1. 48-0783
K8Ni{H2O}CuW11O39*12H2O
Triklin
Dexp Dcal d(D) h k l
11.2401 11.2258 .0143 1 0 0
10.7477 10.7445 .0032 0 1 0
10.4436 10.4543 -.0108 0 0 1
9.9722 9.9521 .0201 -1 1 0
7.5964 7.5896 .0067 -1 0 1
7.1437 7.1347 .0090 -1 1 1
5.2293 5.2272 .0021 0 0 2
4.7924 4.7918 .0006 0 -2 1
3.5673 3.5673 -.0000 -2 2 2
3.0862 3.0862 .0000 1 1 3
2.9682 2.9683 -.0001 -1 2 3
2.9392 2.9394 -.0002 -2 0 3
2.6742 2.6742 -.0001 3 -4 1
2.5932 2.5932 .0000 2 3 0
A= 12.205 DA= .002
B= 11.681 DB= .001
C= 10.4568 DC= .0007
GAMMA=113.102 DGAMMA= .003
BETA = 88.8306 DBETA = .0003
ALPHA= 90.833 DALPHA= .001
V= 1371.0
2. 48-0869
Li2Ni{SO4}2
Triklin
Dexp Dcal d(D) h k l
5.8175 5.8100 .0074 1 1 0
5.4422 5.4451 -.0028 -2 1 0
5.1364 5.1247 .0117 0 1 2
4.9584 4.9634 -.0050 0 2 0
4.6573 4.6593 -.0020 -2 2 0
4.5513 4.5450 .0063 2 0 2
4.2643 4.2608 .0035 0 -2 2
4.2264 4.2290 -.0026 -2 0 1
3.7793 3.7812 -.0018 2 1 0
3.4953 3.4950 .0003 -2 0 2
3.1862 3.1844 .0018 3 -3 3
3.0292 3.0300 -.0008 3 0 3
A= 11.758 DA= .003
B= 11.604 DB= .008
C= 14.227 DC= .001
GAMMA=120.172 DGAMMA= .006
BETA = 68.10 DBETA = .02
ALPHA=107.701 DALPHA= .002
V=1539.5
3. 48-0879
Ni2Mo{NH3}12{CN}8*3H2O
Triklin
Dexp Dcal d(D) h k l
7.8107 7.8244 -.0136 0 2 1
6.6005 6.5843 .0161 1 1 0
5.7905 5.8046 -.0140 -1 1 1
5.1704 5.1666 .0038 1 -1 1
4.8694 4.8748 -.0055 -1 3 0
4.5113 4.5119 -.0007 1 3 1
4.2023 4.2011 .0012 -1 -1 2
3.7232 3.7239 -.0006 1 5 0
3.5512 3.5496 .0017 -1 5 1
3.2232 3.2231 .0001 -2 2 0
2.7072 2.7104 -.0032 0 8 0
2.5832 2.5833 -.0001 2 -2 2
A= 6.872 DA= .001
B= 21.787 DB= .003
C= 10.358 DC= .004
GAMMA= 88.4421 DGAMMA= .0007
BETA = 95.975 DBETA = .006
ALPHA= 84.85 DALPHA= .04
V=1534
4. 48-1269
In22Ni57P21
Triklin
Dexp Dcal d(D) h k l
3.5563 3.5585 -.0022 2 0 1
2.9562 2.9544 .0018 1 2 1
2.8522 2.8501 .0021 0 2 1
2.7322 2.7342 -.0020 -1 2 0
2.6942 2.6914 .0028 -2 0 1
2.5802 2.5805 -.0003 3 0 1
2.3522 2.3507 .0014 1 -2 1
2.2562 2.2570 -.0008 -2 2 0
2.1322 2.1317 .0005 0 2 2
2.0851 2.0853 -.0001 1 3 1
2.0441 2.0464 -.0023 -3 0 1
2.0242 2.0245 -.0003 0 3 1
A= 8.0935 DA= .0003
B= 6.3598 DB= .0006
C= 5.359 DC= .001
GAMMA= 79.20 DGAMMA= .01
BETA = 71.838 DBETA = .005
ALPHA= 77.38 DALPHA= .01
V=253.8
5. 48-1466
Al10Mn3Ni
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.0604 5.0710 -.0106 1 0 1
3.9153 3.9199 -.0046 2 0 0
3.3203 3.3253 -.0050 0 1 1
3.0563 3.0613 -.0050 1 1 1
