== Соединения Pb (томa 29-30) == |
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268. 29-1763 C4H4O4Pb Tetragon Groupa 90,113
Dexp. Dcal. d(D) h k l 6.3200 6.2731 .0469 1 1 1 5.9400 5.9585 -.0185 2 0 0 3.7700 3.7685 .0015 3 1 0 3.6700 3.6588 .0112 3 0 1 3.5000 3.4976 .0024 3 1 1 3.1400 3.1365 .0035 2 2 2 3.0000 2.9793 .0207 4 0 0 2.6500 2.6647 -.0147 4 2 0 2.5100 2.5134 -.0034 2 2 3 2.0300 2.0295 .0005 4 2 3 1.9600 1.9592 .0008 6 1 0
a= 11.917 c=9.39 da= .004 dc= .01 v=1334
Triklin
Dexp Dcal d(D) h k l 6.3200 6.3188 .0012 -1 0 1 5.9400 5.9358 .0042 0 1 0 3.7700 3.7694 .0006 0 -1 2 3.6700 3.6700 -.0000 -2 -1 1 3.5000 3.4993 .0007 -2 1 0 3.1400 3.1403 -.0003 -2 1 1 3.0000 2.9999 .0001 -1 1 2 2.6500 2.6501 -.0001 0 -2 2 2.5100 2.5100 -.0000 -1 2 1 2.0300 2.0300 .0000 4 0 2 1.9600 1.9600 -.0000 2 -2 3
A= 9.345 DA= .005 B= 6.0498 DB= .0004 C= 8.6409 DC= .0009 GAMMA= 84.26 DGAMMA= .01 BETA = 91.652 DBETA = .009 ALPHA= 99.680 DALPHA= .005 V= 479.1
270. 30-0060 NH4PbI3*xH2O Triklin
Dexp Dcal d(D) h k l 9.0700 9.0741 -.0041 1 0 0 7.4300 7.4652 -.0352 0 1 1 5.5700 5.5562 .0138 0 -1 1 4.9100 4.8971 .0129 1 -1 1 4.2100 4.2112 -.0012 -2 1 1 4.1100 4.1086 .0014 -2 0 1 3.8900 3.8943 -.0043 1 0 2 3.7400 3.7326 .0074 0 2 2 3.4900 3.4948 -.0048 -2 2 0 3.3600 3.3575 .0025 1 -1 2 3.2600 3.2606 -.0006 1 2 2 3.0900 3.0919 -.0019 2 0 2
A= 9.238 DA= .002 B= 9.583 DB= .001 C= 9.24 DC= .01 GAMMA=100.52 DGAMMA= .03 BETA = 95.53 DBETA = .03 ALPHA= 72.63 DALPHA= .01 V= 766.6
271. 30-0346 CdPb2O5 Triklin
Dexp Dcal d(D) h k l 5.0100 5.0061 .0039 1 1 0 4.0700 4.0711 -.0011 -1 1 2 3.8500 3.8498 .0002 0 3 0 3.7700 3.7673 .0027 0 2 2 3.2700 3.2696 .0004 -1 -2 2 3.1100 3.1057 .0043 0 3 2 2.9700 2.9726 -.0026 -1 3 2 2.8000 2.8011 -.0011 0 2 3 2.4600 2.4604 -.0004 -2 2 0 2.2600 2.2605 -.0005 2 3 0 2.0400 2.0400 -.0000 -2 -1 4 1.8400 1.8397 .0003 -3 2 2
A= 5.79998 DA= .00002 B= 11.62298 DB= .00002 C= 9.59062 DC= .00003 GAMMA= 90.8224 DGAMMA= .0004 BETA =108.5900 DBETA = .0002 ALPHA= 83.68683 DALPHA= .00003 V=609.0
272. 30-0346 CdPb2O5 Triklin
