1. 25-0587
NiTe2O5
Triklin
Dexp Dcal d(D) h k l
5.4706 5.4697 .0009 1 1 1
4.2303 4.2283 .0020 -1 -1 1
3.8143 3.8145 -.0002 2 1 1
3.7403 3.7381 .0022 0 -1 2
3.6503 3.6500 .0002 2 1 0
3.6002 3.6036 -.0034 -2 1 1
3.4003 3.4001 .0002 2 1 2
3.3002 3.2942 .0060 0 2 2
3.2303 3.2267 .0036 2 -2 1
3.0603 3.0597 .0006 3 -1 1
3.0403 3.0417 -.0015 -2 2 1
2.9862 2.9866 -.0004 3 0 0
A= 9.469 DA= .001
B= 8.324 DB= .004
C= 9.574 DC= .005
GAMMA= 98.52 DGAMMA= .01
BETA = 74.31 DBETA = .01
ALPHA= 83.96 DALPHA= .03
V=710.6
2. 25-1731
C6H10N8NiO6
Triklin
Dexp Dcal d(D) h k l
8.8406 8.8306 .0101 1 0 0
7.9508 7.9450 .0058 -1 1 0
6.5405 6.5394 .0011 0 1 1
5.2004 5.2101 -.0098 0 -1 1
4.6004 4.6001 .0003 0 2 1
4.3703 4.3713 -.0010 -2 1 1
3.8403 3.8352 .0051 1 2 0
3.4403 3.4404 -.0001 -1 0 2
3.1602 3.1601 .0001 -2 2 2
2.9712 2.9732 -.0020 -3 2 0
2.8152 2.8153 -.0001 1 3 0
2.7162 2.7190 -.0028 2 2 1
A= 9.5251 DA= .0006
B= 10.9047 DB= .0006
C= 7.4686 DC= .0009
GAMMA=110.88 DGAMMA= .06
BETA =102.46 DBETA = .04
ALPHA= 73.02 DALPHA= .01
V= 687.8
3. 25-1732
C6H18N10NiO6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9103 5.8937 .0166 1 1 0
4.8503 4.8424 .0078 0 0 2
4.0503 4.0546 -.0043 1 0 2
3.6303 3.6365 -.0062 1 1 2
3.3302 3.3286 .0016 -2 0 2
3.1102 3.1058 .0044 -1 0 3
2.9502 2.9469 .0033 2 2 0
2.8642 2.8654 -.0012 2 1 2
2.6792 2.6786 .0006 -2 0 3
2.3882 2.3877 .0004 1 2 3
2.3232 2.3241 -.0009 3 2 0
2.2252 2.2246 .0006 3 2 1
a= 8.484 b= 8.22 c= 9.7206 beta= 94.9
da=.006 db=.02 dc=.0004 dbeta=.1
V= 675.6
Triklin
Dexp Dcal d(D) h k l
5.9103 5.9050 .0052 0 1 1
4.8503 4.8536 -.0034 0 -1 1
4.0503 4.0552 -.0049 -1 0 1
3.6303 3.6284 .0019 0 2 1
3.3302 3.3365 -.0063 1 2 0
3.1102 3.1084 .0019 0 -2 1
2.9502 2.9449 .0053 1 2 2
2.8642 2.8649 -.0006 -1 0 2
2.6792 2.6804 -.0012 2 0 0
2.3882 2.3891 -.0010 2 0 2
2.3232 2.3218 .0014 2 2 2
2.2252 2.2246 .0005 -2 1 1
A= 5.569 DA= .004
B= 7.762 DB= .002
C= 7.8835 DC= .0006
GAMMA= 77.77 DGAMMA= .03
BETA = 77.73 DBETA = .01
ALPHA= 76.71 DALPHA= .01
V= 319.2
4. 25-1733
C6H6Br2N2NiS2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.8105 8.8517 -.0412 0 0 1
7.6207 7.6356 -.0149 1 1 0
6.0104 6.0251 -.0147 1 1 1
5.5503 5.5443 .0060 2 0 0
