144. 23-0604
TiH{SO4}2*4H2O
Triklin
Dexp Dcal d(D) h k l
4.0000 4.0012 -.0012 1 1 1
3.3300 3.3309 -.0009 1 2 0
3.2600 3.2583 .0017 1 -1 1
3.0400 3.0401 -.0001 0 2 0
2.5660 2.5670 -.0010 2 2 1
2.3000 2.2995 .0005 -1 -2 2
2.1590 2.1578 .0012 3 0 1
2.1140 2.1155 -.0015 1 2 2
2.0560 2.0554 .0006 0 2 2
2.0260 2.0267 -.0007 0 3 0
1.7740 1.7751 -.0011 4 0 0
1.7500 1.7507 -.0007 -2 0 3
A= 7.806 DA= .002
B= 6.6863 DB= .0007
C= 5.8961 DC= .0003
GAMMA= 65.611 DGAMMA= .008
BETA = 94.579 DBETA = .002
ALPHA= 94.765 DALPHA= .003
V=279.0
145. 23-1243
Mn0.345Ti0.315Si0.340
Triklin
Dexp Dcal d(D) h k l
3.2600 3.2610 -.0010 -1 2 0
2.4090 2.4091 -.0001 2 1 2
2.3470 2.3478 -.0008 2 -1 2
2.2070 2.2079 -.0009 -1 3 0
2.1560 2.1558 .0002 0 2 2
2.1370 2.1370 .0000 1 2 2
2.0860 2.0861 -.0001 2 3 0
2.0490 2.0465 .0025 4 1 2
2.0250 2.0250 .0000 6 1 0
2.0140 2.0131 .0009 1 -3 1
1.8870 1.8890 -.0020 -4 -1 2
1.7880 1.7880 .0000 -7 1 0
A= 12.908 DA= .001
B= 6.6991 DB= .0004
C= 5.40749 DC= .00003
GAMMA= 91.61 DGAMMA= .03
BETA = 86.43 DBETA = .04
ALPHA= 87.01 DALPHA= .02
V=465.7
146. 23-1574
C10H28Br5CrN2O2
Triklin
Dexp Dcal d(D) h k l
11.0000 11.0045 -.0045 1 0 0
8.3000 8.2824 .0176 0 1 0
7.7600 7.7537 .0063 0 -1 1
5.4000 5.3963 .0037 -2 1 0
4.7900 4.7950 -.0050 2 -1 1
4.5300 4.5335 -.0035 0 0 2
4.0500 4.0530 -.0030 2 1 0
3.8800 3.8768 .0032 0 -2 2
3.8500 3.8491 .0009 -2 0 2
3.5800 3.5811 -.0011 -1 1 2
3.2800 3.2822 -.0022 -3 2 0
3.1200 3.1200 .0000 -2 -2 1
A= 11.574 DA= .004
B= 9.2666 DB= .0001
C= 9.8247 DC= .0006
GAMMA=104.97 DGAMMA= .01
BETA = 94.06 DBETA = .01
ALPHA=110.344 DALPHA= .001
V=939.9
147. 23-1575
C12H28Br5CrN2O2
Triklin
Dexp Dcal d(D) h k l
11.3000 11.3130 -.0130 1 0 0
10.9000 10.8919 .0081 0 1 1
9.5100 9.5225 -.0125 -1 0 1
8.6700 8.6945 -.0245 -1 1 0
7.3200 7.3134 .0066 -1 -1 1
6.9200 6.9318 -.0118 1 0 1
5.8300 5.8147 .0153 -2 0 1
5.6100 5.6085 .0015 -2 1 1
4.7000 4.7008 -.0008 1 1 2
4.2700 4.2662 .0038 2 2 1
4.1100 4.1144 -.0044 -1 1 3
3.7900 3.7869 .0031 -1 4 1
A= 11.893 DA= .001
B= 15.9404 DB= .0005
C= 12.397 DC= .007
GAMMA= 91.66 DGAMMA= .02
BETA =107.400 DBETA = .05
ALPHA= 70.301 DALPHA= .004