Dexp Dcal d(D) h k l 5.0100 5.0130 -.0030 0 2 0 4.0700 4.0780 -.0080 2 0 1 3.8500 3.8516 -.0016 -2 2 1 3.7700 3.7708 -.0008 0 0 2 3.2700 3.2731 -.0031 0 2 2 3.1100 3.1136 -.0036 -1 -1 2 2.9700 2.9726 -.0026 2 2 1 2.8000 2.8000 .0000 -1 3 2 2.4600 2.4603 -.0003 4 0 0 2.2600 2.2599 .0001 -2 0 3 2.0400 2.0390 .0010 4 0 2 1.8400 1.8408 -.0008 5 1 0
A= 10.235 DA= .002 B= 10.558 DB= .007 C= 7.6563 DC= .0006 GAMMA=105.9095 DGAMMA= .0003 BETA = 93.951 DBETA = .001 ALPHA= 80.16 DALPHA= .03 V= 783.8
273. 30-0689 PbAl2SiO6 Triklin
Dexp Dcal d(D) h k l 11.3000 11.2854 .0146 1 0 0 7.8300 7.8385 -.0085 1 1 0 6.5900 6.5957 -.0057 0 -1 1 6.5100 6.5138 -.0038 1 -1 1 5.6700 5.6681 .0019 1 -2 1 5.4100 5.4164 -.0064 1 2 0 5.1100 5.1226 -.0126 -1 -1 1 4.4200 4.4163 .0037 -2 3 0 4.1900 4.1923 -.0023 2 -3 1 4.0700 4.0702 -.0002 2 1 1 3.9200 3.9193 .0007 2 2 0 3.8100 3.8088 .0012 -2 -1 1
A= 12.083 DA= .005 B= 15.63 DB= .01 C= 7.087 DC= .003 GAMMA=109.46 DGAMMA= .04 BETA = 78.949 DBETA = .009 ALPHA=101.18 DALPHA= .03 V= 1226.6
274. 30-0692 Pb2S5Sb2 Triklin
Dexp Dcal d(D) h k l 7.6900 7.6938 -.0038 1 0 0 6.8600 6.8508 .0092 0 1 0 6.2100 6.2036 .0064 -1 0 1 4.1000 4.1028 -.0028 0 0 2 3.8500 3.8507 -.0007 2 1 0 3.7400 3.7472 -.0072 1 -1 1 3.5900 3.5955 -.0055 0 1 2 3.4500 3.4487 .0013 0 -1 2 3.2700 3.2713 -.0013 -1 1 2 2.9300 2.9284 .0016 -2 -2 1 2.7800 2.7811 -.0011 -1 2 1 2.6900 2.6882 .0018 2 -1 1
A= 8.147 DA= .002 B= 7.1418 DB= .0001 C= 8.34478 DC= .00080 GAMMA= 73.8106 DGAMMA= .01 BETA =100.14 DBETA = .01 ALPHA= 90.26 DALPHA= .01 V=458.1
275. 30-0702 Pb3.25Ge3N1.507 Triklin
Dexp Dcal d(D) h k l 4.4400 4.4409 -.0009 -1 -1 1 3.6900 3.6912 -.0012 0 2 2 3.6400 3.6396 .0004 0 3 0 3.5600 3.5581 .0019 -1 0 2 3.4200 3.4184 .0016 -1 1 2 3.3500 3.3487 .0013 -1 -1 2 3.3000 3.3000 .0000 2 0 0 3.2000 3.2008 -.0008 -2 1 0 3.1200 3.1185 .0015 2 1 0 3.0300 3.0298 .0002 -1 2 2 2.9500 2.9509 -.0009 0 3 2 2.9200 2.9206 -.0006 -2 0 1
A= 6.8201 DA= .0002 B= 10.9310 DB= .0004 C= 10.2174 DC= .0001 GAMMA= 92.596 DGAMMA= .008 BETA = 75.653 DBETA = .002 ALPHA= 89.907 DALPHA= .003 V=736.9
