1.19-0065
NH4TaCl6
Triklin
Dexp Dcal d(D) h k l
5.9100 5.9088 .0012 0 1 1
5.8700 5.8685 .0015 0 -1 1
5.2000 5.2028 -.0028 1 0 0
4.8100 4.8098 .0002 1 -1 1
4.6600 4.6591 .0009 0 -3 1
3.7900 3.7898 .0002 1 4 0
3.3600 3.3590 .0010 -1 1 1
3.3400 3.3393 .0007 -1 5 0
3.0500 3.0488 .0012 1 -2 2
2.9340 2.9343 -.0003 0 -2 2
2.8900 2.8906 -.0006 -1 4 1
2.8030 2.8029 .0001 0 7 1
A= 5.587 DA= .001
B= 21.9318 DB= .0003
C= 6.565 DC= .001
GAMMA= 89.19 DGAMMA= .01
BETA = 68.6382 DBETA = .0008
ALPHA= 89.005 DALPHA= .009
V= 749.0
2. 19-0792
Mn1.4TaO4.2
Triklin
Dexp Dcal d(D) h k l
7.0300 7.0308 -.0008 0 1 1
5.9500 5.9434 .0066 1 0 0
5.6400 5.6487 -.0087 0 -1 1
3.5100 3.5076 .0024 1 2 0
3.4700 3.4709 -.0009 -1 1 2
3.2900 3.2910 -.0010 1 0 2
3.2400 3.2380 .0020 -1 2 2
3.2000 3.1991 .0009 1 1 2
2.8600 2.8584 .0016 0 -3 1
2.7900 2.7932 -.0032 -2 0 1
2.5400 2.5402 -.0002 2 -2 1
2.4800 2.4810 -.0010 -2 3 1
A= 6.0668 DA= .0006
B= 10.470 DB= .003
C= 8.172 DC= .002
GAMMA=101.567 DGAMMA= .005
BETA = 93.17 DBETA = .01
ALPHA= 76.86 DALPHA= .01
V= 495.2
3. 19-0793
Mn1.4TaO3.9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.2900 7.2889 .0011 0 1 0
4.4400 4.4360 .0040 2 1 0
4.1300 4.1291 .0009 -1 0 2
3.9500 3.9454 .0046 2 1 1
3.4900 3.4913 -.0013 -2 0 2
3.1200 3.1202 -.0002 -3 1 1
2.8700 2.8697 .0003 -3 0 2
2.7200 2.7200 -.0000 1 2 2
2.6200 2.6215 -.0015 -2 0 3
2.5000 2.5018 -.0018 2 2 2
2.4400 2.4399 .0001 2 1 3
2.2500 2.2489 .0011 -1 2 3
a= 11.18 b= 7.289 c= 8.834 beta= 90.85
da=.01 db=.001 dc= .003 dbeta=
V= 720
4. 19-0794
Mn6Ta2O11
Triklin
Dexp Dcal d(D) h k l
5.6100 5.6084 .0016 -1 0 1
4.4500 4.4492 .0008 0 1 1
4.2100 4.2097 .0003 0 -1 1
4.0500 4.0460 .0040 1 1 0
3.1200 3.1207 -.0007 1 1 2
2.7300 2.7328 -.0028 2 0 1
2.6700 2.6708 -.0008 -1 1 3
2.4100 2.4087 .0013 2 0 2
2.3400 2.3400 -.0000 1 2 0
2.3000 2.2995 .0005 -2 1 2
2.2600 2.2599 .0001 1 0 4
2.2300 2.2301 -.0001 0 -1 4
A= 6.1030 DA= .0008
B= 4.8158 DB= .0002
C= 10.689 DC= .001
GAMMA= 81.095 DGAMMA= .001
BETA = 99.61 DBETA = .01
ALPHA= 87.37 DALPHA= .01
V= 305.2
5. 19-1295
TaCl15*7H2O
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
8.7700 8.8034 -.0334 0 1 0
8.0600 8.0952 -.0352 1 0 0
5.9600 5.9588 .0012 1 1 0
4.4000 4.4017 -.0017 0 2 0
4.1300 4.1333 -.0033 0 1 2
4.0500 4.0476 .0024 2 0 0
3.8700 3.8670 .0030 1 2 0
3.6800 3.6812 -.0012 1 1 2
3.2100 3.2068 .0032 0 2 2
3.0600 3.0618 -.0018 2 0 2
2.8900 2.8919 -.0019 2 1 2
2.7600 2.7588 .0012 1 3 0
a= 8.0952 b= 8.803 c= 9.363
da= .0004 db= .003 dc= .008
V= 667.2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.7700 8.8055 -.0355 1 0 0
8.0600 8.0976 -.0376 0 1 0
5.9600 5.9604 -.0004 1 1 0
4.4000 4.4027 -.0027 2 0 0
4.1300 4.1310 -.0010 1 0 1
4.0500 4.0488 .0012 0 2 0
