== Соединения Pb (томa 20-21) == |
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151. 20-0220 Ca2Pb3Si3O11 Triklin
Dexp Dcal d(D) h k l 4.9400 4.9360 .0040 -1 0 2 4.4400 4.4356 .0044 0 1 1 4.2700 4.2706 -.0006 -1 1 1 3.5500 3.5591 -.0091 0 1 2 3.3900 3.3914 -.0014 0 -1 2 3.2300 3.2310 -.0010 -2 1 2 3.1500 3.1471 .0029 -2 0 3 3.0800 3.0793 .0007 -2 -1 2 2.9760 2.9731 .0029 -3 1 0 2.8500 2.8492 .0008 -4 0 1 2.8010 2.8030 -.0020 4 0 0 2.7300 2.7290 .0010 3 1 1
A= 11.4404 DA= .0003 B= 4.84111 DB= .00006 C= 10.19513 DC= .00004 GAMMA= 91.2265 DGAMMA= .0002 BETA =101.456 DBETA = .001 ALPHA= 87.0534 DALPHA= .0005 V=552.7
152. 20-0566 Pb15Sb!6S39 Triklin
Dexp Dcal d(D) h k l 4.1900 4.1944 -.0044 1 1 1 3.8200 3.8179 .0021 -1 -1 1 3.3400 3.3392 .0008 2 0 0 3.2400 3.2422 -.0022 2 0 2 2.9500 2.9476 .0024 -2 0 1 2.8500 2.8464 .0036 1 -2 1 2.6900 2.6893 .0007 -2 1 1 2.4500 2.4499 .0001 2 1 3 2.3600 2.3578 .0022 1 1 4 2.2200 2.2210 -.0010 3 -1 1 2.1400 2.1400 .0000 2 1 4 2.1000 2.1000 .0000 3 1 1
A= 6.97634 DA= .00002 B= 6.0533 DB= .0002 C= 10.7865 DC= .0002 GAMMA= 95.066 DGAMMA= .003 BETA = 73.622 DBETA = .002 ALPHA= 95.070 DALPHA= .004 V=434.4
153. 20-0569 Pb11As8S31 Triklin
Dexp Dcal d(D) h k l 5.3300 5.3299 .0001 0 -1 1 4.2300 4.2290 .0010 1 0 1 3.6000 3.5995 .0005 0 -3 1 3.4600 3.4511 .0089 1 2 1 3.1900 3.1879 .0021 1 3 0 3.0400 3.0379 .0021 0 3 1 2.8400 2.8401 -.0001 -1 3 0 2.6700 2.6730 -.0030 1 4 0 2.6100 2.6094 .0006 -1 -3 1 2.4400 2.4412 -.0012 1 -3 2 2.3200 2.3204 -.0004 2 1 1 2.2100 2.2110 -.0010 1 3 2
A= 4.694 DA= .001 B= 12.572 DB= .006 C= 5.885 DC= .002 GAMMA= 86.73 DGAMMA= .09 BETA = 69.73 DBETA = .01 ALPHA= 98.26 DALPHA= .09 V= 320.2
154. 20-0573 Pb5B8O17 Triklin
Dexp Dcal d(D) h k l 6.7600 6.7624 -.0024 0 1 1 6.0600 6.0738 -.0138 0 -1 1 5.0400 5.0417 -.0017 1 -1 1 4.2400 4.2438 -.0038 1 1 1 3.8700 3.8736 -.0036 -1 2 0 3.7600 3.7662 -.0062 0 -2 1 3.4700 3.4698 .0002 -1 2 1 3.3900 3.3812 .0088 0 2 2 3.1000 3.1039 -.0039 0 1 3 3.0400 3.0369 .0031 0 -2 2 3.0100 3.0119 -.0019 1 -1 3 2.8580 2.8592 -.0012 0 3 0
A= 5.832 DA= .003 B= 8.867 DB= .002 C= 9.99 DC= .01 GAMMA=103.34 DGAMMA= .07 BETA = 74.72 DBETA = .08 ALPHA= 87.701 DALPHA= .003 V= 482.1
