== Соединения Pb (томa 41-45) == |
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363. 41-0677 PbCO)*2H2O Triklin
Dexp Dcal d(D) h k l 4.4504 4.4457 .0047 0 -1 2 4.2704 4.2693 .0011 2 -1 0 3.5971 3.5968 .0003 0 1 2 3.5065 3.5042 .0023 0 2 0 3.0789 3.0811 -.0022 -2 0 2 2.5923 2.5920 .0003 2 -1 4 2.5286 2.5286 .0000 3 -2 3 2.4946 2.4952 -.0006 2 2 2 2.2168 2.2162 .0006 -4 1 1 2.0826 2.0820 .0006 3 -3 1 2.0102 2.0096 .0006 1 0 5 1.9831 1.9838 -.0007 2 -2 5
A= 11.448 DA= .002 B= 7.222 DB= .002 C= 10.513 DC= .001 GAMMA= 95.32 DGAMMA= .03 BETA = 69.228 DBETA = .003 ALPHA=103.98 DALPHA= .01 V=789.1
364. 41-0838 Pb4Gd2O7 Triklin
Dexp Dcal d(D) h k l 3.4100 3.4107 -.0007 0 2 1 3.1700 3.1721 -.0021 0 -2 1 3.0400 3.0414 -.0014 -2 2 1 2.9700 2.9707 -.0007 4 0 0 2.8800 2.8809 -.0009 0 4 0 2.8300 2.8320 -.0020 -2 -2 1 2.7650 2.7647 .0003 1 3 1 2.1990 2.1998 -.0008 -4 -2 1 2.0440 2.0459 -.0019 -5 3 0 1.9180 1.9206 -.0026 0 6 0 1.7890 1.7884 .0006 4 -4 1 1.7620 1.7613 .0007 -6 2 1 1.7020 1.7019 .0001 -6 -2 1 1.6650 1.6649 .0001 1 -6 1 1.6530 1.6530 -.0000 -6 4 0
A= 11.907 DA= .002 B= 11.564 DB= .004 C= 4.017 DC= .001 GAMMA= 91.807 DGAMMA= .002 BETA = 93.272 DBETA = .007 ALPHA= 85.48 DALPHA= .01 V=549.9
365. 42-0749 Cs2Pb{OH}6 Triklin
Dexp Dcal d(D) h k l 5.4050 5.3954 .0096 1 1 0 4.9830 5.0010 -.0180 0 0 1 3.9170 3.9122 .0048 0 -2 1 3.6780 3.6723 .0057 1 -2 1 3.4400 3.4367 .0033 2 0 0 3.2740 3.2737 .0003 0 3 0 3.1750 3.1806 -.0056 -1 -2 1 2.9980 2.9985 -.0005 2 0 1 2.8520 2.8521 -.0001 1 3 0 2.8230 2.8250 -.0020 2 -2 1 2.6910 2.6911 -.0001 -2 0 1 2.5780 2.5745 .0035 -2 1 1
A= 6.971 DA= .005 B= 10.094 DB= .008 C= 5.151 DC= .003 GAMMA= 96.96 DGAMMA= .08 BETA = 82.100 DBETA = .02 ALPHA=102.20 DALPHA= .05 V= 349.3
366. 42-1219 Cs3Sb0.53Pb5.31Cl15 Monoklin Grupa 14
Dexp Dcal d(D) h k l 8.2679 8.2633 .0046 1 1 0 7.3750 7.3662 .0088 0 1 1 6.4634 6.4671 -.0037 1 1 1 4.5521 4.5520 .0001 1 1 2 4.0767 4.0781 -.0014 4 0 0 3.6776 3.6831 -.0055 0 2 2 3.5617 3.5630 -.0013 0 1 3 3.0998 3.0997 .0001 4 0 2 3.0998 3.0988 .0010 2 1 3 2.9308 2.9345 -.0037 -2 2 3 2.7303 2.7300 .0003 -3 3 1 2.4551 2.4554 -.0003 0 3 3 2.2924 2.2929 -.0005 -7 0 2 2.1080 2.1076 .0004 -4 1 5 2.0446 2.0441 .0005 5 3 2 1.8413 1.8415 -.0002 0 4 4
a= 16.530 b= 9.5840 c= 11.6680 beta= 99.304 da= .002 db=.0008 dc=.0005 dbet=.004 V= 1824.1
367. 42-1637 C8H6N4O4PbS282H2O Triklin
