210. 32-0859
K2TiF5
Triklin
Dexp Dcal d(D) h k l
5.7900 5.7957 -.0057 1 1 0
3.3900 3.3860 .0040 0 1 1
3.2300 3.2286 .0014 0 -1 1
2.8980 2.8978 .0002 2 2 0
2.7440 2.7431 .0009 1 3 0
2.5810 2.5804 .0006 2 1 1
2.4670 2.4662 .0008 2 2 1
2.4130 2.4148 -.0018 2 3 0
2.2250 2.2263 -.0013 1 -2 1
2.1770 2.1769 .0001 -2 0 1
1.9370 1.9367 .0003 3 2 1
1.7950 1.7950 .0000 2 -2 1
A= 6.376 DA= .005
B= 8.304 DB= .005
C= 3.7046 DC= .0009
GAMMA= 68.10 DGAMMA= .05
BETA = 81.77 DBETA = .02
ALPHA= 83.71 DALPHA= .03
V= 179.8
211. 32-0860
K3Ti2F9
Triklin
Dexp Dcal d(D) h k l
6.5300 6.5462 -.0162 0 1 1
6.3400 6.3388 .0012 1 0 0
6.1900 6.2005 -.0105 0 -1 1
6.0500 6.0497 .0003 1 0 1
5.5000 5.4955 .0045 1 0 2
5.3900 5.4171 -.0271 0 1 3
5.1400 5.1498 -.0098 -1 0 3
4.4400 4.4355 .0045 1 1 1
4.2500 4.2532 -.0032 1 1 2
3.9400 3.9379 .0021 -1 1 4
3.7400 3.7370 .0030 0 -1 5
3.5600 3.5606 -.0006 -1 -1 4
A= 6.35625 DA= .00008
B= 6.6397 DB= .0001
C= 24.611 DC= .001
GAMMA= 92.601 DGAMMA= .002
BETA = 93.634 DBETA = .002
ALPHA= 83.6790 DALPHA= .0003
V=1029.6
212. 32-1045
NaBiTi6O14
Triklin
Dexp Dcal d(D) h k l
10.0000 10.0055 -.0055 1 0 0
6.5000 6.5015 -.0015 0 1 0
5.3000 5.2988 .0012 -1 0 1
3.8700 3.8721 -.0021 0 0 2
3.5200 3.5184 .0016 2 1 0
3.2500 3.2507 -.0007 0 2 0
3.2200 3.2170 .0030 1 2 1
3.1600 3.1583 .0017 -2 2 0
3.0600 3.0608 -.0008 1 -1 2
3.0100 3.0121 -.0021 2 -1 2
2.9500 2.9502 -.0002 -3 1 1
2.8500 2.8485 .0015 0 -1 2
A= 10.8049 DA= .0006
B= 7.234 DB= .002
C= 8.822 DC= .003
GAMMA= 99.15 DGAMMA= .04
BETA = 74.66 DBETA = .01
ALPHA= 69.39 DALPHA= .02
V= 597.6
213. 32-1129
NaMnTiO4
Triklin
Dexp Dcal d(D) h k l
8.4520 8.4362 .0158 0 1 1
6.4500 6.4508 -.0008 0 -1 1
6.2330 6.2373 -.0043 -1 0 1
5.2800 5.2791 .0009 -1 2 1
4.5400 4.5430 -.0030 1 -2 1
4.0090 4.0115 -.0025 -1 0 2
3.9220 3.9267 -.0047 2 1 0
3.3090 3.3080 .0010 0 1 3
2.8700 2.8708 -.0008 3 1 1
2.7610 2.7610 .0000 2 -1 3
2.6260 2.6262 -.0002 1 3 3
2.4930 2.4930 .0000 0 -4 1
A= 10.080 DA= .006
B= 12.0406 DB= .0007
C= 9.967 DC= .001
GAMMA=107.179 DGAMMA= .008
BETA = 84.861 DBETA = .003
ALPHA= 76.966 DALPHA= .002
V= 1109.9
214. 32-1179
