1. 35-1192
YTa3O9
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
7.7500 7.7503 -.0003 0 2 0
3.8740 3.8751 -.0011 0 4 0
3.8410 3.8377 .0033 2 3 0
3.4320 3.4322 -.0002 1 1 1
2.7250 2.7268 -.0018 2 5 0
2.6880 2.6879 .0001 4 2 0
2.6060 2.6053 .0007 1 4 1
1.9380 1.9376 .0004 0 8 0
1.9150 1.9159 -.0009 3 7 0
1.8230 1.8232 -.0002 5 3 1
1.7974 1.7986 -.0012 0 2 2
1.7276 1.7281 -.0005 3 8 0
1.7203 1.7212 -.0009 1 3 2
1.5744 1.5730 .0014 1 5 2
1.5561 1.5557 .0004 5 6 1
a=11.4632 b=15.501 c= 3.698
da= .0006 db= .003 dc= .001
v= 657.1
2. 35-1193
alfa-Ta2O5
Triklin
Dexp Dcal d(D) h k l
3.7860 3.7871 -.0011 0 1 1
3.6180 3.6160 .0020 0 -1 1
3.3650 3.3653 -.0003 -1 1 1
3.0390 3.0399 -.0009 0 2 1
2.9760 2.9748 .0012 1 -1 1
2.4490 2.4490 .0000 -2 1 1
2.2540 2.2541 -.0001 2 0 1
2.2340 2.2335 .0005 -2 2 1
1.9530 1.9532 -.0002 -2 3 1
1.8940 1.8936 .0004 0 2 2
1.8440 1.8442 -.0002 1 1 2
1.6926 1.6926 -.0000 1 -2 2
A= 5.826 DA= .002
B= 8.497 DB= .001
C= 4.1443 DC= .0004
GAMMA= 93.73 DGAMMA= .02
BETA = 96.35 DBETA = .03
ALPHA= 86.253 DALPHA= .001
V= 203.1
3. 35-1226
Ta6Br12{OH}2*8H2O
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
9.0300 9.0543 -.0243 1 0 0
8.3900 8.4617 -.0717 1 0 1
7.9400 7.9265 .0135 0 0 3
7.2700 7.2034 .0666 1 0 2
4.5500 4.5582 -.0082 0 1 0
4.2100 4.2104 -.0004 1 0 5
3.1860 3.1832 .0028 2 1 1
3.0170 3.0181 -.0011 3 0 0
2.6420 2.6422 -.0002 0 0 9
a= 9.05 b= 4.558 c=23.78
da= .01 db= .004 dc= .01
V= 981
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.0300 9.1005 -.0705 0 1 0
8.3900 8.4150 -.0250 1 0 0
7.9400 7.9263 .0137 0 0 1
7.2700 7.2602 .0098 1 0 1
4.5500 4.5503 -.0003 0 2 0
4.2100 4.2075 .0025 2 0 0
3.1860 3.1852 .0008 2 2 1
3.0170 3.0177 -.0007 3 0 1
2.6420 2.6421 -.0001 0 0 3
a=9.054 b=9.10 c= 8.53 beta=68.3
da=.006 db=.03 dc=.04 dbeta=.4
V= 653
4. 36-0055
TaH{PO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
10.2800 10.1692 .1108 0 0 1
5.2200 5.2192 .0008 1 0 0
4.3500 4.3505 -.0005 1 1 1
3.8700 3.8676 .0024 -1 -1 1
3.1400 3.1388 .0012 0 -1 3
2.9700 2.9704 -.0004 0 -2 2
2.5400 2.5399 .0001 1 0 4
2.1710 2.1710 .0000 -2 1 1
2.0900 2.0910 -.0010 2 0 4
2.0150 2.0148 .0002 2 -2 1
1.9730 1.9730 -.0000 1 1 5
1.9330 1.9338 -.0008 -2 -2 2
A= 5.416 DA= .002
B= 7.008 DB= .005
C= 10.490 DC= .001
GAMMA= 83.22 DGAMMA= .06
BETA = 76.44051 DBETA = .00002
ALPHA= 92.51 DALPHA= .02
V= 383.3
5. 36-0056
TaH{PO4}2
Triklin
Dexp Dcal d(D) h k l
6.6600 6.6583 .0017 0 1 0
4.4000 4.4024 -.0024 0 -1 2
3.6800 3.6810 -.0010 -1 -1 1
3.3300 3.3291 .0009 0 2 0
3.0700 3.0683 .0017 1 1 1
2.9000 2.8979 .0021 1 0 2
2.7900 2.7912 -.0012 -1 -2 1
2.6500 2.6488 .0012 1 2 0
2.3900 2.3909 -.0009 -1 -2 3
2.2010 2.2012 -.0002 0 -2 4
2.0940 2.0942 -.0002 -1 -3 1
1.9850 1.9851 -.0001 -2 -1 2
A= 4.2015 DA= .0003
B= 7.02644 DB= .00001
C= 9.4913 DC= .0008
GAMMA= 85.738 DGAMMA= .002
BETA = 97.1863 DBETA = .0007
ALPHA=108.521 DALPHA= .001
V=263.4
6. 36-0057
Ta4{PO4}6*O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.8000 4.8028 -.0028 2 0 0
3.8500 3.8471 .0029 1 1 0
3.5600 3.5545 .0055 1 0 4
3.1600 3.1610 -.0010 2 1 0
2.5800 2.5812 -.0012 2 0 5
2.4200 2.4158 .0042 3 1 2
2.2810 2.2781 .0029 3 1 3
2.1270 2.1259 .0011 1 1 6
2.0100 2.0112 -.0012 4 1 2
1.9570 1.9574 -.0004 3 1 5
1.8010 1.8020 -.0010 3 1 6
1.7460 1.7469 -.0009 5 1 0
a= 9.606 b= 4.199 c=15.304
da= .006 db= .004 dc= .009
V= 617
Triklin
Dexp Dcal d(D) h k l
4.8000 4.7942 .0058 0 1 1
3.8500 3.8498 .0002 -1 1 0
3.5600 3.5602 -.0002 -1 0 1
3.1600 3.1596 .0004 -1 1 1