2.4302 2.4322 -.0020 3 0 1
2.3921 2.3935 -.0013 1 1 2
2.2152 2.2165 -.0013 0 0 3
2.1322 2.1329 -.0007 1 0 3
2.1151 2.1159 -.0007 2 1 2
2.0542 2.0547 -.0005 3 1 1
1.9601 1.9599 .0002 4 0 0
1.9191 1.9200 -.0008 0 2 0
a= 7.840 b= 3.840 c= 6.649
da= .001 db= .001 dc= .001
v= 200.1
6. 48-1943
C30H14N4NiO4*2H2O
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
12.9236 12.9125 .0112 1 0 0
7.4373 7.4338 .0035 -1 1 1
5.3403 5.3404 -.0001 -1 1 2
4.5752 4.5762 -.0010 -2 1 2
3.6482 3.6479 .0003 -2 1 3
3.3023 3.3023 -.0000 0 2 3
a= 13.212 b= 11.04 c= 12.65 beta= 102.22
da=.008 db=.01 dc=.02 dbet=.02
V= 1803
7. 48-1973
C42H34Cl2N6NiO6
Triklin
Dexp Dcal d(D) h k l
11.6052 11.5874 .0179 1 0 0
5.7026 5.7069 -.0043 -2 1 0
5.0021 4.9949 .0071 1 0 1
4.6021 4.5977 .0044 0 2 0
4.3019 4.2999 .0021 1 1 1
4.0018 4.0004 .0014 -3 1 0
3.6015 3.6015 .0000 -3 0 1
3.5015 3.5008 .0007 -3 2 0
3.3014 3.3015 -.0000 1 2 1
3.2014 3.2023 -.0009 -1 3 0
3.1014 3.1017 -.0003 -1 1 2
3.0013 3.0022 -.0009 3 0 1
A= 12.4650 DA= .0003
B= 9.7351 DB= .0003
C= 6.2915 DC= .0001
GAMMA=108.466 DGAMMA= .001
BETA =103.7061 DBETA = .0006
ALPHA= 80.827 DALPHA= .005
V=700.7
8. 48-2192
C10H20N2NiO4S2*H2O
Triklin
Dexp Dcal d(D) h k l
15.2384 15.2418 -.0034 1 0 0
7.6296 7.6332 -.0035 1 1 0
5.0998 5.0806 .0192 3 0 0
4.7696 4.7838 -.0142 0 -1 1
4.5996 4.6008 -.0012 -3 1 0
4.3097 4.3122 -.0025 3 1 0
4.1798 4.1865 -.0067 0 1 1
3.9198 3.9232 -.0034 3 0 1
3.8297 3.8292 .0006 2 1 1
3.7498 3.7439 .0060 -2 -1 1
3.6197 3.6206 -.0009 -4 1 0
3.2898 3.2906 -.0008 3 2 0
A= 15.525 DA= .009
B= 9.384 DB= .004
C= 5.233 DC= .001
GAMMA= 95.99 DGAMMA= .03
BETA = 79.95 DBETA = .02
ALPHA= 99.89 DALPHA= .07
V= 737.5
9. 48-2249
C12H25N4O4*NiCl2*2H2O
Triklin
Dexp Dcal d(D) h k l
9.3406 9.3322 .0084 1 0 0
8.0205 8.0258 -.0053 0 1 0
7.6303 7.6226 .0077 -1 0 1
6.1906 6.1905 .0001 -1 1 0
5.9803 5.9777 .0026 1 1 1
5.4506 5.4532 -.0026 -1 -1 1
4.6503 4.6469 .0034 1 0 4
4.2704 4.2692 .0012 2 0 3
3.9903 3.9896 .0007 1 1 4
3.9203 3.9216 -.0012 0 2 1
3.8203 3.8206 -.0003 2 -1 3
3.6403 3.6396 .0007 1 2 1
A= 9.636 DA= .007
B= 8.031 DB= .002
C= 19.206 DC= .001
GAMMA= 92.05 DGAMMA= .03
BETA = 75.71 DBETA = .04
ALPHA= 90.59 DALPHA= .01
V=1441
10. 48-2250
C12H28N4*Ni{NO3}2*2H2O
Triklin
Dexp Dcal d(D) h k l
9.3811 9.3978 -.0167 1 0 0
8.7102 8.7500 -.0398 0 1 0
8.1907 8.1650 .0257 0 1 1