Dexp Dcal d(D) h k l 9.6100 9.6057 .0043 0 1 1 9.2100 9.2116 -.0016 1 0 0 7.8700 7.8730 -.0030 0 -1 1 5.7200 5.7151 .0049 0 2 0 5.5700 5.5722 -.0022 1 0 2 4.9000 4.8945 .0055 0 -2 1 4.6200 4.6231 -.0031 -1 1 2 4.3900 4.3809 .0091 2 2 0 4.0900 4.0855 .0045 1 0 3 3.8700 3.8698 .0002 0 3 1 3.7100 3.7131 -.0031 2 3 1 3.6200 3.6196 .0004 0 3 2
A= 9.926 DA= .002 B= 12.52 DB= .01 C= 13.551 DC= .003 GAMMA= 68.69 DGAMMA= .05 BETA = 80.37 DBETA = .02 ALPHA= 75.95 DALPHA= .03 V= 1515.8
368. 43-0743 C4H6O4Pb Triklin
Dexp Dcal d(D) h k l 9.6120 9.6134 -.0014 1 1 0 6.1338 6.1316 .0022 0 1 1 5.7535 5.7517 .0018 1 0 1 4.8165 4.8172 -.0007 1 2 1 4.6225 4.6222 .0003 3 1 0 4.3744 4.3838 -.0094 2 2 1 3.9689 3.9685 .0004 3 2 0 3.7385 3.7401 -.0016 3 2 1 3.4796 3.4807 -.0011 -3 -1 1 3.3022 3.3012 .0010 -1 3 0 3.1382 3.1395 -.0013 4 2 1 2.9214 2.9228 -.0014 -4 -1 1
A= 14.225 DA= .005 B= 11.511 DB= .002 C= 6.487 DC= .001 GAMMA= 75.96 DGAMMA= .03 BETA = 84.44 DBETA = .01 ALPHA= 74.08 DALPHA= .01 V= 990.3
369. 43-0859 RbPbI3*3H2O Triklin
Dexp Dcal d(D) h k l 9.2000 9.1953 .0047 1 0 0 4.1000 4.1008 -.0008 0 1 0 3.9300 3.9291 .0009 -2 0 1 3.6500 3.6505 -.0005 0 -1 1 3.5200 3.5215 -.0015 -1 -1 1 3.3800 3.3799 .0001 2 1 0 3.2800 3.2775 .0025 1 -1 1 3.1100 3.1065 .0035 -2 0 2 3.0600 3.0576 .0024 3 0 1 3.0200 3.0166 .0034 -2 -1 1 2.9120 2.9086 .0034 -1 0 3 2.7220 2.7237 -.0017 2 -1 1
A= 9.492 DA= .005 B= 4.204 DB= .001 C= 9.86 DC= .02 GAMMA= 78.52 DGAMMA= .02 BETA = 80.11 DBETA = .06 ALPHA= 82.67 DALPHA= .02 V= 378.2
370. 43-1451 Pb5Sn3Bi4S17 Triklin
Dexp Dcal d(D) h k l 5.8643 5.8633 .0010 0 -2 1 4.0250 4.0272 -.0022 0 -4 1 3.9151 3.9223 -.0072 2 0 0 3.8698 3.8733 -.0035 0 4 1 3.6769 3.6790 -.0021 -2 2 0 3.5970 3.5988 -.0018 2 -2 1 3.3328 3.3328 -.0000 0 2 2 3.2866 3.2854 .0012 0 5 1 3.1884 3.1855 .0029 -2 0 1 3.1395 3.1394 .0001 0 6 0 3.1395 3.1394 .0001 0 6 0 3.0543 3.0573 -.0030 -1 0 2
A= 8.028 DA= .002 B= 18.881 DB= .001 C= 7.411 DC= .002 GAMMA= 93.11 DGAMMA= .04 BETA = 78.001 DBETA = .005 ALPHA= 93.04 DALPHA= .01 V=1094.4
371. 43-1542 C6HN3O8Pb Rombik Groupa 33,49,62
Dexp. Dcal. d(D) h k l 7.7500 7.6871 .0629 1 1 0 5.6800 5.7116 -.0316 1 2 0 4.3300 4.3218 .0082 1 3 0 3.7000 3.6953 .0047 0 4 0 3.1900 3.1862 .0038 1 2 1 3.0300 3.0283 .0017 0 3 1 2.9400 2.9400 -.0000 3 1 0 2.5500 2.5530 -.0030 1 4 1
a= 9.0001 b=14.78 c= 3.839 da= .0001 db= .03 dc= .008 V= 510.7
372. 43-1543 C6HN3O8Pb*H2O Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 8.5600 8.5602 -.0002 1 1 0 7.7900 7.7917 -.0017 0 1 1 4.6200 4.6206 -.0006 -1 0 2 3.9900 3.9904 -.0004 1 1 2 3.8900 3.8905 -.0005 -2 0 2 3.1900 3.1901 -.0001 2 3 1 2.9400 2.9395 .0005 -2 0 3