2.5800 2.5808 -.0008 -1 -2 1
2.4200 2.4205 -.0005 0 3 0
2.2810 2.2807 .0003 -2 -1 1
2.1270 2.1274 -.0004 1 -1 2
2.0100 2.0094 .0006 -1 3 0
1.9570 1.9563 .0007 1 4 1
1.8010 1.8009 .0001 3 0 0
1.7460 1.7452 .0008 0 0 3
A= 5.732 DA= .002
B= 7.858 DB= .001
C= 5.477 DC= .002
GAMMA= 71.59 DGAMMA= .01
BETA = 78.98 DBETA = .03
ALPHA= 74.24 DALPHA= .01
V= 223.8
7. 36-0199
TaOPO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6700 5.6725 -.0025 -1 1 1
4.3300 4.3316 -.0016 -1 0 2
4.1700 4.1733 -.0033 1 2 2
3.9100 3.9111 -.0011 2 2 0
3.7230 3.7230 -.0000 0 3 0
3.2900 3.2924 -.0024 -2 0 2
2.8720 2.8741 -.0021 4 1 1
2.7930 2.7923 .0007 0 4 0
2.7400 2.7396 .0004 4 0 0
2.6560 2.6547 .0013 0 3 3
2.6010 2.6006 .0004 -3 0 2
2.5220 2.5222 -.0002 2 0 5
a= 12.169 b=11.1691 c=12.614 beta= 64.22
da=.001 db=.0008 dc=.003 dbeta=.03
V= 1544
Triklin
Dexp Dcal d(D) h k l
5.6700 5.6689 .0011 1 2 0
4.3300 4.3285 .0015 3 0 0
4.1700 4.1765 -.0065 -1 1 1
3.9100 3.9145 -.0045 -3 1 0
3.7230 3.7223 .0007 3 2 0
3.2900 3.2928 -.0028 1 -2 1
2.8720 2.8720 .0000 -2 -3 1
2.7930 2.7950 -.0020 -4 -1 1
2.7400 2.7393 .0007 -2 3 1
2.6560 2.6549 .0011 -3 -3 1
2.6010 2.6017 -.0007 3 4 0
2.6010 2.6017 -.0007 3 4 0
A= 13.1836 DA= .0004
B= 11.964 DB= .001
C= 4.5954 DC= .0001
GAMMA= 83.1085 DGAMMA= .0001
BETA = 97.018 DBETA = .002
ALPHA= 89.028 DALPHA= .002
V=714.4
8. 36-0200
Ta{PO4}2*H2O
Triklin
Dexp Dcal d(D) h k l
6.7300 6.7336 -.0036 -1 1 0
4.5340 4.5295 .0045 1 1 0
4.4440 4.4530 -.0090 0 1 1
3.7880 3.7879 .0001 2 0 0
3.7230 3.7295 -.0065 0 2 0
3.6540 3.6589 -.0049 -2 1 1
3.3460 3.3470 -.0010 -1 -1 2
3.0960 3.0927 .0033 -2 -1 1
2.6810 2.6812 -.0002 -3 1 1
2.5940 2.5937 .0003 -3 2 0
2.5380 2.5354 .0026 2 -3 1
2.4230 2.4244 -.0014 1 -3 2
A= 8.2722 DA= .0007
B= 8.28718 DB= .00004
C= 7.381 DC= .001
GAMMA=109.09 DGAMMA= .01
BETA = 98.604 DBETA = .004
ALPHA=103.657 DALPHA= .007
V=450.2
9. 36-0202
Ta2{PO4}2P2O7
Triklin
Dexp Dcal d(D) h k l
7.6200 7.6178 .0022 1 0 0
5.0600 5.0560 .0040 -1 1 0
4.8600 4.8612 -.0012 -1 -1 2
3.9800 3.9805 -.0005 -1 0 2
3.9400 3.9386 .0014 1 -1 2
3.8100 3.8089 .0011 2 0 0
3.6600 3.6614 -.0014 1 -2 1
3.5500 3.5495 .0005 -2 0 1
3.2300 3.2296 .0004 -2 -3 1
3.1300 3.1301 -.0001 2 -1 1
3.0200 3.0200 -.0000 0 3 0
2.6900 2.6904 -.0004 3 1 0
A= 8.300 DA= .001
B= 11.285 DB= .003
C= 10.801 DC= .009
GAMMA= 66.653 DGAMMA= .005
BETA =103.08 DBETA = .03
ALPHA=121.57 DALPHA= .03
V=791.4
10. 36-0919
Ta6Br12*xH2O
Triklin
Dexp Dcal d(D) h k l
9.0600 9.0660 -.0060 0 1 1
8.3600 8.3534 .0066 1 0 0
6.8800 6.8829 -.0029 0 -1 1
6.7300 6.7225 .0075 0 2 0
6.2300 6.2358 -.0058 1 2 0
6.0800 6.0754 .0046 -1 0 1
5.6100 5.6144 -.0044 -1 -1 1
4.1800 4.1767 .0033 2 0 0
4.1200 4.1206 -.0006 0 -1 2
3.6840 3.6861 -.0021 -2 1 0
3.5450 3.5448 .0002 -1 3 1
3.4420 3.4415 .0005 0 -2 2
A= 8.8846 DA= .0007
B= 14.887 DB= .005
C= 10.0397 DC= .0006
GAMMA= 70.44 DGAMMA= .01
BETA = 80.45 DBETA = .02
ALPHA= 71.31 DALPHA= .03
V=1181
11. 36-0921
Ta6Cl12{OH}2*8H2O
Triklin
Dexp Dcal d(D) h k l
8.4300 8.4407 -.0107 0 1 1
7.8200 7.8264 -.0064 0 -1 1
7.6000 7.5954 .0046 1 0 1
6.9300 6.9099 .0201 1 1 0
6.8200 6.8121 .0079 1 1 1
5.8300 5.8248 .0052 -1 -1 1
5.6500 5.6532 -.0032 1 1 2
4.3400 4.3411 -.0011 -1 1 2
4.2600 4.2579 .0021 0 -1 3
4.0000 4.0019 -.0019 2 1 0
3.9110 3.9132 -.0022 0 -2 2
3.8210 3.8196 .0014 -1 2 0
A= 8.3322 DA= .0002
B= 9.9886 DB= .0007
C= 15.1171 DC= .0002
GAMMA= 77.191 DGAMMA= .005
BETA = 79.150 DBETA = .004
ALPHA= 83.084 DALPHA= .004
V=1202