155. 20-0574 Pb9B16O33 TRiklin
Dexp Dcal d(D) h k l 6.1000 6.1049 -.0049 -1 1 0 5.8200 5.8243 -.0043 0 1 1 5.6300 5.6344 -.0044 0 -1 1 5.1600 5.1617 -.0017 1 1 0 4.8600 4.8639 -.0039 -1 1 2 4.4500 4.4515 -.0015 2 -1 1 4.0300 4.0290 .0010 -3 0 1 3.7100 3.7098 .0002 -3 0 2 3.6300 3.6296 .0004 -2 1 3 3.5500 3.5503 -.0003 1 -1 3 3.4500 3.4508 -.0008 1 1 3 3.4000 3.3964 .0036 2 1 2
A= 12.5498 DA= .0007 B= 6.42003 DB= .00002 C= 14.212 DC= .001 GAMMA=102.199 DGAMMA= .001 BETA = 97.3891 DBETA = .0002 ALPHA= 85.972 DALPHA= .003 V=1108.6
156. 20-0575 alfa-PbB2O4 Triklin
Dexp Dcal d(D) h k l 8.0400 8.0356 .0044 0 1 1 7.5800 7.5862 -.0062 -1 1 0 6.3300 6.3297 .0003 2 0 0 6.0200 6.0448 -.0248 2 1 0 5.6000 5.6174 -.0174 -2 0 1 5.5500 5.5445 .0055 0 0 2 5.1700 5.1731 -.0031 -1 0 2 5.0700 5.0630 .0070 0 1 2 4.7400 4.7442 -.0042 -1 -1 2 4.6500 4.6509 -.0009 2 2 0 4.4400 4.4432 -.0032 -1 2 1 4.3400 4.3416 -.0016 1 -1 2
A= 12.939 DA= .001 B= 11.271 DB= .009 C= 11.1133 DC= .0004 GAMMA= 78.41 DGAMMA= .05 BETA = 92.25 DBETA = .01 ALPHA= 87.47 DALPHA= .01 V=1584.6
157. 20-0576 beta-PbB2O4 Monoklin Grupa 3
Dexp Dcal d(D) h k l 5.7500 5.7399 .0101 1 1 2 5.6800 5.6990 -.0190 0 2 1 5.5900 5.5816 .0084 2 0 0 5.2800 5.2880 -.0080 2 1 1 5.1200 5.1137 .0063 2 1 0 4.9000 4.9022 -.0022 -1 0 2 4.5300 4.5278 .0022 1 2 2 4.4200 4.4295 -.0095 1 0 3 4.2500 4.2533 -.0033 0 3 0 4.1900 4.1845 .0055 1 1 3 3.8300 3.8311 -.0011 2 1 3 3.6400 3.6385 .0015 1 2 3
a= 11.733 b= 12.760 c= 13.3250 beta= 72.062 da= .001 db=.001 dc=.0008 dbet= .005 V= 1898
158. 20-0577 gamma-PbB2O4 Triklin
Dexp Dcal d(D) h k l 8.6100 8.6215 -.0115 1 0 0 7.0300 7.0147 .0153 1 1 0 4.9600 4.9562 .0038 1 -1 1 4.8300 4.8208 .0092 -1 -2 1 4.6200 4.6105 .0095 0 -2 1 4.3300 4.3278 .0022 2 1 0 4.0400 4.0345 .0055 -1 -2 2 3.8900 3.8948 -.0048 -2 -2 1 3.8200 3.8255 -.0055 0 -2 2 3.4800 3.4803 -.0003 -2 1 0 3.2600 3.2613 -.0013 -1 -3 1 3.2100 3.2085 .0015 0 2 1
A= 9.214 DA= .002 B= 9.8634 DB= .0001 C= 9.155 DC= .007 GAMMA= 70.127 DGAMMA= .006 BETA =104.04 DBETA = .04 ALPHA=117.96 DALPHA= .03 V= 687.7
159. 20-0578 Pb{H2PO4}2 Triklin
