== Соединения Pb (том 3) == |
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29. 3-0033 K2Pb4Si8O21 Triklin
Dexp Dcal d(D) h k l 8.3200 8.3194 .0006 1 0 0 6.5900 6.5901 -.0001 -1 1 0 5.8900 5.8839 .0061 -1 1 1 4.3800 4.3816 -.0016 0 -1 1 4.2000 4.1960 .0040 -1 2 1 3.9600 3.9606 -.0006 1 -1 1 3.7300 3.7339 -.0039 -2 0 1 3.5200 3.5239 -.0039 -2 2 1 3.2900 3.2951 -.0051 -2 2 0 2.7800 2.7797 .0003 0 3 1 2.7100 2.7072 .0028 -1 3 0 2.6300 2.6317 -.0017 0 3 0
A= 8.8129 DA= .0008 B= 8.787 DB= .008 C= 7.128 DC= .002 GAMMA=107.874 DGAMMA= .005 BETA =103.17 DBETA = .01 ALPHA= 67.94 DALPHA= .03 V= 482.93
30. 3-0092 Pb5B8O17 Triklin
Dexp Dcal d(D) h k l 5.8900 5.9095 -.0195 0 1 0 4.8600 4.8610 -.0010 1 0 0 4.4500 4.4610 -.0110 0 -1 2 3.7000 3.6997 .0003 -1 0 2 3.3900 3.3909 -.0009 -1 1 0 3.1600 3.1599 .0001 -1 1 1 3.0700 3.0707 -.0007 1 1 2 2.9600 2.9579 .0021 -1 0 3 2.8300 2.8303 -.0003 1 2 0 2.7100 2.7113 -.0013 0 2 1 2.6000 2.5976 .0024 1 2 1 2.2800 2.2802 -.0002 0 1 4
A= 5.0205 DA= .0001 B= 6.22820 DB= .00007 C= 11.0593 DC= .0003 GAMMA= 75.7920 DGAMMA= .0003 BETA = 95.803 DBETA = .001 ALPHA=102.8537 DALPHA= .0008 V=326.5
31. 3-0131 Ca2PbO4 Triklin
Dexp Dcal d(D) h k l 5.0100 5.0141 -.0041 -1 1 0 2.8100 2.8102 -.0002 -2 0 1 2.5000 2.5001 -.0001 -1 -1 2 2.4400 2.4396 .0004 0 -1 2 2.1700 2.1695 .0005 2 -1 1 2.0100 2.0115 -.0015 0 1 2 1.9100 1.9107 -.0007 -2 -2 2 1.8500 1.8500 -.0000 0 3 1 1.7000 1.7002 -.0002 -2 4 0 1.6600 1.6598 .0002 -1 -2 3 1.6300 1.6298 .0002 3 1 0 1.6000 1.5999 .0001 2 -1 2
A= 5.8910 DA= .0001 B= 7.4791 DB= .0004 C= 5.1087 DC= .0001 GAMMA=101.263 DGAMMA= .001 BETA =107.2291 DBETA = .0009 ALPHA=103.9108 DALPHA= .0002 V=199.9
32. 3-0317 K2PbSi4O10 Triklin
Dexp Dcal d(D) h k l 6.2200 6.2383 -.0183 0 1 1 5.8100 5.8311 -.0211 1 0 1 5.5500 5.5536 -.0036 1 -1 1 5.2000 5.1944 .0056 0 0 2 4.8100 4.8137 -.0037 -1 0 1 4.4500 4.4573 -.0073 1 0 2 3.7000 3.6995 .0005 0 2 0 3.5000 3.4918 .0082 1 1 2 3.3300 3.3373 -.0073 1 0 3 3.2200 3.2196 .0004 1 -1 3 3.0800 3.0802 -.0002 2 -1 2 2.9900 2.9884 .0016 2 -2 1
A= 6.7359 DA= .0009 B= 8.0164 DB= .009 C= 10.64 DC= .01 GAMMA=112.30 DGAMMA= .05 BETA = 78.09 DBETA = .03 ALPHA= 90.83 DALPHA= .03 V= 519.06
33. 3-0339 alfa-Pb2B2O5 Triklin