12. 37-0779
TaOCl3
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
5.3700 5.3705 -.0005 0 0 3
4.8200 4.8303 -.0103 1 0 3
3.5600 3.5608 -.0008 0 1 0
2.9700 2.9678 .0022 0 1 3
2.7200 2.7183 .0017 3 0 4
2.6100 2.6093 .0007 1 0 6
2.4400 2.4400 .0000 3 1 2
2.1600 2.1607 -.0007 3 1 4
1.8920 1.8922 -.0002 2 0 8
a=11.051 b= 3.5608 c=16.111
da= .001 db= .0001 dc= .002
V= 634.0
13. 38-0204
NaTa{PO4}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.9300 7.9305 -.0005 1 1 0
4.7100 4.7102 -.0002 2 1 2
4.4600 4.4590 .0010 -1 0 2
4.3000 4.2973 .0027 -2 0 1
3.7100 3.7100 .0000 0 1 3
3.3600 3.3586 .0014 -2 0 2
3.1100 3.1125 -.0025 -3 0 1
2.9300 2.9294 .0006 -1 3 2
2.6100 2.6103 -.0003 0 4 2
2.5200 2.5202 -.0002 -1 1 4
2.4300 2.4298 .0002 -4 0 1
2.1400 2.1399 .0001 5 2 1
a= 11.831 b=11.657 c= 12.837 beta= 66.14
da=.003 db=.001 dc=.003 dbeta=.01
V= 1619
14. 38-0205
CsTa{PO4}
Triklin
Dexp Dcal d(D) h k l
8.8400 8.8378 .0022 1 0 0
4.4400 4.4417 -.0017 0 2 1
4.4300 4.4306 -.0006 -2 0 1
4.4200 4.4189 .0011 2 0 0
4.0900 4.0901 -.0001 -1 2 1
4.0400 4.0382 .0018 -2 1 1
3.9700 3.9738 -.0038 -2 -1 1
3.3300 3.3283 .0017 2 1 1
3.1700 3.1693 .0007 0 3 1
3.0900 3.0907 -.0007 1 3 0
3.0000 3.0003 -.0003 1 1 2
2.6000 2.6008 -.0008 0 -3 1
2.5300 2.5286 .0014 -2 -3 1
A= 9.370 DA= .002
B= 9.725 DB= .002
C= 7.449 DC= .004
GAMMA= 86.14 DGAMMA= .01
BETA =107.575 DBETA = .006
ALPHA= 76.958 DALPHA= .006
V= 623.7
15. 38-0611
TaOCl2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.2200 6.2173 .0027 1 1 0
3.6500 3.6480 .0020 1 2 0
3.2100 3.2097 .0003 0 0 3
2.6000 2.5998 .0002 2 1 3
2.3300 2.3299 .0001 -1 0 4
1.9590 1.9590 .0000 5 1 1
1.9150 1.9151 -.0001 3 3 2
1.8310 1.8311 -.0001 -1 1 5
1.6670 1.6670 .0000 0 4 3
a=10.2933 b= 7.80289 c= 9.633 beta=88.42
da=.0003 db=.000001 dc=.001 dbeta=.02
V= 773.4
16. 39-0029
ScTaO4
Triklin
Dexp Dcal d(D) h k l
3.3330 3.3339 -.0009 0 1 1
3.1290 3.1298 -.0008 0 -1 1
2.6050 2.6034 .0016 -1 0 2
2.3650 2.3644 .0006 -1 -1 1
2.0740 2.0735 .0005 -1 -1 3
1.9190 1.9205 -.0015 -1 1 0
1.7540 1.7541 -.0001 1 1 5
1.7410 1.7405 .0005 -1 1 4
1.6700 1.6701 -.0001 0 2 0
1.6010 1.6010 .0000 1 2 0
1.4980 1.4978 .0002 0 -1 7
1.4100 1.4102 -.0002 -1 0 8
A= 2.8375 DA= .0007
B= 3.4536 DB= .0005
C= 12.619 DC= .001
GAMMA= 77.174 DGAMMA= .003
BETA = 93.199 DBETA = .009
ALPHA= 83.647 DALPHA= .009
V= 119.4
17. 39-0114
LiTa{PO4}2
Triklin
Dexp Dcal d(D) h k l
7.6900 7.7211 -.0311 1 0 0
4.6200 4.6108 .0092 0 1 1
4.3900 4.3916 -.0016 0 -1 1
4.2600 4.2656 -.0056 -1 0 1
4.1300 4.1199 .0101 1 -1 1
3.9300 3.9341 -.0041 1 1 1
3.8600 3.8606 -.0006 2 0 0
3.7200 3.7190 .0010 -2 1 0
3.1100 3.1127 -.0027 1 -2 1
3.0200 3.0187 .0013 -2 0 1
2.6600 2.6591 .0009 0 3 0
2.6100 2.6103 -.0003 -2 2 1
2.4400 2.4402 -.0002 0 3 1
A= 7.854 DA= .003
B= 8.090 DB= .001
C= 5.47 DC= .01
GAMMA= 99.09 DGAMMA= .02
BETA = 85.05 DBETA = .04
ALPHA= 87.84 DALPHA= .02
V= 341.6
18. 39-0115
KTa{PO4}2
Triklin
Dexp Dcal d(D) h k l
8.0000 8.0193 -.0193 1 0 0
4.3900 4.3867 .0033 -1 1 0
4.2300 4.2253 .0047 0 1 1
4.0100 4.0096 .0004 2 0 0
3.9200 3.9207 -.0007 1 1 0
3.6700 3.6738 -.0038 2 0 1
3.1100 3.1128 -.0028 0 1 2
3.0100 3.0110 -.0010 -2 1 1
2.9200 2.9186 .0014 -1 1 2
2.8500 2.8501 -.0001 1 -1 2
2.5900 2.5884 .0016 3 0 1
2.4800 2.4794 .0006 -2 1 2
2.3300 2.3306 -.0006 -3 1 1
A= 8.105 DA= .003
B= 4.8741 DB= .0004
C= 7.69 DC= .01
GAMMA= 96.98 DGAMMA= .05
BETA = 85.94 DBETA = .09
ALPHA= 86.29 DALPHA= .01
V= 300.1
19. 39-0116
RbTa{PO4}2
Rombik
Groupa 33,49,62
romb.
