== Соединения Pb (томa 37-40) == |
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343.37-0200 PbSiO3*xH2O Triklin
Dexp Dcal d(D) h k l 8.4700 8.4849 -.0149 0 1 0 4.9300 4.9307 -.0007 0 -1 1 4.5500 4.5517 -.0017 -1 0 1 4.2750 4.2831 -.0081 1 0 2 4.1330 4.1324 .0006 -1 1 1 3.4470 3.4476 -.0006 2 3 2 3.2310 3.2319 -.0009 0 -1 2 3.2010 3.2003 .0007 -1 1 2 2.9970 2.9973 -.0003 1 0 3 2.6390 2.6391 -.0001 2 4 4 2.5900 2.5899 .0001 -2 1 1 2.1380 2.1374 .0006 0 0 4
A= 8.257 DA= .002 B= 11.5302 DB= .0009 C= 11.807 DC= .001 GAMMA= 57.702 DGAMMA= .004 BETA = 56.281 DBETA = .006 ALPHA= 50.024 DALPHA= .005 V= 688.0
344. 37-0201 Pb2SiO4*xH2O Triklin
Dexp Dcal d(D) h k l 6.6200 6.6192 .0008 0 2 0 6.4100 6.4202 -.0102 0 -1 1 6.3300 6.3361 -.0061 1 -1 0 6.2700 6.2695 .0005 1 1 0 4.8900 4.8935 -.0035 -1 2 0 4.8300 4.8323 -.0023 1 2 0 4.6500 4.6558 -.0058 1 0 1 4.4180 4.4128 .0052 0 3 0 3.8270 3.8353 -.0083 1 2 1 3.7760 3.7790 -.0030 -1 3 0 3.6130 3.6106 .0024 -1 3 1 3.5870 3.5834 .0036 2 0 0
A= 7.3806 DA= .00007 B= 13.2509 DB= .0002 C= 7.7233 DC= .0007 GAMMA= 91.277 DGAMMA= .001 BETA =103.814 DBETA = .003 ALPHA= 87.625 DALPHA= .008 V=732.6
345. 37-0203 Pb2SiO4 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 9.6700 9.7293 -.0593 0 0 1 6.0500 6.0487 .0013 1 1 0 4.4600 4.4565 .0035 -1 0 2 3.7200 3.7241 -.0040 2 0 2 3.6800 3.6813 -.0013 -2 0 2 3.2125 3.2164 -.0039 1 2 1 3.1245 3.1293 -.0048 1 0 3 3.0176 3.0144 .0032 3 0 2 3.0176 3.0243 -.0067 2 2 0 2.8752 2.8760 -.0008 0 2 2 2.7759 2.7766 -.0007 3 1 2 2.3842 2.3846 -.0004 1 0 4 2.0327 2.0329 -.0002 4 2 2 1.9836 1.9823 .0013 1 2 4 1.7941 1.7943 -.0002 5 2 2
a= 11.417 b= 7.132 c= 9.7300 beta= 89.323 da= .001 db= .0006 dc=.0002 dbet=.004 V= 792.2
346. 37-0306 Pb2O{WO4} Triklin
Dexp. Dcal. d(D) h k l 6.4400 6.4400 .0000 0 -2 0 5.6000 5.6000 .0000 2 -1 0 5.3400 5.3441 -.0041 0 1 1 5.2000 5.2092 -.0092 2 0 0 4.3100 4.3084 .0016 -2 -1 0 3.6670 3.6716 -.0046 2 0 1 3.6160 3.6158 .0002 -2 -1 1 3.4740 3.4721 .0019 -2 -2 0 3.4550 3.4570 -.0020 1 -4 0 3.4120 3.4127 -.0007 0 -3 1 3.2100 3.2038 .0062 2 -3 1 3.1470 3.1461 .0009 -3 0 1
A= 11.312 DA= .001 B= 13.894 DB= .006 C= 5.8634 DC= .0003 GAMMA=111.99 DGAMMA= .06 BETA = 97.76 DBETA = .02 ALPHA= 85.81 DALPHA= .03 V= 846.5
347. 37-0631 Cd4Pb{br4O11} Triklin