7.9909 8.0537 -.0629 -1 0 1
7.5008 7.4972 .0036 1 0 1
6.7607 6.7907 -.0300 0 -1 1
6.4002 6.3932 .0070 1 1 0
6.3006 6.3178 -.0172 -1 1 1
6.0403 6.0300 .0102 0 1 2
5.7903 5.7663 .0239 -1 0 2
5.2302 5.2437 -.0135 -1 1 2
4.6904 4.6989 -.0085 2 0 0
A= 9.4274 DA= .0008
B= 8.934 DB= .001
C= 14.091 DC= .001
GAMMA= 91.111 DGAMMA= .002
BETA = 94.5405 DBETA = .0004
ALPHA= 78.3463 DALPHA= .0001
V=1157.8
11. 48-2446
C32H16N8Ni*Bi2Sr2CaCu2Ox
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
11.6805 11.6652 .0152 1 0 0
7.6805 7.6901 -.0097 1 0 1
3.8503 3.8451 .0052 2 0 2
3.2702 3.2722 -.0020 1 0 3
2.6702 2.6696 .0006 0 1 2
2.3702 2.3718 -.0016 3 1 1
2.0901 2.0887 .0014 4 1 1
1.8701 1.8706 -.0005 5 1 0
a=11.665 b= 3.130 c=10.227
da= .007 db= .001 dc= .001
V=373.4
12. 48-2447
C32H16N8Ni*Bi2Sr2CaCu2Ox
Triklin
Dexp Dcal d(D) h k l
7.5103 7.5081 .0022 1 0 0
3.9203 3.9207 -.0003 0 2 1
3.4803 3.4805 -.0003 -2 0 1
3.3703 3.3704 -.0001 1 2 0
3.2702 3.2687 .0015 2 1 1
2.9002 2.9032 -.0029 0 -2 1
2.8002 2.7978 .0024 -2 0 2
2.6702 2.6698 .0005 -2 2 1
2.4402 2.4418 -.0016 -1 3 1
2.3602 2.3605 -.0004 1 3 0
2.2601 2.2595 .0006 0 -2 2
2.0802 2.0800 .0002 -3 2 1
A= 7.5355 DA= .0003
B= 7.890 DB= .003
C= 8.342 DC= .005
GAMMA= 87.73 DGAMMA= .01
BETA = 93.17 DBETA = .04
ALPHA= 68.03 Dalfa= .02
V= 458.2
13. 49-0669
K2NiP2O7*4H2O
Triklin
Dexp Dcal d(D) h k l
8.9502 8.9474 .0028 1 0 0
7.3404 7.3315 .0089 0 1 0
6.1404 6.1484 -.0080 -1 0 1
5.6506 5.6413 .0093 1 1 0
5.2605 5.2517 .0089 -1 -1 1
4.4803 4.4737 .0066 2 0 0
4.3503 4.3457 .0046 1 0 2
3.9202 3.9206 -.0004 2 -1 1
3.6602 3.6658 -.0056 0 2 0
3.4402 3.4377 .0025 2 1 1
3.1703 3.1664 .0039 -1 1 2
3.1203 3.1223 -.0020 0 0 3
A= 9.009 DA= .008
B= 7.729 DB= .003
C= 9.93 DC= .01
GAMMA= 92.70 DGAMMA= .01
BETA = 83.30 DBETA = .09
ALPHA=108.45 DALPHA= .02
V= 651.5
14. 49-0671
K2Ni7{P2O7}4*24H2O
Triklin
Dexp Dcal d(D) h k l
6.3206 6.3295 -.0089 -1 1 1
6.2003 6.1891 .0111 -1 -1 1
5.5105 5.5072 .0033 -1 0 2
4.7005 4.7005 -.0000 1 1 1
3.6403 3.6430 -.0027 -1 -2 2
3.4303 3.4291 .0012 -1 2 2
3.4003 3.3970 .0033 -1 1 3
3.2503 3.2488 .0015 -2 -1 3
3.0702 3.0678 .0024 0 3 0
3.0403 3.0404 -.0001 1 -1 3
2.9703 2.9688 .0014 1 -3 1
2.8502 2.8500 .0002 -1 0 4
A= 9.846 DA= .006
B= 9.364 DB= .003
C= 11.473 DC= .004
GAMMA= 96.341 DGAMMA= .001
BETA =108.212 DBETA = .008
ALPHA= 96.08 DALPHA= .02
V=987.5
15. 49-0672
Ni2P2O7*8H2O