Dexp. Dcal. d(D) h k l
8.3400 8.3372 .0028 1 1 0
4.4400 4.4362 .0038 0 2 0
4.2900 4.2724 .0176 5 1 0
4.1900 4.1945 -.0045 0 1 1
3.9700 3.9662 .0038 2 1 1
3.7300 3.7271 .0029 3 1 1
3.0900 3.0900 -.0000 6 0 1
2.9900 2.9960 -.0060 6 2 0
2.9200 2.9181 .0019 6 1 1
2.5900 2.5902 -.0002 9 1 0
2.5100 2.5115 -.0015 8 2 0
2.4000 2.4000 .0000 3 3 1
2.2100 2.2090 .0010 1 4 0
a=24.37 b= 8.872 c= 4.7601
da= .01 db= .006 dc= .0001
V=1029.4
20. 39-0404
RbTaF11
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7500 4.7460 .0040 2 1 0
3.7360 3.7373 -.0013 2 2 1
3.6860 3.6838 .0022 -2 1 2
3.6220 3.6203 .0017 0 0 4
3.4710 3.4716 -.0006 3 0 2
3.3620 3.3631 -.0011 3 1 0
3.3120 3.3137 -.0017 2 0 4
3.2400 3.2389 .0011 -1 0 4
3.1760 3.1757 .0003 3 0 3
2.9740 2.9740 -.0000 3 2 1
2.6250 2.6248 .0002 -3 0 3
2.1480 2.1481 -.0001 -2 2 5
a= 10.871 b=10.437 c= 14.771 beta= 78.62
da= .007 db=.004 dc=.003 dbeta=.05
V= 1643
Triklin
Dexp Dcal d(D) h k l
4.7500 4.7511 -.0011 0 -1 1
3.7360 3.7360 .0000 -1 -1 3
3.6860 3.6862 -.0002 0 -1 3
3.6220 3.6229 -.0009 1 -1 2
3.4710 3.4702 .0008 -2 -1 2
3.3620 3.3658 -.0038 2 1 0
3.3120 3.3095 .0025 0 1 3
3.2400 3.2401 -.0001 -1 -1 4
3.1760 3.1737 .0023 1 0 4
2.9740 2.9748 -.0008 -2 -1 4
2.6250 2.6267 -.0017 -1 0 6
2.1480 2.1481 -.0001 -4 0 5
A= 9.577 DA= .001
B= 4.8680 DB= .0007
C= 15.878 DC= .005
GAMMA= 86.50 DGAMMA= .01
BETA =107.25 DBETA = .05
ALPHA= 96.93 DALPHA= .03
V= 701.6
21. 39-0677
CsTaO{ClO4}4
Triklin
Dexp Dcal d(D) h k l
5.3187 5.3240 -.0053 0 1 1
5.2557 5.2554 .0003 1 0 1
4.1788 4.1800 -.0012 0 -1 1
3.8229 3.8263 -.0034 0 2 0
3.7340 3.7339 .0001 1 2 0
3.5572 3.5575 -.0003 2 -1 1
3.4884 3.4866 .0018 1 2 1
3.0496 3.0516 -.0020 4 1 1
2.9642 2.9641 .0001 -1 0 2
2.7686 2.7680 .0006 4 -1 1
2.6626 2.6620 .0006 0 2 2
2.5283 2.5276 .0007 1 3 1
2.4087 2.4086 .0001 -5 1 2
2.2871 2.2869 .0002 -6 2 1
2.1342 2.1347 -.0005 -3 3 2
A= 16.624 DA= .002
B= 7.89874 DB= .00007
C= 6.120 DC= .001
GAMMA= 91.794 DGAMMA= .004
BETA = 99.310 DBETA = .004
ALPHA= 75.672 DALPHA= .008
V=768.1
22. 39-0678
TaO{ClO4}3
Triklin
Dexp Dcal d(D) h k l
3.9015 3.9060 -.0045 1 1 0
3.6519 3.6550 -.0031 1 2 0
3.4861 3.4847 .0014 0 0 1
3.2092 3.2104 -.0012 0 -2 1
3.1651 3.1633 .0018 1 0 1
3.0147 3.0106 .0041 1 2 1
2.7439 2.7454 -.0015 1 -3 1
2.6108 2.6127 -.0019 1 4 1
2.5112 2.5124 -.0012 0 5 1
2.3808 2.3800 .0008 1 6 0
2.0292 2.0292 .0000 2 0 1
1.9581 1.9576 .0005 0 9 0
1.7615 1.7618 -.0003 0 10 0
1.7047 1.7045 .0002 -1 7 1
1.6052 1.6052 .0000 0 -4 2
A= 4.20799 DA= .00001
B= 17.62900 DB= .00002
C= 3.67210 DC= .00000
GAMMA= 88.7376 DGAMMA= .0001
BETA = 71.6869 DBETA = .0001
ALPHA= 88.11455 DALPHA= .00006
V=258.4
23. 39-0679
TaO2ClO4
Triklin
Dexp Dcal d(D) h k l
8.8073 8.8110 -.0037 1 0 0
4.1942 4.1939 .0003 -1 1 1
4.0621 4.0640 -.0019 -2 0 1
3.8671 3.8653 .0018 1 1 1
3.6713 3.6720 -.0007 -1 0 2
3.4582 3.4580 .0002 -2 -1 1
2.8453 2.8446 .0007 -1 -2 1
2.4625 2.4632 -.0007 3 -1 1
2.3815 2.3812 .0003 2 1 2
2.3371 2.3369 .0002 -2 0 3
2.0631 2.0631 .0000 -4 1 1
1.8737 1.8737 -.0000 0 -1 4
1.8543 1.8545 -.0002 1 3 1
1.8098 1.8097 .0001 -4 2 0
A= 8.8990 DA= .0002
B= 6.18709 DB= .00007
C= 7.70471 DC= .00005
GAMMA= 90.364 DGAMMA= .001
BETA = 97.9653 DBETA = .0002
ALPHA= 96.7021 DALPHA= .0001
V=417.1
24. 39-0680
Cs{ClO4}6
Triklin
Dexp Dcal d(D) h k l
5.2815 5.2784 .0031 1 1 0
5.1782 5.1724 .0058 0 1 1
4.1151 4.1138 .0013 0 -1 1
3.7641 3.7600 .0041 1 2 1
3.5842 3.5796 .0046 0 2 0
3.3912 3.3956 -.0044 1 2 0
3.2902 3.2941 -.0039 -1 1 1
3.1877 3.1867 .0010 -1 -1 1
3.0915 3.0924 -.0009 2 2 1
2.9785 2.9789 -.0004 0 1 2
2.7888 2.7899 -.0011 0 -2 1
2.4990 2.4987 .0003 -1 -2 1
2.4186 2.4180 .0006 -2 0 1
2.3851 2.3850 .0001 2 -1 2
A= 7.5572 DA= .0003
B= 7.7563 DB= .0005
C= 6.99554 DC= .00001
GAMMA= 71.500 DGAMMA= .003
BETA = 60.063 DBETA = .001
ALPHA= 69.712 DALPHA= .003
V= 328.0
25. 39-1093
LiTa2PdSe6
Rombik
Groupa 50
Dexp. Dcal. d(D) h k l
6.8463 6.8483 -.0020 0 0 3
3.4848 3.4849 -.0001 1 1 3
3.0114 3.0114 .0000 0 2 0