3.9702 3.9694 .0008 1 1 2
3.8203 3.8178 .0025 2 2 0
3.7003 3.7027 -.0024 -1 1 2
3.6103 3.6123 -.0020 2 2 1
3.4102 3.4079 .0023 -2 2 1
3.3302 3.3237 .0065 1 2 2
3.2602 3.2628 -.0026 0 3 1
3.1702 3.1670 .0032 1 3 1
a= 11.164 b= 10.530 c= 8.912 beta= 83.32
da=.002 db= .004 dc=.007 dbeta=.02
V= 1040.6
Triklin
Dexp Dcal d(D) h k l
8.8105 8.8433 -.0328 1 0 0
7.6207 7.6305 -.0098 0 1 0
6.0104 6.0111 -.0007 1 0 1
5.5503 5.5582 -.0079 -1 1 0
3.9702 3.9681 .0021 2 1 0
3.8203 3.8153 .0050 0 2 0
3.7003 3.6977 .0026 -2 1 0
3.6103 3.6114 -.0012 1 2 0
3.4102 3.4040 .0062 -1 2 0
3.3302 3.3282 .0020 0 0 2
3.2602 3.2618 -.0016 2 2 1
3.1702 3.1682 .0020 2 1 2
A= 9.196 DA= .004
B= 8.10 DB= .01
C= 7.227 DC= .002
GAMMA= 80.82 DGAMMA= .04
BETA = 74.76 DBETA = .04
ALPHA= 71.01 DALPHA= .04
V= 489.3
5. 25-1735
C12H12Cl2N4NiS4
Triklin
Dexp Dcal d(D) h k l
8.6709 8.6696 .0013 1 0 0
7.5503 7.5578 -.0075 0 1 0
7.0503 7.0559 -.0056 -1 0 1
6.3303 6.3329 -.0026 0 -1 1
5.7003 5.7012 -.0009 1 0 1
5.4005 5.3977 .0027 0 1 1
3.7803 3.7789 .0014 0 2 0
3.1802 3.1845 -.0043 -2 1 2
2.8362 2.8364 -.0001 -3 1 0
2.7602 2.7599 .0003 -1 2 2
2.6002 2.6004 -.0002 3 0 1
2.4302 2.4299 .0003 -3 2 1
A= 8.9234 DA= .0002
B= 7.70587 DB= .00006
C= 9.377 DC= .003
GAMMA= 96.404 DGAMMA= .005
BETA =101.07 DBETA = .02
ALPHA= 97.81 DALPHA= .01
V= 620.7
6. 25-1738
C10H12NiO8S4*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.9104 6.8722 .0382 0 1 1
6.6505 6.6574 -.0070 1 1 0
5.1202 5.1425 -.0223 1 1 1
4.5004 4.5027 -.0024 2 0 0
3.8203 3.8206 -.0002 1 2 1
3.5603 3.5553 .0050 2 1 1
3.3302 3.3287 .0015 2 2 0
3.1202 3.1154 .0048 0 3 1
2.8902 2.8908 -.0006 1 3 1
2.7102 2.7131 -.0029 0 3 2
2.5701 2.5713 -.0011 2 2 2
2.4002 2.3997 .0005 2 0 3
a= 9.164 b= 9.886 c= 9.73 beta= 100.68
da=.001 db=.007 dc=.01 dbeta=.07
V= 866.1
Triklin
Dexp Dcal d(D) h k l
6.9104 6.9285 -.0181 1 0 0
6.6505 6.6568 -.0064 -1 1 0
5.1202 5.1157 .0045 0 0 1
4.5004 4.5002 .0002 1 -1 1
3.8203 3.8156 .0047 1 1 1
3.5603 3.5613 -.0010 2 -1 1
3.3302 3.3284 .0018 -2 2 0
3.1202 3.1208 -.0006 -1 2 1
2.8902 2.8904 -.0003 0 -2 1
2.7102 2.7075 .0027 -2 1 1
2.5701 2.5711 -.0009 -2 2 1
2.4002 2.4005 -.0003 3 0 1