Dexp Dcal d(D) h k l 7.0100 7.0124 -.0024 1 1 0 6.4100 6.4088 .0012 1 1 1 5.8600 5.8564 .0036 1 -1 1 4.6200 4.6138 .0062 1 -2 1 4.3500 4.3449 .0051 1 3 0 3.6900 3.6897 .0003 2 2 1 3.4900 3.4876 .0024 0 4 0 3.3200 3.3186 .0014 0 -4 1 3.1600 3.1601 -.0001 1 3 2 2.9260 2.9282 -.0022 2 -2 2 2.8440 2.8447 -.0007 -1 1 2 2.8090 2.8092 -.0002 1 5 0
A= 7.93358 DA= .00009 B= 14.278 DB= .008 C= 8.613 DC= .001 GAMMA= 79.16 DGAMMA= .01 BETA = 67.70 DBETA = .02 ALPHA= 91.19 DALPHA= .03 V= 882.0
348. 37-0632 Cd2Pb{BO3}2 Triklin
Dexp Dcal d(D) h k l 5.4300 5.4283 .0017 0 1 1 4.9800 4.9820 -.0020 0 -1 1 4.2200 4.2217 -.0017 -1 1 0 4.0700 4.0765 -.0065 -1 0 1 3.6800 3.6757 .0043 0 1 2 3.2500 3.2426 .0074 1 0 2 2.9540 2.9542 -.0002 1 -1 2 2.8710 2.8746 -.0036 1 1 2 2.7120 2.7142 -.0022 0 2 2 2.4910 2.4910 .0000 0 -2 2 2.0550 2.0545 .0005 -2 -1 1 1.9740 1.9713 .0027 1 2 3
A= 4.885 DA= .001 B= 6.7391 DB= .0005 C= 8.368 DC= .002 GAMMA= 98.58 DGAMMA= .01 BETA = 87.55 DBETA = .04 ALPHA= 85.40 DALPHA= .01 V= 271.1
349. 37-1053 PbSnF6 Triklin
Dexp Dcal d(D) h k l 5.0120 5.0134 -.0014 1 -2 1 4.8970 4.8968 .0002 -1 0 1 3.8870 3.8939 -.0069 1 2 0 3.7410 3.7405 .0005 2 -2 1 3.6160 3.6136 .0024 -2 2 0 3.4950 3.4957 -.0007 1 -2 2 3.4060 3.4060 -.0000 0 0 2 3.2590 3.2583 .0007 1 0 2 2.9820 2.9801 .0019 2 -1 2 2.5100 2.5094 .0006 2 2 1 2.4320 2.4304 .0016 3 -2 2 2.1010 2.1009 .0001 0 -5 2
A= 8.341 DA= .001 B= 11.529 DB= .003 C= 7.375 DC= .002 GAMMA=108.11 DGAMMA= .01 BETA = 77.831 DBETA = .004 ALPHA=111.692 DALPHA= .006 V=622.5
350. 37-1054 Pb3GeF10 Triklin
Dexp Dcal d(D) h k l 10.5670 10.5557 .0113 1 0 0 5.2850 5.2893 -.0043 1 0 1 4.3000 4.3032 -.0032 -1 2 0 3.9830 3.9831 -.0001 2 -2 0 3.7920 3.7925 -.0005 2 1 0 3.5250 3.5254 -.0004 -1 0 2 3.4580 3.4541 .0039 -3 0 1 3.3410 3.3372 .0038 1 2 0 3.2450 3.2445 .0005 3 -1 1 3.1840 3.1844 -.0004 -2 2 1 3.0430 3.0420 .0010 -1 -2 2 2.8570 2.8571 -.0001 0 -3 1
A= 11.442 DA= .001 B= 9.071 DB= .002 C= 7.480 DC= .001 GAMMA=109.09 DGAMMA= .01 BETA = 95.24 DBETA = .01 ALPHA=108.426 DALPHA= .001 V= 679.5
351. 37-1055 Pb3Be2F14 Triklin
Dexp Dcal d(D) h k l 6.7530 6.7665 -.0135 1 2 0 4.8330 4.8353 -.0023 2 2 0 4.3580 4.3601 -.0021 0 -1 1 4.0880 4.0864 .0016 2 3 0 4.0080 4.0079 .0001 1 2 1 3.7820 3.7866 -.0046 -1 3 0 3.5590 3.5589 .0001 1 3 1 3.4550 3.4603 -.0053 3 2 0 3.3510 3.3487 .0023 3 0 0 3.1770 3.1765 .0005 1 -2 1 3.0700 3.0712 -.0012 1 4 1 2.8950 2.8950 -.0000 3 4 0