2.9350 2.9350 .0000 0 0 7
2.2619 2.2613 .0006 0 2 6
2.1291 2.1291 .0000 2 1 5
a= 5.468 b= 6.023 c=20.545
da= .001 db= .001 dc= .001
V= 676.6
26. 40-0575
Ta3O7Cl
Triklin
Dexp Dcal d(D) h k l
13.1750 13.1594 .0156 1 0 0
9.5510 9.5413 .0097 -1 0 1
5.4620 5.4622 -.0002 1 1 0
4.4590 4.4596 -.0006 -1 -1 2
3.9470 3.9489 -.0019 -1 1 2
3.7310 3.7300 .0010 0 1 3
3.6520 3.6497 .0023 -1 0 4
3.5330 3.5315 .0015 3 1 2
3.2890 3.2898 -.0008 4 0 0
3.1550 3.1547 .0003 -3 1 0
3.0880 3.0893 -.0013 4 1 1
2.9670 2.9667 .0003 -3 -1 3
A= 13.491 DA= .003
B= 5.61125 DB= .00008
C= 15.855 DC= .006
GAMMA= 79.333 DGAMMA= .006
BETA = 83.32 DBETA = .01
ALPHA= 90.87 DALPHA= .01
V= 1170.6
27. 40-0665
Ta{ClO4}5
Triklin
Dexp Dcal d(D) h k l
8.2372 8.2445 -.0073 -1 0 1
7.6152 7.6132 .0020 0 1 0
7.2441 7.2440 .0001 0 1 1
7.0015 6.9939 .0076 -1 1 0
5.8021 5.8062 -.0041 -1 0 2
5.6149 5.6138 .0011 -1 1 2
5.2362 5.2326 .0036 1 0 2
4.0125 4.0128 -.0003 -1 -1 2
3.8915 3.8921 -.0006 1 0 3
3.8620 3.8615 .0005 0 2 1
3.4671 3.4670 .0001 -2 0 3
3.1041 3.1042 -.0001 2 0 3
2.7526 2.7525 .0001 -1 1 5
2.7147 2.7147 -.0000 -1 3 1
A= 10.147 DA= .002
B= 8.156 DB= .001
C= 13.882 DC= .002
GAMMA=108.02 DGAMMA= .01
BETA =100.04 DBETA = .01
ALPHA= 76.52 DALPHA= .01
V= 1056.0
28. 40-0666
Cs2Ta{ClO4}7
Triklin
Dexp Dcal d(D) h k l
4.1904 4.1907 -.0003 1 2 0
3.8261 3.8263 -.0002 2 -1 1
3.7433 3.7427 .0006 3 0 0
3.5656 3.5651 .0005 -2 0 1
3.3688 3.3690 -.0002 2 2 0
3.0639 3.0642 -.0003 -2 -1 1
2.9796 2.9791 .0005 1 3 0
2.7888 2.7882 .0006 3 -2 1
2.6859 2.6854 .0005 4 0 1
2.5381 2.5388 -.0007 -2 -2 1
2.4175 2.4167 .0008 -4 1 1
2.3468 2.3470 -.0002 1 3 2
2.2915 2.2924 -.0009 -5 1 0
2.2475 2.2472 .0003 4 2 0
A= 11.56351 DA= .00009
B= 10.2980 DB= .0003
C= 5.5688 DC= .0002
GAMMA= 99.501 DGAMMA= .001
BETA = 82.5700 DBETA = .0008
ALPHA= 76.401 DALPHA= .001
V=626.2
29. 40-0701
N2H5TaF6
Triklin
Dexp Dcal d(D) h k l
7.4000 7.4003 -.0003 0 1 1
6.8000 6.7934 .0066 -1 0 1
6.1000 6.1178 -.0178 0 -1 1
5.3400 5.3384 .0016 -1 1 1
5.0600 5.0665 -.0065 -1 1 0
4.6000 4.5836 .0164 1 2 0
4.1700 4.1589 .0111 -1 -1 2
3.9800 3.9770 .0030 1 2 1
3.6800 3.6829 -.0029 -2 0 1
3.5200 3.5197 .0003 2 1 0
3.4200 3.4220 -.0020 -1 2 2
3.3200 3.3218 -.0018 -2 -1 2
A= 7.51428 DA= .00003
B= 10.2523 DB= .0001
C= 9.78233 DC= .00007
GAMMA= 78.6191 DGAMMA= .0001
BETA =109.6967 DBETA = .0003
ALPHA= 83.8229 DALPHA= .0005
V=683.1
30. 40-0702
NHTaF6
Triklin
Dexp Dcal d(D) h k l
7.4100 7.4372 -.0272 -1 0 1
5.2900 5.2918 -.0018 0 1 1
4.9000 4.8986 .0014 0 -1 1
4.7000 4.7009 -.0009 -1 0 3
4.4500 4.4484 .0016 1 -1 1
4.2600 4.2607 -.0007 1 0 3
4.1000 4.1000 -.0000 1 1 0
3.7200 3.7186 .0014 -2 0 2
3.5100 3.5103 -.0003 -2 1 0
3.0300 3.0303 -.0003 2 -1 2
2.8940 2.8937 .0003 -2 -1 1
2.8190 2.8198 -.0008 -1 -1 4
A= 8.138 DA= .001
B= 5.5117 DB= .0004
C= 16.491 DC= .005
GAMMA=101.59 DGAMMA= .01
BETA = 97.623 DBETA = .002
ALPHA= 81.249 DALPHA= .001
V= 712.2
31. 40-1027
LiTa2PdSe6
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
10.7600 10.7709 -.0109 0 1 0
9.4007 9.4659 -.0652 0 1 1
6.6169 6.6133 .0036 0 0 3
5.7563 5.7589 -.0026 1 0 0
2.8483 2.8496 -.0013 2 0 1
2.4225 2.4210 .0015 1 4 1
2.3317 2.3305 .0012 2 0 5
2.2403 2.2406 -.0003 1 3 6
2.1711 2.1715 -.0004 2 0 6
2.0175 2.0176 -.0001 1 5 0
a= 5.759 b=10.771 c=19.84
da= .004 db= .003 dc= .03
V=1231
32. 43-0951
Pb2BiTaO6
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
3.0300 3.0358 -.0058 1 0 0
2.7900 2.7915 -.0015 1 0 2
2.3700 2.3679 .0021 0 0 6
1.9800 1.9819 -.0019 0 1 6
1.8100 1.8110 -.0010 0 2 0
1.8000 1.8001 -.0001 1 1 5
1.6600 1.6596 .0004 1 1 6
1.5200 1.5193 .0007 1 2 2
a= 3.0357 b= 3.6219 c=14.207
da= .0001 db= .0005 dc= .001
V= 156.22
33. 44-0999
Na2Ta2{SO4}6*xH2O
Triklin
Dexp Dcal d(D) h k l
5.0500 5.0521 -.0021 1 0 1
4.5400 4.5390 .0010 0 1 0
3.5100 3.5090 .0010 1 0 2
3.1700 3.1713 -.0013 -1 -1 1
2.8700 2.8706 -.0006 -1 1 1
2.7800 2.7797 .0003 2 1 0
2.4300 2.4315 -.0015 1 2 2
2.3400 2.3385 .0015 1 -1 2