276. 30-0708 PbH2P2O5 Triklin
Dexp Dcal d(D) h k l 7.6000 7.5976 .0024 1 2 0 6.9000 6.9577 -.0577 0 2 0 4.7000 4.7019 -.0019 3 0 0 4.3000 4.2995 .0005 3 3 0 4.0000 4.0004 -.0004 -1 -1 1 3.5000 3.4996 .0004 2 -1 1 3.3000 3.3030 -.0030 -2 3 0 3.1000 3.0953 .0047 -1 4 0 2.9700 2.9717 -.0017 1 5 0 2.7600 2.7602 -.0002 4 3 1 2.5800 2.5797 .0003 5 5 0 2.4000 2.3999 .0001 2 5 1
A= 15.48746 DA= .00007 B= 15.2854 DB= .0003 C= 4.2222 DC= .0006 GAMMA= 66.064 DGAMMA= .003 BETA = 87.034 DBETA = .009 ALPHA= 93.434 DALPHA= .004 V=908.3
277. 30-0715 3Pb{NO3}2**7PbO*1.5H2O Triklin
Dexp Dcal d(D) h k l 9.3000 9.3048 -.0048 0 1 1 7.4300 7.4237 .0063 -1 1 0 7.0400 7.0445 -.0045 0 -1 1 5.8600 5.8593 .0007 0 0 2 4.2100 4.2128 -.0028 1 0 2 3.9300 3.9308 -.0008 1 1 2 3.7100 3.7119 -.0019 -2 2 0 3.5300 3.5280 .0020 -1 -2 1 3.3200 3.3148 .0052 1 -2 2 3.2500 3.2499 .0001 1 -3 1 3.1400 3.1396 .0004 1 1 3 3.0100 3.0092 .0008 1 -1 3
A= 8.3789 DA= .0003 B= 12.356 DB= .003 C= 12.876 DC= .003 GAMMA=114.69 DGAMMA= .07 BETA =108.95 DBETA = .06 ALPHA= 68.32 DALPHA= .02 V= 1102.4
278. 30-0718 Pb{ReO4}2 Triklin
Dexp Dcal d(D) h k l 4.1500 4.1489 .0011 -2 1 0 4.0900 4.0923 -.0023 -2 0 1 3.6400 3.6405 -.0005 0 -2 1 3.5000 3.5005 -.0005 1 -2 1 3.3100 3.3097 .0003 -2 2 0 3.2000 3.2056 -.0056 2 -1 1 2.8400 2.8387 .0013 -3 0 1 2.6700 2.6736 -.0036 3 0 0 2.3700 2.3724 -.0024 2 -3 1 2.2800 2.2801 -.0001 1 1 2 2.2100 2.2118 -.0018 -4 1 1 2.1100 2.1102 -.0002 -3 3 1
A= 8.86 DA= .01 B= 7.899 DB= .006 C= 6.958 DC= .003 GAMMA=105.38 DGAMMA= .09 BETA =106.159 DBETA = .003 ALPHA=100.40 DALPHA= .03 V= 433.7
279. 30-0719 Pb{ReO4}2*2H2O Rombik Groupa 26,28,51
Dexp. Dcal. d(D) h k l 3.4900 3.4782 .0118 1 0 1 3.4300 3.4192 .0108 2 2 0 3.3500 3.3582 -.0082 0 3 0 2.9300 2.9204 .0096 2 0 1 2.5300 2.5265 .0035 2 2 1 2.4300 2.4313 -.0013 1 4 0 2.3300 2.3265 .0035 3 1 1 2.3300 2.3281 .0019 4 0 0 2.2000 2.2037 -.0037 2 3 1 1.9600 1.9558 .0042 3 4 0 1.9100 1.9073 .0027 2 4 1 1.8500 1.8492 .0008 2 5 0
a= 9.312 b=10.075 c= 3.750 da= .018 db= .007 dc= .007 V= 351.8
