1. 38-0309
Ag3Ni6{PO4}5
Triklin
Dexp Dcal d(D) h k l
5.5805 5.5774 .0031 2 1 0
4.6703 4.6762 -.0059 1 1 1
4.5804 4.5857 -.0053 -1 -1 1
4.2504 4.2511 -.0007 3 1 0
3.7053 3.7036 .0016 3 1 1
3.3362 3.3358 .0005 0 -2 1
3.2922 3.2959 -.0037 -3 -1 1
3.1272 3.1265 .0007 4 1 1
3.0372 3.0348 .0024 0 0 2
2.9588 2.9570 .0018 -4 1 0
2.8555 2.8570 -.0015 -1 0 2
2.7752 2.7746 .0006 -1 -1 2
A= 14.18 DA= .01
B= 7.698 DB= .002
C= 6.1795 DC= .0002
GAMMA= 81.15 DGAMMA= .02
BETA = 80.16 DBETA = .02
ALPHA= 92.89 DALPHA= .03
V=654.6
2. 38-0519
CsFe0.5Ni0.5Cl3*2H2O
Triklin
Dexp Dcal d(D) h k l
5.6305 5.6306 -.0001 -1 1 1
4.8104 4.8113 -.0009 0 -1 1
4.6804 4.6846 -.0042 1 -1 1
4.4902 4.4991 -.0089 1 1 0
4.2504 4.2506 -.0002 -2 1 0
3.9003 3.9121 -.0118 -1 -1 1
3.7203 3.7154 .0049 2 -1 1
3.5603 3.5597 .0006 0 -1 2
3.1603 3.1579 .0024 2 1 1
2.9902 2.9882 .0021 -2 -1 1
2.8402 2.8418 -.0015 3 -1 1
2.7702 2.7687 .0015 0 -2 1
A= 9.449 DA= .002
B= 6.5186 DB= .0008
C= 10.410 DC= .001
GAMMA=107.04 DGAMMA= .03
BETA = 94.64 DBETA = .03
ALPHA= 77.340 DALPHA= .007
V=598.1
3. 38-0590
NO2Ni{ClO4}3
Triklin
Dexp Dcal d(D) h k l
6.2706 6.2773 -.0067 1 0 2
4.4303 4.4396 -.0094 0 1 0
4.0002 4.0082 -.0080 1 1 1
3.9603 3.9502 .0100 0 -1 2
3.6503 3.6535 -.0032 1 0 4
3.6103 3.6120 -.0017 -1 0 4
3.3803 3.3865 -.0063 -3 0 1
3.1502 3.1570 -.0068 -3 0 2
2.8702 2.8653 .0050 -3 0 3
2.8402 2.8401 .0002 0 1 4
2.8102 2.8111 -.0009 -3 -1 1
2.5802 2.5827 -.0025 0 0 6
A= 10.483 DA= .009
B= 4.45920 DB= .00006
C= 15.523 DC= .003
GAMMA= 85.740 DGAMMA= .009
BETA = 89.24 DBETA = .04
ALPHA= 93.20 DALPHA= .06
V=719.8
4. 38-0591
NiClO4
Triklin
Dexp Dcal d(D) h k l
7.3905 7.3898 .0007 1 0 0
4.0703 4.0674 .0029 -1 1 1
3.5803 3.5815 -.0012 1 -1 1
3.3602 3.3604 -.0002 0 2 1
2.4402 2.4398 .0003 1 1 2
2.3802 2.3796 .0006 2 3 0
2.3502 2.3500 .0001 0 2 2
2.2702 2.2706 -.0004 -3 1 0
2.0301 2.0303 -.0002 -3 0 2
1.9902 1.9900 .0002 -3 2 0
1.7001 1.7001 .0000 0 -2 3
1.4401 1.4402 -.0001 4 0 2
1.4301 1.4302 -.0001 -2 5 0
1.3701 1.3701 .0000 -2 1 4
1.3501 1.3500 .0001 4 -3 1
A= 7.575 DA= .001
B= 8.339 DB= .001
C= 5.7251 DC= .0004
GAMMA= 81.619 DGAMMA= .001
BETA = 99.50 DBETA = .01
ALPHA= 90.34 DALPHA= .01
V= 352.8
5. 38-0714
Ni2{OH}2CO3*4H2O
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
9.0582 9.0488 .0094 -1 0 1
5.9831 5.9908 -.0077 1 1 0
5.1554 5.1522 .0032 0 0 2