Dexp Dcal d(D) h k l 3.8800 3.8777 .0023 2 2 1 3.8700 3.8708 -.0008 0 -2 1 3.7200 3.7188 .0012 2 2 0 3.7100 3.7093 .0007 -1 -2 1 3.5900 3.5926 -.0026 1 -2 1 3.5800 3.5819 -.0019 3 0 2 3.2400 3.2395 .0005 -2 -2 1 3.2200 3.2205 -.0005 0 -2 2 3.0600 3.0589 .0011 3 -1 2 3.0500 3.0487 .0013 -1 -2 2 2.9300 2.9311 -.0011 1 3 1 2.9100 2.9111 -.0011 -2 2 1
A= 11.80602 DA= .00003 B= 8.83823 DB= .00004 C= 11.49056 DC= .00006 GAMMA= 77.33869 DGAMMA= .00009 BETA = 70.5792 DBETA = .0001 ALPHA= 81.00771 DALPHA= .00008 V=1099.1
160. 20-0581 Pb{H2PO3}2 Triklin
Dexp Dcal d(D) h k l 8.8000 8.9361 -.1361 0 0 1 7.9000 7.9015 -.0015 0 1 0 6.5700 6.5668 .0032 0 1 1 5.8900 5.8776 .0124 1 1 0 4.7200 4.7165 .0035 1 1 1 4.3800 4.3763 .0037 -2 0 2 4.2500 4.2483 .0017 0 1 2 4.1100 4.1069 .0031 -1 2 1 3.9500 3.9507 -.0007 0 2 0 3.7400 3.7420 -.0020 -2 2 1 3.6000 3.6009 -.0009 1 0 2 3.5100 3.5057 .0043 -3 0 2
A= 11.684 DA= .001 B= 8.306 DB= .007 C= 10.179 DC= .007 GAMMA=104.38400 DGAMMA= .00001 BETA =116.63 DBETA = .09 ALPHA= 74.05 DALPHA= .08 V= 840.11
161. 20-0582 PbHPO3*H2O Triklin
Dexp Dcal d(D) h k l 7.7000 7.6945 .0055 1 1 0 6.9000 6.9079 -.0079 -1 0 1 5.8800 5.8965 -.0165 0 -1 1 5.7500 5.7619 -.0119 -1 1 1 4.6400 4.6440 -.0040 0 1 2 4.4000 4.3894 .0106 -1 0 2 3.7900 3.7881 .0019 1 3 1 3.6000 3.5994 .0006 0 3 0 3.4800 3.4808 -.0008 2 2 1 3.2200 3.2212 -.0012 -1 -3 1 2.9700 2.9724 -.0024 -2 -3 1 2.9200 2.9205 -.0005 0 0 3
A= 8.5151 DA= .0006 B= 11.885 DB= .001 C= 9.4857 DC= .0001 GAMMA= 74.930 DGAMMA= .007 BETA =101.000 DBETA = .008 ALPHA= 74.258 DALPHA= .003 V=856.1
162. 20-0590 Pb3O2HPO3*0.5H2O Triklin
Dexp Dcal d(D) h k l 7.5000 7.4970 .0030 0 1 1 5.4000 5.3991 .0009 -1 -1 1 5.2100 5.2064 .0036 0 -1 1 4.5700 4.5680 .0020 0 0 2 3.9500 3.9439 .0061 -1 1 2 3.7400 3.7387 .0013 2 2 0 3.3700 3.3726 -.0026 2 0 1 3.2900 3.2876 .0024 0 -2 1 3.1400 3.1402 -.0002 1 3 1 2.9200 2.9204 -.0004 -2 1 2 2.8800 2.8803 -.0003 2 3 0 2.6900 2.6895 .0005 0 3 0
A= 8.682 DA= .002 B= 9.432 DB= .006 C= 9.766 DC= .001 GAMMA= 66.06 DGAMMA= .03 BETA = 91.92 DBETA = .05 ALPHA= 72.07 DALPHA= .03 V= 683.7
163. 20-0595 alfa-PbS2 Rombik Groupa 29,57
romb.