A= 10.6599 DA= .0004 B= 14.691 DB= .001 C= 4.95822 DC= .00002 GAMMA= 73.386 DGAMMA= .003 BETA = 98.041 DBETA = .003 ALPHA= 83.475 DALPHA= .001 V=726.8
352. 37-1069 TlI*2PBI2 Triklin
Dexp Dcal d(D) h k l 4.8400 4.8358 .0042 0 1 1 4.3400 4.3322 .0078 1 0 0 3.8470 3.8443 .0027 0 -1 1 3.4900 3.4895 .0005 1 -1 1 3.2480 3.2447 .0033 0 2 0 3.1330 3.1380 -.0050 0 2 1 2.8180 2.8186 -.0006 0 0 2 2.5220 2.5229 -.0009 1 1 2 2.4090 2.4058 .0032 1 2 1 2.1020 2.1021 -.0001 -1 2 2 1.9840 1.9845 -.0005 2 1 1 1.8940 1.8939 .0001 -2 2 1 1.7570 1.7575 -.0005 1 3 0 1.6120 1.6119 .0001 0 3 3 1.5690 1.5690 -.0000 0 4 2
A= 4.581 DA= .001 B= 6.8366 DB= .0007 C= 5.902 DC= .001 GAMMA=102.89 DGAMMA= .04 BETA = 78.80 DBETA = .01 ALPHA= 79.96 DALPHA= .01 V= 172.1
353. 38-0047 alfa-AgPbPO4 Triklin
Dexp Dcal d(D) h k l 4.7100 4.7126 -.0026 0 1 1 4.5100 4.5102 -.0002 0 -1 1 4.1800 4.1816 -.0016 1 1 1 4.0800 4.0807 -.0007 0 -1 2 3.9620 3.9620 -.0000 1 -1 1 3.3160 3.3135 .0025 -1 -1 3 3.2090 3.2092 -.0002 2 1 1 3.1120 3.1111 .0009 -2 -1 1 3.0540 3.0517 .0023 0 1 5 2.9400 2.9381 .0019 2 -1 2 2.9280 2.9277 .0003 1 0 6 2.8220 2.8235 -.0015 -2 1 3
A= 8.500 DA= .002 B= 4.7807 DB= .0005 C= 18.53 DC= .01 GAMMA= 88.41 DGAMMA= .05 BETA = 87.53 DBETA = .05 ALPHA= 84.74 DALPHA= .04 V= 748.9 | 354. 40-0208 Pb2{P4O12} Triklin
Dexp Dcal d(D) h k l 5.7176 5.7105 .0071 1 2 0 5.1552 5.1546 .0006 0 0 1 4.2908 4.2931 -.0023 0 -2 1 3.9515 3.9513 .0002 1 3 1 3.7078 3.7058 .0020 1 -2 1 3.4930 3.4890 .0040 -1 -2 1 3.2203 3.2202 .0001 2 2 0 3.1644 3.1677 -.0033 -2 1 0 3.0178 3.0195 -.0017 2 1 1 2.9688 2.9697 -.0009 2 0 1 2.8400 2.8402 -.0002 0 6 1 2.7466 2.7461 .0005 2 4 1
A= 6.699 DA= .002 B= 19.120 DB= .007 C= 5.267 DC= .002 GAMMA= 81.868 DGAMMA= .001 BETA = 80.631 DBETA = .002 ALPHA= 81.518 DALPHA= .001 V= 653.6
355. 40-0210 Pb2{P4O12} Triklin
Dexp Dcal d(D) h k l 6.2809 6.2859 -.0050 0 -1 2 5.1552 5.1561 -.0009 1 0 0 4.5063 4.5059 .0004 0 2 0 4.0953 4.0927 .0026 -1 -1 2 3.7855 3.7856 -.0001 -1 0 3 3.6607 3.6601 .0006 -1 2 0 3.4930 3.4907 .0023 0 0 4 3.4399 3.4337 .0062 0 2 2 3.2433 3.2405 .0028 -1 -2 2 3.1754 3.1768 -.0014 1 2 0 2.9308 2.9310 -.0002 1 2 1 2.7883 2.7884 -.0001 1 -3 1
A= 5.26048 DA= .00002 B= 9.32853 DB= .00008 C= 14.5132 DC= .0002 GAMMA= 96.1330 DGAMMA= .0001 BETA = 98.0383 DBETA = .0001 ALPHA=102.602 DALPHA= .001 V=681.3