Triklin
Dexp Dcal d(D) h k l
13.5816 13.5740 .0076 0 0 1
7.0306 7.0332 -.0026 1 1 0
6.3905 6.3844 .0061 0 -2 1
6.0203 6.0243 -.0040 -1 1 0
5.6104 5.6136 -.0033 1 2 0
5.3204 5.3218 -.0013 -1 -2 1
5.0203 5.0205 -.0002 0 -2 2
4.8802 4.8823 -.0021 1 0 2
4.7602 4.7544 .0058 0 2 2
4.6403 4.6420 -.0017 -1 2 0
4.4102 4.4107 -.0004 1 -2 1
3.9603 3.9577 .0025 0 -3 2
A= 7.4289 DA= .0003
B= 14.338 DB= .001
C= 13.6087 DC= .0008
GAMMA= 79.039 DGAMMA= .004
BETA = 92.656 DBETA = .009
ALPHA= 93.572 DALPHA= .007
V=1419.8
16. 49-1173
C4H6NiO4*4H2O
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
6.8104 6.7913 .0191 1 1 0
4.7803 4.7826 -.0022 1 2 0
4.1903 4.1760 .0143 2 0 0
3.9683 3.9562 .0121 0 1 2
3.9542 3.9562 -.0020 0 1 2
3.5752 3.5754 -.0001 1 1 2
3.5613 3.5618 -.0005 2 1 1
3.1552 3.1581 -.0029 1 2 2
3.1423 3.1487 -.0064 2 2 1
2.8592 2.8553 .0039 0 3 2
2.7172 2.7080 .0092 3 1 0
2.5142 2.5125 .0016 3 2 0
a= 8.352 b=11.67 c= 8.4106
da= .001 db= .01 dc= .0005
v= 819.6
Triklin
Dexp Dcal d(D) h k l
6.8104 6.7726 .0377 1 0 0
4.7803 4.7768 .0035 1 0 1
4.1903 4.1985 -.0081 0 1 1
3.9683 3.9686 -.0002 0 -1 1
3.9542 3.9514 .0028 -1 1 0
3.5752 3.5725 .0027 2 1 0
3.5613 3.5725 -.0112 2 1 0
3.1552 3.1490 .0062 0 2 0
3.1423 3.1490 -.0067 0 2 0
2.8592 2.8594 -.0003 2 2 1
2.7802 2.7844 -.0042 0 2 1
2.7172 2.7151 .0021 1 0 2
A= 7.557 DA= .003
B= 6.844 DB= .001
C= 5.5735 DC= .0008
GAMMA= 67.18 DGAMMA= .01
BETA = 74.15 DBETA = .02
ALPHA= 81.00 DALPHA= .01
V=255.1
17. 49-1174
C4H6K2O4*C4H6NiO4*4H2O
Triklin
Dexp Dcal d(D) h k l
7.0805 7.0777 .0028 0 1 1
6.7107 6.7099 .0008 0 -1 1
6.1906 6.1878 .0028 -1 0 1
5.7503 5.7511 -.0008 -1 1 1
5.3705 5.3671 .0035 -1 -2 1
4.2504 4.2413 .0090 1 3 1
3.9942 3.9959 -.0017 2 2 0
3.9683 3.9657 .0026 -2 -1 1
3.8242 3.8276 -.0034 -2 -2 1
3.6773 3.6840 -.0067 0 1 2
3.6043 3.6049 -.0006 1 -3 1
3.5752 3.5765 -.0013 0 -1 2
A= 8.424 DA= .003
B= 19.230 DB= .006
C= 7.593 DC= .001
GAMMA= 80.02 DGAMMA= .02
BETA =102.28 DBETA = .04
ALPHA= 87.79 DALPHA= .01
V= 1180
18. 49-1609
{Fe0.51Mo0.46Ni0.03O3}6c
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
2.7802 2.7823 -.0021 0 0 2
2.5502 2.5497 .0005 0 1 2
2.2602 2.2590 .0012 2 2 1
2.1402 2.1375 .0027 2 1 2
1.9601 1.9604 -.0003 4 0 0
1.8501 1.8490 .0011 4 0 1
1.6701 1.6694 .0007 4 2 0
1.5601 1.5604 -.0003 1 4 0
1.4401 1.4403 -.0002 4 3 0
1.3601 1.3598 .0003 3 4 0