Dexp Dcal d(D) h k l 7.2000 7.2021 -.0021 -1 0 1 5.8100 5.8081 .0019 0 1 1 5.5200 5.5209 -.0009 0 -1 1 3.9000 3.9039 -.0039 0 2 0 3.6200 3.6165 .0035 -1 -1 2 3.3900 3.3858 .0042 -2 -1 1 3.2600 3.2600 -.0000 1 2 0 3.1800 3.1781 .0019 -1 2 2 2.9700 2.9681 .0019 -2 2 2 2.8800 2.8815 -.0015 1 1 2 2.7600 2.7604 -.0004 0 -2 2 2.7000 2.7004 -.0004 -3 0 2
A= 8.5305 DA= .0002 B= 7.994 DB= .001 C= 9.0218 DC= .0009 GAMMA=102.042 DGAMMA= .006 BETA =114.28 DBETA = .01 ALPHA= 82.48 DALPHA= .01 V= 547.8
34. 3-0344 PbSiO3 Triklin
Dexp Dcal d(D) h k l 5.8200 5.8267 -.0067 0 1 0 3.5800 3.5799 .0001 1 -1 1 3.3600 3.3587 .0013 0 -1 2 3.2400 3.2369 .0031 2 0 0 3.0200 3.0163 .0037 -2 0 1 2.8900 2.8916 -.0016 2 0 1 2.7800 2.7803 -.0003 1 -1 2 2.7300 2.7311 -.0011 2 1 1 2.6600 2.6585 .0015 1 1 2 2.5900 2.5913 -.0013 -2 1 0 2.5200 2.5200 .0000 1 2 1 2.4700 2.4690 .0010 2 -1 1
A= 6.6828 DA= .0004 B= 6.11606 DB= .00004 C= 7.3675 DC= .0002 GAMMA= 75.998 DGAMMA= .008 BETA = 95.96865 DBETA = .00009 ALPHA=102.012 DALPHA= .005 V=285.6
35. 3-0346 Pb6Al2Si6O21 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 8.6200 8.5981 .0219 1 1 0 6.7500 6.7409 .0091 1 0 1 4.4100 4.4031 .0069 2 1 1 3.5600 3.5571 .0029 0 3 1 3.3100 3.3091 .0009 2 3 0 3.0400 3.0400 .0000 3 2 1 2.7600 2.7614 -.0014 0 4 1 2.6300 2.6287 .0013 -5 0 1 2.3800 2.3799 .0001 4 0 2 2.3200 2.3201 -.0001 2 2 3 2.0700 2.0692 .0008 -4 4 2 2.0200 2.0195 .0005 1 4 3
a= 13.1640 b= 11.5908 c= 9.3560 beta= 103.097 da=.0008 db=.0002 dc=.0006 dbet=.001 V= 1390.4
Triklin
Dexp Dcal d(D) h k l 8.6200 8.6529 -.0329 0 0 1 6.7500 6.7609 -.0109 1 0 0 4.4100 4.4069 .0031 0 1 0 3.5600 3.5615 -.0015 0 -1 2 3.3100 3.3100 -.0000 1 1 1 3.0400 3.0393 .0007 -1 1 1 2.7600 2.7630 -.0030 0 1 2 2.6300 2.6317 -.0017 2 1 0 2.3800 2.3789 .0011 3 0 1 2.3200 2.3208 -.0008 -2 0 2 2.0700 2.0707 -.0007 1 2 0 2.0200 2.0187 .0013 0 2 1
A= 7.21807 DA= .00000 B= 4.5903 DB= .0006 C= 9.530 DC= .002 GAMMA= 97.63 DGAMMA= .01 BETA = 69.63 DBETA = .05 ALPHA=106.10 DALPHA= .01 V=283.9
36. 3-0351 PbCO3 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 3.9000 3.8947 .0053 2 1 0 3.5300 3.5290 .0010 -1 0 2 3.0500 3.0514 -.0014 3 0 0 2.5500 2.5478 .0022 -2 1 2 2.4800 2.4794 .0006 3 2 1 2.1900 2.1893 .0007 -2 2 2 2.0600 2.0592 .0008 2 2 4 1.9900 1.9896 .0004 2 0 5 1.9600 1.9595 .0005 3 3 2 1.9200 1.9205 -.0005 3 3 0 1.8400 1.8410 -.0010 5 0 4 1.6800 1.6792 .0008 4 3 0