3.4338 3.4348 -.0010 0 0 3
3.0873 3.0879 -.0006 3 1 0
2.7107 2.7105 .0002 -4 0 1
2.5296 2.5297 -.0001 -3 2 2
1.8931 1.8932 -.0000 1 3 3
1.5437 1.5438 -.0001 5 2 2
1.4751 1.4752 -.0001 2 0 6
a= 10.919 b= 7.405 c= 11.0392 beta= 111.017
da=.001 db=.001 dc= .0003 dbet= .001
V= 833.2
6. 38-935
Ni3SnTe5
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
6.2318 6.2318 .0000 0 1 0
5.3216 5.3086 .0129 1 0 1
3.1581 3.1642 -.0061 3 0 0
2.8384 2.8368 .0016 3 0 1
2.6535 2.6543 -.0008 2 0 2
2.2263 2.2252 .0011 4 0 1
1.9467 1.9467 -.0001 2 0 3
1.8201 1.8202 -.0001 5 0 1
a= 9.4925 b= 6.2318 c= 6.4036
da= .0007 db= .0001 dc= .0006
V=378.81
7. 38-1501
C14H12N2NiS4
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
11.0507 11.0625 -.0118 1 0 0
6.8005 6.7981 .0024 0 1 1
6.3203 6.3198 .0004 1 1 0
5.5303 5.5313 -.0010 2 0 0
4.4303 4.4301 .0002 -2 0 2
2.7102 2.7100 .0002 0 1 5
2.4902 2.4897 .0005 3 2 2
a= 11.0640 b= 7.700 c= 14.478 beta= 90.933
da=.0004 db=.001 dc=.001 dbet=.002
V= 1233
8. 38-1502
C66H60N2NiP4S4
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
9.8208 9.8076 .0132 1 1 0
7.3707 7.3814 -.0107 1 1 1
6.3203 6.3264 -.0062 1 2 0
5.5303 5.5320 -.0017 2 1 1
4.6704 4.6727 -.0023 0 1 2
4.4303 4.4271 .0032 -1 0 2
4.2303 4.2301 .0003 -1 1 2
4.0403 4.0367 .0036 1 2 2
a= 13.600 b= 14.340 c= 10.000 beta= 81.293
da= .001 db=.001 dc=.001 dbet=.004
V= 1927.8
9. 38-1989
C22H22Cl2CuNiO14*2H2O
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
5.3705 5.3770 -.0065 2 1 0
4.7204 4.7139 .0065 2 1 1
4.5203 4.5220 -.0017 0 0 3
4.0902 4.0878 .0024 0 2 1
3.8803 3.8841 -.0038 2 1 2
3.6303 3.6310 -.0007 -2 2 1
3.3703 3.3711 -.0008 -2 0 4
3.1302 3.1289 .0013 1 0 4
2.9302 2.9291 .0011 -4 1 3
2.7502 2.7509 -.0007 3 1 3
2.5102 2.5104 -.0002 -3 2 4
2.3902 2.3897 .0005 2 3 2
2.1402 2.1402 .0000 -5 1 5
2.0702 2.0700 .0002 -4 1 6
2.0002 2.0001 .0001 -6 0 5
a= 14.198 b=8.574 c= 13.951 beta= 103.484
da=.001 db=.001 dc=.001 dbet=.002
V= 1651.4
Triklin
Dexp Dcal d(D) h k l
5.3705 5.3791 -.0086 0 1 0
4.7204 4.7184 .0020 0 -1 2
4.5203 4.5152 .0051 1 0 0
4.0902 4.0889 .0013 1 0 2
3.8803 3.8783 .0020 -1 0 2
3.6303 3.6330 -.0027 1 0 3
3.3703 3.3690 .0013 0 0 5
3.1302 3.1290 .0012 1 1 0
2.9302 2.9281 .0021 1 1 2
2.7502 2.7523 -.0020 0 1 5
2.5102 2.5099 .0003 0 -2 3
2.3902 2.3894 .0008 -1 2 2
2.1402 2.1407 -.0005 -2 1 2