Dexp. Dcal. d(D) h k l 6.0000 6.0000 .0000 0 1 0 2.8500 2.8473 .0027 1 2 0 2.1300 2.1260 .0040 3 2 0 1.6800 1.6800 .0000 0 0 2 1.2300 1.2298 .0002 4 2 2 1.1600 1.1598 .0002 2 5 0
a= 9.040 b= 6.000 c= 3.360 da= .001 db= .005 dc= .001 V= 182.2
164. 20-0898 K{Pb{NH2}3} Triklin
Dexp Dcal d(D) h k l 5.6700 5.6701 -.0001 1 1 0 5.4600 5.4598 .0002 -1 0 1 4.7200 4.7176 .0024 -1 -1 1 4.5200 4.5263 -.0063 0 -1 1 3.3700 3.3723 -.0023 -1 -1 2 3.3000 3.3005 -.0005 1 2 1 3.1800 3.1762 .0038 -1 1 2 2.9700 2.9702 -.0002 2 0 0 2.7600 2.7599 .0001 0 0 3 2.6100 2.6108 -.0008 2 0 1 2.5000 2.4991 .0009 -1 -1 3 2.4650 2.4643 .0007 1 1 3
A= 6.6381 DA= .0002 B= 6.97118 DB= .00004 C= 8.5963 DC= .0007 GAMMA= 66.8834 DGAMMA= .0008 BETA = 98.877 DBETA = .009 ALPHA= 81.84 DALPHA= .01 V=352.4
165. 20-0899 K4PbO4 Triklin
Dexp Dcal d(D) h k l 5.6500 5.6524 -.0024 0 1 1 5.1800 5.1796 .0004 0 -1 1 4.8900 4.8903 -.0003 1 0 0 4.4100 4.4084 .0016 0 -1 2 4.1100 4.1112 -.0012 -1 1 0 3.6000 3.5960 .0040 1 0 3 3.2300 3.2306 -.0006 1 1 2 3.1000 3.0995 .0005 1 0 4 3.0300 3.0305 -.0005 0 1 5 2.7240 2.7243 -.0003 -1 2 1 2.6880 2.6888 -.0008 1 0 5 2.5160 2.5157 .0003 0 2 4 2.4090 2.4093 -.0003 2 0 1 2.3720 2.3718 .0002 -2 1 2
A= 4.98300 DA= .00005 B= 5.88509 DB= .00004 C= 16.558 DC= .001 GAMMA=100.98 DGAMMA= .01 BETA = 93.05 DBETA = .03 ALPHA= 81.536 DALPHA= .001 V= 471.3 | 166. 20-0900 KPbO2 Triklin
Dexp Dcal d(D) h k l 6.3200 6.3251 -.0051 -1 0 1 5.9400 5.9383 .0017 -1 1 0 4.9400 4.9384 .0016 -1 -2 1 4.5500 4.5504 -.0004 -1 2 0 3.9800 3.9794 .0006 -2 -1 1 3.5700 3.5687 .0013 -1 3 0 3.5000 3.5007 -.0007 -1 -1 2 3.3000 3.3026 -.0026 1 -2 1 3.1300 3.1291 .0009 0 2 2 2.9980 2.9957 .0023 -2 -2 2 2.8890 2.8876 .0014 0 -2 2 2.8550 2.8516 .0034 -1 3 2
A= 8.141 DA= .001 B= 14.328 DB= .001 C= 7.2454 DC= .0007 GAMMA= 78.071 DGAMMA= .004 BETA =112.68 DBETA = .09 ALPHA= 89.24 DALPHA= .02 V= 758.9
167. 21-0464 Pb12Sb10S27 Triklin
Dexp Dcal d(D) h k l 9.4000 9.3969 .0031 1 0 1 7.6000 7.6022 -.0022 0 1 1 6.8000 6.7893 .0107 -1 1 1 6.2700 6.2685 .0015 2 0 1 6.1300 6.1146 .0154 0 0 2 4.2900 4.2966 -.0066 -3 1 0 4.1700 4.1684 .0016 -1 2 1 4.1200 4.1191 .0009 -3 1 1 4.0700 4.0764 -.0064 0 0 3 4.0000 3.9985 .0015 0 -2 1 3.8800 3.8828 -.0028 0 1 3 3.8200 3.8196 .0004 -2 2 0