NaTiF3*H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.6720 3.6770 -.0050 3 0 0
3.6250 3.6270 -.0020 1 1 0
3.4380 3.4328 .0052 3 0 1
3.1530 3.1517 .0013 2 1 0
2.9130 2.9165 -.0035 3 0 2
2.7640 2.7632 .0008 2 0 3
2.1500 2.1499 .0001 5 0 1
2.0040 2.0038 .0002 5 0 2
a=11.031 b= 3.8405 c= 9.58
da= .007 db= .0005 dc= .03
V= 405.8
215. 32-1363
C2H3Cl3O2Ti
Triklin
Dexp Dcal d(D) h k l
9.2800 9.2826 -.0026 1 0 0
7.4600 7.4567 .0033 -1 1 0
6.9600 6.9613 -.0013 -1 0 1
5.6200 5.6160 .0040 1 1 0
4.9700 4.9737 -.0037 0 -1 2
4.5100 4.5034 .0066 0 0 2
4.2900 4.2906 -.0006 -1 0 2
4.0100 4.0001 .0099 1 -2 2
3.8400 3.8333 .0067 -2 -1 1
3.6900 3.6915 -.0015 2 1 0
3.3300 3.3299 .0001 2 -2 2
3.1900 3.1895 .0005 0 -3 1
A= 9.6619 DA= .0003
B= 9.93928 DB= .001
C= 9.99 DC= .01
GAMMA=104.08 DGAMMA= .03
BETA = 91.20 DBETA = .05
ALPHA=114.51 DALPHA= .01
V= 839.0
216. 32-1364
C2H3Cl3O2i
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.0000 10.9717 .0283 1 0 0
7.4600 7.4529 .0071 1 1 0
5.4900 5.4858 .0042 2 0 0
5.0800 5.0777 .0023 0 2 0
3.7200 3.7220 -.0020 -1 2 1
3.2600 3.2607 -.0007 -2 2 1
3.1100 3.1091 .0009 -3 1 1
2.9890 2.9871 .0019 3 0 1
2.8640 2.8657 -.0017 3 1 1
2.7420 2.7429 -.0009 4 0 0
2.2400 2.2398 .0002 3 3 1
a= 11.03 b= 10.1554 c= 5.9905 beta= 95.72
da=.01 db=.0004 dc=.004 dbeta=.09
V= 667.5
217. 32-1365
C4H6Cl2O4Ti
Triklin
Dexp Dcal d(D) h k l
9.3300 9.3329 -.0029 1 0 0
7.2000 7.1947 .0053 1 1 0
6.6400 6.6487 -.0087 -1 0 1
6.3200 6.3180 .0020 -1 -1 1
6.0000 5.9863 .0137 0 2 0
5.4200 5.4260 -.0060 0 1 1
4.9200 4.9127 .0073 -1 -2 1
4.6700 4.6664 .0036 2 0 0
3.7700 3.7694 .0006 -2 2 0
3.6000 3.5974 .0026 2 2 0
3.3800 3.3810 -.0010 1 -3 1
3.2700 3.2688 .0012 -3 0 1
A= 9.896 DA= .001
B= 12.279 DB= .007
C= 7.391 DC= .002
GAMMA= 88.453 DGAMMA= .007
BETA =109.25 DBETA = .03
ALPHA=102.54 DALPHA= .04
V= 826.9
218. 32-1366
C12Bi2O27Ti3**4H2O
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3084 .0016 -1 0 1
5.2400 5.2366 .0034 0 -1 2
4.5500 4.5525 -.0025 1 1 1
4.0500 4.0416 .0084 0 1 2
3.7100 3.7082 .0018 2 1 0
3.2400 3.2378 .0022 1 -2 3
3.0000 3.0008 -.0008 0 1 3
2.8510 2.8512 -.0002 -2 3 0
2.5630 2.5622 .0008 3 1 1