a= 10.039 b= 7.414 c= 9.9490 beta= 65.762 da=.001 db=.001 dc=.0004 dbet=.009 V= 675.2
Triklin
Dexp Dcal d(D) h k l 3.9000 3.9003 -.0003 2 1 0 3.5300 3.5316 -.0016 2 1 1 3.0500 3.0529 -.0029 2 -1 1 2.5500 2.5483 .0017 2 2 1 2.4800 2.4811 -.0011 -2 -1 1 2.1900 2.1914 -.0014 2 -2 1 2.0600 2.0604 -.0004 -2 -2 1 1.9900 1.9915 -.0015 0 1 2 1.9600 1.9594 .0006 4 1 2 1.9200 1.9213 -.0013 2 3 0 1.8400 1.8392 .0008 -1 3 0 1.6800 1.6798 .0002 -2 3 0
A= 9.8593 DA= .0004 B= 5.975 DB= .001 C= 4.6222 DC= .0005 GAMMA= 78.749 DGAMMA= .009 BETA = 66.60 DBETA = .01 ALPHA= 85.79 DALPHA= .01 V=244.8
37. 3-0356 K2O*SiO2 Triklin
Dexp Dcal d(D) h k l 8.3200 8.3350 -.0150 1 0 0 6.0500 6.0477 .0023 0 1 1 5.8500 5.8475 .0025 1 0 2 4.3600 4.3655 -.0055 1 1 1 4.1200 4.1310 -.0110 0 1 3 3.5100 3.5094 .0006 1 1 3 3.1800 3.1782 .0018 0 2 0 2.9500 2.9494 .0006 -2 -1 1 2.8400 2.8398 .0002 -2 2 2 2.7400 2.7386 .0014 -1 1 5 2.6500 2.6523 -.0023 0 -1 5 2.5100 2.5101 -.0001 2 1 4
A= 8.805 DA= .004 B= 6.717 DB= .001 C= 15.249 DC= .001 GAMMA=108.26 DGAMMA= .01 BETA = 86.78 DBETA = .01 ALPHA= 86.421 DALPHA= .005 V=852.5
38. 3-0366 5PbO*Al2O3*10SiO2 Triklin
Dexp Dcal d(D) h k l 10.0000 9.9990 .0010 -1 1 0 8.5800 8.5566 .0234 1 1 0 3.7100 3.7102 -.0002 0 1 1 3.4900 3.4868 .0032 1 1 1 3.3000 3.2993 .0007 -4 2 0 3.1200 3.1160 .0040 -3 1 1 2.8900 2.8915 -.0015 -1 -2 1 2.7400 2.7438 -.0038 -4 1 1 2.6700 2.6718 -.0018 -4 0 1 2.5200 2.5197 .0003 1 -3 1 2.4100 2.4078 .0022 0 5 0 2.2600 2.2602 -.0002 -5 3 1 2.0600 2.0597 .0003 -7 1 0 2.0000 1.9998 .0002 -5 5 0 1.9100 1.9098 .0002 -5 5 1
A= 14.494 DA= .001 B= 12.364 DB= .006 C= 3.7754 DC= .0006 GAMMA= 99.84 DGAMMA= .03 BETA = 95.843 DBETA = .03 ALPHA= 80.3795 DALPHA= .0004 V=654.9
39. 3-0373 Pb*Al*Si*O Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 6.6000 6.5959 .0041 1 1 0 5.8600 5.8403 .0197 -1 0 1 4.6400 4.6386 .0014 0 2 1 3.9500 3.9421 .0079 2 0 0 3.8200 3.8288 -.0088 1 2 1 3.6400 3.6387 .0013 0 0 2 3.4800 3.4831 -.0031 0 1 2 3.3000 3.2980 .0020 2 2 0 3.0200 3.0177 .0023 1 1 2 2.9200 2.9201 -.0001 -2 0 2 2.7800 2.7815 -.0015 0 4 1 2.5700 2.5676 .0024 3 1 0