A= 7.935 DA= .001
B= 8.3222 DB= .0009
C= 5.3777 DC= .0007
GAMMA=113.409 DGAMMA= .003
BETA = 73.2936 DBETA = .0004
ALPHA= 90.699 DALPHA= .005
V=310.1
7. 25-1739
C18H18Cl2N6NiO8S6
Triklin
Dexp Dcal d(D) h k l
8.7710 8.7809 -.0098 1 0 0
7.2305 7.2141 .0164 -1 -1 1
7.1406 7.1536 -.0130 -1 0 1
5.9604 5.9613 -.0009 1 0 1
5.1204 5.1165 .0038 -1 -1 2
4.4304 4.4289 .0015 -2 -1 1
4.3202 4.3214 -.0012 0 -2 2
4.0403 4.0462 -.0059 1 -1 2
3.8903 3.8914 -.0012 -1 2 0
3.6702 3.6764 -.0062 0 1 2
3.3502 3.3474 .0028 0 -2 3
3.1002 3.1015 -.0013 -2 -2 3
A= 9.1338 DA= .0004
B= 10.311 DB= .002
C= 10.87 DC= .01
GAMMA= 77.83 DGAMMA= .01
BETA =104.601 DBETA = .004
ALPHA=116.24 DALPHA= .04
V= 883.0
8. 25-1740
C14H16N2NiO8*4H2O
Triklin
Dexp Dcal d(D) h k l
10.7016 10.7006 .0010 1 0 0
7.8013 7.8095 -.0082 0 1 0
6.4608 6.4640 -.0032 -1 0 1
6.0909 6.0912 -.0003 0 -1 1
5.6109 5.6165 -.0056 -1 1 1
5.3406 5.3358 .0048 -2 1 0
5.1606 5.1592 .0014 1 1 1
5.0008 4.9923 .0085 0 0 2
4.5207 4.5195 .0012 -1 -1 1
4.2905 4.2882 .0023 2 0 2
4.2507 4.2524 -.0017 -2 0 1
4.1705 4.1678 .0027 0 -1 2
A= 11.8686 DA= .0007
B= 8.327 DB= .001
C= 10.42 DC= .01
GAMMA=110.279 DGAMMA= .004
BETA = 73.378 DBETA = .007
ALPHA= 94.638 DALPHA= .005
V= 925.6
9. 25-1972
C24H18N4NiS2
Triklin
Dexp Dcal d(D) h k l
14.0000 14.0001 -.0001 0 0 1
12.8005 12.8011 -.0007 -1 0 1
8.2906 8.2800 .0106 0 1 1
7.5405 7.5403 .0003 0 -1 1
6.2405 6.2402 .0003 -2 1 1
5.6104 5.6033 .0071 -1 -1 2
5.0704 5.0691 .0013 3 0 1
4.5604 4.5628 -.0024 -3 1 2
4.2504 4.2554 -.0050 -2 1 3
4.0703 4.0681 .0022 3 0 2
3.9904 3.9942 -.0038 3 2 0
3.7403 3.7407 -.0004 -5 0 1
3.6203 3.6197 .0005 -3 2 1
A= 18.808 DA= .007
B= 9.643 DB= .002
C= 14.540 DC= .001
GAMMA= 83.96 DGAMMA= .01
BETA =104.59 DBETA = .09
ALPHA= 85.99 DALPHA= .02
V= 2525
10. 25-1973
C6H16N10NiO6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9404 5.9383 .0020 1 1 0
5.2704 5.2700 .0004 -1 1 2
4.6603 4.6637 -.0034 1 0 5
4.0503 4.0467 .0036 0 2 0
3.8503 3.8515 -.0013 2 1 1
3.6303 3.6300 .0002 2 1 3
3.5102 3.5139 -.0037 2 0 5
3.1902 3.1907 -.0005 -2 1 4
3.0102 3.0101 .0001 0 1 8
2.9062 2.9032 .0030 3 0 2
2.7582 2.7591 -.0008 3 0 4
2.7582 2.7592 -.0010 -2 1 6
