== Соединения Pb (томa 31-32) == |
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294. 31-0056 {NH4}2{Pb{SeO3}3} Triklin
Dexp Dcal d(D) h k l 8.9000 8.9041 -.0041 1 1 1 8.2200 8.2346 -.0146 2 0 0 6.4400 6.4410 -.0010 1 -1 1 5.6700 5.6746 -.0046 -1 -1 1 5.1400 5.1456 -.0056 -2 2 0 5.0000 5.0002 -.0002 3 1 1 4.9400 4.9357 .0043 2 1 2 4.7800 4.7795 .0005 3 1 0 4.6500 4.6458 .0042 -3 1 1 4.4500 4.4520 -.0020 2 2 2 4.1200 4.1205 -.0005 -2 2 2 3.9100 3.9094 .0006 -1 3 2
A= 16.78230 DA= .00002 B= 13.19923 DB= .00001 C= 11.14828 DC= .00007 GAMMA= 92.6651 DGAMMA= .0001 BETA = 81.2720 DBETA = .0001 ALPHA= 66.1168 DALPHA= .0001 V=2215.8
295. 31-0278 Ca3PbSiO6 Triklin
Dexp Dcal d(D) h k l 4.9100 4.9066 .0034 -1 0 1 4.6200 4.6163 .0037 -1 2 0 3.8100 3.8104 -.0004 0 -2 1 3.3700 3.3715 -.0015 1 -2 1 3.1000 3.1020 -.0020 -2 2 0 3.0400 3.0421 -.0021 -2 2 1 3.0000 3.0022 -.0022 -1 0 2 2.8700 2.8675 .0025 0 4 1 2.7800 2.7803 -.0003 -1 4 1 2.7400 2.7401 -.0001 -1 3 2 2.6000 2.5971 .0029 2 -2 1 2.5400 2.5396 .0004 1 4 1
A= 7.035 DA= .008 B= 11.78 DB= .05 C= 6.662 DC= .001 GAMMA= 96.69 DGAMMA= .05 BETA = 95.77 DBETA = .05 ALPHA= 75.22 DALPHA= .07 V= 528.8
296. 31-0279 Ca2Pb3SiO7 Triklin
Dexp Dcal d(D) h k l 4.6000 4.5974 .0026 -1 1 1 3.3700 3.3707 -.0007 3 -1 1 3.1300 3.1298 .0002 -1 3 1 3.0500 3.0498 .0002 3 -3 1 2.9200 2.9200 -.0000 2 0 2 2.8800 2.8815 -.0015 2 -4 1 2.7500 2.7496 .0004 3 1 1 2.6900 2.6884 .0016 -1 -1 2 2.6600 2.6616 -.0016 3 -4 1 2.6200 2.6201 -.0001 4 -2 1 2.4700 2.4691 .0009 -3 3 1 2.4500 2.4500 .0000 -4 3 0
A= 10.6125 DA= .0002 B= 12.1630 DB= .0001 C= 6.4871 DC= .0004 GAMMA=112.544 DGAMMA= .004 BETA = 74.8362 DBETA = .0001 ALPHA= 99.664 DALPHA= .004 V= 744.3
297. 31-0366 Cs2{Pb{SeO3}3} Triklin
Dexp Dcal d(D) h k l 8.5200 8.5363 -.0163 1 -1 0 7.5400 7.5460 -.0060 0 2 0 6.8200 6.8214 -.0014 1 -1 1 6.0300 6.0382 -.0082 1 2 0 5.6600 5.6471 .0129 0 -2 1 5.0300 5.0307 -.0007 0 3 0 4.8300 4.8344 -.0044 2 1 0 4.7700 4.7576 .0124 1 0 2 4.6700 4.6706 -.0006 -1 -2 1 4.4000 4.3986 .0014 1 3 1 4.2300 4.2322 -.0022 0 2 2 4.1000 4.1013 -.0013 2 -2 1