a= 7.9900 b=12.0400 c= 7.375 beta= 99.324 da= .0008 db=.0006 dc=.003 dbet=.004 V= 700.1
Triklin
Dexp Dcal d(D) h k l 6.6000 6.5997 .0003 1 1 0 5.8600 5.8445 .0155 0 1 1 4.6400 4.6399 .0001 0 -1 1 3.9500 3.9436 .0064 1 -1 1 3.8200 3.8191 .0009 2 2 1 3.6400 3.6442 -.0042 0 1 2 3.4800 3.4764 .0036 1 2 2 3.3000 3.2999 .0001 2 2 0 3.0200 3.0199 .0001 0 -1 2 2.9200 2.9223 -.0023 0 2 2 2.7800 2.7791 .0009 3 1 0 2.5700 2.5706 -.0006 3 2 3
A= 9.493 DA= .003 B= 8.407 DB= .007 C= 8.664 DC= .007 GAMMA= 60.59 DGAMMA= .04 BETA = 61.44 DBETA = .03 ALPHA= 65.90 DALPHA= .06 V= 515.2
| 40. 3-0384 Al2O3*12PbO*20SiO2 Triklin
Dexp Dcal d(D) h k l 9.1200 9.1313 -.0113 -1 0 1 8.0400 8.0238 .0162 1 0 1 3.4600 3.4626 -.0026 1 2 1 3.1000 3.0976 .0024 2 2 0 2.9400 2.9405 -.0005 0 -2 2 2.7000 2.7020 -.0020 -4 1 0 2.6200 2.6204 -.0004 4 1 1 2.5900 2.5905 -.0005 -3 -2 1 2.4600 2.4599 .0001 0 3 1 2.3800 2.3792 .0008 1 0 5 2.3500 2.3494 .0006 -5 0 1 2.2700 2.2695 .0005 -4 2 0
A= 11.7683 DA= .0001 B= 7.3837 DB= .0005 C= 12.7634 DC= .0002 GAMMA= 90.880 DGAMMA= .003 BETA = 97.45 DBETA = .04 ALPHA= 80.47 DALPHA= .06 V=1083.5
41. 3-0422 PbSO4*PbO Monoklin Grupa 14
Dexp Dcal d(D) h k l 4.2800 4.3007 -.0207 3 0 0 4.0300 4.0337 -.0037 0 1 1 3.8400 3.8360 .0040 1 1 1 3.7000 3.6923 .0077 -3 0 2 3.5400 3.5372 .0028 2 1 0 3.7000 3.6923 .0077 -3 0 2 3.5400 3.5372 .0028 2 1 0 3.3500 3.3519 -.0019 0 0 4 3.2100 3.2110 -.0010 1 0 4 3.0100 3.0085 .0015 -1 1 3 2.9700 2.9689 .0011 1 1 3 2.8600 2.8593 .0007 4 0 2
a= 12.914 b= 4.230 c= 13.4200 beta= 92.442 da=.001 db=.001 dc=.0001 dbet=.004 V= 732.4
Triklin
Dexp. Dcal. d(D) h k l 4.2800 4.2800 .0000 0 -3 0 4.0300 4.0300 .0000 -3 -2 0 3.8400 3.8422 -.0022 2 -2 0 3.7000 3.6879 .0121 1 -3 0 3.5400 3.5400 .0000 -3 -3 0 3.3500 3.3472 .0028 -1 0 1 3.2100 3.2100 .0000 0 -4 0 3.0100 3.0130 -.0030 -3 -4 0 2.9700 2.9765 -.0065 -2 0 1 2.8600 2.8597 .0003 0 -3 1 2.7800 2.7805 -.0005 3 1 1 2.7000 2.7002 -.0002 1 3 1
A= 12.7476 DA= .0005 B= 13.5549 DB= .0004 C= 3.568 DC= .002 GAMMA= 71.990 DGAMMA= .001 BETA = 87.64 DBETA = .06 ALPHA= 94.09 DALPHA= .03 V= 583.5
42. 3-0469 Pb8Al2Si4O19 Triklin