Monoklin Grupa 3
Dexp Dcal d(D) h k l 3.4900 3.4882 .0018 1 1 0 3.4300 3.4324 -.0024 1 0 3 3.3500 3.3487 .0013 -1 1 1 2.9300 2.9286 .0014 2 0 3 2.5300 2.5286 .0014 -4 0 1 2.4300 2.4283 .0017 3 1 1 2.3300 2.3292 .0008 -3 1 2 2.2000 2.2009 -.0009 -1 1 4 1.9600 1.9609 -.0009 -5 0 2 1.9100 1.9090 .0010 -3 1 4 1.8500 1.8498 .0002 -1 0 6 1.8300 1.8299 .0001 0 2 1
a= 10.2600 b= 3.710 c= 11.18190 beta= 93.394 da= .0009 db=.001 dc=.00004 dbet= .005 V= 424.9
280. 30-0723 Pb2SiO4 Triklin
Dexp Dcal d(D) h k l 9.5600 9.5676 -.0076 0 1 0 6.0400 6.0463 -.0063 -1 -1 1 3.7300 3.7300 .0000 0 -1 2 3.5300 3.5294 .0006 1 2 1 3.2200 3.2196 .0004 0 -2 2 3.1300 3.1318 -.0018 -2 -1 2 3.0400 3.0404 -.0004 -2 1 0 2.9920 2.9917 .0003 2 1 1 2.8090 2.8057 .0033 2 3 0 2.7830 2.7822 .0008 0 2 2 2.7660 2.7690 -.0030 1 3 1 2.5810 2.5813 -.0003 1 -2 2
A= 7.6877 DA= .0001 B= 10.26636 DB= .00007 C= 8.01057 DC= .00004 GAMMA= 70.4696 DGAMMA= .0005 BETA =106.2117 DBETA = .0005 ALPHA=103.1864 DALPHA= .0001 V=589.1
| 281. 30-0724 Pb2SiO4 Triklin
Dexp Dcal d(D) h k l 9.5400 9.5198 .0202 0 1 0 6.0300 6.0300 -.0000 2 1 0 4.7900 4.7881 .0019 -2 0 1 4.1100 4.1079 .0021 -2 1 1 3.7600 3.7609 -.0009 2 1 1 3.5100 3.5142 -.0042 4 0 0 3.2100 3.2113 -.0013 -2 2 1 3.1500 3.1488 .0012 2 2 1 3.0400 3.0398 .0002 2 3 0 2.9790 2.9795 -.0005 2 -2 1 2.8070 2.8055 .0015 -1 0 2 2.7760 2.7768 -.0008 0 -3 1
A= 14.42855 DA= .01095 B= 9.60694 DB= .00020 C= 5.61736 DC= .00122 GAMMA= 82.38358 DGAMMA= .03527 BETA =100.86590 DBETA = .02533 ALPHA= 92.65418 DALPHA= .00203 V-758.7
282. 30-0725 Pb2SiO4 Triklin
Dexp Dcal d(D) h k l 8.5800 8.5744 .0056 -1 0 1 6.3000 6.2886 .0114 0 1 1 5.8800 5.8890 -.0090 0 -1 1 5.3100 5.2902 .0198 -2 1 1 4.9600 4.9603 -.0003 -1 0 2 4.3200 4.3229 -.0029 -2 1 2 3.9200 3.9201 -.0001 -2 -1 1 3.4400 3.4364 .0036 1 2 0 3.3200 3.3204 -.0004 -1 0 3 3.2100 3.2112 -.0012 -2 0 3 3.1600 3.1602 -.0002 1 2 1 3.0900 3.0896 .0004 2 -2 1
A= 11.4976 DA= .0008 B= 8.4492 DB= .0002 C= 10.13898 DC= .00008 GAMMA=107.99 DGAMMA= .03 BETA =112.88 DBETA = .05 ALPHA= 79.747 DALPHA= .008 V= 861.3