V=2104.0
148. 23-1940
C15H21I1.3O4.7Ti
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3042 .0058 1 0 0
6.6700 6.6911 -.0211 1 1 0
6.0500 6.0522 -.0022 -1 0 1
3.8300 3.8262 .0038 2 1 0
3.7100 3.7085 .0015 -1 -2 1
3.6000 3.5972 .0028 0 0 2
3.5200 3.5220 -.0020 0 1 2
3.3700 3.3693 .0007 -1 1 2
3.2500 3.2500 .0000 -1 2 0
3.2000 3.2000 .0000 -2 -2 1
2.9800 2.9796 .0004 1 3 0
2.7800 2.7800 -.0000 -1 2 2
2.5500 2.5505 -.0005 0 -2 2
2.4800 2.4804 -.0004 3 2 0
A= 7.953 DA= .001
B= 8.990 DB= .005
C= 7.523 DC= .005
GAMMA= 73.25 DGAMMA= .01
BETA =104.34 DBETA = .05
ALPHA= 85.55 DALPHA= .05
V= 492.5
149. 23-1941
C24H54O9P3Ti
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
16.0000 16.1100 -.1100 1 0 0
14.2000 14.2400 -.0400 0 1 0
7.6200 7.6215 -.0015 0 0 2
6.3700 6.3696 .0004 2 1 1
a=16.110 b=14.240 c=15.243
da= .001 db= .001 dc= .001
V=3496.8
150. 23-1942
C60H40As2N6S6Ti
Triklin
Dexp Dcal d(D) h k l
10.2000 10.1457 .0543 2 0 0
9.1000 9.0954 .0046 0 -1 0
8.3400 8.3602 -.0202 0 0 1
5.9000 5.9493 -.0493 2 0 1
7.7500 7.7463 .0037 -1 1 0
7.3800 7.2833 .0967 1 0 1
7.1300 7.1082 .0218 -2 0 1
6.7500 6.7638 -.0138 3 0 0
6.2400 6.2624 -.0224 -2 -1 1
5.6900 5.6910 -.0010 1 1 1
5.4700 5.4735 -.0035 -3 -1 1
5.1200 5.1212 -.0012 2 1 1
A= 21.128 DA= .001
B= 9.3460 DB= .0005
C= 8.5591 DC= .0005
GAMMA= 77.493 DGAMMA= .005
BETA =101.528 DBETA = .007
ALPHA= 96.846 DALPHA= .004
V=1611.3
151. 23-1943
C6H18O9P3Ti
Rombik
Groupa 34, 58
romb.
Dexp. Dcal. d(D) h k l
10.2000 10.1921 .0079 1 1 0
9.2100 9.3213 -.1113 2 0 0
6.3200 6.3251 -.0051 0 1 1
5.2400 5.2339 .0061 2 1 1
4.7700 4.7596 .0104 3 0 1
4.3500 4.3481 .0019 3 2 0
4.3500 4.3525 -.0025 4 1 0
3.7000 3.7015 -.0015 0 0 2
3.7000 3.7202 -.0202 2 3 0
3.7000 3.7003 -.0003 4 2 0
a=18.64 b=12.17 c= 7.403
da= .02 db= .09 dc= .003
V=1680
152. 23-1944
C6H18O12P3T
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
15.2000 15.4597 -.2597 0 0 1
12.8000 12.6151 .1849 1 0 1
10.8000 10.9117 -.1117 2 0 0
9.3000 9.2660 .0340 0 1 1
5.1500 5.1532 -.0032 0 0 3
4.5300 4.5291 .0009 3 2 0
3.5400 3.5406 -.0006 6 0 1
a=21.823 b=11.57 c=15.46
da= .006 db= .03 dc= .09