a= 8.78117 b= 8.093 c= 26.06 beta= 84.44
da=.00008 db= .005 dc=.02 dbeta=.02
V= 1844
Triklin
Dexp Dcal d(D) h k l
5.9404 5.9424 -.0020 1 0 0
5.2704 5.2803 -.0099 -1 1 0
4.6603 4.6676 -.0073 1 -1 2
4.0503 4.0527 -.0024 -1 0 2
3.8503 3.8514 -.0012 1 -2 1
3.6303 3.6320 -.0017 -1 2 0
3.5102 3.5057 .0045 -1 1 2
3.1902 3.1930 -.0028 -1 2 1
3.0102 3.0095 .0007 1 2 0
2.9062 2.9059 .0003 0 2 2
2.7582 2.7582 -.0000 2 0 2
2.7162 2.7140 .0022 2 -2 2
A= 6.144 DA= .001
B= 8.499 DB= .006
C= 12.762 DC= .002
GAMMA=103.914 DGAMMA= .09
BETA = 80.93 DBETA = .04
ALPHA=109.29 DALPHA= .02
V= 608.4
11. 25-1974
C6H4N6NiO6*6H2O
Triklin
Dexp Dcal d(D) h k l
9.7608 9.7686 -.0078 1 0 0
8.3409 8.3580 -.0171 1 1 0
6.9405 6.9441 -.0037 -1 0 1
5.7703 5.7659 .0044 -1 1 0
5.5304 5.5298 .0006 0 1 2
5.2204 5.2229 -.0024 1 2 1
4.9504 4.9608 -.0104 1 -1 1
4.2804 4.2793 .0011 -2 0 1
4.2303 4.2285 .0018 -1 1 2
3.9702 3.9685 .0018 2 0 2
3.3202 3.3205 -.0002 2 3 2
3.2902 3.2910 -.0008 -1 1 3
A= 10.81 DA= .01
B= 10.52 DB= .02
C= 12.141 DC= .008
GAMMA= 65.76 DGAMMA= .09
BETA = 75.19 DBETA = .08
ALPHA= 69.98 DALPHA= .07
V=1172
12. 26-1451
{Ni2Al}{Si,Al}O5{OH}4
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
7.0501 7.0916 -.0415 0 0 1
4.5304 4.5170 .0134 2 0 0
3.5302 3.5458 -.0156 0 0 2
2.6102 2.6137 -.0035 3 1 0
2.4672 2.4670 .0002 0 2 1
2.3601 2.3639 -.0037 0 0 3
2.1112 2.1130 -.0019 0 2 2
1.9911 1.9919 -.0008 4 1 1
1.7531 1.7532 -.0001 3 1 3
1.6611 1.6613 -.0002 5 1 1
1.5211 1.5185 .0026 3 2 3
1.4891 1.4895 -.0004 5 2 0
1.4681 1.4672 .0009 3 1 4
1.3971 1.3981 -.0010 2 2 4
a= 9.034 b= 5.2626 c= 7.092
da= .004 db= .0003 dc= .002
V= 337.1
Triklin
Dexp Dcal d(D) h k l
7.0501 7.0567 -.0065 1 0 0
4.5304 4.5348 -.0044 0 1 1
3.5302 3.5305 -.0003 0 -1 1
2.6102 2.6100 .0002 0 2 1
2.4672 2.4675 -.0004 2 1 2
2.3601 2.3598 .0003 2 2 1
2.1112 2.1114 -.0002 2 2 2
1.9911 1.9914 -.0003 -3 1 0
1.7531 1.7532 -.0000 -2 2 2
1.6611 1.6610 .0001 3 1 3
1.5211 1.5211 -.0000 -2 -3 1
1.4891 1.4890 .0001 -3 2 2
1.4681 1.4681 .0000 -4 -1 2
1.3971 1.3971 -.0000 -2 1 4
A= 7.2322 DA= .0006
B= 5.4268 DB= .0005
C= 6.3747 DC= .0002
GAMMA= 77.490 DGAMMA= .002
BETA = 85.013 DBETA = .004
ALPHA= 74.858 DALPHA= .007