A= 10.527 DA= .006 B= 15.1711 DB= .0001 C= 9.849 DC= .002 GAMMA= 89.46 DGAMMA= .04 BETA = 76.955 DBETA = .008 ALPHA= 84.21 DALPHA= .02 V=1523.2
298. 31-0681 PbCr2.3Ti2.3O9 Triklin
Dexp Dcal d(D) h k l 7.2000 7.2051 -.0051 1 0 0 7.1000 7.1013 -.0013 0 0 1 3.5300 3.5284 .0016 0 -2 1 3.2500 3.2503 -.0003 -1 -1 2 3.2100 3.2089 .0011 1 -1 2 3.1600 3.1618 -.0018 -2 -1 1 3.1300 3.1287 .0013 -1 0 2 3.6000 3.6026 -.0026 2 0 0 2.9280 2.9281 -.0001 2 1 1 2.5660 2.5667 -.0007 -1 1 2 2.4730 2.4729 .0001 -2 0 2 2.2070 2.2077 -.0007 2 -2 2 2.1890 2.1882 .0008 -3 1 0 1.8880 1.8881 -.0001 -1 3 1 1.8510 1.8509 .0001 2 1 3
A= 7.257 DA= .003 B= 7.246 DB= .001 C= 7.42227 DC= .00002 GAMMA= 83.64 DGAMMA= .01 BETA = 89.34 DBETA = .01 ALPHA=106.72 DALPHA= .01 V= 371.1
299. 31-0683 PbGd2TiMo3O15 Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.5300 3.5320 -.0020 0 1 0 3.2600 3.2616 -.0016 -1 1 1 3.2100 3.2089 .0011 3 0 0 3.1620 3.1645 -.0025 0 1 3 3.1290 3.1327 -.0037 -3 0 1 2.9940 2.9936 .0004 2 0 6 2.8310 2.8331 -.0021 -3 0 3 2.7180 2.7163 .0017 -2 1 2 2.6910 2.6889 .0021 2 0 7 2.6360 2.6356 .0004 1 0 8 2.4970 2.4972 -.0002 3 0 6 2.3560 2.3551 .0009 1 0 9
a= 9.665 b= 3.532 c= 21.460 beta= 84.89 da= .001 db= .009 dc=.001 dbet=.01 V= 729.7
Triklin
Dexp Dcal d(D) h k l 3.5300 3.5297 .0003 -1 1 0 3.2600 3.2603 -.0003 -1 -1 2 3.2100 3.2103 -.0003 1 -1 1 3.1620 3.1627 -.0007 0 -1 2 3.1290 3.1296 -.0006 -3 0 1 2.9940 2.9887 .0053 -3 0 2 2.8310 2.8312 -.0002 -2 1 0 2.7180 2.7216 -.0036 2 1 2 2.6910 2.6922 -.0012 -3 0 3 2.6360 2.6328 .0032 0 -1 3 2.4970 2.4964 .0006 1 0 4 2.3560 2.3561 -.0001 -3 0 4
A= 9.4854 DA= .009 B= 4.1435 DB= .0002 C= 11.4856 DC= .0004 GAMMA= 82.03 DGAMMA= .02 BETA =103.47 DBETA = .01 ALPHA= 86.96 DALPHA= .01 V= 433.0
300. 31-0688 C4H4O5Pb Triklin
Dexp Dcal d(D) h k l 9.5000 9.4989 .0011 1 0 0 5.9800 5.9775 .0025 -1 1 1 4.8100 4.8138 -.0038 -1 -1 1 4.6700 4.6756 -.0056 1 -1 1 4.2500 4.2489 .0011 -2 1 1 4.1200 4.1267 -.0067 -1 3 1 3.9000 3.8928 .0072 1 -2 1 3.4100 3.4086 .0014 -1 1 2 3.3000 3.3005 -.0005 0 4 0 3.2400 3.2407 -.0007 2 2 1 3.0200 3.0204 -.0004 2 3 0 2.9300 2.9281 .0019 1 4 1