2.1000 2.0995 .0005 -1 0 3
2.0300 2.0283 .0017 3 1 2
1.9310 1.9315 -.0005 3 1 0
1.9000 1.9000 -.0000 0 1 4
A= 6.182 DA= .001
B= 5.081 DB= .002
C= 8.198 DC= .002
GAMMA= 66.93 DGAMMA= .03
BETA = 70.36 DBETA = .02
ALPHA= 70.19 DALPHA= .03
V= 216.6
34. 44-1039
K2TaF7
Triklin
Dexp Dcal d(D) h k l
5.3100 5.3149 -.0049 -1 0 2
5.1800 5.1746 .0054 0 1 1
5.1100 5.1091 .0009 0 -1 1
4.9000 4.9066 -.0066 -1 1 1
4.6000 4.5926 .0074 -1 -1 1
3.8300 3.8198 .0102 -1 -1 2
3.5700 3.5712 -.0012 1 -1 2
3.2900 3.2932 -.0032 -2 0 3
3.1100 3.1104 -.0004 -3 0 2
2.9900 2.9884 .0016 -3 1 1
2.9000 2.9006 -.0006 0 2 0
A= 10.0672 DA= .0001
B= 5.81810 DB= .00003
C= 11.34070 DC= .0001
GAMMA= 94.292 DGAMMA= .002
BETA =101.743 DBETA = .001
ALPHA= 88.2681 DALPHA= .0004
V=648.3
35. 45-0160
LiTaF6
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
4.5300 4.5397 -.0097 3 0 0
4.3650 4.3562 .0088 1 0 3
3.8110 3.8105 .0005 2 0 3
3.5620 3.5636 -.0016 2 1 0
3.1690 3.1659 .0031 2 1 2
2.7370 2.7362 .0008 4 0 3
2.6600 2.6605 -.0005 0 1 4
2.2900 2.2896 .0004 4 1 3
2.2700 2.2698 .0002 6 0 0
1.9070 1.9075 -.0005 4 1 5
a=13.619 b= 4.182 c=13.79
da= .004 db= .001 dc= .01
V= 786
36. 45-1183
KTaF6
Triklin
Dexp Dcal d(D) h k l
5.2000 5.2086 -.0086 0 1 1
5.0500 5.0538 -.0038 -1 1 1
4.5100 4.5141 -.0041 0 -1 1
4.2400 4.2423 -.0023 1 -1 1
3.6600 3.6610 -.0010 0 0 2
3.5900 3.5900 -.0000 1 1 1
3.4100 3.4091 .0009 2 0 0
3.1600 3.1572 .0028 1 0 2
2.9500 2.9511 -.0011 -2 2 0
2.5800 2.5829 -.0029 2 -2 1
2.4600 2.4607 -.0007 -2 -1 1
2.3100 2.3077 .0023 1 -2 2
A= 7.4023 DA= .0004
B= 7.0254 DB= .0002
C= 7.44829 DC= .00006
GAMMA=112.7325 DGAMMA= .0003
BETA = 96.644 DBETA = .001
ALPHA= 79.8687 DALPHA= .0001
V=351.0
37. 46-0093
Li8Ta2O9
Triklin
Dexp Dcal d(D) h k l
8.1900 8.1901 -.0001 1 0 0
4.5700 4.5705 -.0005 2 1 0
4.1300 4.1302 -.0002 2 0 1
3.9900 3.9914 -.0014 -2 -1 1
3.7230 3.7243 -.0013 2 2 0
3.2830 3.2817 .0013 2 1 2
2.8120 2.8125 -.0005 3 0 1
2.7390 2.7401 -.0011 -1 1 2
2.4400 2.4395 .0005 2 -2 1
2.3920 2.3921 -.0001 0 -3 3
2.2810 2.2811 -.0001 3 1 3
2.1250 2.1250 .0000 2 3 2
2.1030 2.1030 -.0000 -1 -3 4
2.0360 2.0358 .0002 -1 0 4
A= 9.236 DA= .002
B= 8.763 DB= .002
C= 9.681 DC= .002
GAMMA= 66.23 DGAMMA= .02
BETA = 84.48 DBETA = .01
ALPHA=107.28 DALPHA= .03
V= 663.4
38. 46-0095
Li10Ta2O10
Triklin
Dexp Dcal d(D) h k l
7.5200 7.5210 -.0010 -1 0 1
5.5000 5.5013 -.0013 1 1 1
5.3300 5.3318 -.0018 -1 -1 1
3.9900 3.9904 -.0004 -1 1 2
3.7200 3.7192 .0008 -1 0 3
3.1900 3.1896 .0004 3 1 1
2.8760 2.8767 -.0007 -3 0 2
2.8280 2.8274 .0006 0 1 4
2.5290 2.5289 .0001 2 -2 3
2.4930 2.4925 .0005 -4 0 1
2.4260 2.4258 .0002 0 -2 4
2.3940 2.3940 -.0000 3 1 4
A= 10.635 DA= .004
B= 7.067 DB= .001
C= 12.838 DC= .002
GAMMA= 87.66 DGAMMA= .01
BETA = 81.12 DBETA = .05
ALPHA= 92.91 DALPHA= .03
V= 950.8
37. 46-0954
TaTe7O29
Triklin
Dexp Dcal d(D) h k l
6.6000 6.5785 .0215 1 0 0
5.6200 5.6249 -.0049 1 1 1
5.1400 5.1334 .0066 -1 -1 1
4.5400 4.5436 -.0036 1 -1 1
4.4900 4.4856 .0044 1 2 1
4.0000 3.9932 .0068 0 2 2
3.8300 3.8276 .0024 -1 -1 2
3.7300 3.7303 -.0003 -1 1 2
3.6100 3.6081 .0019 1 -1 2
3.5500 3.5459 .0041 0 3 0
3.4900 3.4928 -.0028 0 3 1
3.4500 3.4503 -.0003 1 3 0
A= 6.753 DA= .001
B= 10.997 DB= .004
C= 10.616 DC= .001
GAMMA= 77.10 DGAMMA= .01
BETA = 86.441 DBETA = .003
ALPHA= 82.317 DALPHA= .006
V=762.5
38. 46-0955
TaTe2O9
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
10.0200 10.0516 -.0316 2 0 0
7.3200 7.3215 -.0015 0 0 2
6.8700 6.8795 -.0095 1 0 2
6.0900 6.0933 -.0033 3 0 1
5.9100 5.9180 -.0080 2 0 2
4.9400 4.9432 -.0032 3 0 2
4.5800 4.5954 -.0154 0 1 2
4.4000 4.3907 .0093 2 0 3
3.9400 3.9453 -.0053 3 0 3
3.8800 3.8771 .0029 5 0 1
3.7600 3.7616 -.0016 0 1 3
3.7100 3.7024 .0076 4 1 1
a=20.103 b= 5.90 c=14.643
da= .008 db= .01 dc= .006
V=1738
Triklin
Dexp Dcal d(D) h k l
10.0200 10.0155 .0045 -1 1 0
7.3200 7.3162 .0038 0 1 1
6.8700 6.8796 -.0096 0 -1 1
6.0900 6.0879 .0021 1 -1 1
5.9100 5.9104 -.0004 2 0 0
4.9400 4.9388 .0012 2 1 0
4.5800 4.5848 -.0048 -2 2 1