Dexp Dcal d(D) h k l 9.8200 9.7423 .0777 1 0 0 8.8200 8.8238 -.0038 1 0 1 4.3100 4.3000 .0100 1 -1 1 3.2700 3.2698 .0002 0 -1 3 3.0600 3.0596 .0004 2 0 4 2.7600 2.7577 .0023 2 -1 4 2.6200 2.6205 -.0005 3 0 4 2.4700 2.4699 .0001 4 0 2 2.3700 2.3699 .0001 -3 0 3 2.1700 2.1695 .0005 2 -2 1 2.0000 1.9998 .0002 -4 1 2 1.8900 1.8901 -.0001 2 2 1 1.7400 1.7402 -.0002 4 -2 4 1.6500 1.6500 -.0000 5 0 6 1.5800 1.5800 -.0000 -5 2 0
A= 10.1445 DA= .0007 B= 4.5024 DB= .0005 C= 13.6125 DC= .0002 GAMMA= 99.94 DGAMMA= .01 BETA = 76.127 DBETA = .003 ALPHA= 97.58 DALPHA= .01 V= 591.9
43. 3-0539 alfa-Pb{BO2}2 Triklin
Dexp Dcal d(D) h k l 4.2000 4.1960 .0040 2 0 0 3.8700 3.8718 -.0018 0 2 0 3.5900 3.5897 .0003 -2 1 1 3.4400 3.4381 .0019 -2 0 1 3.3400 3.3417 -.0017 0 2 1 3.1200 3.1153 .0047 1 2 0 3.0700 3.0667 .0033 2 -2 1 3.0000 2.9979 .0021 -3 1 0 2.9400 2.9364 .0036 1 0 2 2.8600 2.8597 .0003 -1 1 2 2.7100 2.7127 -.0027 3 -1 1 2.5500 2.5501 -.0001 -3 2 1
A= 8.994 DA= .001 B= 8.303 DB= .001 C= 6.21659 DC= .00001 GAMMA=111.051 DGAMMA= .008 BETA = 89.312 DBETA = .003 ALPHA= 88.281 DALPHA= .002 V=433.0
44. 3-0554 Alfa_Pb4SiO6 Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.6400 3.6435 -.0035 2 1 0 3.3600 3.3634 -.0034 1 0 3 3.1000 3.0997 .0003 -4 0 1 3.0300 3.0299 .0001 -3 1 1 2.9100 2.9078 .0022 -4 0 2 2.8300 2.8287 .0013 4 0 1 2.7000 2.7003 -.0003 1 1 3 2.4900 2.4902 -.0002 -5 0 1 2.3100 2.3101 -.0001 5 0 1 2.2500 2.2494 .0006 -4 1 3 2.1700 2.1695 .0005 1 2 1 2.1200 2.1197 .0003 3 0 4
a= 12.464 b= 4.5292 c= 11.21 beta= 100.2 da= .006 db=.0002 dc=.01 dbeta=.05 V= 622.9
Triklin
Dexp Dcal d(D) h k l 3.6400 3.6402 -.0002 3 2 0 3.3600 3.3608 -.0008 1 3 0 3.1000 3.0994 .0006 -1 3 0 3.0300 3.0320 -.0020 -1 -1 1 2.9100 2.9103 -.0003 3 3 0 2.8300 2.8301 -.0001 1 -1 1 2.7000 2.7001 -.0001 -3 0 1 2.4900 2.4906 -.0006 0 4 0 2.3100 2.3099 .0001 -4 -2 1 2.2500 2.2506 -.0006 6 1 0 2.1700 2.1714 -.0014 6 2 0 2.1200 2.1206 -.0006 3 -2 1
A= 13.6184 DA= .0002 B= 10.124 DB= .002 C= 3.14297 DC= .00003 GAMMA= 79.856 DGAMMA= .001 BETA = 96.859 DBETA = .004 ALPHA= 92.655 DALPHA= .002 V=423.3
45. 3-00561 beta-PbO Triklin
Dexp Dcal d(D) h k l 5.0700 5.0705 -.0005 1 0 0 3.1000 3.1007 -.0007 1 2 0 2.7900 2.7868 .0032 1 1 2 2.4900 2.4909 -.0009 1 -1 2 2.1100 2.1091 .0009 -1 1 2 2.0600 2.0616 -.0016 0 4 0 1.9700 1.9683 .0017 1 4 1 1.8600 1.8603 -.0003 2 3 2 1.6700 1.6662 .0038 2 -1 3 1.5300 1.5302 -.0002 2 -2 3 1.4300 1.4319 -.0019 -1 5 2