1.3101 1.3111 -.0010 2 0 4
1.2801 1.2803 -.0002 6 1 0
a= 7.8417 b= 6.369 c= 5.565
da= .0005 db= .004 dc= .003
V= 277.9
Triklin
Dexp Dcal d(D) h k l
2.7802 2.7809 -.0007 0 1 1
2.5502 2.5495 .0007 -1 1 1
2.2602 2.2608 -.0006 0 -1 1
2.1402 2.1381 .0021 1 1 1
1.9601 1.9610 -.0008 -1 2 1
1.8501 1.8494 .0007 -2 1 1
1.6701 1.6693 .0008 -2 2 1
1.5601 1.5596 .0005 0 0 2
1.4401 1.4394 .0007 -1 0 2
1.3601 1.3602 -.0001 0 3 1
1.3101 1.3107 -.0007 -2 1 2
1.2801 1.2802 -.0002 2 0 2
A= 4.456 DA= .004
B= 4.4504 DB= .0002
C= 3.1926 DC= .0005
GAMMA=109.79 DGAMMA= .02
BETA = 91.55 DBETA = .05
ALPHA= 77.98 DALPHA= .01
V= 58.2
19. 49-1634
NiSnTb
Triklin
Dexp Dcal d(D) h k l
8.3335 8.3272 .0064 1 0 0
6.4320 6.4399 -.0080 -1 1 0
5.6008 5.6028 -.0020 -1 0 1
5.0459 5.0411 .0048 1 1 0
4.5314 4.5447 -.0133 0 0 2
4.2206 4.2172 .0033 -1 -1 1
3.6885 3.6886 -.0001 -1 0 2
3.5747 3.5755 -.0008 1 1 2
3.4841 3.4824 .0017 0 2 1
3.2883 3.2927 -.0044 2 1 1
3.0534 3.0518 .0016 1 0 3
2.9436 2.9434 .0002 0 -2 2
A= 8.781 DA= .001
B= 7.8518 DB= .0003
C= 9.304 DC= .005
GAMMA=104.49 DGAMMA= .01
BETA = 77.73 DBETA = .01
ALPHA= 94.10 DALPHA= .05
V= 606.7
20. 49-1635
NiSnTb
Triklin
Dexp Dcal d(D) h k l
35.4186 35.4671 -.0485 0 0 1
8.7406 8.7234 .0171 1 0 1
7.5286 7.5299 -.0014 0 -1 2
6.2107 6.2153 -.0046 0 -1 4
4.7145 4.7163 -.0018 1 -1 6
4.0546 4.0562 -.0017 -1 -1 6
3.9160 3.9157 .0003 -2 1 4
3.6975 3.6976 -.0001 1 -2 5
3.6175 3.6176 -.0000 0 -2 5
3.5165 3.5166 -.0001 0 2 4
3.2954 3.3021 -.0067 1 1 8
2.9830 2.9828 .0002 1 -2 9
A= 9.3637 DA= .0003
B= 8.3344 DB= .0007
C= 35.632 DC= .001
GAMMA=106.24 DGAMMA= .01
BETA = 88.245 DBETA = .004
ALPHA= 95.5189 DALPHA= .0004
V=2658
21. 49-1668
DyGe2Ni2
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
7.8310 7.8461 -.0151 1 1 0
5.0968 5.0859 .0109 0 2 0
2.5427 2.5430 -.0002 0 4 0
2.0536 2.0548 -.0012 6 0 0
1.8881 1.8880 .0001 0 0 2
1.7618 1.7612 .0006 7 0 0
1.7011 1.7012 -.0001 2 2 2
a=12.329 b=10.172 c= 3.77590
da= .004 db= .008 dc= .00009
v= 473.5
22. 49-1669
Ge2HoNi2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.5638 7.4815 .0823 0 1 0
4.9012 4.9072 -.0060 -1 0 1
2.6907 2.6914 -.0007 1 0 3
2.5220 2.5214 .0005 -1 2 2
2.3326 2.3314 .0012 -2 1 2
2.2222 2.2232 -.0010 -1 3 1
2.1367 2.1370 -.0003 0 0 4
2.0536 2.0548 -.0012 0 1 4
1.9650 1.9654 -.0004 -2 1 3
1.9373 1.9375 -.0002 2 3 1
1.9142 1.9118 .0024 2 2 3