356. 40-0551 Pb2O{NO3}2 Triklin
Dexp Dcal d(D) h k l 9.3020 9.2868 .0152 0 1 1 7.3690 7.3778 -.0088 0 -1 1 7.0190 7.0165 .0025 -1 0 1 5.8620 5.8613 .0007 0 2 1 4.5480 4.5489 -.0009 1 2 0 4.2230 4.2224 .0006 1 0 2 4.1070 4.1097 -.0027 -1 -2 1 3.9220 3.9217 .0003 -2 0 1 3.6930 3.6889 .0041 0 -2 2 3.5200 3.5211 -.0011 2 0 1 3.2500 3.2509 -.0009 1 -3 1 3.1730 3.1743 -.0013 -2 -1 2
A= 8.058 DA= .001 B= 12.432 DB= .001 C= 11.705 DC= .001 GAMMA= 98.33 DGAMMA= .04 BETA =101.57 DBETA = .03 ALPHA= 75.601 DALPHA= .004 V= 1107.1
357. 40-0778 Pb{ClO4}2 Triklin
Dexp Dcal d(D) h k l 4.5900 4.5703 .0197 -1 1 1 4.4000 4.3958 .0042 1 -1 1 4.1700 4.1724 -.0024 0 -1 1 3.7900 3.8011 -.0111 1 1 0 3.5000 3.4999 .0001 -2 1 0 3.4700 3.4739 -.0039 -1 1 2 3.3500 3.3540 -.0040 -1 0 2 3.3200 3.3219 -.0019 1 -1 2 3.1400 3.1421 -.0021 1 0 3 3.0300 3.0312 -.0012 0 1 3 2.9900 2.9887 .0013 -2 0 1 2.8600 2.8604 -.0004 0 2 1
A= 7.6664 DA= .0009 B= 5.8901 DB= .0003 C= 9.7182 DC= .0003 GAMMA=103.75 DGAMMA= .01 BETA = 75.75 DBETA = .01 ALPHA= 77.596 DALPHA= .005 V=394.9
358. 40-0779 Pb{ClO4}2*H2O Triklin
Dexp Dcal d(D) h k l 7.6500 7.6364 .0136 -1 1 0 6.8700 6.8965 -.0265 1 1 0 5.3800 5.3554 .0246 -3 1 0 4.6400 4.6374 .0026 3 1 0 4.3700 4.3623 .0077 -2 0 1 4.2300 4.2238 .0063 1 -1 1 4.0800 4.0811 -.0011 2 0 1 3.9000 3.9058 -.0058 0 2 0 3.8000 3.8004 -.0004 -1 1 1 3.5900 3.5917 -.0017 3 -1 1 3.5000 3.5093 -.0093 -4 0 1 3.2700 3.2691 .0009 5 1 0
A= 19.494 DA= .008 B= 7.980 DB= .007 C= 4.7551 DC= .0005 GAMMA= 97.75 DGAMMA= .04 BETA = 93.637 DBETA = .003 ALPHA= 98.33 DALPHA= .02 V=732.4
Triklin
Dexp Dcal d(D) h k l 7.6500 7.6390 .0110 -1 0 1 6.8700 6.8720 -.0020 1 1 0 5.3800 5.3689 .0111 -1 -2 1 4.6400 4.6393 .0007 1 1 1 4.3700 4.3715 -.0015 -2 0 1 4.2300 4.2240 .0060 -1 1 2 4.0800 4.0799 .0001 2 0 0 3.9000 3.8945 .0055 -2 1 0 3.8000 3.8009 -.0009 -1 3 0 3.5900 3.5940 -.0040 -1 -3 2 3.5000 3.4999 .0001 -1 3 1 3.2700 3.2743 -.0043 -1 0 3
A= 8.7996 DA= .0001 B= 13.1575 DB= .0001 C= 10.0575 DC= .0006 GAMMA= 85.6718 DGAMMA= .0006 BETA =111.992 DBETA = .001 ALPHA=102.405 DALPHA= .001 V=1054.7
359. 40-0780 Pb{ClO4}2*3H2O Triklin
Dexp Dcal d(D) h k l 6.3200 6.3210 -.0010 -1 0 1 5.3700 5.3686 .0014 0 -1 1 3.9400 3.9430 -.0030 1 0 3 3.6700 3.6697 .0003 2 0 1 3.4400 3.4412 -.0012 -2 1 1 3.0300 3.0299 .0001 2 -1 3 3.0100 3.0126 -.0026 1 -1 4 2.9700 2.9689 .0011 1 -2 1 2.8300 2.8279 .0021 0 2 0 2.6900 2.6902 -.0002 -2 2 0 2.5300 2.5305 -.0005 -2 -1 2 2.4800 2.4798 .0002 0 -2 3
