== Соединения Pb (томa 33-34) == |
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316. 33-0158 BaPb2MoO6 Triklin
Dexp Dcal d(D) h k l 3.3300 3.3330 -.0030 2 0 0 3.1700 3.1680 .0020 -1 3 0 3.0900 3.0847 .0053 2 1 0 3.0400 3.0406 -.0006 0 0 1 2.9300 2.9316 -.0016 1 3 0 2.8500 2.8520 -.0020 -1 0 1 2.7700 2.7708 -.0008 -1 1 1 2.6900 2.6880 .0020 1 0 1 2.5100 2.5095 .0005 -2 3 0 2.3100 2.3109 -.0009 -2 1 1 1.9500 1.9501 -.0001 -3 3 0 1.8600 1.8593 .0007 -3 1 1 1.7100 1.7100 -.0000 0 6 0 1.6900 1.6909 -.0009 -3 3 1 1.6700 1.6703 -.0003 -4 1 0
A= 6.7167 DA= .0001 B= 10.3071 DB= .0003 C= 3.0499 DC= .0005 GAMMA= 95.449 DGAMMA= .001 BETA = 94.468 DBETA = .004 ALPHA= 90.12 DALPHA= .06 V=209.5
317. 33-0159 Ba3Pb2MoO8 Rombik Groupa 19
Dexp. Dcal. d(D) h k l 4.2100 4.2295 -.0195 0 0 1 3.1100 3.1175 -.0075 0 2 0 3.0000 3.0012 -.0012 4 0 0 2.7700 2.7666 .0034 2 2 0 2.1300 2.1260 .0040 3 2 1 2.0900 2.0880 .0020 5 0 1 1.8700 1.8697 .0003 3 0 2 1.7300 1.7287 .0013 4 0 2 1.6900 1.6906 -.0006 3 3 1 1.5000 1.5006 -.0006 8 0 0 1.3900 1.3900 .0000 3 3 2 1.3400 1.3404 -.0004 2 1 3
a=12.005 b= 6.235 c= 4.229 da= .009 db= .001 dc= .001 V= 316.6
318. 33-0681 Pb2SrMoO6 Triklin
Dexp Dcal d(D) h k l 3.2100 3.2053 .0047 0 1 1 3.1200 3.1208 -.0008 2 0 0 3.0700 3.0683 .0017 0 -1 1 2.9300 2.9275 .0025 2 2 0 2.8000 2.8035 -.0035 1 -2 1 2.7200 2.7215 -.0015 2 1 1 2.6900 2.6909 -.0009 2 0 1 2.5000 2.4993 .0007 -1 -1 1 2.3600 2.3614 -.0014 -1 -2 1 2.1800 2.1807 -.0007 -2 4 0 1.9000 1.9003 -.0003 0 7 0 1.8600 1.8598 .0002 2 6 1 1.7600 1.7593 .0007 2 -5 1 1.7100 1.7101 -.0001 0 7 1 1.6300 1.6284 .0016 2 3 2
A= 6.606 DA= .001 B= 13.468 DB= .001 C= 3.416 DC= .002 GAMMA= 82.835 DGAMMA= .009 BETA = 71.54 DBETA = .02 ALPHA= 82.584 DALPHA= .007 V=285.0
319. 33-0752 beta-Pb2GeS4 Triklin
Dexp Dcal d(D) h k l 4.9700 4.9703 -.0003 -1 0 3 4.5000 4.5065 -.0065 1 1 0 4.3500 4.3511 -.0011 -1 -1 2 4.0700 4.0742 -.0042 0 1 2 3.8000 3.7997 .0003 -1 -1 3 3.7600 3.7603 -.0003 -1 0 4 3.6400 3.6391 .0009 -2 -1 1 3.4700 3.4691 .0009 -3 1 0 3.3900 3.3895 .0005 -3 1 2 3.3600 3.3577 .0023 0 1 3 3.3200 3.3197 .0003 -2 -1 3 3.2500 3.2505 -.0005 0 -1 4
A= 11.7734 DA= .0006 B= 5.7391 DB= .0005 C= 15.1049 DC= .0007 GAMMA=102.3265 DGAMMA= .0004 BETA =106.337 DBETA = .009 ALPHA= 95.159 DALPHA= .002 V=944.8
320. 33-0764 Pb6Mo6O17 Triklin