a= 11.181 b= 13.494 c= 9.636 beta= 97.944 da= .001 db=.001 dc=.002 dbet= .004 V= 1439.8
| 373. 43-1544 C6HN3O8Pb Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 12.1800 12.1419 .0381 0 0 1 6.4300 6.4421 -.0121 0 1 1 5.8600 5.8631 -.0031 1 1 1 4.8400 4.8444 -.0044 2 1 0 4.1000 4.0924 .0076 3 0 1 3.6500 3.6499 .0001 -2 1 2 3.5200 3.5203 -.0003 1 1 3 3.4600 3.4567 .0033 -1 2 1 3.1200 3.1212 -.0012 4 0 1 3.0700 3.0716 -.0016 3 0 3 2.8500 2.8492 .0008 2 0 4
a= 12.640 b= 7.600 c= 12.205 beta= 84.163 da= .001 db.001 dc=.002 dbet=.005 V= 1166
374. 44-0827 PbPr{WO4}7 Monoklin Grupa 3
Dexp Dcal d(D) h k l 6.7700 6.7668 .0032 1 1 0 5.9200 5.9239 -.0039 1 1 1 5.4600 5.4572 .0028 -2 0 1 5.1300 5.1278 .0022 2 0 1 4.8900 4.8918 -.0018 -1 1 2 4.0100 4.0078 .0022 -2 1 2 3.4590 3.4589 .0001 -3 0 2
a= 11.5400 b= 8.370 c= 13.4800 beta= 94.924 da= .0009 db=.001 dc=.0003 dbet=.004 V= 1297.2
375. 44-0828 PbTb2{WO4}4 Triklin
Dexp Dcal d(D) h k l 8.0000 7.9981 .0019 1 1 0 7.1200 7.1255 -.0055 0 1 1 6.3900 6.4038 -.0138 0 -1 1 5.9100 5.9182 -.0082 2 1 1 5.3000 5.3009 -.0009 1 1 2 4.8800 4.8824 -.0024 0 0 2 4.4300 4.4270 .0030 2 2 1 4.2700 4.2715 -.0015 1 -1 2 3.9930 3.9990 -.0060 2 2 0 3.9570 3.9592 -.0022 -2 0 1 3.8070 3.8014 .0056 -1 -2 1 3.7510 3.7519 -.0009 3 0 2
A= 12.4446 DA= .0008 B= 9.891 DB= .002 C= 11.2521 DC= .0008 GAMMA= 71.08 DGAMMA= .01 BETA = 60.789 DBETA = .005 ALPHA= 75.752 DALPHA= .007 V-1137.1
376. 44-0950 Pb2Sb3F13 Triklin
Dexp Dcal d(D) h k l 16.4500 16.4495 .0005 1 0 0 4.0600 4.0580 .0020 0 2 1 3.7600 3.7605 -.0005 4 0 1 3.7100 3.7089 .0011 -4 1 0 3.6800 3.6816 -.0016 3 -1 1 3.6300 3.6291 .0009 2 2 1 3.3900 3.3911 -.0011 2 2 0 3.3600 3.3585 .0015 -3 -1 1 3.2900 3.2899 .0001 5 0 0 3.2600 3.2657 -.0057 -1 2 2 3.2500 3.2511 -.0011 3 2 1 2.9600 2.9588 .0012 1 -1 2
A= 16.532 DA= .005 B= 8.214 DB= .004 C= 8.061 DC= .005 GAMMA= 91.27 DGAMMA= .05 BETA = 85.27 DBETA = .04 ALPHA= 68.62 DALPHA= .02 V= 1014.2
377. 44-1999 C36H70O6Pb3 Triklin
Dexp Dcal d(D) h k l 50.0000 49.7406 .2594 1 0 0 24.9000 24.8703 .0297 2 0 0 16.5000 16.5802 -.0802 3 0 0 12.4000 12.4352 -.0352 4 0 0 9.8800 9.9481 -.0681 5 0 0 8.2400 8.2901 -.0501 6 0 0 7.3000 7.2992 .0008 -4 2 0 7.0500 7.0503 -.0003 3 2 0 6.7200 6.7222 -.0022 2 -2 1 6.3300 6.3067 .0233 -7 0 1 5.8900 5.8522 .0378 7 -1 1 5.4700 5.4747 -.0047 6 -2 1