A= 14.5264 DA= .0001 B= 8.89031 DB= .00001 C= 12.3191 DC= .0001 GAMMA= 91.6290 DGAMMA= .0001 BETA = 89.6714 DBETA = .0002 ALPHA= 83.10 DALFA= .05 V=1579.1
168. 21-0465 Pb6Sb10S21 Triklin
Dexp Dcal d(D) h k l 4.1100 4.1124 -.0024 -1 1 1 4.0700 4.0705 -.0005 -1 -1 1 4.0100 4.0086 .0014 2 0 0 3.9500 3.9497 .0003 -2 1 0 3.8500 3.8456 .0044 2 2 0 3.7800 3.7785 .0015 -1 3 1 3.6700 3.6677 .0023 0 7 0 3.5600 3.5635 -.0035 1 0 1 3.5100 3.5088 .0012 1 -1 1 3.4700 3.4731 -.0031 1 2 1 3.4300 3.4311 -.0011 -1 -4 1 3.3700 3.3730 -.0030 -2 4 0
A= 8.148 DA= .003 B= 25.700 DB= .005 C= 4.422 DC= .002 GAMMA= 89.43 DGAMMA= .01 BETA =100.27 DBETA = .02 ALPHA= 87.641 DALPHA= .009 V= 910.21
169. 21-0469 PbGa2O5 Rombik Groupa 29,57
Dexp. Dcal. d(D) h k l 6.0000 5.9985 .0015 1 1 1 4.7400 4.7407 -.0007 1 2 1 4.0400 4.0423 -.0023 1 3 0 3.8700 3.8684 .0016 0 2 2 3.7200 3.7181 .0019 1 3 1 3.5800 3.5826 -.0026 1 2 2 3.3500 3.3504 -.0004 0 4 0 3.2500 3.2502 -.0002 0 3 2 3.1600 3.1595 .0005 1 4 0 3.0000 2.9992 .0008 2 2 2 2.9300 2.9300 -.0000 3 1 1 2.7400 2.7401 -.0001 3 2 1
a= 9.497 b=13.401 c= 9.4754 da= .001 db= .002 dc= .0004 V=1206.0
Triklin
Dexp Dcal d(D) h k l 6.0000 6.0012 -.0012 1 0 0 4.7400 4.7415 -.0015 1 1 1 4.0400 4.0386 .0014 0 -2 1 3.8700 3.8698 .0002 1 2 0 3.7200 3.7180 .0020 1 0 2 3.5800 3.5830 -.0030 0 -1 2 3.3500 3.3518 -.0018 2 0 1 3.2500 3.2501 -.0001 1 -2 1 3.1600 3.1618 -.0018 2 1 0 3.0000 3.0006 -.0006 2 0 0 2.9300 2.9302 -.0002 -1 1 1 2.7400 2.7405 -.0005 0 1 2
A= 6.833 DA= .001 B= 8.455 DB= .005 C= 7.750 DC= .001 GAMMA= 78.82 DGAMMA= .09 BETA = 68.07 DBETA = .01 ALPHA=104.73 DALPHA= .03 V= 380.3
170. 21-0470 PbGa2O4 Triklin
Dexp Dcal d(D) h k l 4.6800 4.6813 -.0013 0 1 1 4.5500 4.5591 -.0091 0 -1 1 4.2800 4.2801 -.0001 -1 1 0 4.1300 4.1282 .0018 0 2 1 3.1600 3.1593 .0007 -1 3 1 3.1200 3.1201 -.0001 1 4 0 2.7400 2.7402 -.0002 -1 0 2 2.6900 2.6905 -.0005 1 -1 1 2.6000 2.6005 -.0005 -1 -2 2 2.5600 2.5595 .0005 1 3 1 2.5400 2.5403 -.0003 0 5 1 2.4200 2.4203 -.0003 0 1 2 2.3500 2.3501 -.0001 2 2 0 2.2800 2.2795 .0005 0 -2 2
A= 5.3687 DA= .0003 B= 14.6853 DB= .0009 C= 5.4947 DC= .0007 GAMMA= 81.0054 DGAMMA= .0009 BETA =117.417 DBETA = .007 ALPHA= 91.934 DALPHA= .003 V= 379.5
171. 21-0478 Pb3CrO6 Triklin