V=3905
153. 24-0126
BaTiO3
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
3.7100 3.7099 .0001 1 1 1
3.3600 3.3577 .0023 1 2 1
2.9300 2.9262 .0038 0 2 2
2.6400 2.6396 .0004 0 3 2
2.3700 2.3760 -.0060 1 5 0
2.2800 2.2793 .0007 0 6 0
2.0600 2.0587 .0013 1 6 0
1.9500 1.9483 .0017 1 1 3
1.8100 1.8093 .0007 1 7 0
1.7400 1.7426 -.0026 1 7 1
1.6700 1.6727 -.0027 0 7 2
1.5200 1.5195 .0005 0 9 0
1.4500 1.4486 .0014 1 9 0
1.3500 1.3500 -.0000 3 5 1
a= 4.797 b=13.68 c= 6.475
da= .003 db= .01 dc= .006
V= 424.8
154. 24-1237
SrTiF6
Triklin
Dexp Dcal d(D) h k l
10.7000 10.6917 .0083 0 0 1
6.7600 6.7566 .0034 1 1 0
4.8300 4.8303 -.0003 0 -2 1
4.6800 4.6838 -.0038 1 -2 1
4.2200 4.2217 -.0017 1 -2 2
3.9300 3.9289 .0011 2 -2 1
3.8800 3.8799 .0001 1 1 2
3.6800 3.6807 -.0007 -2 2 0
3.5400 3.5400 .0000 1 2 1
3.4200 3.4193 .0007 0 -2 3
3.3800 3.3783 .0017 2 2 0
3.1500 3.1521 -.0021 3 1 1
A= 11.205 DA= .004
B= 9.79993 DB= .00005
C= 11.4919 DC= .0009
GAMMA= 97.84 DGAMMA= .01
BETA = 80.780 DBETA = .006
ALPHA=110.40 DALPHA= .01
V= 1163.1
155. 26-1386
Na4Ti2Si8O22*5H2O
Triklin
Dexp Dcal d(D) h k l
9.2000 9.2055 -.0055 1 0 1
8.2000 8.1848 .0152 0 1 0
6.6200 6.6244 -.0044 -1 1 0
5.9700 5.9660 .0040 1 1 1
5.3200 5.3201 -.0001 0 0 2
4.6500 4.6507 -.0007 1 1 2
4.3800 4.3703 .0097 0 -1 2
4.1000 4.1032 -.0032 2 -1 2
3.9300 3.9264 .0036 2 1 2
3.4200 3.4225 -.0025 -2 -1 1
3.3700 3.3686 .0014 3 -1 1
3.3200 3.3179 .0021 0 2 2
A= 10.722 DA= .003
B= 8.225 DB= .001
C= 11.5221 DC= .0005
GAMMA= 94.98 DGAMMA= .03
BETA = 67.587 DBETA = .006
ALPHA= 89.49 DALPHA= .04
V= 934.7
156. 27-0574
Cs2Ti2O{SO4}4
Triklin
Dexp Dcal d(D) h k l
4.6000 4.6050 -.0050 -1 2 0
4.3400 4.3429 -.0029 0 0 1
4.0900 4.0865 .0035 0 -2 1
3.7400 3.7423 -.0023 -1 4 0
3.5000 3.5006 -.0006 -1 0 1
3.3600 3.3507 .0093 -1 5 0
3.1700 3.1653 .0047 1 0 1
3.0300 3.0324 -.0024 1 -2 1
2.9600 2.9605 -.0005 1 3 1
2.8800 2.8758 .0042 1 7 0
2.7300 2.7287 .0013 -1 5 1
2.6500 2.6528 -.0028 1 5 1
A= 5.18875 DA= .00004
B= 23.31708 DB= .00007
C= 4.36647 DC= .00001
GAMMA= 86.33265 DGAMMA= .00007
BETA = 95.9094 DBETA = .0001
ALPHA= 91.1415 DALPHA= .0002
V=524.3