A= 50.19 DA= .04 B= 16.63 DB= .001 C= 12.38 DC= .03 GAMMA= 97.07 DGAMMA= .01 BETA = 93.1 DBETA = .1 ALPHA= 89.24 DALPHA= .01 V=10279
378. 45-1150 PbHgI4 Monoklin Grupa 14
Dexp Dcal d(D) h k l 7.0300 7.0310 -.0010 0 1 1 6.6019 6.5992 .0027 1 1 0 4.3078 4.3054 .0024 2 1 1 4.0586 4.0545 .0041 0 2 1 3.3482 3.3482 -.0000 -1 1 3 3.2995 3.2996 -.0001 2 2 0 2.7120 2.7123 -.0003 1 3 1 2.6496 2.6502 -.0006 2 1 4 2.5033 2.5037 -.0004 2 3 0 2.1490 2.1489 .0001 0 4 0
a= 10.381 b= 8.596 c= 12.3200 beta= 82.773 da=.001 db=.001 dc=.0005 dbet=.008 V= 1090.6
379. 45-1151 PbHgI4 Rombik Groupa 31,59
Dexp. Dcal. d(D) h k l 7.0081 7.0000 .0081 0 1 1 6.5824 6.5992 -.0168 2 0 0 4.2910 4.2914 -.0004 1 1 2 4.0476 4.0473 .0003 3 0 1 3.3482 3.3482 -.0000 3 0 2 3.2971 3.2996 -.0025 4 0 0 2.7104 2.7104 -.0000 3 0 3 2.6405 2.6397 .0008 5 0 0 2.4979 2.4979 -.0000 3 3 1 2.1434 2.1433 .0001 6 1 0
a=13.198 b= 9.524 c=10.323 da= .002 db= .009 dc= .001 V=1297.7
Monoklin Grupa 7,13
Dexp Dcal d(D) h k l 7.0081 7.0046 .0035 0 1 1 6.5824 6.5837 -.0013 1 1 0 4.2910 4.2873 .0037 0 0 2 4.0476 4.0480 -.0004 0 3 0 3.3482 3.3481 .0001 2 1 1 3.2971 3.2919 .0052 2 2 0 2.7104 2.7105 -.0001 -2 3 1 2.6405 2.6402 .0003 2 3 1 2.4979 2.4975 .0004 -1 2 3 2.1434 2.1437 -.0003 0 0 4
a= 7.8500 b= 12.144 c= 8.591 beta= 93.527 da= .0009 db=.001 dc=.003 dbet=.006 V= 817.4
380. 45-1152 PbHgI4 Rombik Groupa 34,58
Dexp. Dcal. d(D) h k l 6.9971 6.9867 .0104 0 1 1 6.6216 6.6042 .0174 1 1 0 4.2954 4.2934 .0020 1 0 3 4.0404 4.0415 -.0011 0 2 0 3.3408 3.3414 -.0006 1 2 2 3.3019 3.3021 -.0002 2 2 0 2.6992 2.6992 .0000 4 1 0 2.6345 2.6342 .0003 0 2 4 2.1466 2.1467 -.0001 2 0 6
a=11.454 b= 8.083 c=13.893 da= .005 db= .004 dc= .008 v=1286.3
381. 45-1153 PbHgI4 Rombik Groupa 34,58
Dexp. Dcal. d(D) h k l 7.0415 7.1101 -.0686 0 1 1 6.6414 6.6354 .0060 1 1 0 4.3161 4.3159 .0002 1 0 3 4.0623 4.0695 -.0072 0 1 3 3.5556 3.5551 .0005 0 2 2 3.2971 3.2997 -.0026 3 1 1 2.7071 2.7064 .0007 2 2 3 2.6465 2.6461 .0004 4 1 0 2.1434 2.1431 .0003 2 2 5
a=11.175 b= 8.246 c=14.037 da= .004 db= .004 dc= .007 v=1293.6
382. 45-1154 PbHgI4 Rombik Groupa 19
Dexp. Dcal. d(D) h k l 7.0192 6.9821 .0371 0 2 0 6.6414 6.6267 .0147 1 0 1 4.3078 4.3076 .0002 1 3 0 4.0404 4.0427 -.0023 0 3 1 3.3432 3.3372 .0060 1 4 0 3.2932 3.2943 -.0011 2 3 1 2.7104 2.7122 -.0018 1 5 0 2.6420 2.6422 -.0002 0 5 1 2.1450 2.1450 .0000 0 4 3
a=11.37 b=13.964 c= 8.156 da= .02 db= .003 dc= .003 V=1294.6 |
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