A= 7.904 DA= .002 B= 5.984 DB= .002 C= 13.42 DC= .02 GAMMA=108.49 DGAMMA= .08 BETA = 83.98 DBETA = .03 ALPHA= 96.44 DALPHA= .09 V= 596.6
Triklin
Dexp Dcal d(D) h k l 6.3200 6.3104 .0096 -1 0 1 5.3700 5.3686 .0014 1 1 0 3.9400 3.9422 -.0022 1 -2 1 3.6700 3.6724 -.0024 -1 2 1 3.4400 3.4374 .0026 -1 1 2 3.0300 3.0294 .0006 -1 3 0 3.0100 3.0116 -.0016 0 -3 1 2.9700 2.9698 .0002 1 2 1 2.8300 2.8288 .0012 2 1 1 2.6900 2.6899 .0001 0 2 2 2.5300 2.5281 .0019 2 0 2 2.4800 2.4807 -.0007 -3 2 1
A= 8.259 DA= .002 B= 9.335 DB= .001 C= 8.17732 DC= .00239 GAMMA=100.772 DGAMMA= .005 BETA =100.35 DBETA = .09 ALPHA= 99.75 DALPHA= .01 V=596.6
360. 40-1425 Ga6PbTe10 Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.4000 3.3903 .0097 0 0 1 3.0700 3.0725 -.0025 1 1 0 2.7200 2.7207 -.0007 0 1 1 2.4000 2.3996 .0004 -1 1 1 2.2800 2.2800 .0000 0 2 0 2.1700 2.1709 -.0009 1 1 1 2.0800 2.0791 .0009 2 0 0 2.0000 1.9992 .0008 1 2 0 1.8900 1.8904 -.0004 -2 0 1 1.6500 1.6500 .0000 -1 0 2 1.5200 1.5200 .0000 0 3 0
a= 4.197 b= 4.5600 c= 3.422 beta= 97.794 da= ,001 db= .0004 dc=.001 dbet=.007 V= 64.89
361. 40-1933 C6H10O4Pb Triklin
Dexp Dcal d(D) h k l 12.9620 12.9740 -.0120 1 0 0 6.4910 6.4870 .0040 2 0 0 4.8330 4.8345 -.0015 1 -1 1 4.1010 4.0990 .0020 1 2 0 3.9700 3.9677 .0023 -2 2 0 3.6800 3.6807 -.0007 -1 1 2 3.6040 3.6010 .0030 2 1 2 3.4710 3.4751 -.0041 -3 0 1 3.2190 3.2195 -.0005 -2 1 2 2.9810 2.9808 .0002 -2 0 2 2.9580 2.9582 -.0002 4 -1 1 2.8500 2.8509 -.0009 1 3 0
A= 13.203 DA= .002 B= 9.8543 DB= .0006 C= 8.033 DC= .003 GAMMA= 94.334 DGAMMA= .007 BETA = 82.64 DBETA = .01 ALPHA= 67.766 DALPHA= .003 V= 950.6
362. 40-1934 C18H30Ca2O12Pb Triklin
Dexp Dcal d(D) h k l 10.3920 10.4010 -.0090 1 0 0 7.9610 7.9439 .0171 1 -1 1 7.1820 7.1817 .0003 -1 0 1 6.2740 6.2452 .0288 0 -1 2 5.3310 5.3319 -.0009 -1 1 1 5.1130 5.1104 .0026 2 0 1 4.7300 4.7229 .0071 -2 1 0 4.4690 4.4693 -.0003 -2 0 1 4.2970 4.2981 -.0011 1 -1 3 4.0620 4.0632 -.0012 -1 -2 2 3.9570 3.9658 -.0088 1 -2 3 3.9150 3.9154 -.0004 1 0 3
A= 10.68955 DA= .00009 B= 10.834 DB= .008 C= 13.131 DC= .008 GAMMA= 98.42 DGAMMA= .03 BETA = 77.138 DBETA = .006 ALPHA=114.17 DALPHA= .09 V= 1349.9 |
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