V= 235.64
13. 26-1952
C15H17N2NiOS2
Triklin
Dexp Dcal d(D) h k l
8.1106 8.1376 -.0269 1 0 0
7.8907 7.8429 .0478 0 1 0
7.6205 7.6119 .0086 0 0 1
5.9003 5.8862 .0141 1 1 0
5.7105 5.6920 .0185 0 -1 1
5.4703 5.4349 .0354 -1 1 0
5.2704 5.2582 .0121 0 1 1
4.6704 4.6693 .0011 1 0 1
4.4404 4.4432 -.0028 -2 0 1
4.1903 4.1839 .0064 -1 0 2
4.0202 4.0171 .0031 1 -1 1
3.8002 3.8059 -.0057 0 0 2
A= 9.02925 DA= .00003
B= 7.92928 DB= .00004
C= 8.44561 DC= .00001
GAMMA= 82.8520 DGAMMA= .0008
BETA =115.3038 DBETA = .0001
ALPHA= 97.1418 DALPHA= .0001
V=540.7
14. 26-1953
C15H17N2NiOS2
Triklin
Dexp Dcal d(D) h k l
12.3004 12.2480 .0525 1 0 0
7.4906 7.5314 -.0408 0 1 0
6.8005 6.7818 .0187 -1 1 0
6.1803 6.1240 .0563 2 0 0
5.2704 5.2773 -.0069 2 0 1
5.0605 5.0516 .0089 -2 1 0
4.8403 4.8408 -.0004 0 1 1
4.6704 4.6689 .0015 1 1 1
4.5004 4.4992 .0012 2 1 0
4.0703 4.0827 -.0124 3 0 0
3.9803 3.9772 .0030 3 0 1
3.7803 3.7806 -.0003 -3 1 0
A= 12.79932 DA= .00003
B= 7.65129 DB= .00002
C= 7.14755 DC= .00003
GAMMA= 98.5064 DGAMMA= .0001
BETA = 74.5052 DBETA = .0002
ALPHA= 97.5989 DALPHA= .0003
V=663.9
15. 26-1954
C6H8NiO4S2
Triklin
Dexp Dcal d(D) h k l
8.1804 8.1768 .0036 1 0 0
6.2302 6.2276 .0026 1 1 0
4.7602 4.7576 .0027 1 0 1
4.1803 4.1799 .0004 2 1 0
3.5202 3.5203 -.0001 2 1 1
3.0603 3.0611 -.0008 -2 0 1
2.3502 2.3502 .0000 1 -1 2
2.0501 2.0501 .0001 0 2 2
1.9701 1.9702 -.0000 -2 2 1
1.7601 1.7602 -.0000 4 2 2
1.5901 1.5901 .0000 -5 -1 1
A= 8.8196 DA= .0005
B= 6.869 DB= .001
C= 5.3870 DC= .0006
GAMMA= 69.212 DGAMMA= .008
BETA = 82.16 DBETA = .006
ALPHA= 87.34 DALPHA= .01
V=302.2
16. 26-1955
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.1804 8.1929 -.0125 1 1 0
6.0605 6.0685 -.0080 0 2 0
5.7905 5.8144 -.0239 1 0 1
5.2405 5.2437 -.0033 1 1 1
5.0302 5.0491 -.0188 2 1 0
4.0703 4.0852 -.0149 2 1 1
3.5403 3.5406 -.0002 3 1 0
3.3503 3.3524 -.0021 0 0 2
3.1703 3.1671 .0031 3 1 1
2.8902 2.8860 .0042 3 2 1
2.5201 2.5213 -.0011 3 0 2
2.3201 2.3211 -.0010 -2 3 2
a= 11.109 b=12.1369 c= 6.708 beta= 88.34
da= .003 db=.0006 dc=.006 dbeta=.02
V= 904.0
26-1956
C14H8N2NiO8*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.6105 6.6105 .0000 1 0 1
6.3009 6.2874 .0135 1 1 0