2.4540 2.4550 -.0010 -2 -2 3
2.3670 2.3680 -.0010 0 1 4
2.2850 2.2850 -.0000 -2 3 2
A= 10.097 DA= .003
B= 9.287 DB= .005
C= 11.16 DC= .02
GAMMA=108.10 DGAMMA= .05
BETA = 87.3843 DBETA = .0005
ALPHA=106.31 DALPHA= .09
V= 954.1
219. 32-1367
Ti{ClO4}4
Triklin
Dexp Dcal d(D) h k l
4.1500 4.1517 -.0017 -1 0 1
3.9200 3.9196 .0004 -1 -1 1
3.7600 3.7597 .0003 1 -2 1
3.6900 3.6939 -.0039 -2 2 0
3.3200 3.3161 .0039 2 -2 1
3.0700 3.0683 .0017 -2 -1 1
2.8100 2.8104 -.0004 3 1 0
2.7100 2.7101 -.0001 1 3 0
2.5600 2.5591 .0009 -1 -3 1
2.4300 2.4297 .0003 3 -3 1
2.3800 2.3783 .0017 4 0 0
2.3100 2.3098 .0002 1 -4 1
A= 9.8097 DA= .0001
B= 9.528 DB= .005
C= 4.9239 DC= .0008
GAMMA=103.59 DGAMMA= .03
BETA = 83.075 DBETA = .002
ALPHA=103.85 DALPHA= .03
V= 433.3
220. 32-1368
Ti{CN}2Cl6
Triklin
Dexp Dcal d(D) h k l
8.1400 8.1396 .0004 0 1 1
6.3500 6.3403 .0097 0 -1 1
5.8400 5.8411 -.0011 1 0 0
5.6400 5.6371 .0029 1 0 1
5.2700 5.2634 .0066 -1 1 0
4.8000 4.8141 -.0141 1 -1 1
4.3600 4.3615 -.0015 -1 0 1
4.1100 4.1153 -.0053 1 0 2
3.9620 3.9680 -.0060 0 3 1
3.3930 3.3909 .0021 0 3 2
3.2740 3.2734 .0006 -1 3 0
3.1680 3.1701 -.0021 0 -2 2
A= 6.0821 DA= .0002
B= 12.142 DB= .001
C= 9.5489 DC= .0003
GAMMA= 86.75 DGAMMA= .01
BETA = 73.85 DBETA = .01
ALPHA= 74.954 DALPHA= .007
V=654.2
221. 32-1369
Ti{HPO4}2
Triklin
Dexp Dcal d(D) h k l
7.4100 7.4155 -.0055 0 1 0
4.2500 4.2444 .0056 0 -1 2
4.0400 4.0409 -.0009 -1 -1 1
3.9100 3.9062 .0038 0 0 2
3.7200 3.7190 .0010 1 -1 1
3.5800 3.5865 -.0065 -1 1 0
3.1000 3.1008 -.0008 -1 -1 2
2.8070 2.8029 .0041 -1 0 2
2.5030 2.5021 .0009 1 -1 3
2.4700 2.4718 -.0018 0 3 0
2.3660 2.3667 -.0007 -1 -2 3
2.2420 2.2412 .0008 1 2 2
A= 4.7796 DA= .0007
B= 8.274 DB= .003
C= 8.571 DC= .002
GAMMA= 79.096 DGAMMA= .004
BETA = 86.98 DBETA = .05
ALPHA=113.01 DALPHA= .09
V= 303.4
222. 32-1370
alfa-Ti{HPO4}2
Triklin
Dexp Dcal d(D) h k l
7.1700 7.1629 .0071 1 0 0
6.1700 6.1618 .0082 0 1 1
5.5300 5.5293 .0007 0 -1 1
4.9200 4.9208 -.0008 1 1 1
4.3000 4.2980 .0020 -1 2 0
4.0700 4.0652 .0048 1 0 2
3.7000 3.6954 .0046 0 1 2
3.5800 3.5814 -.0014 2 0 0
3.4000 3.4106 -.0106 0 -1 2
3.0800 3.0809 -.0009 0 2 2
