1. 15-0049
Ni{NH3}{CN2}*0.25H2O
Triklin
Dexp Dcal d(D) h k l
7.5200 7.5243 -.0043 1 0 0
7.1300 7.1272 .0028 1 1 0
4.8100 4.8091 .0009 1 0 1
4.4000 4.4045 -.0045 -1 1 0
3.5900 3.5898 .0002 -2 -2 2
3.5000 3.5024 -.0024 0 1 2
3.2100 3.2129 -.0029 2 1 1
2.9400 2.9374 .0026 0 -2 2
2.8700 2.8708 -.0008 -1 2 0
2.7200 2.7196 .0004 3 2 0
2.5300 2.5310 -.0010 0 1 3
2.2700 2.2702 -.0002 2 2 2
A= 9.4270 DA= .0007
B= 8.7828 DB= .0004
C= 9.430 DC= .006
GAMMA= 58.671 DGAMMA= .009
BETA =116.83 DBETA = .05
ALPHA=108.19 DALPHA= .05
V= 592.1
Triklin
2. 15-0093
NiY
Triklin
Dexp Dcal d(D) h k l
3.2900 3.2766 .0134 1 0 1
2.7900 2.7927 -.0027 -1 0 1
2.6900 2.6893 .0007 1 -2 1
2.5500 2.5551 -.0051 1 2 1
2.4200 2.4229 -.0029 2 2 0
2.1800 2.1805 -.0005 0 4 0
2.0500 2.0505 -.0005 3 0 1
1.9300 1.9294 .0006 3 1 1
1.8600 1.8616 -.0016 1 -4 1
1.7000 1.7030 -.0030 -4 1 0
1.6500 1.6527 -.0027 4 -1 1
1.6300 1.6276 .0024 3 -4 1
A= 6.94 DA= .01
B= 8.907 DB= .003
C= 3.434 DC= .001
GAMMA=101.4 DGAMMA= .1
BETA = 78.96 DBETA = .07
ALPHA= 89.55 DALPHA= .03
V=204.0
3. 15-0099
NiY3
Triklin
Dexp Dcal d(D) h k l
3.1500 3.1523 -.0023 1 4 0
2.8600 2.8608 -.0008 -1 1 1
2.7700 2.7698 .0002 -1 -1 1
2.7400 2.7391 .0009 0 3 1
2.6300 2.6293 .0007 -1 -2 1
2.5400 2.5416 -.0016 0 4 1
2.4500 2.4471 .0029 0 7 0
2.3900 2.3924 -.0024 1 0 1
2.3400 2.3368 .0032 0 5 1
2.2500 2.2490 .0010 2 3 0
2.1500 2.1497 .0003 -2 2 1
2.0900 2.0922 -.0022 -1 -5 1
A= 5.176 DA= .001
B= 17.2296 DB= .0004
C= 3.0903 DC= .0009
GAMMA= 95.12 DGAMMA= .07
BETA =101.74 DBETA = .01
ALPHA= 85.58 DALPHA= .03
V=268.3
4. 15-0103
Ni4Y
Triklin
Dexp Dcal d(D) h k l
3.0900 3.0908 -.0008 0 1 1
2.7500 2.7502 -.0002 0 -1 1
2.4200 2.4201 -.0001 -1 1 0
2.0900 2.0889 .0011 -2 -1 1
1.9900 1.9893 .0007 0 2 0
1.8600 1.8607 -.0007 1 0 2
1.7500 1.7518 -.0018 -2 -2 1
1.5600 1.5595 .0005 -2 0 2
1.4100 1.4098 .0002 1 -2 1
1.3500 1.3498 .0002 -2 -3 1
1.3100 1.3101 -.0001 -1 -1 3
1.2200 1.2200 .0000 -2 -1 3
A= 4.821 DA= .004
B= 4.491 DB= .002
C= 4.2828 DC= .0003
GAMMA= 63.14 DGAMMA= .02
BETA = 90.56 DBETA = .04
ALPHA= 84.29 DALPHA= .02
V= 82.1
5. 15-0118
Ni3Y
Triklin
Dexp Dcal d(D) h k l
2.6700 2.6701 -.0001 1 -1 1
2.5130 2.5130 .0000 1 -1 2
2.4660 2.4660 .0000 1 1 0
2.1020 2.1020 -.0000 -1 -2 1
2.0130 2.0131 -.0001 1 -3 2
2.7400 2.7401 -.0001 1 0 0
1.9550 1.9562 -.0012 0 -4 2
1.8120 1.8123 -.0003 1 -2 5
1.6140 1.6133 .0007 0 -3 7
1.4660 1.4658 .0002 0 -3 8