6.0008 6.0054 -.0046 0 1 1
5.1905 5.1675 .0230 2 0 0
5.0705 5.0755 -.0050 1 1 1
4.3306 4.3281 .0025 2 1 0
4.0204 4.0252 -.0048 -2 1 1
3.8205 3.8171 .0034 2 1 1
3.6404 3.6386 .0018 0 2 1
3.4704 3.4676 .0028 -1 2 1
3.1404 3.1428 -.0024 3 0 1
3.0104 3.0108 -.0004 -1 0 3
2.9204 2.9213 -.0009 3 1 1
2.5903 2.5893 .0010 -2 1 3
a= 10.37 b= 7.922 c= 9.24 beta= 94.7
da= .04 db=.006 dc=.03 dbeta=.2
V= 756
Triklin
Dexp Dcal d(D) h k l
6.6105 6.6261 -.0156 1 0 0
6.3009 6.2841 .0168 0 1 0
6.0008 5.9856 .0152 0 1 1
5.1905 5.1808 .0097 1 0 1
5.0705 5.0670 .0035 -1 0 1
4.3306 4.3279 .0026 0 -1 1
4.0204 4.0250 -.0046 1 1 2
3.8205 3.8177 .0028 -1 1 0
3.6404 3.6416 -.0012 2 1 0
3.4704 3.4701 .0003 1 2 0
3.1404 3.1420 -.0016 0 2 0
3.0104 3.0103 .0001 2 2 0
2.9204 2.9195 .0008 2 2 2
2.5903 2.5904 -.0001 2 0 2
A= 7.4606 DA= .0003
B= 7.475 DB= .004
C= 8.69 DC= .01
GAMMA= 62.67 DGAMMA= .02
BETA = 79.18 DBETA = .04
ALPHA= 68.39 DALPHA= .04
V= 400.2
17. 26-1957
C14H8N2NiO8*3H2O
Triklin
Dexp Dcal d(D) h k l
12.4008 12.3471 .0537 1 0 0
6.1108 6.1004 .0104 0 1 0
5.8706 5.8702 .0004 -1 0 1
5.1905 5.1881 .0023 -1 1 0
4.9604 4.9484 .0120 2 1 1
4.6778 4.6796 -.0017 2 1 0
4.0604 4.0639 -.0035 -2 1 0
3.3804 3.3787 .0017 0 2 1
3.2604 3.2606 -.0002 2 2 1
3.1304 3.1316 -.0013 1 2 2
3.0503 3.0502 .0001 0 2 0
2.9003 2.9009 -.0006 2 2 0
2.5503 2.5502 .0001 -3 0 2
2.4403 2.4404 -.0001 0 2 3
2.2702 2.2702 -.0000 -1 0 3
A= 12.69 DA= .01
B= 6.907 DB= .005
C= 7.970 DC= .003
GAMMA= 78.04 DGAMMA= .02
BETA = 79.24 DBETA = .02
ALPHA= 63.13 DALPHA= .03
V= 606.3
18. 26-1958
C12H8N2NiO4*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.6312 8.6675 -.0363 1 1 0
6.1506 6.1600 -.0095 0 2 0
5.5006 5.4985 .0021 1 2 0
4.5105 4.5058 .0047 1 2 1
4.3705 4.3777 -.0073 2 1 1
4.0405 4.0416 -.0012 0 1 2
3.6004 3.6001 .0002 -1 3 1
3.3904 3.3931 -.0027 3 2 0
3.1904 3.1912 -.0008 2 1 2
3.0803 3.0800 .0003 0 4 0
2.9404 2.9411 -.0007 -1 3 2
2.8903 2.8892 .0012 3 3 0
2.7603 2.7597 .0007 4 0 1
2.7003 2.6997 .0006 1 0 3
2.2503 2.2502 .0000 -5 0 2
a= 12.303 b= 12.320 c=8.6318 beta= 97.55
da=.009 db=.004 dc=.0008 dbeta=.01
V= 1297.0
Triklin
Dexp Dcal d(D) h k l
8.6312 8.6467 -.0155 1 0 0