2.5260 2.5266 -.0006 2 -1 3
2.4600 2.4604 -.0004 2 2 2
A= 7.903 DA= .001
B= 9.1532 DB= .0004
C= 8.287 DC= .004
GAMMA=104.02 DGAMMA= .01
BETA = 69.99 DBETA = .01
ALPHA= 89.07 DALPHA= .02
V= 543.2
223. 32-1373
TiH1.5Na0.5{PO4}2*H2O
Triklin
Dexp Dcal d(D) h k l
11.0000 10.9720 .0280 0 0 1
6.2100 6.2204 -.0104 0 -2 1
5.8800 5.8885 -.0085 1 0 0
5.0600 5.0625 -.0025 1 1 1
4.6700 4.6686 .0014 1 2 0
4.2300 4.2299 .0001 0 3 0
3.7800 3.7792 .0008 0 -1 3
3.7300 3.7288 .0012 1 -2 2
3.6600 3.6573 .0027 0 0 3
3.1300 3.1302 -.0002 1 -2 3
3.1100 3.1102 -.0002 0 -4 2
3.0100 3.0097 .0003 -1 -4 1
A= 5.982 DA= .008
B= 13.211 DB= .002
C= 11.401 DC= .002
GAMMA= 83.29 DGAMMA= .04
BETA = 84.30 DBETA = .01
ALPHA=103.87 DALPHA= .01
V= 861.1
224. 32-1374
TiHNa{PO4}2*3H2O
Triklin
Dexp Dcal d(D) h k l
13.2000 13.2065 -.0065 1 0 0
6.7000 6.7114 -.0114 1 1 1
5.7500 5.7547 -.0047 -1 -1 1
4.6300 4.6273 .0027 0 0 2
4.2500 4.2494 .0006 3 1 1
3.9300 3.9305 -.0005 1 -2 1
3.6600 3.6617 -.0017 -3 0 1
3.5600 3.5607 -.0007 3 1 2
3.2400 3.2399 .0001 3 -1 2
3.1700 3.1700 -.0000 1 0 3
3.0900 3.0893 .0007 3 2 2
3.0300 3.0304 -.0004 4 1 2
A= 13.763 DA= .004
B= 9.512 DB= .003
C= 9.521 DC= .003
GAMMA= 80.42 DGAMMA= .01
BETA = 76.42 DBETA = .02
ALPHA= 87.22 DALPHA= .01
V= 1194.7
225. 32-1375
Ti{NaPO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
12.8000 12.8519 -.0519 1 0 0
6.3200 6.3180 .0020 1 1 1
5.6200 5.6266 -.0066 1 -1 1
4.4800 4.4839 -.0039 2 -1 1
4.2300 4.2321 -.0021 1 -2 1
4.0300 4.0302 -.0002 3 2 0
3.8900 3.8891 .0009 -2 2 0
3.5800 3.5790 .0010 1 1 2
3.5000 3.5001 -.0001 0 -1 2
3.3100 3.3115 -.0015 -1 -1 2
3.2100 3.2111 -.0011 4 2 0
3.1800 3.1809 -.0009 2 -1 2
A= 13.53 DA= .01
B= 12.419 DB= .004
C= 7.405 DC= .003
GAMMA= 74.36 DGAMMA= .02
BETA = 80.36 DBETA = .09
ALPHA= 87.93 DALPHA= .06
V= 1181.1
226. 32-1376
TiHSr0.5{PO4}2*3H2O
Triklin
Dexp Dcal d(D) h k l
13.4000 13.4244 -.0244 1 0 0
6.7200 6.7163 .0037 0 1 1
6.1900 6.1866 .0034 0 -1 1
5.1800 5.1812 -.0012 1 -1 1
5.0000 4.9951 .0049 0 1 2
4.4800 4.4812 -.0012 -1 1 2
4.4400 4.4462 -.0062 2 0 2
3.7000 3.6988 .0012 1 1 3
3.3700 3.3703 -.0003 -1 2 1
3.2900 3.2898 .0002 4 1 1