1.8698 1.8704 -.0005 0 4 0
1.7974 1.7981 -.0007 2 1 4
1.7493 1.7490 .0003 -2 3 2
1.6895 1.6890 .0005 1 0 5
1.6503 1.6506 -.0003 -3 2 2
a= 6.401 b= 7.481 c= 8.581 beta= 84.92
da=.004 db=.002 dc=.006 dbet=.06
V= 409.3
23. 49-1670
ErGe2Ni2
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
8.1623 8.1468 .0155 1 0 1
4.8220 4.8633 -.0413 1 0 2
2.5083 2.5081 .0002 5 0 1
2.2434 2.2411 .0022 3 0 4
2.0580 2.0587 -.0007 2 2 1
1.8881 1.8873 .0007 3 0 5
1.8555 1.8553 .0003 1 2 3
1.7493 1.7499 -.0006 0 0 6
1.6809 1.6807 .0002 1 2 4
1.4061 1.4061 -.0000 7 2 1
1.3859 1.3860 -.0001 7 0 5
a=12.915 b= 4.440165 c=10.499
da= .002 db= .000002 dc= .001
V= 602.1
24. 49-1671
Ni2Si2Yb
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
7.5638 7.5792 -.0154 1 0 0
5.0394 5.0351 .0043 1 1 0
2.4815 2.4779 .0036 0 1 3
1.9978 1.9985 -.0008 0 0 4
1.8954 1.8955 -.0001 1 3 2
1.8450 1.8437 .0012 4 0 1
1.7099 1.7099 .0000 2 1 4
1.6585 1.6594 -.0009 4 1 2
a= 7.579 b= 6.7365 c= 7.9941
da= .002 db= .0003 dc= .0002
V= 408.2
25. 49-1947
C14H12N2NiO4*2C2H4O2*2H2O
Triklin
Dexp Dcal d(D) h k l
13.8111 13.6799 .1312 1 0 0
10.2811 10.2942 -.0131 0 1 1
9.1008 9.1364 -.0356 -1 1 1
8.6205 8.6185 .0020 0 -1 1
8.1907 8.2210 -.0303 0 2 0
6.8104 6.8142 -.0038 1 -1 1
5.7105 5.7096 .0009 0 1 2
5.4905 5.4807 .0098 0 3 0
5.3705 5.3718 -.0012 2 0 1
5.0804 5.0814 -.0011 0 -1 2
4.4803 4.4826 -.0023 -1 -3 1
4.3703 4.3763 -.0059 0 3 2
A= 14.02 DA= .01
B= 16.758 DB= .007
C= 11.85401 DC= .004
GAMMA= 92.66 DGAMMA= .06
BETA =102.69 DBETA = .06
ALPHA= 78.86 DALPHA= .03
V=2660
26. 49-1948
C14H12N2NiO4*2H2O
Triklin
Dexp Dcal d(D) h k l
7.6805 7.6816 -.0011 1 1 0
6.2305 6.2285 .0020 0 1 1
5.4506 5.4496 .0009 0 -1 1
4.4703 4.4700 .0003 2 1 0
4.1003 4.1033 -.0030 1 0 2
3.6403 3.6399 .0004 0 1 2
3.3503 3.3498 .0005 2 3 1
3.3002 3.2994 .0009 1 -2 1
2.8102 2.8100 .0001 2 2 3
2.5701 2.5701 .0001 4 2 2
2.2101 2.2102 -.0001 3 4 3
2.1002 2.1002 -.0001 -3 2 0
2.0601 2.0601 .0000 3 -2 2
A= 10.3620 DA= .0003
B= 10.356 DB= .001
C= 8.684 DC= .001
GAMMA= 63.594 DGAMMA= .005
BETA = 60.366 DBETA = .007
ALPHA= 71.01 DALPHA= .01
V= 718.7
27. 49-1995
C2H12N2NiO8S2*6H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
9.2057 9.1868 .0190 0 0 1
6.4583 6.4323 .0260 2 1 0
6.2322 6.1985 .0337 1 1 1
5.2732 5.2691 .0040 2 1 1
4.5954 4.5934 .0020 0 0 2
4.4360 4.4400 -.0040 1 0 2