Dexp Dcal d(D) h k l 3.9900 3.9892 .0008 1 0 2 3.8100 3.8109 -.0009 2 0 0 3.5000 3.5000 -.0000 -1 -2 2 3.4100 3.4152 -.0052 -2 0 1 3.3200 3.3178 .0022 0 2 2 3.2800 3.2793 .0007 -2 -2 1 3.2200 3.2197 .0003 -1 3 0 3.1700 3.1646 .0054 0 -3 2 3.1000 3.0959 .0041 -2 1 1 3.0100 3.0101 -.0001 2 3 0 2.9130 2.9139 -.0009 2 -2 1 2.8570 2.8578 -.0008 -1 -4 1
A= 7.76593 DA= .0001 B= 11.9328 DB= .0001 C= 9.0511 DC= .0001 GAMMA= 79.8005 DGAMMA= .0003 BETA = 87.1993 DBETA = .0002 ALPHA= 97.7358 DALPHA= .0002 V=815.8
321. 33-0767 beta-Pb7O6Cl2 Triklin
Dexp Dcal d(D) h k l 9.6500 9.6418 .0082 1 0 0 6.1500 6.1496 .0004 0 1 1 4.8000 4.8006 -.0006 2 0 1 3.5700 3.5720 -.0020 1 2 1 3.4600 3.4603 -.0003 2 -1 1 3.3300 3.3310 -.0010 -2 1 1 3.2300 3.2297 .0003 1 2 2 3.0600 3.0649 -.0049 3 1 2 2.8700 2.8725 -.0025 -3 1 0 2.8100 2.8079 .0021 1 -1 2 2.6400 2.6389 .0011 0 -2 1 2.5400 2.5393 .0007 2 2 3
A= 10.374 DA= .004 B= 7.271 DB= .005 C= 8.242 DC= .001 GAMMA= 80.44 DGAMMA= .05 BETA = 68.36 DBETA =.04 ALPHA= 65.72 DALPHA= .04 V= 526.6
322. 33-0770 Pb3TeO6 Triklin
Dexp Dcal d(D) h k l 3.0400 3.0401 -.0001 -1 0 2 2.9450 2.9469 -.0019 0 2 0 2.4520 2.4551 -.0031 0 -2 2 2.3840 2.3842 -.0002 -1 -2 1 2.0850 2.0855 -.0005 -1 2 2 1.9990 1.9980 .0010 -2 -1 2 1.8650 1.8646 .0004 1 2 2 1.8130 1.8132 -.0002 -2 0 3 1.7980 1.7980 .0000 2 2 0 1.7210 1.7221 -.0011 -1 2 3 1.6260 1.6260 .0000 0 3 2 1.5890 1.5889 .0001 -3 2 0
A= 5.1911 DA= .0001 B= 6.0224 DB= .0007 C= 7.242 DC= .001 GAMMA= 98.527 DGAMMA= .008 BETA = 93.01 DBETA = .02 ALPHA= 97.747 DALPHA= .002 V=221.4
| 323. 33-1888 C36H72BrN4PbS2 Rombik Groupa 17
Dexp. Dcal. d(D) h k l 13.7000 13.6142 .0858 0 0 1 12.2000 11.8299 .3701 0 1 0 10.4000 9.8563 .5437 1 1 0 8.5100 8.9297 -.4197 0 1 1 7.4000 7.1179 .2821 2 1 0 6.8100 6.8071 .0029 0 0 2 4.9300 4.9282 .0018 2 2 0 4.3400 4.3310 .0090 1 2 2 4.0000 4.0061 -.0061 3 2 1 3.4800 3.4858 -.0058 2 3 1 3.3400 3.3383 .0017 2 2 3 2.9800 2.9790 .0010 5 2 1 2.7500 2.7491 .0009 2 4 1
a=17.82 b=11.830 c=13.61 da= .05 db= .009 dc= .02 v=2870
324. 34-0676 Pb5Ga16Si2O33 Rombik Groupa 23.24,44,71
Dexp. Dcal. d(D) h k l 5.1000 5.1250 -.0250 2 0 0 3.9600 3.9640 -.0040 0 1 1 3.4600 3.4611 -.0011 0 2 0 3.1300 3.1355 -.0055 2 1 1 3.0600 3.0638 -.0038 3 1 0 2.8680 2.8683 -.0003 2 2 0 2.7880 2.7904 -.0024 3 0 1 2.7100 2.7140 -.0040 1 2 1 2.5590 2.5625 -.0035 4 0 0 2.4160 2.4177 -.0017 0 0 2 2.1500 2.1520 -.0020 4 1 1 2.0830 2.0824 .0006 0 3 1
a=10.250 b= 6.922 c= 4.835 da= .005 db= .002 dc= .002 v= 343.1
325. 34-1149 Pb4Sb2O9 Rombik Groupa 19