3.1800 3.1797 .0003 -1 -2 2
3.0800 3.0803 -.0003 -3 0 3
A= 13.9002 DA= .0004
B= 7.8505 DB= .0005
C= 12.335 DC= .004
GAMMA= 75.131 DGAMMA= .003
BETA = 90.89 DBETA = .01
ALPHA= 85.142 DALPHA= .006
V= 1295.3
227. 32-1384
C4H4O4Ti
Triklin
Dexp Dcal d(D) h k l
8.7300 8.7341 -.0041 -1 1 0
8.0400 8.0458 -.0058 1 1 0
7.3100 7.3332 -.0232 0 1 1
6.6200 6.6319 -.0119 -1 0 1
5.8600 5.8578 .0022 2 0 0
4.6700 4.6665 .0035 2 1 1
4.4900 4.4921 -.0021 -2 1 1
4.2000 4.2025 -.0025 1 0 2
3.8900 3.8929 -.0029 1 -1 2
3.7100 3.7085 .0015 3 0 1
3.3190 3.3159 .0031 -2 0 2
3.0560 3.0548 .0012 -2 2 2
A= 11.8126 DA= .0003
B= 12.0411 DB= .0001
C= 8.726 DC= .003
GAMMA= 94.193 DGAMMA= .004
BETA = 84.353 DBETA = .002
ALPHA= 85.208 DALPHA= .002
V=1226.8
228. 32-1385
C4H2Cl6O4Ti
Triklin
Dexp Dcal d(D) h k l
9.2100 9.2136 -.0036 1 0 0
7.6100 7.6031 .0069 1 1 1
5.9600 5.9604 -.0004 1 -1 1
5.4800 5.4792 .0008 0 0 2
4.9800 4.9733 .0067 0 1 2
4.6000 4.5987 .0013 2 1 2
4.4200 4.4286 -.0086 2 1 0
3.8850 3.8828 .0022 1 -2 1
3.5320 3.5318 .0002 0 1 3
3.3760 3.3733 .0027 3 1 1
3.2660 3.2650 .0010 1 3 1
3.1700 3.1706 -.0006 1 3 0
A= 10.40 DA= .01
B= 9.855 DB= .005
C= 12.28 DC= .01
GAMMA= 77.40 DGAMMA= .06
BETA = 63.76 DBETA = .08
ALPHA= 79.42 DALPHA= .07
V= 1096.0
229. 32-1929
C266H20Cl4O2Ti
Triklin
Dexp Dcal d(D) h k l
8.7800 8.7809 -.0009 1 0 0
7.8500 7.8507 -.0007 1 1 0
7.2000 7.1955 .0045 -1 0 1
6.5500 6.5536 -.0036 0 0 2
5.2800 5.2752 .0048 -1 1 0
5.0100 5.0117 -.0017 0 1 2
4.7000 4.6996 .0004 2 1 0
4.4500 4.4527 -.0027 -2 -1 1
4.1300 4.1258 .0042 -2 0 1
4.0200 4.0264 -.0064 0 2 1
3.6540 3.6569 -.0029 1 2 2
3.4970 3.5003 -.0033 1 -1 3
A= 9.484 DA= .006
B= 9.4744 DB= .0009
C= 13.17 DC= .04
GAMMA= 67.862 DGAMMA= .001
BETA = 90.43 DBETA = .09
ALPHA= 95.37 DALPHA= .07
V= 1090.9
260. 32-1930
C13H10Cl4OTi
Triklin
Dexp Dcal d(D) h k l
8.2100 8.2292 -.0192 0 1 1
7.6400 7.6333 .0067 1 0 0
7.0800 7.0708 .0092 0 -1 1
6.6600 6.6651 -.0051 1 0 1
5.7900 5.7931 -.0031 -1 1 0
5.2400 5.2296 .0104 -1 -1 1
5.0000 4.9975 .0025 -1 1 2
4.7500 4.7442 .0058 0 1 3
4.4100 4.4158 -.0058 -1 -1 2
4.1400 4.1435 -.0035 -1 1 3
3.7800 3.7790 .0010 1 2 0