4.1299 4.1320 -.0021 1 2 1
3.6899 3.6919 -.0020 3 2 0
3.1511 3.1516 -.0005 4 0 2
3.0356 3.0355 .0001 4 2 1
a=17.33 b= 9.601 c= 9.1868
da= .01 db= .001 dc= .0007
V=1528
28. 49-2037
C14H16Cl2N4NiO4
Triklin
Dexp Dcal d(D) h k l
8.3073 8.3073 .0000 1 0 0
6.8104 6.8157 -.0053 1 1 0
5.9459 5.9467 -.0008 1 1 1
5.7318 5.7254 .0064 -1 1 1
4.5432 4.5426 .0006 0 1 2
4.1911 4.1931 -.0020 0 0 2
3.9692 3.9694 -.0002 1 1 2
3.6541 3.6528 .0014 0 3 1
3.4246 3.4221 .0025 2 2 1
3.2564 3.2568 -.0004 1 3 0
3.1482 3.1494 -.0011 -2 2 1
3.0392 3.0384 .0007 -2 0 2
2.8713 2.8706 .0008 2 0 2
2.7953 2.7954 -.0001 0 0 3
2.6751 2.6751 .0000 -3 0 1
A= 8.364 DA= .001
B= 11.0166 DB= .0009
C= 9.091 DC= .004
GAMMA= 84.190 DGAMMA= .009
BETA = 90.777 DBETA = .008
ALPHA= 67.52 DALPHA= .02
V= 768.7
29. 49-2052
C10H30Cl2N6NiO8
Triklin
Dexp Dcal d(D) h k l
7.8907 7.8845 .0062 1 0 0
7.0703 7.0668 .0035 1 1 0
6.7007 6.7009 -.0001 -1 0 1
5.2805 5.2653 .0151 0 1 1
4.5704 4.5635 .0069 -1 1 0
4.4803 4.4808 -.0005 -1 0 2
3.9603 3.9617 -.0015 -1 -2 2
3.8503 3.8491 .0012 0 -2 1
3.5302 3.5299 .0003 -1 -1 3
3.4503 3.4503 .0000 2 0 1
2.8502 2.8506 -.0004 0 -2 3
2.6602 2.6598 .0004 1 2 2
A= 9.1395 DA= .0003
B= 8.855 DB= .002
C= 10.61519 DC= .00001
GAMMA= 61.12 DGAMMA= .03
BETA =108.8 DBETA = .1
ALPHA=112.27 DALPHA= .09
V= 685.9
30. 49-2053
C10H30Cl2N6NiO8
Triklin
Dexp Dcal d(D) h k l
7.4903 7.4640 .0263 0 1 1
7.0703 7.0694 .0009 0 -1 1
6.3603 6.3667 -.0064 -1 0 1
5.9006 5.9111 -.0105 0 -1 2
5.7103 5.7094 .0009 1 -1 1
5.3704 5.3674 .0030 -1 0 2
5.2705 5.2628 .0076 0 1 3
4.9803 4.9734 .0069 0 0 4
4.8403 4.8401 .0002 1 1 0
4.4803 4.4808 -.0005 -1 0 3
4.3503 4.3535 -.0032 0 1 4
4.0903 4.0901 .0002 -1 -1 2
A= 7.348 DA= .001
B= 7.938 DB= .002
C= 20.229 DC= .003
GAMMA= 99.87 DGAMMA= .01
BETA = 80.61 DBETA = .01
ALPHA= 87.16 DALPHA= .02
V=1142.6
31. 49-2119
C58H40N2NiO6
Triklin
Dexp Dcal d(D) h k l
8.7506 8.7549 -.0043 1 0 0
8.5710 8.4978 .0731 -1 1 0
7.5004 7.5011 -.0006 -1 0 1
6.6403 6.6289 .0114 0 1 1
6.4304 6.4462 -.0157 0 0 2
6.0305 6.0203 .0102 0 -1 2
5.6305 5.6180 .0125 1 -1 2
5.0204 5.0193 .0012 1 0 2
4.6303 4.6350 -.0047 0 -2 1
4.1303 4.1292 .0012 1 -1 3
3.8603 3.8634 -.0031 2 -2 2
3.8003 3.8023 -.0020 -2 1 2
A= 9.842 DA= .002
B= 10.442 DB= .002
C= 13.35 DC= .01
GAMMA=116.892 DGAMMA= .009
BETA = 87.117 DBETA = .003
ALPHA=104.52 DALPHA= .04
V= 1181.7
32. 49-2121