2.0702 2.0698 .0003 -1 0 7
2.0002 2.0006 -.0005 -1 -2 3
A= 4.651 DA= .001
B= 5.549 DB= .001
C= 16.967 DC= .007
GAMMA=103.401 DGAMMA= .006
BETA = 85.13 DBETA = .02
ALPHA= 95.85 DALPHA= .01
V= 422.9
10. 38-1991
C22H22Cl2Ni2O14*4H2O
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
5.3305 5.3226 .0079 0 0 2
4.6404 4.6406 -.0002 -1 1 1
4.3804 4.3699 .0105 2 0 0
4.1503 4.1427 .0076 -2 0 1
3.7402 3.7412 -.0010 -1 1 2
3.3302 3.3315 -.0013 2 1 1
3.1002 3.1020 -.0018 0 2 0
2.9102 2.9132 -.0030 3 0 0
2.7602 2.7625 -.0023 3 0 1
2.5302 2.5295 .0007 2 2 0
2.4502 2.4504 -.0002 2 1 3
2.1802 2.1801 .0001 3 0 3
2.0702 2.0714 -.0012 -4 0 2
2.0201 2.0198 .0003 0 2 4
a= 8.760 b= 6.204000 c= 10.6700 beta= 93.894
da=.001 db=.001 dc= .0003 dbet=.006
V= 578.5
Triklin
Dexp Dcal d(D) h k l
5.3305 5.3283 .0022 1 0 0
4.6404 4.6541 -.0137 0 1 1
4.3804 4.3828 -.0025 0 -1 1
4.1503 4.1492 .0011 -1 2 0
3.7402 3.7397 .0005 1 1 1
3.3302 3.3302 .0000 -1 0 1
3.1002 3.1036 -.0034 -1 -1 1
2.9102 2.9103 -.0001 0 4 0
2.7602 2.7598 .0004 1 3 1
2.5302 2.5302 -.0001 2 0 1
2.4502 2.4500 .0001 1 4 0
2.1802 2.1802 -.0000 1 -2 2
2.0702 2.0702 -.0001 -1 -4 1
2.0201 2.0196 .0006 -1 -1 2
A= 5.4314 DA= .0003
B= 11.730 DB= .001
C= 4.981 DC= .003
GAMMA= 95.19 DGAMMA= .02
BETA = 80.50 DBETA = .01
ALPHA= 86.13 DALPHA= .04
V= 310.6
11. 39-0502
ClO2Ni{ClO4}3
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
6.3004 6.3073 -.0069 0 1 1
4.4703 4.4639 .0064 2 0 2
4.0002 3.9998 .0004 3 0 0
3.8103 3.8101 .0002 2 1 2
3.6103 3.6121 -.0018 0 1 3
3.3803 3.3837 -.0034 1 2 1
3.1703 3.1718 -.0015 2 1 3
2.8402 2.8387 .0015 2 0 4
2.6102 2.6110 -.0008 -3 1 3
2.5902 2.5917 -.0015 4 1 2
2.4402 2.4392 .0010 -3 2 2
2.3201 2.3192 .0009 4 2 0
2.2402 2.2399 .0003 1 3 2
2.1401 2.1399 .0002 -4 2 2
a=12.023 b= 7.313 c= 12.4870 beta= 86.403
da= .001 db=.0013 dc=.0002 dbet=.004
V= 1095.7
Triklin
Dexp Dcal d(D) h k l
6.3004 6.3057 -.0053 0 1 0
4.4703 4.4613 .0089 0 -1 2
4.0002 4.0018 -.0016 -1 0 1
3.8103 3.8103 .0000 1 -1 1
3.6103 3.6129 -.0026 -1 -1 1
3.3803 3.3846 -.0043 0 0 3
3.1703 3.1696 .0006 -1 0 2
2.8402 2.8398 .0004 0 2 1
2.6102 2.6102 .0000 0 -2 3
2.5902 2.5906 -.0005 1 -2 2
2.4402 2.4401 .0001 1 0 4
2.3201 2.3199 .0003 2 0 2
2.2402 2.2402 -.0001 2 -1 1
2.1401 2.1402 -.0001 2 0 3
A= 4.818 DA= .001
B= 6.4645 DB= .0008
C= 10.586 DC= .003
GAMMA= 88.84 DGAMMA= .02