3.8700 3.8680 .0020 2 1 0
3.6800 3.6798 .0002 1 1 1
3.2100 3.2043 .0057 2 0 1
3.0600 3.0628 -.0028 0 2 1
2.8900 2.8915 -.0015 1 2 1
2.7600 2.7595 .0005 3 1 0
a= 8.805 b= 8.098 c= 4.683 beta= 90.11
da= 2.725601E-03 db=.004 dc=.003 dbeta= .07
V= 333.9
6. 19-1818
C2H3Br5NTa
Triklin
Dexp Dcal d(D) h k l
6.2700 6.2652 .0048 0 1 1
5.2600 5.2543 .0057 0 -1 1
4.6900 4.6931 -.0031 -1 1 0
4.2300 4.2337 -.0037 0 2 0
4.0300 4.0179 .0121 0 2 1
3.7200 3.7167 .0033 -1 1 1
3.5300 3.5284 .0016 2 1 2
3.3400 3.3425 -.0025 2 0 0
3.1300 3.1326 -.0026 0 2 2
3.0700 3.0715 -.0015 1 3 1
3.0300 3.0291 .0009 2 2 0
2.9750 2.9752 -.0002 2 -1 1
A= 7.813 DA= .003
B= 9.223 DB= .001
C= 8.824 DC= .007
GAMMA= 68.82 DGAMMA= .02
BETA = 62.30 DBETA = .03
ALPHA= 71.80 DALPHA= .03
V=516.6
7. 18-1912
C8H20Br6NTa
Triklin
Dexp. Dcal. d(D) h k l
8.1900 8.1421 .0479 1 -1 0
6.1700 6.1656 .0044 0 -1 1
5.9700 5.9685 .0015 -1 -1 0
5.4900 5.4901 -.0001 -2 1 1
4.3300 4.3311 -.0011 1 -2 0
4.2700 4.2804 -.0104 -2 -1 0
3.8300 3.8314 -.0014 1 -2 1
3.5500 3.5514 -.0014 -1 -2 0
3.2600 3.2652 -.0052 3 0 1
3.0600 3.0607 -.0007 4 0 0
3.0100 3.0129 -.0029 2 0 2
2.9750 2.9759 -.0009 -4 0 2
A= 13.635 DA= .009
B= 8.6626 DB= .0004
C= 8.814 DC= .001
GAMMA=108.09 DGAMMA= .07
BETA =108.269 DBETA = .09
ALPHA= 89.77 DALPHA= .01
V= 934.8
8. 19-1922
C4H12Br6NTa
Triklin
Dexp Dcal d(D) h k l
8.5000 8.4932 .0068 0 1 1
7.7400 7.7372 .0028 -1 0 1
6.7300 6.7252 .0048 0 -1 1
6.1800 6.1777 .0023 -1 2 0
5.9400 5.9627 -.0227 1 -1 1
5.4900 5.4897 .0003 -2 1 0
5.3400 5.3319 .0081 -1 1 2
5.2300 5.2302 -.0002 -1 -1 1
4.7800 4.7788 .0012 -2 0 1
4.4800 4.4745 .0055 0 -2 1
4.2900 4.2794 .0106 2 -1 1
3.9400 3.9382 .0018 2 1 0
A= 11.5784 DA= .0002
B= 13.32332 DB= .00004
C= 10.79438 DC= .00007
GAMMA=119.8208 DGAMMA= .0005
BETA =108.5178 DBETA = .0006
ALPHA= 69.6491 DALPHA= .0001
V=1333
9. 19-1923
C5H12Br6NTa
Rombik
Groupa 32,55
romb.
Dexp. Dcal. d(D) h k l
7.0300 7.0430 -.0130 1 1 0
5.8500 5.8442 .0058 0 2 0
5.0900 5.0867 .0033 0 0 1
4.8700 4.8726 -.0026 1 2 0
4.1200 4.1236 -.0036 1 1 1
3.8400 3.8369 .0031 0 2 1
3.5200 3.5187 .0013 1 2 1
3.2100 3.2054 .0046 2 1 1
2.9220 2.9221 -.0001 0 4 0
2.8940 2.8954 -.0014 2 2 1
2.8540 2.8527 .0013 3 1 0
2.6280 2.6276 .0004 3 2 0
a= 8.8249 b=11.68845 c= 5.0867
da= .0009 db= .00003 dc= .0001
V= 524.69
10. 20-1230
TaCl5
Triklin
Dexp Dcal d(D) h k l
8.8700 8.8651 .0049 1 0 0
5.7600 5.7753 -.0153 -1 1 1
5.3000 5.3136 -.0136 -1 -1 1
4.9500 4.9455 .0045 0 2 0
4.4300 4.4325 -.0025 2 0 0
4.2400 4.2495 -.0095 -2 0 1
4.0800 4.0786 .0014 0 0 2
3.6600 3.6657 -.0057 1 -2 1
3.3000 3.2992 .0008 1 1 2
3.0600 3.0579 .0021 0 -2 2
2.9970 2.9950 .0020 0 -3 1
2.7920 2.7903 .0017 3 1 0
A= 9.0511 DA= .0001
B= 9.93092 DB= .00002