Dexp Dcal d(D) h k l 8.1200 8.1278 -.0078 1 0 0 6.1500 6.1446 .0054 -1 0 1 4.7500 4.7524 -.0024 -1 -2 1 4.4800 4.4778 .0022 -1 1 1 4.2000 4.2001 -.0001 -2 -1 1 3.9700 3.9659 .0041 -2 0 1 3.6700 3.6704 -.0004 0 -1 2 3.5700 3.5652 .0048 0 0 2 3.3100 3.3093 .0007 0 -2 2 3.0700 3.0723 -.0023 -2 0 2 3.0400 3.0406 -.0006 -1 1 2 3.0000 3.0010 -.0010 1 -1 2
A= 8.7169 DA= .0005 B= 10.394 DB= .004 C= 7.7674 DC= .0003 GAMMA= 73.90 DGAMMA= .01 BETA =108.01 DBETA = .02 ALPHA=108.94 DALPHA= .01 V= 620.7
172. 21-0479 PbSeO3 Monoklin Grupa 7,13
Dexp Dcal d(D) h k l 5.9100 5.9171 -.0071 0 1 1 3.8800 3.8760 .0040 2 1 1 3.4800 3.4800 .0000 0 3 0 3.2600 3.2601 -.0001 2 2 1 3.2000 3.2024 -.0024 2 0 2 2.9600 2.9586 .0014 0 2 2 2.8300 2.8286 .0014 -1 3 1 2.7700 2.7718 -.0018 -2 2 1 2.7300 2.7297 .0003 2 2 2 2.5000 2.4991 .0009 0 3 2 2.1300 2.1305 -.0005 1 4 2 1.9700 1.9698 .0002 -3 0 2 1.7600 1.7600 .0000 -2 5 1 1.6900 1.6898 .0002 5 0 0
a= 8.784 b= 10.440 c= 7.467 beta=74.11 da=.002 db=.001 dc=.002 dbet=.01 V= 658.6
173. 21-0938 Pb4SbO6 Rombik Groupa 29,57
Dexp. Dcal. d(D) h k l 3.2200 3.2266 -.0066 0 2 2 3.1700 3.1794 -.0094 0 3 0 2.8400 2.8380 .0020 1 1 1 2.2400 2.2413 -.0013 1 3 0 1.8600 1.8600 -.0000 1 4 1 1.7500 1.7491 .0009 0 5 2 1.5800 1.5800 .0000 2 0 0
a= 3.15994 b= 9.538 c= 8.76 da= .00005 db= .002 dc= .02 v= 264.1
174. 21-0939 PbSb2O5 Rombik Groupa 29,57
Dexp. Dcal. d(D) h k l 3.2100 3.2092 .0008 0 3 0 3.0200 3.0246 -.0046 2 1 0 2.6600 2.6567 .0033 2 2 0 1.9270 1.9255 .0015 0 5 0 1.8430 1.8432 -.0002 1 5 0 1.6550 1.6559 -.0009 1 5 1 1.6000 1.5998 .0002 2 1 2
a= 6.372 b= 9.628 c= 3.7702 da= .006 db= .002 dc= .0008 V= 231.3
175. 21-0941 Pb5Sb4O11 Monoklin Grupa 4,11
Dexp Dcal d(D) h k l 7.9400 7.9182 .0218 1 0 1 3.2100 3.2111 -.0011 -1 1 1 3.1700 3.1709 -.0009 3 0 0 2.8400 2.8412 -.0012 2 1 1 2.6300 2.6305 -.0005 1 1 3 2.3500 2.3498 .0002 -3 0 3 2.0300 2.0295 .0005 3 0 5 1.9860 1.9855 .0005 4 1 0 1.9280 1.9280 -.0000 -4 1 1 1.7110 1.7110 .0000 -4 1 3 1.6890 1.6888 .0002 -1 2 2 1.6080 1.6084 -.0004 4 1 5 1.5860 1.5859 .0001 -2 1 6
a= 9.580 b= 3.607 c= 12.0500 beta= 83.173 da=.001 db= .002 dc=.0001 Dbeta= .0o9 V= 413.4
176. 21-0943 Pb8As2O13 Triklin
Dexp Dcal d(D) h k l 7.1500 7.1453 .0047 1 1 0 6.8500 6.8549 -.0049 1 0 1 3.6800 3.6809 -.0009 1 -2 1 3.1700 3.1718 -.0018 0 -2 2 3.0900 3.0918 -.0018 1 -2 2 2.8700 2.8709 -.0009 3 1 0 2.6800 2.6805 -.0005 2 -2 2 2.5900 2.5907 -.0007 0 -3 2 2.4600 2.4596 .0004 -1 -3 2 2.4000 2.3989 .0011 1 -2 3 2.3500 2.3497 .0003 0 -2 3 2.3000 2.3003 -.0003 -3 0 1