BETA = 79.45 DBETA = .02
ALPHA=102.24 DALPHA= .03
V= 316.2
12. 39-0503
{NO2}2Ni{ClO4}4
Triklin
Dexp Dcal d(D) h k l
6.3004 6.2916 .0088 -1 0 1
4.4603 4.4609 -.0006 0 1 0
4.0102 4.0125 -.0023 0 -1 2
3.9603 3.9605 -.0002 1 -1 1
3.6602 3.6618 -.0016 1 -1 2
3.6103 3.6110 -.0007 -1 -1 1
3.4902 3.4907 -.0005 2 0 1
2.8502 2.8498 .0004 2 0 3
2.5302 2.5312 -.0010 -1 0 5
2.4202 2.4198 .0004 -1 1 4
2.2301 2.2304 -.0003 0 2 0
2.1802 2.1801 .0000 -2 -1 4
2.1302 2.1297 .0004 0 -2 3
1.9101 1.9101 .0000 -3 1 3
1.8701 1.8700 .0001 -1 0 7
1.8201 1.8202 -.0000 3 0 5
A= 7.2156 DA= .0007
B= 4.5325 DB= .0007
C= 13.803 DC= .001
GAMMA= 95.772 DGAMMA= .005
BETA = 87.828 DBETA = .005
ALPHA= 98.60 DALPHA= .01
V= 443.97
13. 39-0510
SnNi{PO4}2*7H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
17.2304 17.1049 .1255 1 0 0
8.5105 8.5525 -.0420 2 0 0
4.3002 4.2762 .0240 4 0 0
3.9903 3.9993 -.0090 0 2 0
3.6203 3.6228 -.0025 2 2 0
3.2702 3.2742 -.0040 3 2 0
2.4801 2.4815 -.0014 6 0 1
2.1402 2.1381 .0020 8 0 0
2.0301 2.0293 .0008 5 0 2
1.6185 1.6198 -.0013 10 0 1
1.4401 1.4397 .0004 10 3 0
a=17.10 b= 8.00 c= 5.04
da= .03 db= .03 dc= .03
v= 690
14. 39-0594
Ni{HPO3NH2}2*5H2O
Triklin
Dexp Dcal d(D) h k l
6.4606 6.4478 .0128 1 1 0
5.5204 5.5180 .0024 -1 0 1
4.8104 4.8083 .0021 -1 -2 1
4.7005 4.7003 .0001 0 2 0
4.6204 4.6132 .0072 0 -2 1
4.3503 4.3490 .0013 1 1 1
4.0903 4.0934 -.0031 1 -1 1
3.5302 3.5308 -.0006 0 -2 2
3.4703 3.4690 .0012 2 1 0
3.2102 3.2103 -.0001 1 -2 1
2.4802 2.4804 -.0002 1 4 0
2.3502 2.3502 .0000 0 4 0
2.2301 2.2301 .0000 -3 -1 2
A= 7.201 DA= .001
B= 10.539 DB= .001
C= 8.567 DC= .003
GAMMA= 67.582 DGAMMA= .007
BETA =105.44 DBETA = .03
ALPHA=109.61 DALPHA= .02
V= 559.0
15. 39-1001
Ni3Sn3Te5
Triklin
Dexp Dcal d(D) h k l
3.1581 3.1568 .0012 1 0 2
2.8490 2.8489 .0000 0 -1 2
2.6175 2.6152 .0023 1 -1 2
2.2263 2.2249 .0014 1 -1 3
2.0795 2.0793 .0003 -1 -1 2
1.9626 1.9632 -.0006 -1 0 4
1.8242 1.8248 -.0006 2 -1 2
1.6157 1.6157 .0000 -1 -1 4
1.5773 1.5772 .0001 -2 2 0
1.5594 1.5594 -.0000 -2 2 1
1.4106 1.4107 -.0001 1 1 6
1.3148 1.3148 -.0000 1 -2 5
1.2900 1.2899 .0000 -1 3 2
1.2467 1.2466 .0001 -1 -2 4
1.1544 1.1544 .0000 3 1 1
A= 4.0414 DA= .0004
B= 3.962 DB= .001
C= 9.6101 DC= .0005
GAMMA=104.09 DGAMMA= .02
BETA = 86.428 DBETA = .009
ALPHA= 85.349 DALPHA= .006
V= 148.2
16. 39-1516
C18H16N2NiO6*18H2O
Triklin