C= 8.3311 DC= .0001
GAMMA= 93.839 DGAMMA= .001
BETA =101.229 DBETA = .001
ALPHA= 85.8989 DALPHA= .0009
V=731.8
11. 20-1237
Ta2Zn3O8
Trikli
Dexp Dcal d(D) h k l
5.8000 5.7994 .0006 0 1 1
4.2000 4.2006 -.0006 0 -1 1
4.1000 4.1072 -.0072 1 2 0
3.9900 3.9899 .0001 1 0 1
3.9000 3.9023 -.0023 1 2 1
3.7800 3.7796 .0004 -1 -1 1
3.0600 3.0597 .0003 2 1 0
3.0000 3.0005 -.0005 0 -2 1
2.9500 2.9475 .0025 1 3 0
2.9000 2.8997 .0003 0 2 2
2.7700 2.7688 .0012 2 1 1
2.7400 2.7408 -.0008 2 2 1
A= 6.129 DA= .001
B= 9.545 DB= .001
C= 6.180 DC= .003
GAMMA= 72.20 DGAMMA= .07
BETA = 87.46 DBETA = .03
ALPHA= 70.58 DALPHA= .02
V=323.6
12. 21-0687
K8Ta6O19*4H2O
Triklin
Dexp Dcal d(D) h k l
7.7200 7.7273 -.0073 1 0 0
7.2500 7.2581 -.0081 0 1 1
7.1100 7.1073 .0027 0 -1 1
6.8600 6.8549 .0051 0 0 2
6.4100 6.4059 .0041 -1 1 0
6.0300 6.0298 .0002 1 -1 1
3.9000 3.9015 -.0015 1 -1 3
3.8600 3.8597 .0003 2 0 1
3.2500 3.2505 -.0005 -1 -2 1
3.0100 3.0098 .0002 1 1 4
2.9700 2.9703 -.0003 -1 2 3
2.8400 2.8395 .0005 -1 3 0
A= 7.977 DA= .002
B= 8.6232 DB= .0001
C= 13.841 DC= .008
GAMMA=102.06 DGAMMA= .01
BETA = 82.22 DBETA = .02
ALPHA= 90.32 DALPHA= .02
V= 922.3
13. 21-0460
LaTa12O33
Triklin
Dexp Dcal d(D) h k l
3.6300 3.6281 .0019 0 1 1
3.0800 3.0824 -.0024 0 -1 1
3.0200 3.0201 -.0001 -1 0 1
2.7200 2.7212 -.0012 -1 1 0
1.9350 1.9367 -.0017 1 -1 2
1.7370 1.7384 -.0014 0 0 4
1.6420 1.6419 .0001 1 -2 1
1.5890 1.5890 .0000 -2 0 1
1.3800 1.3798 .0002 -2 2 2
1.3000 1.2999 .0001 -2 1 4
1.2310 1.2307 .0003 0 -1 5
1.1290 1.1290 .0000 0 3 4
A= 3.28846 DA= .00005
B= 3.9585 DB= .0003
C= 7.170 DC= .002
GAMMA=103.22 DGAMMA= .01
BETA = 98.811 DBETA = .004
ALPHA= 77.29 DALPHA= .01
V= 88.1
14. 21-0685
K4Ta6O17
Triklin
Dexp Dcal d(D) h k l
6.0300 6.0360 -.0060 0 0 1
3.1800 3.1798 .0002 0 -2 1
3.0500 3.0479 .0021 -1 2 0
2.6500 2.6502 -.0002 -1 -1 2
2.4300 2.4314 -.0014 0 -2 2
2.1700 2.1705 -.0005 1 0 2
2.0400 2.0395 .0005 1 -2 2
1.8700 1.8697 .0003 0 1 3
1.7800 1.7801 -.0001 -2 3 0
1.6100 1.6099 .0001 0 4 1
1.5900 1.5899 .0001 0 -4 2
1.5300 1.5300 -.0000 -1 3 3
A= 4.5547 DA= .0004
B= 7.1228 DB= .0003
C= 6.3446 DC= .0006
GAMMA=101.69 DGAMMA= .01
BETA =106.46 DBETA = .01
ALPHA= 93.516 DALPHA= .00562
V= 191.8
15. 21-0686
K8Ta6O19*12H2O
Triklin
Dexp Dcal d(D) h k l
8.8700 8.7480 .1220 0 0 1
8.2600 8.2428 .0172 1 0 0
6.2900 6.2872 .0028 0 1 0
3.9700 3.9709 -.0009 0 -1 2
3.3600 3.3597 .0003 -1 0 2
3.1400 3.1371 .0029 2 -1 2
2.9900 2.9921 -.0021 3 1 1
2.9500 2.9488 .0012 2 2 0
2.8400 2.8402 -.0002 3 1 0
2.8100 2.8110 -.0010 1 -2 1
2.6900 2.6893 .0007 2 -1 3
2.4600 2.4608 -.0008 3 -1 1
A= 9.217 DA= .003
B= 6.601 DB= .001
C= 9.538 DC= .003
GAMMA= 76.17 DGAMMA= .01
BETA = 69.24 DBETA = .01
ALPHA= 95.27 DALPHA= .03