A= 5.399 DA= .002 B= 8.437 DB= .004 C= 5.759 DC= .001 GAMMA= 89.58 DGAMMA= .01 BETA = 70.25 DBETA = .03 ALPHA= 78.39 DALPHA= .01 V=241.2
46. 3-0562 PbAl2O4 Monoklin Grupa-3
Dexp Dcal d(D) h k l 4.6700 4.6669 .0031 2 1 0 4.4400 4.4386 .0014 0 1 2 4.2300 4.2338 -.0038 -1 0 2 4.0600 4.0577 .0023 -1 2 1 3.0900 3.0898 .0002 2 2 2 2.6300 2.6309 -.0009 3 2 2 2.5100 2.5117 -.0017 3 1 3 2.3700 2.3694 .0006 -3 2 2 2.3100 2.3097 .0003 3 2 3 2.2300 2.2312 -.0012 1 2 4 2.1700 2.1699 .0001 3 0 4 2.1400 2.1405 -.0005 -4 1 2
a= 10.6146 b= 10.182 c= 9.970 beta= 81.64 da=.0005 db=.005 dc=.003 dbeta=.01 V= 1066.0
Triklin
Dexp Dcal d(D) h k l 4.6700 4.6714 -.0014 0 1 1 4.4400 4.4448 -.0048 1 0 0 4.2300 4.2194 .0106 0 -1 1 4.0600 4.0552 .0048 -1 0 1 3.0900 3.0901 -.0001 -1 3 1 2.6300 2.6301 -.0001 -1 -3 1 2.5100 2.5093 .0007 -1 0 2 2.3700 2.3697 .0003 0 -4 1 2.3100 2.3112 -.0012 -1 3 2 2.2300 2.2313 -.0013 -1 -4 1 2.1700 2.1693 .0007 2 1 0 2.1400 2.1395 .0005 -2 3 1
A= 4.7827 DA= .0001 B= 12.0623 DB= .0001 C= 5.1875 DC= .0001 GAMMA= 95.6669 DGAMMA= .001 BETA =111.568 DBETA = .002 ALPHA= 80.109 DALPHA= .001 V=274.0
47. 3-0573 PbO Triklin
Dexp Dcal d(D) h k l 3.1600 3.1598 .0002 0 1 1 3.0800 3.0793 .0007 0 -1 1 2.7800 2.7806 -.0006 -1 1 0 2.4900 2.4901 -.0001 -1 0 2 2.1100 2.1112 -.0012 -2 -1 1 1.9700 1.9709 -.0009 2 -1 1 1.8600 1.8614 -.0014 1 1 3 1.6700 1.6685 .0015 3 1 2 1.5500 1.5498 .0002 2 2 2 1.5400 1.5396 .0004 0 -2 2 1.4000 1.4003 -.0003 0 -1 4 1.2700 1.2699 .0001 3 2 3
A= 5.636 DA= .001 B= 3.6920 DB= .0002 C= 6.267 DC= .002 GAMMA= 78.674 DGAMMA= .00628 BETA = 79.05 DBETA = .01 ALPHA= 86.236 DALPHA= .003 V= 125.5
48. 3-0576 beta-Pb4B2O7 Triklin
Dexp Dcal d(D) h k l 4.5800 4.5854 -.0054 0 -1 2 3.9200 3.9200 -.0000 2 1 0 3.7900 3.7926 -.0026 0 1 2 3.2600 3.2594 .0006 -2 -2 2 3.0700 3.0701 -.0001 -2 0 2 3.0200 3.0234 -.0034 -1 -2 3 2.9400 2.9343 .0057 1 -2 1 2.8700 2.8712 -.0012 -2 1 0 2.7500 2.7465 .0035 2 -1 1 2.6900 2.6937 -.0037 -2 -3 2 2.6300 2.6313 -.0013 -3 -2 1 2.4900 2.4865 .0035 -2 1 2
A= 8.05 DA= .001 B= 8.799 DB= .003 C= 10.2168 DC= .0008 GAMMA= 64.56 DGAMMA= .02 BETA =102.38 DBETA = .02 ALPHA=106.01 DALPHA= .01 V=624.7 |
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