Dexp Dcal d(D) h k l
6.8104 6.8239 -.0135 1 0 1
6.0674 6.0667 .0008 0 1 1
5.0969 5.1050 -.0082 0 -1 1
4.8482 4.8564 -.0083 1 1 1
4.4398 4.4401 -.0004 0 0 2
4.0771 4.0881 -.0110 2 0 1
3.9003 3.9050 -.0047 -1 -1 1
3.4532 3.4546 -.0014 -2 0 1
3.1646 3.1597 .0050 1 -2 1
3.0482 3.0477 .0005 2 1 2
2.8579 2.8589 -.0009 -2 -1 1
2.6985 2.6985 .0000 2 0 3
A= 8.531 DA= .001
B= 7.2533 DB= .0008
C= 9.1916 DC= .0006
GAMMA= 98.89 DGAMMA= .01
BETA = 78.921 DBETA = .008
ALPHA= 81.93 DALPHA= .01
V=542.7
17. 39-1744
C21H14Ni3O10*6H2O
Triklin
Dexp Dcal d(D) h k l
12.9802 12.9803 -.0001 1 0 0
7.4217 7.4085 .0131 0 1 0
6.3996 6.3850 .0145 1 0 1
5.1993 5.1909 .0083 2 0 1
4.8394 4.8285 .0110 2 1 0
4.5154 4.5088 .0065 -1 -1 1
4.0552 4.0577 -.0025 2 1 1
3.6753 3.6782 -.0029 3 -1 1
3.5333 3.5409 -.0076 -2 1 1
3.1752 3.1753 -.0001 2 -2 1
2.9952 2.9972 -.0020 -4 1 0
2.9072 2.9064 .0008 1 1 2
A= 13.32029 DA= .0002
B= 7.460 DB= .004
C= 6.686 DC= .001
GAMMA= 92.72 DGAMMA= .03
BETA = 77.097 DBETA = .002
ALPHA= 96.61 DALPHA= .03
V= 643.2
18. 39-1746
C21H14Ni3O10
Triklin
Dexp Dcal d(D) h k l
12.7003 12.6915 .0088 1 0 0
7.3356 7.3416 -.0060 0 0 1
6.3346 6.3458 -.0112 2 0 0
5.1714 5.1743 -.0029 2 -1 1
4.8224 4.8167 .0056 2 0 1
4.4573 4.4597 -.0024 -1 1 1
4.1683 4.1688 -.0005 -3 1 0
4.0494 4.0538 -.0044 1 1 1
3.7302 3.7313 -.0011 0 2 0
3.5203 3.5200 .0002 -1 0 2
3.1732 3.1729 .0003 4 0 0
2.9882 2.9881 .0001 -1 -2 2
A= 13.20947 DA= .00001
B= 8.29799 DB= .00009
C= 7.88908 DC= .00003
GAMMA=106.1012 DGAMMA= .0004
BETA = 83.8417 DBETA = .0005
ALPHA=111.47620 DALPHA= .00007
V=773.2
19. 39-1885
C6H12Cl2N4NiO4*H2O
Triklin
Dexp Dcal d(D) h k l
6.9705 6.9792 -.0087 1 1 0
6.8105 6.8253 -.0149 0 1 1
6.7074 6.7134 -.0060 0 -1 1
6.3446 6.3419 .0027 -1 0 1
6.0839 6.0813 .0027 -1 -1 1
5.0794 5.0792 .0002 -1 2 0
4.4930 4.4820 .0110 1 1 1
3.8670 3.8699 -.0028 -1 0 2
3.6928 3.6927 .0002 1 4 0
3.6189 3.6186 .0003 1 3 1
3.4799 3.4822 -.0023 0 -4 1
3.3266 3.3263 .0003 -1 4 0
A= 7.777 DA= .005
B= 16.045 DB= .002
C= 7.897 DC= .005
GAMMA= 82.90 DGAMMA= .03
BETA =108.703 DBETA = .007
ALPHA= 91.1202 DALPHA= .0004
V= 926
20. 39-1886
C12H24Cl2N8NiO8*4H2O
Triklin
Dexp Dcal d(D) h k l
9.0629 9.0905 -.0276 -1 1 0
7.1966 7.1832 .0133 1 1 0
6.9163 6.8869 .0294 -1 0 1
6.7074 6.7028 .0047 1 0 2
6.4633 6.4511 .0122 1 1 1
6.1939 6.1915 .0023 0 -2 1
5.9459 5.9541 -.0082 0 2 0