V= 516.8
16. 21-0687
K8Ta6O19*4H2O
Triklin
Dexp Dcal d(D) h k l
7.7200 7.7273 -.0073 1 0 0
7.2500 7.2581 -.0081 0 1 1
7.1100 7.1073 .0027 0 -1 1
6.8600 6.8549 .0051 0 0 2
6.4100 6.4059 .0041 -1 1 0
6.0300 6.0298 .0002 1 -1 1
3.9000 3.9015 -.0015 1 -1 3
3.8600 3.8597 .0003 2 0 1
3.2500 3.2505 -.0005 -1 -2 1
3.0100 3.0098 .0002 1 1 4
2.9700 2.9703 -.0003 -1 2 3
2.8400 2.8395 .0005 -1 3 0
A= 7.977 DA= .002
B= 8.6232 DB= .0001
C= 13.841 DC= .008
GAMMA=102.06 DGAMMA= .01
BETA = 82.22 DBETA = .02
ALPHA= 90.32 DALPHA= .02
V= 922.3
17. 21-0688
K4Ta2O7*xH2O
Triklin
Dexp Dcal d(D) h k l
13.1000 13.3590 -.2590 1 0 0
8.6600 8.6607 -.0007 -1 0 1
7.2500 7.2660 -.0160 0 1 0
5.2300 5.2312 -.0012 -2 1 0
4.1200 4.1191 .0009 2 0 2
3.6300 3.6305 -.0005 0 0 3
3.6000 3.6010 -.0010 0 -2 2
3.2600 3.2603 -.0003 -2 0 3
3.1800 3.1802 -.0002 2 1 2
3.1300 3.1294 .0006 4 -1 1
2.9400 2.9392 .0008 -4 -1 1
2.9200 2.9196 .0004 3 -2 2
A= 13.452 DA= .007
B= 7.713 DB= .001
C= 11.498 DC= .004
GAMMA= 96.10 DGAMMA= .01
BETA = 90.84 DBETA = .05
ALPHA=108.48 DALPHA= .01
V= 1124
18. 21-0689
K8Ta6O19*9H2O
Triklin
Dexp Dcal d(D) h k l
8.4600 8.4580 .0020 0 1 0
8.1600 8.2152 -.0552 1 1 0
5.9300 5.9253 .0047 3 0 0
4.6000 4.5952 .0048 1 0 1
4.2500 4.2521 -.0021 4 1 0
4.1100 4.1076 .0024 2 2 0
3.7800 3.7827 -.0027 0 1 1
3.7000 3.7098 -.0098 -2 -2 1
3.3800 3.3814 -.0014 -4 0 1
3.2100 3.2081 .0019 2 -2 1
3.1500 3.1477 .0023 -3 1 1
2.9900 2.9911 -.0011 5 2 0
A= 18.178 DA= .001
B= 8.965 DB= .001
C= 5.059 DC= .004
GAMMA= 78.482 DGAMMA= .007
BETA = 96.71 DBETA = .06
ALPHA=106.62 DALPHA= .08
V=773.1
19. 21-1398
Ta2O3{SO4}2*4H2O
Triklin
Dexp Dcal d(D) h k l
7.7800 7.7860 -.0060 0 1 0
7.1400 7.1351 .0049 -1 1 0
4.3300 4.3270 .0030 1 -1 2
4.1400 4.1397 .0003 -1 2 0
3.9300 3.9279 .0021 -2 1 1
3.7200 3.7194 .0006 -1 2 1
3.5700 3.5717 -.0017 0 2 1
3.3500 3.3525 -.0025 2 0 2
3.1400 3.1395 .0005 1 2 0
2.5300 2.5299 .0001 -2 3 1
2.3900 2.3897 .0003 -2 -2 1
2.3300 2.3311 -.0011 -2 2 3
A= 9.1032 DA= .0006
B= 8.3563 DB= .0003
C= 10.131 DC= .001
GAMMA=111.11 DGAMMA= .01
BETA = 84.903 DBETA = .006
ALPHA= 94.52 DALPHA= .01
V= 715.2
20. 21-1399
Ta2O3{SO4}2*5H2O
Triklin
Dexp Dcal d(D) h k l
7.0800 7.0801 -.0001 1 0 0
4.3000 4.2990 .0010 1 1 1
4.1200 4.1170 .0030 -1 -1 1
3.6900 3.6887 .0013 1 -1 1
3.5300 3.5302 -.0002 1 0 2
2.4900 2.4901 -.0001 1 0 3
7.6800 7.6785 .0015 0 0 1
2.3400 2.3402 -.0002 2 -1 2
1.6710 1.6709 .0001 4 2 1
1.6150 1.6150 .0000 0 -2 4
1.4900 1.4900 .0000 -2 3 1
1.3080 1.3080 .0000 -5 1 0
1.2810 1.2810 -.0000 5 3 0
A= 7.29834 DA= .00007
B= 5.8579 DB= .0005
C= 7.7194 DC= .0005
GAMMA= 77.2314 DGAMMA= .0009
BETA = 84.35 DBETA = .01
ALPHA= 90.377 DALPHA= .008
V= 320.15
21. 21-1005
K8Ta6O19*16H2O
Triklin