Dexp. Dcal. d(D) h k l 3.2700 3.2703 -.0003 2 1 1 2.9820 2.9858 -.0038 0 0 3 2.7610 2.7640 -.0030 2 1 2 2.5200 2.5186 .0014 0 1 3 2.2880 2.2894 -.0014 1 2 0 2.0760 2.0773 -.0013 0 2 2 1.8890 1.8891 -.0001 5 1 1 1.7230 1.7236 -.0006 4 2 1 1.6380 1.6352 .0028 4 2 2 1.6070 1.6072 -.0002 4 1 4 1.5720 1.5729 -.0009 5 2 0 1.3510 1.3510 -.0000 7 0 3
a=10.605 b= 4.689 c= 8.957 da= .002 db= .002 dc= .001 V= 445.5
326. 34-1323 CaPb2MoO6 Monoklin Grupa 14
Dexp Dcal d(D) h k l 4.7600 4.7620 -.0020 0 1 1 3.4400 3.4397 .0003 1 2 0 3.0900 3.0904 -.0004 2 0 0 2.8900 2.8903 -.0003 -2 0 2 2.5200 2.5201 -.0001 1 3 0 2.2600 2.2602 -.0002 1 0 2 1.9100 1.9101 -.0001 -2 2 3 1.7400 1.7399 .0001 -3 3 2 1.5800 1.5799 .0001 -3 3 3
a= 6.9750 b= 8.2800 c= 6.569 beta= 117.6054 da=.0009 db=.0007 dc=.002 dbet=.0005 V= 336
327. 34-1404 Ca3Pb2WO8 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 4.6500 4.6493 .0007 0 1 1 4.5100 4.5068 .0032 -1 1 1 3.9600 3.9556 .0044 -3 0 1 3.0500 3.0489 .0011 1 2 0 2.9100 2.9098 .0002 -3 0 2 2.8800 2.8804 -.0004 -2 1 2 2.8200 2.8212 -.0012 -1 2 1 2.3700 2.3701 -.0001 -4 1 2 1.9900 1.9892 .0008 3 2 2 1.7800 1.7796 .0004 -3 2 3 1.7700 1.7699 .0001 7 0 1 1.6400 1.6401 -.0001 5 3 0 1.6000 1.6001 -.0001 -5 2 3
a= 13.350 b= 6.2660 c= 6.9900 beta= 97.19 da= .006 db= .0008 dc=.0007 dbet=.01 V= 580.1
328. 34-1432 K4Pb{P3O9}2 Triklin
Dexp Dcal d(D) h k l 7.3200 7.3370 -.0170 1 0 0 7.0500 7.0519 -.0019 1 1 0 5.9800 5.9821 -.0021 -1 0 1 5.4800 5.5127 -.0327 1 0 1 4.1900 4.1892 .0008 -1 -1 2 3.9500 3.9565 -.0065 0 2 1 3.6700 3.6685 .0015 2 0 0 3.5000 3.4972 .0028 -2 -2 1 3.4200 3.4231 -.0031 2 1 1 3.3700 3.3658 .0042 -1 1 2 3.2800 3.2812 -.0012 1 3 0 3.1200 3.1188 .0012 2 2 1
A= 7.8820 DA= .0001 B= 10.0021 DB= .0004 C= 9.3354 DC= .0003 GAMMA= 69.094 DGAMMA= .002 BETA = 97.664 DBETA = .002 ALPHA= 99.054 DALPHA= .003 V=676.5
329. 34-1442 Pb2Sr3MoO8 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 4.1400 4.1413 -.0013 2 1 0 3.2000 3.2003 -.0003 0 2 1 2.9900 2.9910 -.0010 -3 0 1 2.9300 2.9297 .0003 1 0 2 2.6800 2.6787 .0013 3 1 1 2.0800 2.0807 -.0007 2 3 1 2.0000 1.9992 .0008 0 1 3 1.9000 1.8985 .0015 4 0 2 1.8700 1.8699 .0001 5 0 1 1.8300 1.8295 .0005 -2 3 2 1.7700 1.7706 -.0006 1 2 3 1.7000 1.7000 -.0000 -3 3 2 1.6900 1.6896 .0004 -2 4 1 1.6400 1.6408 -.0008 5 0 2 1.6000 1.6001 -.0001 0 4 2
a= 9.9689 b= 7.4621 c= 6.2330 beta= 92.844 da= .0009 db=.0002 dc=.0004 dbet=.003 V= 463.1 |
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