C44H30N2NiO4
Triklin
Dexp Dcal d(D) h k l
13.1612 13.1620 -.0008 0 0 1
11.5012 11.5181 -.0169 1 0 0
7.3804 7.3743 .0062 0 1 1
6.5904 6.5909 -.0005 0 -1 1
5.4305 5.4251 .0054 1 -1 1
4.8704 4.8707 -.0003 -1 1 2
4.0803 4.0822 -.0019 2 -1 1
3.7002 3.6999 .0004 -1 2 1
3.4502 3.4549 -.0047 1 -2 1
3.3703 3.3696 .0006 -2 -2 1
3.2302 3.2294 .0008 2 2 2
2.9502 2.9517 -.0015 3 2 1
A= 11.621 DA= .005
B= 8.3087 DB= .0009
C= 13.2764 DC= .0004
GAMMA= 83.064 DGAMMA= .001
BETA = 92.316 DBETA = .007
ALPHA= 83.182 DALPHA= .007
V= 1262
33. 49-2214
C30H24Br4N6NiZn*2H2O
Triklin
Dexp Dcal d(D) h k l
7.6507 7.6256 .0250 0 1 1
6.9607 6.9694 -.0087 0 -1 1
6.7356 6.7362 -.0006 1 1 0
6.2602 6.2745 -.0143 -1 1 0
5.8804 5.8991 -.0187 0 -2 1
5.4506 5.4607 -.0102 -1 2 0
5.2104 5.2087 .0017 1 0 1
4.8903 4.8855 .0048 -1 1 1
4.7403 4.7469 -.0066 0 4 1
4.5504 4.5485 .0019 -1 2 1
4.3804 4.3762 .0042 1 -2 1
4.3163 4.3121 .0042 0 5 0
A= 6.8727 DA= .0005
B= 21.96599 DB= .00006
C= 7.81957 DC= .00001
GAMMA= 82.52 DGAMMA= .01
BETA = 86.762 DBETA = .006
ALPHA= 81.542 DALPHA= .004
V=1157.6
34. 49-2325
C5H5Cl2NNiO*H2O
Geksagon
Groupa 143
Dexp. Dcal. d(D) h k l
8.9929 8.9494 .0436 1 0 1
6.7124 6.6641 .0482 1 1 0
6.0506 6.0383 .0123 1 0 2
4.8723 4.8543 .0180 1 1 2
4.4794 4.4747 .0047 2 0 2
3.3872 3.3867 .0005 1 0 4
3.1203 3.1227 -.0024 3 1 1
3.0162 3.0153 .0010 2 2 2
2.5201 2.5188 .0013 4 1 0
2.3722 2.3733 -.0011 4 1 2
2.0251 2.0243 .0008 0 0 7
2.0101 2.0102 -.0000 3 3 3
a= 13.33 c= 14.17
da=.02 dc= .01
V=2180
35. 50-0043
{NH3}4{Ni,Mn}S2O6*2H2O
Triklin
Dexp Dcal d(D) h k l
5.9135 5.9161 -.0026 1 0 0
5.3005 5.2910 .0095 0 1 1
3.9283 3.9260 .0023 0 -1 1
3.4582 3.4560 .0022 -1 0 1
3.1382 3.1377 .0005 1 0 2
2.9242 2.9226 .0016 2 1 2
2.7152 2.7160 -.0008 2 2 2
2.5292 2.5296 -.0004 1 -1 2
2.2272 2.2269 .0003 3 1 1
2.1821 2.1824 -.0003 2 2 3
1.9071 1.9071 .0001 0 0 3
1.6631 1.6632 -.0001 3 4 2
1.5421 1.5421 .0000 1 5 2
1.4831 1.4831 -.0000 4 -1 2
A= 6.784 DA= .002
B= 7.769 DB= .003
C= 6.819 DC= .004
GAMMA= 73.57 DGAMMA= .07
BETA = 61.48 DBETA = .03
ALPHA= 67.35 DALPHA= .08
V= 289.2
36. 50-0424
{Na0.72H0.28}1.00{Mg1.58Ni1.19}2.77Ge3.79O10{OH}2.28
Geksagon
Groupa 186,190.194
Dexp. Dcal. d(D) h k l
9.8208 9.7810 .0398 0 0 1
4.9403 4.9593 -.0190 1 0 1
3.2602 3.2603 -.0001 0 0 3
2.4801 2.4796 .0005 2 0 2
1.9871 1.9871 .0000 2 1 2
a= 6.64 c= 9.78
da=.01 dc=.02
V= 373.