Dexp Dcal d(D) h k l
10.9000 10.8981 .0019 0 1 1
10.2000 10.1974 .0026 0 -1 1
8.7500 8.7510 -.0010 1 0 0
8.3000 8.3226 -.0226 -1 1 0
7.9400 7.9482 -.0082 0 2 1
7.6900 7.6656 .0244 1 1 0
6.9200 6.9222 -.0022 1 1 1
6.4500 6.4517 -.0017 0 3 0
6.2100 6.2180 -.0080 -1 -1 1
6.1000 6.1008 -.0008 0 1 2
5.9600 5.9543 .0057 -1 2 1
5.1000 5.0987 .0013 0 -2 2
A= 8.84559 DA= .00005
B= 19.50922 DB= .00009
C= 12.64345 DC= .00001
GAMMA= 95.8925 DGAMMA= .0007
BETA = 84.4303 DBETA = .0003
ALPHA= 86.4517 DALPHA= .0002
V=2147.8
22. 21-1158
Na3TaF8
Monoklin
Triklin
Dexp Dcal d(D) h k l
4.9500 4.9393 .0107 1 0 1
4.7300 4.7324 -.0024 0 1 0
3.8600 3.8681 -.0081 0 -1 2
3.0900 3.0878 .0022 1 -1 1
3.0100 3.0118 -.0018 0 -1 3
2.8800 2.8807 -.0007 2 0 0
2.8000 2.7996 .0004 -2 -1 2
2.6800 2.6810 -.0010 -1 -2 1
2.5900 2.5876 .0024 1 2 0
2.4700 2.4696 .0004 2 0 2
2.4200 2.4196 .0004 -2 -1 3
2.3900 2.3891 .0009 0 -1 4
2.3500 2.3497 .0003 1 2 1
2.1700 2.1708 -.0008 2 2 1
2.1100 2.1103 -.0003 -2 1 0
A= 6.340 DA= .001
B= 5.362 DB= .001
C= 9.983 DC= .008
GAMMA= 65.334 DGAMMA= .009
BETA = 96.41 DBETA = .03
ALPHA=105.18 DALPHA= .05
V=297.6
Grupa 3
Dexp Dcal d(D) h k l
4.9500 4.9448 .0052 1 1 0
4.7300 4.7254 .0046 1 1 1
3.8600 3.8599 .0001 0 0 3
3.0900 3.0914 -.0014 3 1 0
3.0100 3.0085 .0015 2 1 3
2.8800 2.8790 .0010 4 0 1
2.8000 2.8008 -.0008 4 0 0
2.6800 2.6805 -.0005 0 2 1
2.5900 2.5887 .0013 -4 0 1
2.4700 2.4700 -.0000 2 2 1
2.4200 2.4184 .0016 -3 0 3
2.3900 2.3938 -.0038 -1 1 4
2.3500 2.3499 .0001 3 1 4
2.1700 2.1704 -.0004 -1 0 5
2.1100 2.1105 -.0005 -5 0 1
a= 11.517 b= 5.511 c= 11.904 beta= 76.59
da=.003 db=.002 dc= .002 dbeta=.009
V= 734.9
23. 21-1344
Ag2Ta8O21
Triklin
Dexp Dcal d(D) h k l
5.4300 5.4334 -.0034 -1 1 0
4.3900 4.3852 .0048 -1 1 1
3.8900 3.8892 .0008 -1 -1 1
3.5500 3.5502 -.0002 -1 2 0
3.4400 3.4430 -.0030 -2 1 0
3.0000 2.9996 .0004 0 -2 1
2.9200 2.9191 .0009 1 3 0
2.7700 2.7679 .0021 0 0 2
2.5700 2.5705 -.0005 -1 3 0
2.3900 2.3908 -.0008 -1 -1 2
2.3420 2.3420 .0000 -2 1 2
2.2730 2.2739 -.0009 1 -1 2
A= 8.354 DA= .003
B= 9.303 DB= .007
C= 5.816 DC= .001
GAMMA= 78.55 DGAMMA= .08
BETA = 88.70 DBETA = .05
ALPHA= 72.31 DALPHA= .04
V=422.1
24. 21-1345
Ag2Ta4O11
Triklin
Dexp Dcal d(D) h k l
6.1400 6.1504 -.0104 0 1 1
5.4000 5.3971 .0029 -1 1 0
5.1700 5.1690 .0010 0 -1 1
3.0600 3.0601 -.0001 1 -1 2
3.0000 2.9989 .0011 -2 1 1
2.7700 2.7710 -.0010 2 1 0
2.6600 2.6600 .0000 -2 2 1
2.5700 2.5710 -.0010 -2 1 2
2.4690 2.4701 -.0011 2 -2 1
2.1770 2.1782 -.0012 1 2 3
2.1110 2.1106 .0004 1 3 2
2.0420 2.0416 .0004 3 -1 1
A= 6.450 DA= .001
B= 7.9993 DB= .0009
C= 8.214 DC= .001
GAMMA=100.314 DGAMMA= .004
BETA = 92.0157 DBETA = .0008
ALPHA= 79.89 DALPHA= .01078
V= 410.5
25. 21-1398
Ta2O3{SO4}2*4H2O