A= 9.7108 DA= .0008 B= 13.794 DB= .006 C= 6.967 DC= .004 GAMMA=100.10 DGAMMA= .01 BETA = 98.79 DBETA = .02 ALPHA= 75.23 DALPHA= .01 V= 882.8
301. 31-0694 C4H4O4PbS Triklin
Dexp Dcal d(D) h k l 10.2000 10.2046 -.0046 1 0 0 4.7800 4.7845 -.0045 0 1 1 4.4200 4.4181 .0019 -2 -1 1 4.3000 4.2942 .0058 -1 0 2 4.0600 4.0658 -.0058 -2 1 1 3.7100 3.7093 .0007 0 -2 2 3.5200 3.5193 .0007 -3 0 1 3.4700 3.4641 .0059 1 2 0 3.3000 3.2954 .0046 -1 1 2 3.1600 3.1620 -.0020 0 1 2 3.0700 3.0681 .0019 2 -1 2 3.0300 3.0308 -.0008 0 -1 3
A= 10.661 DA= .002 B= 8.586 DB= .006 C= 9.393 DC= .005 GAMMA= 92.8953 DGAMMA= .0009 BETA =104.073 DBETA = .001 ALPHA=112.85 DALPHA= .01 V= 758.5
302. 31-0695 PbSO3 Triklin
Dexp Dcal d(D) h k l 5.1200 5.1206 -.0006 -1 0 1 4.2500 4.2509 -.0009 1 -2 1 3.9250 3.9264 -.0014 2 -1 1 3.7370 3.7348 .0022 0 2 2 3.3940 3.3953 -.0013 1 -1 2 3.1960 3.1897 .0063 0 4 0 3.1030 3.1031 -.0001 -2 -1 1 2.8840 2.8845 -.0005 0 -2 2 2.7280 2.7277 .0003 -2 -2 1 2.6980 2.6975 .0005 3 1 0 2.4550 2.4536 .0014 3 -3 1 2.2410 2.2410 .0000 -1 -3 2
A= 8.84321 DA= .00005 B= 13.41177 DB= .00003 C= 7.94815 DC= .00002 GAMMA= 96.3551 DGAMMA= .0003 BETA = 79.7657 DBETA = .0003 ALPHA= 74.7270 DALPHA= .0004 V=882.6
303. 31-0697 C4O9PbTi4*4H2O Triklin
Dexp Dcal d(D) h k l 9.5900 9.5938 -.0038 0 0 1 7.8100 7.8100 .0000 1 0 0 7.6300 7.6532 -.0232 0 -2 1 7.3700 7.3709 -.0009 1 -1 0 6.5900 6.5777 .0123 1 2 0 6.2400 6.2325 .0075 -1 -1 1 6.0700 6.0702 -.0002 -1 1 1 5.9400 5.9333 .0067 0 3 1 5.6500 5.6431 .0069 1 -1 1 5.4800 5.4876 -.0076 -1 2 1 4.9100 4.9139 -.0039 0 4 1 4.8300 4.8305 -.0005 -1 3 1
A= 7.850 DA= .007 B= 23.68 DB= .02 C= 9.655 DC= .006 GAMMA= 88.52 DGAMMA= .02 BETA = 95.69 DBETA = .02 ALPHA= 93.233 DALPHA= .005 V= 1782.5
304. 31-1044 K2{Pb{SeO3}3} Triklin
Dexp Dcal d(D) h k l 8.4900 8.5100 -.0200 1 0 0 8.1800 8.1817 -.0017 1 1 0 7.5800 7.5930 -.0130 0 0 1 6.8100 6.8206 -.0106 -1 -1 1 6.4900 6.4976 -.0076 0 -1 1 5.7200 5.7188 .0012 -1 1 0 5.0400 5.0423 -.0023 1 0 1 4.8700 4.8592 .0108 -1 1 1 4.6100 4.6165 -.0065 -2 -1 1 4.2400 4.2438 -.0038 -2 -2 1 4.1000 4.0909 .0091 2 2 0 3.9300 3.9311 -.0011 1 2 1