5.5054 5.5097 -.0043 2 -2 2
5.2158 5.2164 -.0005 0 -2 2
4.9283 4.9109 .0174 1 1 2
4.3747 4.3682 .0064 2 -3 2
4.1522 4.1522 .0001 2 -3 1
A= 12.880 DA= .003
B= 13.80 DB= .01
C= 15.40 DC= .01
GAMMA=114.52 DGAMMA= .02
BETA = 58.91 DBETA = .02
ALPHA=117.47 DALPHA= .07
V=2022.8
21. 39-1887
C12H24N10NiO14*2H2O
Triklin
Dexp Dcal d(D) h k l
8.4257 8.4150 .0107 -1 0 1
6.9705 6.9463 .0242 0 1 1
6.8105 6.8128 -.0024 0 -1 1
6.4175 6.4174 .0001 1 -1 1
6.1512 6.1520 -.0008 0 0 2
5.9063 5.9131 -.0068 1 1 0
5.4714 5.4761 -.0047 -1 0 2
5.3407 5.3425 -.0019 -2 1 0
4.9223 4.9331 -.0107 -1 1 2
4.7064 4.7088 -.0024 1 -1 2
4.1220 4.1209 .0010 2 1 0
4.0403 4.0416 -.0012 2 0 2
A= 11.5634 DA= .0006
B= 8.6329 DB= .0002
C= 12.32084 DC= .00005
GAMMA=106.019 DGAMMA= .002
BETA = 92.760 DBETA = .002
ALPHA= 88.0956 DALPHA= .0003
V=1182
22. 39-1888
C12H24N10NiO14
Triklin
Dexp Dcal d(D) h k l
8.2686 8.2774 -.0088 -1 0 2
6.9163 6.9058 .0105 0 1 1
6.7074 6.7080 -.0006 0 -1 1
6.3260 6.3271 -.0011 -1 0 3
6.0098 6.0234 -.0136 -2 0 1
5.7914 5.7880 .0034 1 -1 1
5.4054 5.4032 .0022 -1 -1 2
5.2089 5.2067 .0021 1 -1 2
4.9832 4.9831 .0001 0 -1 3
4.7706 4.7722 -.0016 -2 0 3
4.0586 4.0596 -.0010 2 1 3
3.6778 3.6758 .0021 3 1 0
A= 12.495 DA= .005
B= 7.179 DB= .005
C= 21.854 DC= .007
GAMMA= 87.25 DGAMMA= .04
BETA = 90.74 DBETA = .04
ALPHA= 87.24 DALPHA= .04234
V=1956
23 39-1902
C30H24N6NiO4W*6H2O
Triklin
Dexp Dcal d(D) h k l
11.1918 11.2230 -.0312 1 0 0
8.8457 8.8133 .0325 0 1 0
7.6290 7.6052 .0238 0 0 1
6.9163 6.9236 -.0073 0 -1 1
5.9459 5.9401 .0059 -1 -1 1
5.5054 5.5059 -.0006 -2 1 0
5.0394 5.0337 .0057 0 1 1
4.5757 4.5743 .0014 -1 2 0
4.4618 4.4640 -.0022 0 -2 1
4.3536 4.3537 -.0001 1 -2 1
3.9345 3.9337 .0008 -1 -1 2
3.7858 3.7824 .0035 -3 0 1
3.6335 3.6324 .0011 -2 0 2
3.3146 3.3161 -.0015 -3 -1 1
3.2321 3.2338 -.0018 -2 1 2
A= 11.95 DA= .01
B= 9.516 DB= .004
C= 8.163 DC= .007
GAMMA=102.91 DGAMMA= .04
BETA =101.31 DBETA = .07
ALPHA=104.74 DALPHA= .02
V= 843
24. 39-1929
C42H42N2NiO9S3
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
12.9615 13.1184 -.1570 0 0 1
6.5704 6.5592 .0112 0 0 2
4.3804 4.3728 .0076 0 0 3
4.2103 4.2121 -.0017 3 0 1
3.9504 3.9448 .0056 0 1 0
3.3903 3.3956 -.0053 2 1 0
3.3403 3.3357 .0046 4 0 0
2.8803 2.8792 .0010 3 1 1
2.6502 2.6521 -.0019 4 0 3
a=13.34 b= 3.945 c=13.12
da= .02 db= .001 dc= .02
V= 690