Triklin
Dexp Dcal d(D) h k l
7.7800 7.7853 -.0053 1 0 0
7.1400 7.1349 .0051 0 1 1
4.3300 4.3294 .0006 0 -1 1
4.1400 4.1375 .0025 0 2 1
3.9300 3.9288 .0012 1 2 1
3.7200 3.7286 -.0086 1 1 2
3.5700 3.5675 .0025 0 2 2
3.3500 3.3507 -.0007 2 0 1
3.1400 3.1382 .0018 -2 -1 1
2.5300 2.5306 -.0006 -1 2 3
2.3900 2.3896 .0004 -3 -1 1
2.3300 2.3275 .0025 3 2 0
A= 7.917 DA= .003
B= 8.3966 DB= .0003
C= 8.414 DC= .003
GAMMA= 80.44 DGAMMA= .03
BETA = 89.39 DBETA = .04
ALPHA= 62.80 DALPHA= .02
V= 489.2
26. 21-1399
Ta2O3{SO4}*5H2O
Triklin
Dexp Dcal d(D) h k l
7.6800 7.6769 .0031 0 1 0
7.0800 7.0776 .0024 0 -1 1
4.3000 4.2999 .0001 0 -1 3
4.1200 4.1188 .0012 1 0 0
3.6900 3.6897 .0003 1 1 1
3.5300 3.5291 .0009 -1 0 2
2.4900 2.4899 .0001 0 -3 2
2.3400 2.3399 .0001 -1 0 5
1.6710 1.6710 -.0000 2 -2 3
1.6150 1.6150 .0000 -1 3 5
1.4900 1.4900 -.0000 -1 0 9
1.3080 1.3080 -.0000 2 5 0
1.2810 1.2810 .0000 2 1 9
A= 4.150 DA= .001
B= 7.764 DB= .008
C= 14.676 DC= .002
GAMMA= 83.33 DGAMMA= .01
BETA = 88.41 DBETA = .01
ALPHA= 95.23 DALPHA= .07
V= 467.4
27. 22-0908
TaSix
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.6200 3.6191 .0009 -2 1 2
3.0000 2.9996 .0004 -3 0 2
2.8400 2.8401 -.0001 2 1 2
2.7300 2.7295 .0005 0 3 1
2.5800 2.5803 -.0003 3 1 1
2.4800 2.4798 .0002 0 3 2
2.4300 2.4302 -.0002 2 0 3
2.4000 2.4028 -.0028 2 3 0
2.3000 2.3004 -.0004 -3 0 4
2.2700 2.2716 -.0016 4 0 0
2.2200 2.2204 -.0004 -3 1 4
2.1000 2.0986 .0014 4 0 1
a= 9.459 b= 8.493 c= 10.702 beta= 106.14
da=.002 db= .001 dc=.007 dbeta=.05
V= 825.9
Triklin
Dexp Dcal d(D) h k l
3.6200 3.6190 .0010 -1 0 1
3.0000 3.0002 -.0002 0 -2 1
2.8400 2.8390 .0010 1 -2 1
2.7300 2.7284 .0016 -2 0 1
2.5800 2.5793 .0007 -2 -1 1
2.4800 2.4788 .0012 2 3 0
2.4300 2.4310 -.0010 -3 1 0
2.4000 2.4004 -.0004 0 -3 1
2.3000 2.3004 -.0004 3 0 1
2.2700 2.2703 -.0003 -1 -3 1
2.2200 2.2202 -.0002 0 4 1
2.1000 2.1000 .0000 -3 0 1
A= 7.6714 DA= .0006
B= 9.600 DB= .007
C= 4.42319 DC= .00003
GAMMA= 86.99 DGAMMA= .01
BETA = 83.641 DBETA = .003
ALPHA= 81.519 DALPHA= .001
V= 320.0
28. 22-1450
TaCl5*CNCl
Triklin
Dexp Dcal d(D) h k l
6.1200 6.1211 -.0011 1 1 1
5.9000 5.8970 .0030 -1 -1 1
5.3200 5.3242 -.0042 2 1 0
5.1500 5.1444 .0056 0 0 2
4.9600 4.9646 -.0046 2 0 1
4.8200 4.8194 .0006 -2 -1 1
4.6500 4.6427 .0073 2 1 1
4.3000 4.3035 -.0035 1 1 2
3.8700 3.8688 .0012 -1 2 1
3.7100 3.7111 -.0011 -1 -2 1
3.4300 3.4296 .0004 0 0 3
3.3600 3.3606 -.0006 -1 1 3
A= 12.721 DA= .001
B= 8.5617 DB= .0001
C= 10.5573 DC= .0001
GAMMA= 84.579 DGAMMA= .008
BETA = 99.056 DBETA = .002
ALPHA= 81.720 DALPHA= .003
V=1112.6
29. 22-1937
C10H12Br12Cl6N2Ta6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
9.5200 9.5487 -.0287 1 0 1
6.8800 6.8632 .0168 0 1 0