A= 9.13364 DA= .00000 B= 9.3282 DB= .0008 C= 7.8596 DC= .0001 GAMMA= 77.095 DGAMMA= .008 BETA = 70.612 DBETA = .001 ALPHA= 97.696 DALPHA= .004 V=599.9
177. 21-0944 Pb3As2O8 Triklin
Dexp Dcal d(D) h k l 4.8700 4.8714 -.0014 0 1 2 3.5700 3.5678 .0022 1 -1 3 3.4000 3.4012 -.0012 2 0 1 3.1500 3.1506 -.0006 -2 0 1 3.0900 3.0883 .0017 1 -2 2 3.0000 3.0003 -.0003 0 -2 3 2.9100 2.9097 .0003 2 0 3 2.8300 2.8269 .0031 -2 0 2 2.8000 2.8001 -.0001 1 -2 3 2.4900 2.4909 -.0009 2 -2 1 2.2600 2.2601 -.0001 2 0 5 2.1500 2.1495 .0005 1 3 3
A= 6.847 DA= .001 B= 7.7693 DB= .0002 C= 13.381 DC= .001 GAMMA= 86.625 DGAMMA= .007 BETA = 81.06 DBETA = .01 ALPHA= 93.04 DALPHA= .01 V=700.5
178. 21-0946 Pb2CrO5 Triklin
Dexp Dcal d(D) h k l 6.4100 6.3901 .0199 1 1 0 6.0200 6.0326 -.0126 0 1 1 4.4500 4.4714 -.0214 -1 -2 1 3.7800 3.7846 -.0046 1 -2 1 3.5600 3.5584 .0016 0 0 2 3.3900 3.3912 -.0012 -1 -1 2 3.2400 3.2430 -.0030 0 -2 2 2.9900 2.9887 .0013 -2 2 0 2.8800 2.8775 .0025 0 -3 2 2.8500 2.8504 -.0004 -1 -3 2 2.5100 2.5109 -.0009 1 5 0 2.4800 2.4793 .0007 -1 -5 1
A= 7.1319 DA= .0004 B= 13.149 DB= .003 C= 7.246 DC= .001 GAMMA= 84.541 DGAMMA= .001 BETA = 99.66 DBETA = .01 ALPHA= 95.77 DALPHA= .02 V=663.9
179. 21-0947 Pb5CrO8 Triklin
Dexp Dcal d(D) h k l 8.3100 8.3061 .0039 1 0 0 7.4900 7.4714 .0186 0 1 0 6.3200 6.2624 .0576 0 0 1 5.8500 5.8537 -.0037 -1 0 1 5.5400 5.5420 -.0020 1 -1 0 5.2100 5.1992 .0108 -1 -1 1 4.3300 4.3287 .0013 0 1 1 3.6200 3.6228 -.0028 -2 1 0 3.2500 3.2466 .0034 -1 0 2 3.1600 3.1623 -.0023 0 -1 2 3.1200 3.1181 .0019 1 -2 1 2.9200 2.9227 -.0027 0 2 1
A= 8.680 DA= .001 B= 7.7044 DB= .0003 C= 6.7290 DC= .0005 GAMMA= 85.698 DGAMMA= .004 BETA =106.8776 DBETA = .0003 ALPHA=104.1320 DALPHA= .0009 V=417.5
180. 21-0991 K4PbO3 Triklin
Dexp Dcal d(D) h k l 5.4900 5.4920 -.0020 0 1 1 5.3100 5.2985 .0115 0 -1 1 4.7200 4.7234 -.0034 -1 2 0 4.1400 4.1338 .0062 -1 -1 1 3.8400 3.8402 -.0002 1 3 0 3.0700 3.0732 -.0032 0 -4 1 2.9640 2.9659 -.0019 2 -1 0 2.8660 2.8657 .0003 0 1 2 2.7710 2.7713 -.0003 -2 0 1 2.6470 2.6492 -.0022 0 -2 2 2.5490 2.5468 .0022 2 -1 1 2.4940 2.4931 .0009 -1 -2 2
A= 6.063 DA= .006 B= 15.03 DB= .01 C= 5.806 DC= .003 GAMMA= 90.67 DGAMMA= .09 BETA = 94.69 DBETA = .09 ALPHA= 86.90 DALPHA= .05 V= 526.
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