1.4270 1.4275 -.0005 1 -3 7
1.4070 1.4068 .0002 -1 1 8
A= 2.7796 DA= .0001
B= 8.07 DB= .01
C= 13.153 DC= .009
GAMMA= 99.27 DGAMMA= .01
BETA = 91.745 DBETA = .006
ALPHA= 96.275 DALPHA= .004
V= 289
6. 15-0146
Ni7Y2
Triklin
Dexp Dcal d(D) h k l
2.7200 2.7195 .0005 0 -1 1
2.5800 2.5796 .0004 -1 1 1
2.4400 2.4389 .0011 1 -1 1
2.1200 2.1191 .0009 -2 1 1
2.0900 2.0887 .0013 -1 2 0
1.9870 1.9872 -.0002 -3 0 1
1.9200 1.9219 -.0019 -1 -2 1
1.8890 1.8881 .0009 0 -2 1
1.8290 1.8292 -.0002 -2 -2 1
1.7110 1.7105 .0005 -1 0 2
1.6540 1.6534 .0006 4 2 0
1.4610 1.4612 -.0002 3 1 2
A= 7.5118 DA= .0007
B= 4.8794 DB= .0006
C= 3.5422 DC= .0001
GAMMA= 75.297 DGAMMA= .002
BETA = 88.18 DBETA = .01
ALPHA= 85.07 DALPHA= .01
V=125.2
7. 15-0384
Ni3Si4O10{OH}2
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
9.4200 9.3650 .0551 1 0 0
4.6800 4.6825 -.0025 2 0 0
4.5600 4.5801 -.0201 1 1 0
3.1240 3.1216 .0024 3 0 0
2.6280 2.6255 .0025 0 2 0
2.3420 2.3412 .0008 4 0 0
1.5590 1.5589 .0001 0 0 2
1.5240 1.5243 -.0003 4 2 1
a= 9.365 b= 5.251 c= 3.1178
da= .006 db= .006 dc= .0003
V= 153.3
15-0458
Gd3Ni
Triklin
Dexp Dcal d(D) h k l
3.3440 3.3441 -.0001 -3 1 0
3.2380 3.2358 .0022 1 1 1
3.1390 3.1402 -.0012 1 3 0
3.0230 3.0249 -.0019 3 2 0
2.8850 2.8852 -.0002 -2 0 1
2.8650 2.8627 .0023 2 3 0
2.8160 2.8165 -.0005 -3 2 0
2.7500 2.7493 .0007 4 0 0
2.6960 2.6966 -.0006 4 1 0
2.6350 2.6354 -.0004 3 0 1
2.5940 2.5933 .0007 -4 1 0
2.5610 2.5611 -.0001 2 -2 1
A= 11.05203 DA= .00001
B= 9.64358 DB= .00001
C= 3.54292 DC= .00001
GAMMA= 85.84248 DGAMMA= .00001
BETA = 86.18651 DBETA = .00001
ALPHA= 90.95300 DALPHA= .00002
V=375.8
8. 15-0472
NiSeO3*2H2O
Triklin
Dexp Dcal d(D) h k l
5.7200 5.7201 -.0001 1 0 1
5.2600 5.2584 .0016 0 1 0
4.4300 4.4297 .0003 0 1 1
4.0000 4.0000 .0000 -1 1 0
3.7700 3.7698 .0002 1 1 0
3.4000 3.4006 -.0006 -1 -1 1
2.9800 2.9803 -.0003 1 -1 3
2.7200 2.7200 .0000 2 -1 1
2.6300 2.6292 .0008 0 2 0
2.5300 2.5300 .0000 1 0 4
2.4700 2.4704 -.0004 0 2 1
2.3500 2.3499 .0001 -1 -1 3
2.2000 2.2000 .0000 2 0 4
A= 6.0240 DA= .0004
B= 5.31730 DB= .00005
C= 10.3260 DC= .0005
GAMMA= 95.534 DGAMMA= .001
BETA = 72.910 DBETA = .005
ALPHA= 97.8349 DALPHA= .0005
V= 312.6
9. 15-0913
C7H8N4Ni
Triklin
Dexp Dcal d(D) h k l
8.2900 8.3092 -.0192 1 0 0
7.5700 7.5528 .0172 -1 1 0
7.0200 6.9901 .0299 0 0 1
6.5800 6.5609 .0191 1 0 1
5.9600 5.9300 .0300 1 -1 1
5.4900 5.4899 .0001 0 -1 1
4.8600 4.8669 -.0069 0 2 0
4.6300 4.6290 .0010 -1 0 1