6.6500 6.6548 -.0048 2 0 1
5.5700 5.5730 -.0030 1 1 1
4.7800 4.7776 .0024 2 1 1
4.3300 4.3239 .0061 1 1 2
4.2200 4.2232 -.0032 3 1 0
3.9600 3.9568 .0032 0 0 3
3.8100 3.8061 .0039 4 0 1
3.4300 3.4316 -.0016 0 2 0
3.2300 3.2294 .0006 1 2 1
3.1800 3.1829 -.0029 3 0 3
a=16.07 b= 6.8632 c=11.87
da= .03 db= .0005 dc= .02
V=1309
Triklin
Dexp Dcal d(D) h k l
9.5200 9.5354 -.0154 1 0 0
6.8800 6.8778 .0022 0 1 0
6.6500 6.6440 .0060 -1 0 1
5.5700 5.5712 -.0012 1 1 0
4.7800 4.7776 .0024 0 0 2
4.3300 4.3273 .0027 1 0 2
4.2200 4.2177 .0023 -1 0 2
3.9600 3.9635 -.0035 1 -1 2
3.8100 3.8037 .0063 2 -1 1
3.4300 3.4301 -.0001 2 0 2
3.2300 3.2322 -.0022 1 2 0
3.1800 3.1785 .0015 3 0 0
A= 9.541 DA= .005
B= 6.989 DB= .002
C= 9.71 DC= .01
GAMMA= 90.491 DGAMMA= .009
BETA = 88.11 DBETA = .09
ALPHA=100.24 DALPHA= .09487
V= 637.1
30. 22-1938
C10H12Cl18N2Ta6
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
9.4100 9.3905 .0195 1 0 1
6.7800 6.7569 .0231 0 1 0
6.5200 6.5196 .0004 2 0 1
5.4800 5.4847 -.0047 1 1 1
4.6900 4.6917 -.0017 2 1 1
4.2600 4.2610 -.0010 1 1 2
3.9000 3.9002 -.0002 3 1 1
3.8600 3.9002 -.0402 3 1 1
3.7200 3.7198 .0002 4 0 1
3.3800 3.3792 .0008 3 1 2
3.2600 3.2586 .0014 4 1 1
3.1800 3.1790 .0010 1 2 1
a=15.690 b= 6.757 c=11.721
da= .001 db= .001 dc= .003
v=1242.7
Triklin
Dexp Dcal d(D) h k l
9.4100 9.3802 .0298 1 0 0
6.7800 6.7597 .0203 0 1 0
6.5200 6.5197 .0003 0 0 1
5.4800 5.4810 -.0010 1 -1 0
4.6900 4.6901 -.0001 2 0 0
4.2600 4.2601 -.0001 -1 1 1
3.9000 3.9023 -.0023 -2 0 1
3.8600 3.8555 .0045 2 1 0
3.7200 3.7190 .0010 2 0 1
3.3800 3.3799 .0001 -2 -1 1
3.2600 3.2599 .0001 0 0 2
3.1800 3.1809 -.0009 1 2 0
A= 9.392 DA= .001
B= 6.760 DB= .001
C= 6.528 DC= .002
GAMMA= 89.94 DGAMMA= .01
BETA = 92.913 DBETA = .002
ALPHA= 89.94 DALPHA= .01
V= 413.93
31. 23-0563
Ta6Br14*8H2O
Triklin
Dexp Dcal d(D) h k l
9.1600 9.1372 .0228 -1 1 0
8.5100 8.5132 -.0032 1 1 1
8.0500 8.0588 -.0087 1 -1 1
7.8400 7.8357 .0043 -1 0 1
7.4800 7.4792 .0008 0 2 0
6.9500 6.9604 -.0104 -1 -1 1
6.5400 6.5443 -.0043 0 2 1
6.2200 6.2206 -.0006 -1 2 0
5.8900 5.8877 .0023 1 1 2
5.6100 5.6115 -.0015 2 1 0
4.2200 4.2196 .0004 -1 -3 1
4.1800 4.1794 .0006 -2 -2 1
A= 12.2634 DA= .0001
B= 14.9849 DB= .0002
C= 13.119 DC= .001
GAMMA= 87.152 DGAMMA= .004
BETA = 76.395 DBETA = .008
ALPHA= 87.519 DALPHA= .003
V=2343
32. 23-0564
Ta6Cl14*8H2O
Triklin
Dexp Dcal d(D) h k l
8.6400 8.6241 .0159 1 0 0
8.1000 8.0958 .0042 0 1 0
7.6700 7.6738 -.0038 0 0 1
7.0000 7.0022 -.0022 1 0 1
5.9000 5.9016 -.0016 1 1 0
4.9700 4.9716 -.0016 -1 0 1
4.5800 4.5819 -.0019 0 -2 1
4.4300 4.4268 .0032 1 -2 1
4.3600 4.3517 .0083 0 -1 2
4.3100 4.3121 -.0021 2 0 0
4.0400 4.0387 .0013 1 0 2
3.8800 3.8795 .0005 2 -1 2
A= 9.310 DA= .005
B= 9.3499 DB= .0003