A= 9.60705 DA= .00006 B= 11.573 DB= .008 C= 8.068 DC= .001 GAMMA= 66.707 DGAMMA= .008 BETA =108.88 DBETA = .06 ALPHA=102.65 DALPHA= .06 V=775.9
| 305. 31-1193 Rb2{Pb{SeO3}3} Triklin
Dexp Dcal d(D) h k l 8.8400 8.8343 .0057 1 0 0 8.3000 8.3083 -.0083 0 1 0 7.5800 7.6256 -.0456 -1 0 1 6.6200 6.6215 -.0015 0 -1 1 5.7100 5.6906 .0194 1 -1 1 4.9900 4.9776 .0124 -1 -1 1 4.9300 4.9298 .0002 -2 1 0 4.7000 4.6901 .0099 -1 0 2 4.5600 4.5605 -.0005 -2 0 1 4.4200 4.4172 .0028 2 0 0 4.1500 4.1542 -.0042 0 2 0 3.8100 3.8128 -.0028 -2 0 2
A= 10.297 DA= .001 B= 9.310 DB= .004 C= 9.61 DC= .01 GAMMA=115.723 DGAMMA= .009 BETA =105.99 DBETA = .09 ALPHA= 89.990 DALPHA= .001 V= 790.5
306. 31-1750 C4H5NO4Pb Triklin
Dexp Dcal d(D) h k l 6.3000 6.2959 .0041 -1 1 0 5.4000 5.4006 -.0006 1 1 0 4.6900 4.6946 -.0046 -1 2 0 4.5200 4.5196 .0004 1 0 2 4.3200 4.3205 -.0005 0 -1 2 3.9500 3.9523 -.0023 1 2 2 3.4900 3.4928 -.0028 -1 3 0 3.3600 3.3671 -.0071 1 2 3 3.0600 3.0613 -.0013 0 2 4 2.9500 2.9506 -.0006 -2 2 2 2.8200 2.8168 .0032 1 1 4 2.7600 2.7566 .0034 0 4 0
A= 6.917 DA= .002 B= 12.256 DB= .001 C= 12.310 DC= .005 GAMMA= 98.55 DGAMMA= .03 BETA = 89.06 DBETA = .02 ALPHA= 65.9254 DALPHA= .00053 V=938.7
307. 31-1751 C12H8N2O4Pb Triklin
Dexp Dcal d(D) h k l 6.2000 6.1943 .0057 0 1 0 4.1000 4.0984 .0016 2 0 0 4.0300 4.0306 -.0006 0 1 1 3.9100 3.9105 -.0005 1 1 1 3.3800 3.3810 -.0010 -1 1 1 3.3200 3.3227 -.0027 -2 1 0 3.1800 3.1782 .0018 2 1 1 3.0900 3.0853 .0047 -2 0 1 2.9600 2.9597 .0003 1 2 0 2.8200 2.8195 .0005 1 -1 2 2.7300 2.7323 -.0023 3 0 0 2.6400 2.6428 -.0028 -2 1 1
A= 8.3859 DA= .0004 B= 6.252 DB= .003 C= 6.1098 DC= .0004 GAMMA= 87.87 DGAMMA= .01 BETA = 78.356 DBETA = .006 ALPHA= 96.892 DALPHA= .005 V=310.9
308. 32-0505 PbAl4Si3O16 Triklin
Dexp Dcal d(D) h k l 7.7800 7.7953 -.0153 0 1 1 6.5700 6.5785 -.0085 1 1 0 6.4800 6.4753 .0047 0 -1 1 5.6300 5.6328 -.0028 -1 1 0 5.4100 5.4079 .0021 1 1 2 5.1300 5.1520 -.0220 1 -1 1 4.3600 4.3487 .0113 0 2 1 4.1800 4.1743 .0057 1 -1 2 4.0600 4.0582 .0018 2 1 0 3.9000 3.8976 .0024 0 2 2 3.7500 3.7483 .0017 -2 0 1 3.4100 3.4160 -.0060 1 -2 1
A= 8.878 DA= .009 B= 9.008 DB= .009 C= 12.821 DC= .009 GAMMA= 78.11 DGAMMA= .09 BETA = 74.93 DBETA = .06 ALPHA= 76.29 DALPHA= .05 V= 950.4