4.4000 4.4029 -.0029 -1 3 0
3.9400 3.9402 -.0002 3 0 0
3.8800 3.8764 .0036 1 0 2
3.7600 3.7609 -.0009 1 3 0
3.7100 3.7095 .0005 -3 0 1
A= 12.267 DA= .006
B= 13.369 DB= .001
C= 8.555 DC= .005
GAMMA=104.55 DGAMMA= .09
BETA = 96.57 DBETA = .02
ALPHA= 84.66 DALPHA= .02
V= 1346.1
39. 46-0956
Ta2Te2O9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.5800 7.5912 -.0112 1 0 0
6.2100 6.2162 -.0062 1 1 0
5.8000 5.7968 .0032 1 1 1
3.8100 3.8113 -.0013 -1 2 2
3.2600 3.2602 -.0002 1 3 0
3.0400 3.0383 .0017 -2 2 1
2.9010 2.8984 .0026 2 2 2
2.8430 2.8434 -.0004 -1 0 5
2.6010 2.6039 -.0029 -2 1 4
2.5430 2.5426 .0004 1 2 5
2.4160 2.4172 -.0012 -1 4 2
2.3680 2.3661 .0019 -1 1 6
a= 7.59 b= 10.830 c= 15.45 beta= 88.9
da= .01 db= .001 dc=.08 dbeta=.3
V= 1270
Triklin
Dexp Dcal d(D) h k l
7.5800 7.5838 -.0038 0 1 1
6.2100 6.2078 .0022 0 -1 1
5.8000 5.8039 -.0039 1 0 0
3.8100 3.8087 .0013 0 3 1
3.2600 3.2607 -.0007 -1 3 1
3.0400 3.0424 -.0024 -1 2 2
2.9010 2.9020 -.0010 2 0 0
2.8430 2.8407 .0023 1 3 2
2.6010 2.6016 -.0006 0 -1 3
2.5430 2.5436 -.0006 2 2 1
2.4160 2.4152 .0008 -2 -1 1
2.3680 2.3666 .0014 -2 3 1
A= 5.982 DA= .001
B= 11.865 DB= .001
C= 8.75522 DC= .00008
GAMMA= 96.33 DGAMMA= .01
BETA = 78.944 DBETA = .001
ALPHA= 79.56 DALPHA= .01
V= 592.9
40. 46-1022
BiTaS3
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
11.5500 11.5658 -.0158 1 0 0
5.7700 5.7829 -.0129 2 0 0
3.8490 3.8553 -.0063 3 0 0
2.8900 2.8914 -.0014 4 0 0
2.3110 2.3112 -.0002 1 1 0
1.9280 1.9276 .0004 6 0 0
1.6516 1.6515 .0001 5 1 0
1.4446 1.4446 .0000 2 1 2
a=11.566 b= 2.3588 c= 3.8522
da= .001 db= .0003 dc= .0008
V= 105.09
Rombik
Groupa 39,67
Dexp. Dcal. d(D) h k l
11.5500 11.5665 -.0165 1 0 0
5.7700 5.7833 -.0133 2 0 0
3.8490 3.8555 -.0065 3 0 0
2.8900 2.8901 -.0001 1 1 1
2.3110 2.3112 -.0002 1 2 0
1.9280 1.9278 .0002 6 0 0
1.6516 1.6516 .0000 5 2 0
1.4446 1.4446 .0000 1 3 1
a=11.5665 b= 4.7175 c= 3.854
da= .0006 db= .0004 dc= .002
V= 210.3
41. 46-1209
PbTa2S5
Tetrag.
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
9.0000 9.0013 -.0013 0 0 1
6.0220 5.9971 .0249 1 0 0
4.4970 4.5007 -.0037 0 0 2
3.6010 3.5997 .0013 1 0 2
2.5690 2.5703 -.0013 2 1 1
2.2510 2.2503 .0007 0 0 4
2.0000 1.9996 .0004 2 1 3
1.5001 1.5002 -.0001 0 0 6
a= 5.997 c= 9.001
da= .009 dc= .001
v= 323.7
42. 47-1309
Al7Fe2Ta
Tetrag.
Grupa 134
Dexp. Dcal. d(D) h k l
3.3240 3.3274 -.0034 2 0 0
2.1620 2.1614 .0006 2 2 1
2.0560 2.0557 .0003 3 0 1
1.3780 1.3781 -.0001 3 1 3
1.2650 1.2650 .0000 2 0 4
a= 6.655 c= 5.4705
da= .004 dc= .0001
v= 242.3
Rombik
Groupa 37,66
Dexp. Dcal. d(D) h k l
3.3240 3.3244 -.0004 2 0 0
2.1620 2.1616 .0004 0 1 1
2.0560 2.0557 .0003 1 1 1
1.3780 1.3782 -.0002 0 1 3
1.2650 1.2650 .0000 0 0 4
a= 6.649 b= 2.391 c= 5.060
da= .001 db= .001 dc= .001
v= 80.43
43. 47-1935
C6H24Br14O6Ta6
Triklin
Dexp Dcal d(D) h k l
9.3900 9.3943 -.0043 1 0 0
8.7800 8.7811 -.0011 -1 1 0
6.4200 6.4229 -.0029 0 -1 1
5.0600 5.0585 .0015 -1 2 0
4.4600 4.4593 .0007 -2 1 1
4.3900 4.3906 -.0006 -2 2 0
4.1500 4.1545 -.0045 -2 0 1
3.9760 3.9756 .0004 2 -2 1
3.4500 3.4482 .0018 -1 -1 2
3.3190 3.3193 -.0003 1 1 2
3.2110 3.2114 -.0004 0 -2 2
3.1320 3.1314 .0006 3 0 0
A= 10.521 DA= .001
B= 10.136 DB= .002
C= 8.678 DC= .001
GAMMA=116.75 DGAMMA= .01
BETA = 89.439 DBETA = .001
ALPHA= 92.8948 DALPHA= .0008
V=825.7
44. 49-0746
ZnTa2O6
Triklin
Dexp Dcal d(D) h k l
4.6380 4.6364 .0016 -1 0 1
4.5950 4.5972 -.0022 -1 1 1
4.2590 4.2561 .0029 1 -1 1
4.1410 4.1389 .0021 0 -1 1
3.5590 3.5556 .0034 0 0 2
3.3140 3.3144 -.0004 0 2 0
3.2570 3.2563 .0007 1 2 1
2.7360 2.7356 .0004 3 0 0
2.6440 2.6446 -.0006 3 1 1
2.5760 2.5754 .0006 3 1 2
2.5490 2.5499 -.0009 -2 -1 1
2.4540 2.4546 -.0006 2 0 3
A= 8.759 DA= .006
B= 7.152 DB= .001
C= 8.067 DC= .003
GAMMA= 92.43 DGAMMA= .09
BETA = 71.84 DBETA = .03
ALPHA= 70.05 DALPHA= .05
V=444.8
45. 49-0986
KTa{PO4}2*H2O
Triklin
Dexp Dcal d(D) h k l
8.8900 8.8878 .0022 1 0 0
5.2700 5.2728 -.0028 0 1 1
4.4700 4.4692 .0008 -2 -1 1