C= 9.395 DC= .005
GAMMA=100.883 DGAMMA= .003
BETA = 67.88 DBETA = .03
ALPHA=120.03 DALPHA= .02
V= 656.0
33. 23-0608
delta-Re0.8Ta0.1C0.1
Triklin
Dexp Dcal d(D) h k l
4.2600 4.2618 -.0018 1 0 0
3.3500 3.3484 .0016 1 1 0
3.2500 3.2530 -.0030 0 0 2
2.7700 2.7715 -.0015 0 2 0
2.5700 2.5695 .0005 1 0 2
2.4500 2.4487 .0013 -1 1 2
2.2700 2.2689 .0011 1 -1 2
2.2300 2.2304 -.0004 0 2 2
2.1200 2.1179 .0021 -1 -2 1
1.9760 1.9766 -.0006 2 1 0
1.8190 1.8192 -.0002 1 -2 2
1.8110 1.8116 -.0006 -1 -2 2
A= 4.2630 DA= .0001
B= 5.57595 DB= .00009
C= 6.5441 DC= .0001
GAMMA= 91.169 DGAMMA= .003
BETA = 90.884 DBETA = .0016
ALPHA= 83.8649 DALPHA= .0001
V=154.6
34. 23-0626
SmTa7O19
Triklin
Dexp Dcal d(D) h k l
9.9700 9.9554 .0146 1 0 0
5.3800 5.3832 -.0032 -1 1 1
4.9700 4.9696 .0004 1 -1 1
4.7300 4.7334 -.0034 -2 1 0
3.6500 3.6466 .0034 0 2 1
3.3100 3.3132 -.0032 3 -1 1
3.0700 3.0694 .0006 1 2 0
2.9620 2.9627 -.0007 -2 1 2
2.8200 2.8197 .0003 1 0 3
2.7440 2.7439 .0001 2 2 1
2.6340 2.6359 -.0019 2 2 2
2.5990 2.5990 -.0000 4 0 1
A= 10.6384 DA= .0009
B= 7.548 DB= .001
C= 8.690 DC= .002
GAMMA=102.211 DGAMMA= .006
BETA = 76.921 DBETA = .0005
ALPHA= 76.80 DALPHA= .01
V= 635.7
35. 23-1007
mu-Al23Co23Ta54
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
2.5010 2.4996 .0014 -4 0 3
2.3140 2.3163 -.0023 0 1 0
2.2830 2.2834 -.0004 4 0 2
2.1950 2.1943 .0007 1 1 1
2.1470 2.1489 -.0019 2 1 0
2.0660 2.0657 .0003 2 1 1
2.0260 2.0266 -.0006 0 0 5
1.9330 1.9327 .0003 5 0 2
1.4470 1.4475 -.0005 -6 0 6
1.3800 1.3802 -.0002 -5 0 7
1.3700 1.3703 -.0003 5 0 5
1.2530 1.2525 .0005 -2 1 7
a= 11.85 b= 2.3163 c=10.424 beta= 103.57
da=.01 db=.0008 dc=.005 dbeta=.07
V= 278.0
Triklin
Dexp Dcal d(D) h k l
2.5010 2.5012 -.0002 -1 0 2
2.3140 2.3140 -.0000 0 1 2
2.2830 2.2829 .0001 0 -1 2
2.1950 2.1954 -.0004 1 0 2
2.1470 2.1462 .0008 -2 1 0
2.0660 2.0671 -.0011 -1 2 0
2.0260 2.0260 -.0000 -2 0 2
1.9330 1.9330 .0000 1 -1 2
1.4470 1.4471 -.0001 2 3 1
1.3800 1.3799 .0001 1 3 2
1.3700 1.3700 -.0000 3 1 2
1.2530 1.2530 .0000 1 -3 2
A= 5.47280 DA= .00003
B= 5.01899 DB= .00004
C= 5.27412 DC= .00004
GAMMA= 77.979 DGAMMA= .003
BETA = 99.4342 DBETA = .0004
ALPHA= 91.056 DALPHA= .001
V=140
36. 23-1900
C18H15Cl5PSTa
Triklin
Dexp Dcal d(D) h k l
8.1100 8.1023 .0077 0 0 1
7.8200 7.8452 -.0252 0 1 1
7.2100 7.1841 .0259 0 -1 1
6.9500 6.9283 .0217 1 0 0
6.4900 6.4744 .0156 1 0 1
6.2400 6.2613 -.0213 1 1 0
6.0700 6.0895 -.0195 1 1 1
5.8700 5.9054 -.0354 0 -2 1
5.5000 5.4960 .0040 1 -2 1
5.3400 5.3274 .0126 1 2 1
5.1200 5.1467 -.0267 -1 3 0
4.9500 4.9232 .0268 0 4 0
A= 7.41786 DA= .00008
B= 19.9636 DB= .0001
C= 8.6533 DC= .0001
GAMMA= 96.181 DGAMMA= .001
BETA = 70.6875 DBETA = .0004
ALPHA= 85.3323 DALPHA= .0007
V=1192.9