309. 32-0517 Pb2Ge4S7 Triklin
Dexp Dcal d(D) h k l 4.2400 4.2373 .0027 1 1 1 4.1300 4.1309 -.0009 -1 -1 1 4.0900 4.0913 -.0013 -2 0 2 4.0000 3.9969 .0031 -1 1 2 3.4300 3.4304 -.0004 0 -1 2 3.3600 3.3609 -.0009 -2 0 3 2.9960 2.9969 -.0009 3 0 0 2.9210 2.9203 .0007 -1 0 4 2.8560 2.8552 .0008 2 1 2 2.8310 2.8330 -.0020 -1 -1 3 2.4870 2.4866 .0004 2 -1 2 2.4460 2.4478 -.0018 -1 2 1
A= 9.3370 DA= .0002 B= 5.10195 DB= .00009 C= 11.88723 DC= .00006 GAMMA= 89.044 DGAMMA= .002 BETA =105.193 DBETA = .001 ALPHA= 79.64114 DALPHA= .00001 V=536.3
310. 32-0518 alfa-Pb2GeS4 Triklin
Dexp Dcal d(D) h k l 5.7400 5.7426 -.0026 1 0 0 4.9600 4.9630 -.0030 -1 1 0 4.5600 4.5624 -.0024 -1 0 1 3.8100 3.8103 -.0003 -1 -1 1 3.5200 3.5198 .0002 0 2 0 3.4200 3.4213 -.0013 -1 0 2 3.1500 3.1523 -.0023 1 -2 3 3.0000 3.0016 -.0016 2 -1 2 2.9660 2.9648 .0012 0 -2 3 2.8760 2.8713 .0047 2 0 0 2.7630 2.7645 -.0015 1 2 0 2.5720 2.5709 .0011 1 2 1
A= 6.1812 DA= .0006 B= 7.810 DB= .002 C= 11.25645 DC= .0001 GAMMA=107.41 DGAMMA= .02 BETA = 71.491 DBETA = .008 ALPHA=113.08 DALPHA= .01 V=464.2
311. 32-0519 Pb0.2Ge3.8S7 Triklin
Dexp Dcal d(D) h k l 7.6800 7.6644 .0156 0 1 0 6.4300 6.4410 -.0110 1 -1 1 5.1200 5.1228 -.0028 0 -1 2 5.0000 4.9923 .0077 1 1 0 4.7600 4.7558 .0042 -1 -1 1 4.0000 3.9989 .0011 1 -2 1 3.8300 3.8322 -.0022 0 2 0 3.7100 3.7095 .0005 1 0 3 3.4600 3.4595 .0005 0 -2 2 3.4200 3.4195 .0005 0 1 3 3.3400 3.3402 -.0002 -1 1 3 3.1800 3.1814 -.0014 2 1 1
A= 9.202 DA= .002 B= 8.195 DB= .001 C= 12.3689 DC= .0002 GAMMA=109.37 DGAMMA= .03 BETA = 86.64 DBETA = .01 ALPHA= 98.260 DALPHA= .001 V=870.2
312. 32-0520 PB5Ge5S12 Triklin
Dexp Dcal d(D) h k l 5.0900 5.0958 -.0058 1 1 1 4.3500 4.3505 -.0005 1 -3 1 4.1800 4.1797 .0003 -1 3 1 4.0500 4.0538 -.0038 0 4 0 3.9500 3.9504 -.0004 1 1 3 3.8000 3.8059 -.0059 0 2 4 3.5600 3.5600 .0000 0 4 2 3.3700 3.3648 .0052 1 3 2 3.1200 3.1219 -.0019 1 0 5 3.0500 3.0481 .0019 1 4 1 3.0100 3.0094 .0006 0 -5 3 2.9410 2.9416 -.0006 1 -3 5
A= 6.0968 DA= .0002 B= 16.533 DB= .003 C= 18.44 DC= .01 GAMMA= 99.18 DGAMMA= .04 BETA = 89.257 DBETA = .007 ALPHA= 96.576 DALPHA= .001 V= 1822.5