283. 30-0726 Pb2SiO4 Triklin
Dexp Dcal d(D) h k l 9.5300 9.5219 .0081 1 0 0 8.7500 8.7537 -.0037 1 1 0 6.0100 6.0119 -.0019 -1 -1 1 3.7400 3.7408 -.0008 -2 -2 1 3.5400 3.5395 .0005 3 1 0 3.2100 3.2096 .0004 0 -2 2 3.1300 3.1322 -.0022 2 1 3 3.0300 3.0302 -.0002 2 -1 2 2.9950 2.9909 .0041 1 2 3 2.7790 2.7790 .0000 3 3 2 2.5830 2.5818 .0012 0 -2 3 2.3930 2.3930 .0000 2 2 4 : A= 10.900 DA= .009 B= 10.0483 DB= .0001 C= 10.246 DC= .005 GAMMA= 62.05 DGAMMA= .02 BETA = 78.41 DBETA = .01 ALPHA= 81.18 DALPHA= .03 V= 968.6
284. 30-0727 Pb2Sr3SiO7 Triklin
Dexp Dcal d(D) h k l 5.0100 5.0228 -.0128 -1 0 2 4.6600 4.6588 .0012 0 2 0 4.6200 4.6148 .0052 -1 2 1 4.4700 4.4720 -.0020 0 1 2 4.1600 4.1597 .0003 -2 2 0 3.3100 3.3094 .0006 2 1 0 3.2800 3.2823 -.0023 -1 -1 3 3.2000 3.2015 -.0015 2 -2 2 3.0600 3.0592 .0008 2 0 2 2.8600 2.8607 -.0007 0 -3 2 2.8200 2.8221 -.0021 -3 2 2 2.7500 2.7505 -.0005 1 1 3
A= 9.434 DA= .002 B= 10.40 DB= .01 C= 11.136 DC= .001 GAMMA=115.46 DGAMMA= .04 BETA = 98.393 DBETA = .004 ALPHA= 92.92 DALPHA= .02 V=968.4
285. 30-0728 PbSr2SiO7 Monoklin Grupa 3
Dexp Dcal d(D) h k l 5.8300 5.8317 -.0017 2 0 1 5.0100 5.0110 -.0010 -1 1 1 4.0000 4.0002 -.0002 3 0 0 3.2600 3.2605 -.0005 -2 1 3 3.1100 3.1106 -.0006 -3 0 3 3.0500 3.0525 -.0025 2 0 5 2.9300 2.9243 .0057 0 2 1 2.8500 2.8524 -.0024 1 2 1 2.8300 2.8301 -.0001 -1 2 1 2.8100 2.8092 .0008 -2 0 5 2.7300 2.7406 -.0106 -4 0 2 2.7000 2.6999 .0001 3 0 5
a= 12.058 b= 5.940 c= 16.8170 beta= 84.403 da= .001 db= .002 dc= .0001 dbet=.007 V= 1198.8
Triklin
Dexp Dcal d(D) h k l 5.8300 5.8350 -.0050 0 0 1 5.0100 4.9976 .0124 1 0 1 4.0000 3.9868 .0132 0 -2 1 3.2600 3.2602 -.0002 2 1 0 3.1100 3.1086 .0014 2 1 1 3.0500 3.0503 -.0003 0 -1 2 2.9300 2.9351 -.0051 1 3 0 2.8500 2.8486 .0014 0 -3 1 2.8300 2.8309 -.0009 -1 -3 1 2.8100 2.8116 -.0016 0 -2 2 2.7300 2.7308 -.0008 2 -1 1 2.7000 2.6989 .0011 1 1 2
A= 6.6633 DA= .0002 B= 9.079 DB= .003 C= 6.243 DC= .001 GAMMA= 73.213 DGAMMA= .003 BETA = 78.17 DBETA = .03 ALPHA=102.66 DALPHA= .03 V=338.3