3.5340 3.5354 -.0014 0 -2 2
A= 7.6478 DA= .0004
B= 8.901 DB= .002
C= 15.402 DC= .002
GAMMA= 91.337 DGAMMA= .008
BETA = 93.45 DBETA = .02
ALPHA= 79.946 DALPHA= .007
V= 1030.4
231. 32-1931
C10H18Cl2O4Ti
Triklin
Dexp Dcal d(D) h k l
12.1000 12.3562 -.2562 1 0 0
10.7000 10.7026 -.0026 1 1 0
8.8600 8.8724 -.0124 0 1 1
8.2000 8.2034 -.0034 0 -1 1
7.8000 7.7915 .0085 1 2 0
6.7300 6.7322 -.0022 -1 -1 1
6.4400 6.4467 -.0067 1 2 1
5.7100 5.7002 .0098 1 -2 1
5.5200 5.5220 -.0020 0 3 1
4.9300 4.9234 .0066 2 2 1
4.4200 4.4201 -.0001 0 4 1
4.1200 4.1187 .0013 3 0 0
A= 12.428 DA= .005
B= 19.112 DB= .008
C= 9.612 DC= .001
GAMMA= 85.52 DGAMMA= .02
BETA = 85.34 DBETA = .06
ALPHA= 84.08 DALPHA= .03
V= 2257.7
232. 32-1932
C6H10Cl2O4Ti
Triklin
Dexp Dcal d(D) h k l
8.2300 8.2473 -.0173 0 1 1
7.4500 7.4557 -.0057 -1 1 0
7.0700 7.0723 -.0023 0 -1 1
6.6400 6.6398 .0002 1 1 0
5.8900 5.8951 -.0051 -1 2 0
5.5500 5.5599 -.0099 1 0 1
5.2400 5.2394 .0006 1 1 1
4.7400 4.7441 -.0041 0 3 1
4.1600 4.1617 -.0017 -1 1 2
4.0300 4.0308 -.0008 0 -1 2
3.7100 3.7102 -.0002 1 -3 1
3.5430 3.5382 .0048 -1 -3 1
A= 8.0832 DA= .0003
B= 15.5659 DB= .0005
C= 9.01755 DC= .00004
GAMMA= 99.5020 DGAMMA= .0009
BETA = 98.475 DBETA = .002
ALPHA= 78.7293 DALPHA= .0003
V=1089.8
233. 32-1933
C6H10Cl2O4Ti
Triklin
Dexp Dcal d(D) h k l
9.2400 9.2192 .0208 0 1 1
8.2700 8.2704 -.0004 -1 0 1
7.6100 7.6110 -.0010 0 -1 1
7.0800 7.0823 -.0023 1 0 1
6.6400 6.6359 .0041 -1 -1 1
5.1000 5.0968 .0032 -1 1 2
4.5900 4.5900 .0000 1 1 2
4.1800 4.1848 -.0048 2 2 0
4.0200 4.0166 .0034 1 3 0
3.7140 3.7159 -.0019 0 3 2
3.4730 3.4729 .0001 2 -2 1
3.2220 3.2229 -.0009 -2 3 0
A= 10.710 DA= .003
B= 12.974 DB= .003
C= 11.276 DC= .001
GAMMA= 88.44 DGAMMA= .01
BETA = 98.41 DBETA = .01
ALPHA= 79.320 DALPHA= .005
V= 1520.8
234. 32-1934
C4H6Cl4N2Ti
Triklin
Dexp Dcal d(D) h k l
7.5500 7.5523 -.0023 0 1 1
6.5100 6.5065 .0035 1 0 0
5.9800 5.9728 .0072 -1 0 1
5.4000 5.4017 -.0017 1 0 1
4.7800 4.7783 .0017 -1 1 1
4.3800 4.3751 .0049 0 2 0
4.0800 4.0831 -.0031 1 0 2
3.3620 3.3622 -.0002 1 2 2
3.2530 3.2532 -.0002 2 0 0
3.0620 3.0609 .0011 2 1 1
2.8980 2.8979 .0001 -2 1 0