313. 32-0532 Pb4O3Cl2*H2O Triklin
Dexp Dcal d(D) h k l 6.3900 6.3899 .0001 1 0 0 3.8700 3.8697 .0003 1 -1 1 3.1800 3.1795 .0005 1 -1 3 2.9300 2.9290 .0010 -1 0 4 2.8400 2.8411 -.0011 -1 -1 2 2.1500 2.1499 .0001 3 0 1 2.1300 2.1300 .0000 3 0 0 2.0300 2.0300 -.0000 -3 1 1 1.7840 1.7840 -.0000 -2 0 6 1.7130 1.7130 -.0000 -2 -1 5 1.7000 1.7000 -.0000 3 0 6 1.6870 1.6871 -.0001 -3 2 0
A= 6.62916 DA= .00002 B= 4.2617 DB= .0007 C= 14.3021 DC= .0004 GAMMA=103.347 DGAMMA= .001 BETA = 81.5937 DBETA = .0001 ALPHA= 93.410 DALPHA= .007 V= 388.8
314. 32-0540 Pb10Sn2Sb5S20 Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.8600 3.8565 .0035 2 0 0 3.4900 3.4873 .0027 2 1 0 3.3400 3.3420 -.0020 2 0 1 3.0900 3.0930 -.0030 2 1 1 2.8000 2.7962 .0038 0 1 2 2.7200 2.7223 -.0023 0 3 0 2.5800 2.5766 .0034 -1 1 2 2.3000 2.3039 -.0039 -3 0 1 2.1100 2.1107 -.0007 2 3 1 1.9800 1.9841 -.0041 0 0 3 1.9560 1.9559 .0001 3 1 2 1.9000 1.9002 -.0002 1 1 3
a= 7.731 b= 8.1670 c= 5.966 beta= 86.093 da=.001 db= .0005 dc=.001 dbet=.006 V= 375.8
Triklin
Dexp Dcal d(D) h k l 3.8600 3.8635 -.0035 0 1 1 3.4900 3.4886 .0014 1 1 1 3.3400 3.3382 .0018 -1 1 1 3.0900 3.0881 .0019 0 0 2 2.8000 2.8000 .0000 -1 0 2 2.7200 2.7192 .0008 2 1 1 2.5800 2.5786 .0014 -2 1 1 2.3000 2.3004 -.0004 -1 -1 2 2.1100 2.1098 .0002 -3 1 0 1.9800 1.9789 .0011 1 -2 1 1.9560 1.9561 -.0001 2 2 0 1.9000 1.9011 -.0011 -2 2 0
A= 7.27449 DA= .00002 B= 4.5788 DB= .0001 C= 6.2175 DC= .0001 GAMMA= 87.923 DGAMMA= .001 BETA = 87.3971 DBETA = .0008 ALPHA= 83.857 DALPHA= .001 V=205.6
315. 32-1735 C12H8N2O6Pb*1.5H2O Triklin
Dexp Dcal d(D) h k l 7.1200 7.1409 -.0209 0 0 1 5.7900 5.7665 .0235 0 1 1 5.4300 5.4367 -.0067 0 -2 1 4.6900 4.6746 .0154 -1 -1 1 4.3500 4.3552 -.0052 0 3 0 4.3000 4.3010 -.0010 1 1 1 4.2200 4.2203 -.0003 1 -1 1 3.6600 3.6573 .0027 1 -2 1 3.5700 3.5705 -.0005 0 0 2 3.4100 3.4071 .0029 0 3 1 3.2400 3.2458 -.0058 0 -4 1 3.1800 3.1808 -.0008 1 3 1
A= 5.904 DA= .008 B= 13.70 DB= .01 C= 7.3169 DC= .0004 GAMMA= 77.55 DGAMMA= .03 BETA = 92.18 DBETA = .08 ALPHA=102.59 DALPHA= .09 V= 564.0
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