6.1506 6.1570 -.0065 -1 1 0
5.5006 5.4885 .0121 0 1 1
4.5105 4.5014 .0091 1 0 1
4.3705 4.3716 -.0011 -2 1 1
4.0405 4.0448 -.0043 -1 -1 1
3.6004 3.6060 -.0056 -1 2 0
3.3904 3.3907 -.0003 -2 2 1
3.1904 3.1912 -.0009 0 0 2
3.0803 3.0785 .0018 -2 2 0
2.9404 2.9401 .0002 1 2 1
2.8903 2.8890 .0013 0 -2 1
2.7603 2.7601 .0002 -3 1 2
2.7003 2.7000 .0003 0 -1 2
2.2503 2.2507 -.0004 2 0 2
A= 9.484 DA= .003
B= 7.8197 DB= .0004
C= 7.0837 DC= .0007
GAMMA=106.124 DGAMMA= .007
BETA =112.019 DBETA = .002
ALPHA= 71.711 DALPHA= .009
V=454.6
19. 26-1959
C12H8N2NiO4*4H2O
Triklin
Dexp Dcal d(D) h k l
7.4909 7.4515 .0394 0 0 1
6.5607 6.5412 .0196 -1 -1 1
6.2407 6.2344 .0063 1 1 0
6.0605 6.0343 .0262 -1 1 0
5.3405 5.3288 .0117 -2 0 1
4.2405 4.2441 -.0036 -1 1 1
4.1905 4.1873 .0032 -1 -1 2
3.9505 3.9496 .0009 1 1 1
3.8804 3.8792 .0012 0 -2 1
3.5604 3.5611 -.0007 0 2 0
3.4504 3.4503 .0001 1 2 0
3.3304 3.3320 -.0016 0 -2 2
A= 12.528 DA= .001
B= 7.869 DB= .004
C= 8.46 DC= .02
GAMMA= 81.56 DGAMMA= .04
BETA =105.67 DBETA = .03
ALPHA=115.09 DALPHA= .01
V=725.2
20. 26-1960
C10H8N2NiO6S2*4H2O
Triklin
Dexp Dcal d(D) h k l
7.2011 7.1647 .0364 0 0 2
6.4405 6.4427 -.0022 0 1 1
6.0708 6.0467 .0241 0 -1 1
5.1006 5.1081 -.0074 1 0 1
4.9105 4.9282 -.0177 1 1 0
4.8205 4.8165 .0040 -1 0 1
4.3705 4.3595 .0109 1 1 2
4.3505 4.3595 -.0090 1 1 2
4.0805 4.0789 .0016 -1 0 2
3.7904 3.7913 -.0009 0 -1 3
3.7204 3.7211 -.0007 -1 1 0
3.5804 3.5823 -.0019 0 0 4
A= 5.54765 DA= .00008
B= 7.26780 DB= .00005
C= 14.47870 DC= .00004
GAMMA= 72.9459 DGAMMA= .0007
BETA = 83.192 DBETA = .001
ALPHA= 83.6016 DALPHA= .0007
V=552.6
21. 26-1961
C20H22N2NiO4S
Triklin
Dexp Dcal d(D) h k l
10.8014 10.8166 -.0152 1 0 0
8.8404 8.8393 .0012 0 1 0
8.1907 8.1800 .0108 1 0 1
6.0305 6.0291 .0014 0 -1 1
5.4403 5.4379 .0023 2 0 1
4.5804 4.5797 .0006 1 0 2
4.2704 4.2712 -.0008 2 -2 1
4.1102 4.1113 -.0011 3 -1 1
3.9302 3.9296 .0006 -3 1 0
3.8503 3.8504 -.0001 0 -2 1
3.6332 3.6342 -.0010 -2 2 1
3.3633 3.3632 .0001 1 -2 2
3.2203 3.2204 -.0001 3 -2 2
2.9212 2.9208 .0004 -3 3 0
A= 12.455 DA= .001
B= 9.664 DB= .004
C= 9.2230 DC= .0009
GAMMA=113.61 DGAMMA= .02
BETA = 71.1892 DBETA = .0006
ALPHA= 94.45 DALPHA= .02
V= 961.1