286. 30-0731 Pb{TcO4}2 Triklin
Dexp Dcal d(D) h k l 3.4000 3.3994 .0006 0 1 1 3.3600 3.3616 -.0016 -1 0 1 3.2900 3.2904 -.0004 0 -1 1 3.1700 3.1695 .0005 -1 2 1 3.0700 3.0718 -.0018 0 -2 1 2.5400 2.5433 -.0033 0 -4 1 2.3900 2.3922 -.0022 0 7 0 2.3100 2.3101 -.0001 1 -1 1 2.2300 2.2300 .0000 -2 2 1 2.1300 2.1300 .0000 -2 -3 1 2.1000 2.1011 -.0011 -1 -6 1 2.0100 2.0095 .0005 1 5 1
A= 4.87365 DA= .00005 B= 16.81 DB= .01 C= 3.6577 DC= .0001 GAMMA= 88.751 DGAMMA= .009 BETA =110.60 DBETA = .01 ALPHA= 85.9797 DALPHA= .0005 V= 279.4
287. 30-0732 Pb{TcO4}2*2H2O Triklin
Dexp Dcal d(D) h k l 3.4600 3.4608 -.0008 0 -1 1 3.4000 3.3998 .0002 -1 1 0 3.3000 3.3010 -.0010 1 -1 1 3.0900 3.0889 .0011 -1 1 1 2.9300 2.9305 -.0005 -2 1 0 2.5200 2.5204 -.0004 3 -1 1 2.3100 2.3117 -.0017 -2 1 2 2.2700 2.2712 -.0012 -1 -1 3 2.2100 2.2109 -.0009 5 0 0 2.1700 2.1718 -.0018 -1 1 3 2.0100 2.0107 -.0007 5 1 2 1.9700 1.9703 -.0003 2 -1 4
A= 11.55 DA= .02 B= 3.7251 DB= .0008 C= 9.570 DC= .007 GAMMA= 83.78 DGAMMA= .04 BETA = 74.43 DBETA = .07 ALPHA= 89.49 DALPHA= .05 V= 394.1
288. 30-1453 Y2PbO3F2 Triklin
Dexp Dcal d(D) h k l 3.3200 3.3194 .0006 -1 1 1 2.9100 2.9095 .0005 -1 0 2 2.8300 2.8298 .0002 1 -1 1 2.6400 2.6396 .0004 -1 1 2 2.3800 2.3792 .0008 -2 1 0 2.0430 2.0427 .0003 -1 2 0 2.0290 2.0292 -.0002 -1 1 3 1.7520 1.7516 .0004 -3 1 0 1.7290 1.7290 .0000 2 0 3 1.6640 1.6644 -.0004 3 0 2 1.4560 1.4564 -.0004 1 2 4 1.4320 1.4320 -.0000 4 0 1
A= 5.9376 DA= .0003 B= 4.6239 DB= .0006 C= 6.7274 DC= .0004 GAMMA= 85.465 DGAMMA= .008 BETA = 90.918 DBETA = .004 ALPHA= 77.1236 DALPHA= .0009 V= 179.4
289. 30-1774 C18H16O4Pb Monoklin Grupa 14
Dexp Dcal d(D) h k l 17.7000 17.6562 .0438 0 1 1 8.8300 8.8281 .0019 0 2 2 5.8600 5.8528 .0072 0 4 2 5.4000 5.4064 -.0064 1 4 2 4.7800 4.7867 -.0067 -1 2 4 4.4000 4.3974 .0026 2 4 2 3.9600 3.9552 .0048 -1 6 2 3.8800 3.8809 -.0009 0 0 6 3.5800 3.5807 -.0007 3 4 1 3.5100 3.5100 .0000 -2 4 4 3.4800 3.4789 .0011 -2 2 5 3.3200 3.3188 .0012 1 4 6
a= 12.7101 b= 27.082 c= 23.380 beta= 84.833 da= .0001 db= .001 dc= .001 dbet= .001 V= 8015.