4.1500 4.1546 -.0046 2 0 0
3.7900 3.7918 -.0018 -1 2 1
3.6200 3.6239 -.0039 1 2 1
3.3900 3.3913 -.0013 -1 3 0
A= 9.255 DA= .002
B= 10.222 DB= .002
C= 7.438 DC= .005
GAMMA=107.29 DGAMMA= .07
BETA = 70.452 DBETA = .001
ALPHA= 91.92 DALPHA= .04
V= 631.4
10. 15-0914
C6H8N4Ni
Triklin
Dexp Dcal d(D) h k l
7.9100 7.8926 .0174 1 0 0
7.1800 7.1938 -.0138 1 1 0
6.2000 6.1958 .0042 0 0 1
5.0700 5.0831 -.0131 -1 0 1
4.7100 4.7076 .0024 1 1 1
4.2800 4.2723 .0077 0 2 0
4.1100 4.1109 -.0009 -1 1 1
3.9500 3.9463 .0037 2 0 0
3.6000 3.5969 .0031 2 2 0
3.4600 3.4614 -.0014 -2 0 1
3.4000 3.4049 -.0049 2 1 1
A= 8.44252 DA= .00001
B= 9.1513 DB= .0002
C= 6.23366 DC= .00001
GAMMA= 69.741 DGAMMA= .003
BETA = 93.031 DBETA = .001
ALPHA= 85.863 DALPHA= .001
V=449.1
11. 15-0915
C8H10N4Ni
Triklin
Dexp Dcal d(D) h k l
9.2800 9.2647 .0153 1 0 0
8.5100 8.5310 -.0210 0 1 0
8.0800 8.1053 -.0253 0 0 1
7.5300 7.5319 -.0019 1 0 1
7.1900 7.1993 -.0093 0 -1 1
5.7000 5.6813 .0187 1 -1 1
5.3600 5.3704 -.0104 -1 1 0
5.1000 5.0879 .0121 0 1 1
4.8800 4.8925 -.0125 2 1 0
4.6300 4.6323 -.0023 2 0 0
4.4400 4.4347 .0053 0 -2 1
4.0500 4.0527 -.0027 0 0 2
A= 10.30 DA= .01
B= 9.440 DB= .007
C= 8.896 DC= .006
GAMMA= 73.52 DGAMMA= .05
BETA = 75.17 DBETA = .02
ALPHA=103.73 DALPHA= .05
V= 755.8
12. 15-1168
C20H24N2NiO2
Triklin
Dexp Dcal d(D) h k l
9.9000 9.8460 .0540 1 0 0
8.8200 8.8737 -.0537 0 1 0
8.3000 8.3445 -.0445 0 0 1
7.0200 7.0143 .0057 1 0 1
6.6000 6.6113 -.0113 1 1 1
6.2000 6.1927 .0073 0 1 1
6.0000 5.9711 .0288 0 -1 1
5.4600 5.4592 .0008 -1 -1 1
4.8000 4.8129 -.0129 1 -1 1
4.6200 4.6166 .0034 2 0 1
4.4800 4.4765 .0035 -1 1 1
3.9400 3.9428 -.0028 -2 0 1
A= 10.992 DA= .001
B= 9.753 DB= .002
C= 8.5426 DC= .0007
GAMMA= 65.57 DGAMMA= .01
BETA = 77.816 DBETA = .003
ALPHA= 83.125 DALPHA= .006
V=813.7
13. 15-1171
C22H28N2NiO2
Triklin
Dexp Dcal d(D) h k l
10.5000 10.4800 .0200 1 0 0
8.4100 8.4147 -.0047 0 1 1
8.2000 8.1988 .0012 0 -1 1
6.6000 6.6166 -.0166 1 -1 1
6.4500 6.4371 .0129 -1 1 1
5.9500 5.9535 -.0035 0 1 2
4.9400 4.9394 .0006 -1 -1 2
4.6700 4.6695 .0005 2 -1 0
4.4000 4.4014 -.0014 2 0 2
4.2400 4.2419 -.0019 -1 0 3
4.0800 4.0780 .0020 1 -1 3
3.5900 3.5893 .0007 2 2 1
3.2300 3.2301 -.0001 -1 3 0
2.9100 2.9098 .0002 1 2 4
2.7000 2.7002 -.0002 2 3 2
A= 10.511 DA= .005
B= 10.16942 DB= .00009
C= 14.448 DC= .004
GAMMA= 90.24 DGAMMA= .01
BETA = 85.589 DBETA = .001
ALPHA= 88.45 DALPHA= .01
V= 1539.3