2.7590 2.7595 -.0005 2 2 1
A= 6.625 DA= .002
B= 8.956 DB= .002
C= 11.7154 DC= .0002
GAMMA= 81.445 DGAMMA= .003
BETA = 95.40 DBETA = .03
ALPHA= 82.09 DALPHA= .01
V= 676.2
265. 32-1934
C14H10Cl4Ti
Triklin
Dexp Dcal d(D) h k l
8.8500 8.8555 -.0055 1 0 0
7.0500 7.0484 .0016 0 1 0
4.8600 4.8563 .0037 0 1 1
4.2300 4.2305 -.0005 -1 -1 1
3.8190 3.8182 .0008 -1 2 0
3.5220 3.5242 -.0022 0 2 0
3.4100 3.4076 .0024 2 0 2
3.2290 3.2307 -.0017 2 1 0
3.0930 3.0955 -.0025 -1 2 1
2.9700 2.9709 -.0009 3 0 1
2.8550 2.8572 -.0022 1 0 3
2.6680 2.6672 .0008 1 -3 1
A= 10.139 DA= .001
B= 8.1795 DB= .0004
C= 9.26 DC= .01
GAMMA=117.133 DGAMMA= .007
BETA = 71.15 DBETA = .02
ALPHA=110.99 DALPHA= .04
V= 626.0
236. 32-1936
C3H3Cl5N2Ti
Triklin
Dexp Dcal d(D) h k l
6.5000 6.4984 .0016 0 1 1
5.9800 5.9806 -.0006 1 0 0
5.3800 5.3709 .0091 0 -1 1
4.7800 4.7773 .0027 -1 1 0
4.3700 4.3687 .0013 0 2 0
4.0800 4.0756 .0044 1 1 2
3.3640 3.3637 .0003 0 -1 2
3.2200 3.2191 .0009 2 0 1
3.0630 3.0619 .0011 -1 2 1
2.8790 2.8794 -.0004 2 -1 1
2.6780 2.6780 .0000 1 2 3
2.4680 2.4685 -.0005 0 2 3
2.3480 2.3482 -.0002 2 3 1
2.2430 2.2432 -.0002 2 -2 2
A= 6.518 DA= .002
B= 9.0083 DB= .0004
C= 8.732 DC= .004
GAMMA= 81.037 DGAMMA= .005
BETA = 66.920 DBETA = .009
ALPHA= 76.525 DALPHA= .009
V= 457.5
237. 32-1937
C4H6Cl4O3Ti
Triklin
Dexp Dcal d(D) h k l
6.2800 6.2768 .0032 0 1 1
5.9300 5.9353 -.0053 0 -1 1
5.6400 5.6363 .0037 1 1 0
5.3100 5.3048 .0052 -1 1 0
4.3400 4.3422 -.0022 1 1 1
3.5200 3.5131 .0069 -2 -1 1
3.3800 3.3810 -.0010 2 1 0
3.1600 3.1617 -.0017 1 1 2
3.0400 3.0407 -.0007 -1 -2 2
2.8970 2.8942 .0028 2 1 1
2.8150 2.8181 -.0031 2 2 0
2.7750 2.7753 -.0003 -2 0 3
A= 7.623 DA= .008
B= 8.425 DB= .001
C= 9.397 DC= .004
GAMMA= 87.40 DGAMMA= .06
BETA =109.11 DBETA = .02
ALPHA= 87.83 DALPHA= .01
V= 568.8
238. 32-1938
C4H4Cl6N2Ti
Triklin
Dexp Dcal d(D) h k l
7.8000 7.8071 -.0071 0 1 1
7.0500 7.0436 .0064 1 0 0
6.1400 6.1349 .0051 0 -1 1
5.3000 5.2969 .0031 1 1 2
4.6800 4.6781 .0019 1 2 1
4.5500 4.5452 .0048 1 -1 1
4.3900 4.3884 .0016 -1 1 1
4.1500 4.1517 -.0017 0 -1 2
3.8390 3.8444 -.0054 1 1 3
3.6150 3.6143 .0007 0 1 3
3.4950 3.4923 .0027 1 2 3