290. 30-1775 C18H18O6Pb2 Geksagon Groupa 143
Dexp. Dcal. d(D) h k l 22.1000 21.7853 .3147 0 0 1 17.7000 17.6643 .0357 1 0 0 10.3000 10.1985 .1015 1 1 0 8.7700 8.8321 -.0621 2 0 0 6.8700 6.8603 .0097 2 0 2 3.4300 3.4302 -.0002 4 0 4 2.9350 2.9353 -.0003 2 0 7 2.8210 2.8208 .0002 2 1 7
a= 20.40 c= 21.785 da= .07 dc=.008 V=7849
291. 30-1776 C8H4O4Pb*PbO Triklin
Dexp Dcal d(D) h k l 22.1000 22.0987 .0013 1 0 0 13.1000 13.1160 -.0160 0 1 0 12.7000 12.6835 .0165 0 0 1 8.3600 8.3698 -.0098 -2 -1 1 6.9900 6.9889 .0011 3 1 0 6.7600 6.7701 -.0101 0 -2 1 6.5700 6.5580 .0120 0 -2 0 6.3000 6.2951 .0049 -3 0 1 6.1500 6.1526 -.0026 2 2 0 6.0000 5.9963 .0037 -1 2 0 5.5100 5.5094 .0006 2 -1 2 4.8800 4.8780 .0020 -1 1 2
A= 22.4863 DA= .0008 B= 14.07 DB= .01 C= 13.3859 DC= .0001 GAMMA= 79.468 DGAMMA= .002 BETA = 91.88 DBETA = .01 ALPHA=108.59 DALPHA= .01 V= 3945.8
292. 30-1777 C8H4O4Pb*2PbO Triklin
Dexp Dcal d(D) h k l 14.8000 14.8443 -.0443 1 0 0 12.3000 12.3038 -.0038 0 1 0 9.5500 9.5903 -.0403 -1 0 1 9.1100 9.1232 -.0132 0 -1 1 7.5700 7.5743 -.0043 1 -1 1 6.9600 6.9751 -.0151 -2 0 1 6.7700 6.7834 -.0134 0 1 1 6.1700 6.1519 .0181 0 2 0 5.9500 5.9328 .0172 -2 -1 1 5.6000 5.5969 .0031 2 -1 1 5.1900 5.1938 -.0038 1 2 0 5.0500 5.0436 .0064 -3 0 1
A= 15.862 DA= .003 B= 13.18 DB= .01 C= 10.598 DC= .008 GAMMA=102.248 DGAMMA= .005 BETA =102.97 DBETA = .07 ALPHA=103.50 DALPHA= .01 V= 2015
293. 30-1778 C8H4O4PbO*H2O Triklin
Dexp Dcal d(D) h k l 12.8000 12.8449 -.0449 -1 1 0 12.0000 11.9706 .0294 1 1 0 7.0300 7.0413 -.0113 -1 0 1 6.9100 6.9231 -.0131 0 1 1 6.4000 6.4093 -.0093 1 0 1 6.2300 6.2196 .0104 1 1 1 6.0800 6.0946 -.0146 0 -1 1 6.0000 6.0046 -.0046 -1 -1 1 5.8300 5.8216 .0084 -1 2 1 5.6900 5.6804 .0096 1 -1 1 5.4800 5.4691 .0109 -2 -1 1 4.5900 4.5917 -.0017 0 3 1
A= 20.573 DA= .009 B= 15.967 DB= .008 C= 7.307 DC= .007 GAMMA= 95.78 DGAMMA= .03 BETA = 99.51 DBETA = .07 ALPHA= 79.524 DALPHA= .001 V=2317.7 |
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