4.3300 4.3224 .0076 0 -2 1
4.1800 4.1781 .0019 -2 -1 2
4.1500 4.1533 -.0033 0 2 0
4.0600 4.0630 -.0030 -2 1 1
3.8600 3.8563 .0037 -1 2 0
3.4700 3.4687 .0013 0 1 2
3.3600 3.3599 .0001 2 -1 1
3.3300 3.3301 -.0001 -2 -1 3
3.0600 3.0619 -.0019 1 -2 2
2.7750 2.7743 .0007 0 -3 2
2.5350 2.5359 -.0009 -2 -3 1
A= 9.9619 DA= .0007
B= 8.795 DB= .001
C= 10.4107 DC= .0008
GAMMA= 84.726 DGAMMA= .002
BETA =116.638 DBETA = .002
ALPHA=108.87 DALPHA= .03
V= 770.1
46. 49-1470
NH4TaF6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.2100 5.2188 -.0088 -2 0 2
4.9100 4.9107 -.0007 -1 1 2
3.7800 3.7785 .0015 -2 0 5
3.7100 3.7115 -.0015 1 0 5
3.6600 3.6619 -.0019 -1 0 6
3.4800 3.4792 .0008 -3 0 3
3.4100 3.4070 .0030 2 0 4
3.0800 3.0811 -.0011 0 0 7
3.0800 3.0831 -.0031 0 1 6
3.0100 3.0094 .0006 -3 1 3
2.9190 2.9165 .0025 -2 1 6
2.7950 2.7937 .0013 1 0 7
a= 10.816 b=5.997 c=22.129 beta= 102.93
da=.005 db= .001 dc=.01 dbeta=.05
V= 1399
Triklin
Dexp Dcal d(D) h k l
5.2100 5.2121 -.0021 0 -1 1
4.9100 4.9218 -.0118 1 1 1
3.7800 3.7790 .0010 -1 -1 1
3.7100 3.7154 -.0054 1 2 0
3.6600 3.6600 -.0000 2 1 1
3.4800 3.4822 -.0022 0 -2 1
3.4100 3.4137 -.0037 2 0 0
3.0800 3.0809 -.0009 2 0 2
3.0100 3.0085 .0015 0 2 1
2.9190 2.9164 .0026 2 2 0
2.7950 2.7937 .0013 2 -1 2
2.6060 2.6061 -.0001 0 -2 2
A= 7.801 DA= .004
B= 7.804 DB= .005
C= 6.924 DC= .004
GAMMA= 78.59 DGAMMA= .04
BETA = 64.61321 DBETA = .00009
ALPHA= 93.42 DALPHA= .02
V=368.0
47. 49-1952
C4H12Cl12O4Ta6*4CH4O
Triklin
Dexp Dcal d(D) h k l
8.9500 8.9942 -.0442 0 0 1
8.0800 8.0736 .0064 0 1 1
6.4900 6.4905 -.0005 1 1 0
6.2100 6.2069 .0031 0 -1 1
3.5090 3.5091 -.0001 1 3 1
3.3210 3.3200 .0010 2 0 1
2.7640 2.7640 -.0000 -2 -1 2
2.7170 2.7170 .0000 0 -1 3
2.5990 2.5991 -.0001 2 -2 1
2.4530 2.4530 .0000 0 -4 1
2.3790 2.3790 .0000 -2 1 3
2.3160 2.3161 -.0001 3 0 1
A= 7.35476 DA= .00007
B= 11.4761 DB= .0002
C= 9.3212 DC= .0008
GAMMA= 82.70 DGAMMA= .01
BETA = 90.837 DBETA = .005
ALPHA= 75.042 DALPHA= .004
V= 752.98
48. 49-1953
4CH4O*{Ta6Cl12}cl3*H2O
Triklin
Dexp Dcal d(D) h k l
8.8800 8.8857 -.0057 1 0 0
8.3100 8.3014 .0086 0 1 0
6.0900 6.0907 -.0007 1 0 1
4.2400 4.2408 -.0008 0 -1 2
3.8830 3.8863 -.0033 -2 -2 1
3.1730 3.1723 .0007 2 2 1
3.1290 3.1297 -.0007 -1 -3 1
2.9760 2.9759 .0001 1 3 0
2.7910 2.7896 .0014 -2 -3 2
2.6420 2.6423 -.0003 -3 -3 1
2.5870 2.5872 -.0002 -2 -2 3
2.2450 2.2450 .0000 3 -1 2
2.1690 2.1690 -.0000 0 -4 1
2.1330 2.1330 .0000 -4 -1 2
A= 9.6391 DA= .0007
B= 9.421 DB= .002
C= 8.732 DC= .002
GAMMA= 67.208 DGAMMA= .002
BETA = 96.51 DBETA = .01
ALPHA=108.26 DALPHA= .01
V= 694.2
49. 50-2132
4CH4O{Ta6Cl12}Br3*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.0200 9.0253 -.0053 0 0 1
8.4200 8.4179 .0021 -1 0 1
6.1900 6.1975 -.0075 3 0 0
4.5300 4.5126 .0174 0 0 2
4.3100 4.3070 .0030 1 1 0
4.0000 3.9972 .0028 2 1 0
3.8600 3.8564 .0036 1 1 1
3.3380 3.3355 .0025 5 0 1
3.2090 3.2058 .0032 4 1 0
3.0150 3.0141 .0009 -6 0 1
2.8550 2.8541 .0009 6 0 1
2.6190 2.6168 .0022 3 0 3
a= 18.6662 b= 4.427 c= 9.06 beta= 95.08
da=.0003 db=.001 dc=.03 dbeta=.06
V= 746
Triklin
Dexp Dcal d(D) h k l
9.0200 9.0313 -.0113 0 0 1
8.4200 8.4201 -.0001 1 0 0
6.1900 6.1933 -.0033 1 1 0
4.5300 4.5305 -.0005 0 1 1
4.3100 4.3093 .0007 2 0 1
4.0000 4.0001 -.0001 2 1 1
3.8600 3.8655 -.0055 1 -1 2
3.3380 3.3374 .0006 1 2 0
3.2090 3.2116 -.0026 2 -1 1
3.0150 3.0137 .0013 -2 1 0
2.8550 2.8526 .0024 2 2 1
2.6190 2.6178 .0012 1 1 3
A= 9.218 DA= .007
B= 6.839 DB= .003
C= 9.64 DC= .01
GAMMA= 72.19 DGAMMA= .04
BETA = 78.74 DBETA = .01
ALPHA=102.58 DALPHA= .02
V= 542.0
50. 50-2211
C1.3H1.3Co0.13Na0.19S2Ta*H2O
geksagon
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
11.4200 11.5194 -.0994 0 0 1
5.7460 5.7597 -.0137 0 0 2
3.8340 3.8398 -.0058 0 0 3
2.8770 2.8799 -.0029 0 0 4
2.3030 2.3026 .0004 1 0 1
1.9190 1.9199 -.0009 0 0 6
1.6450 1.6452 -.0002 1 0 5
1.4400 1.4399 .0001 0 0 8
1.2802 1.2799 .0003 0 0 9
1.1519 1.1519 -.0000 0 0 10
a= 2.7135 c= 11.519
da=.0003 dc=.002
V=73.46