3.3640 3.3632 .0008 2 0 2
A= 7.780 DA= .003
B= 9.7586 DB= .006
C= 11.700 DC= .009
GAMMA= 69.53 DGAMMA= .03
BETA = 69.93 DBETA = .04
ALPHA= 70.63 DALPHA= .03
V= 758.7
239. 32-1939
C3H2Cl6N2Ti
Triklin
Dexp Dcal d(D) h k l
7.5300 7.5362 -.0062 1 0 0
5.9200 5.9164 .0036 0 1 0
5.1600 5.1607 -.0007 0 -1 2
4.7600 4.7599 .0001 1 -1 1
4.4800 4.4775 .0025 -1 1 1
4.4100 4.4109 -.0009 1 1 1
3.7510 3.7549 -.0039 -1 0 4
3.2320 3.2321 -.0001 -1 -1 4
2.9780 2.9798 -.0018 2 1 2
2.9130 2.9130 .0000 -2 -1 2
2.7980 2.7997 -.0017 -1 2 0
2.6960 2.6958 .0002 -1 -2 1
A= 7.5832 DA= .0008
B= 5.9448 DB= .0008
C= 18.457 DC= .007
GAMMA= 93.222 DGAMMA= .007
BETA = 84.248 DBETA = .002
ALPHA= 94.89 DALPHA= .03
V= 823.9
240. 32-1940
C4H2Cl8N2Ti
Triklin
Dexp Dcal d(D) h k l
9.4500 9.4511 -.0011 0 1 0
5.8600 5.8617 -.0017 1 1 0
5.4500 5.4502 -.0002 0 -1 2
4.7200 4.7255 -.0055 0 2 0
4.3700 4.3703 -.0003 0 -2 1
4.1200 4.1177 .0023 1 2 0
3.4020 3.4005 .0015 2 0 0
3.2000 3.1998 .0002 2 1 1
3.0350 3.0351 -.0001 1 0 4
2.8850 2.8839 .0011 -2 -2 1
2.7320 2.7319 .0001 -2 -2 2
2.6290 2.6288 .0002 -2 2 1
A= 6.872 DA= .001
B= 9.548 DB= .005
C= 14.29483 DC= .00017
GAMMA= 83.562 DGAMMA= .001
BETA = 94.656 DBETA = .009
ALPHA= 85.552 DALPHA= .001
V= 925.4
241. 32-1941
C8H5Cl5N2Ti
Triklin
Dexp Dcal d(D) h k l
8.7600 8.7669 -.0069 1 1 0
8.0500 8.0558 -.0058 0 -1 1
7.5500 7.5567 -.0067 -1 1 0
7.0600 7.0574 .0026 1 -1 1
6.5100 6.5168 -.0068 0 2 1
5.3600 5.3607 -.0007 1 0 2
4.8900 4.8889 .0011 0 3 1
4.5900 4.5893 .0007 2 -1 1
4.2300 4.2294 .0006 2 3 1
3.6600 3.6612 -.0012 -1 -1 2
3.5040 3.5029 .0011 1 2 3
3.4020 3.4020 -.0000 -1 -2 2
A= 10.5793 DA= .0001
B= 16.5328 DB= .0005
C= 10.9840 DC= .0003
GAMMA= 76.772 DGAMMA= .002
BETA = 64.104 DBETA = .002
ALPHA= 79.542 DALPHA= .002
V=1674.8
242. 32-1942
C4H12F5NTi*H2O
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.9500 6.9582 -.0082 1 1 0
6.5100 6.5055 .0045 0 1 1
4.5700 4.5700 -.0000 0 2 1
4.4900 4.4898 .0002 -2 0 1
4.4600 4.4597 .0003 2 0 0
4.0100 4.0104 -.0004 0 0 2
2.3570 2.3567 .0003 -3 0 3
a= 9.3200 b= 11.1220 c= 8.381 beta= 106.854
da= .0008 db=.0005 dc=.001 dbet=.002
V= 831.4