1. 1-0105
C4H6NiO4*4H2O
Triklin
Dexp Dcal d(D) h k l
7.4000 7.4006 -.0006 1 0 0
6.9000 6.9039 -.0039 0 1 1
5.9000 5.8987 .0013 0 -1 1
4.7500 4.7528 -.0028 0 2 1
4.4800 4.4808 -.0008 1 1 2
4.2500 4.2534 -.0034 1 0 2
4.0000 4.0015 -.0015 1 2 2
3.8200 3.8190 .0010 2 1 0
3.5700 3.5698 .0002 1 -2 1
3.1400 3.1389 .0011 2 3 2
3.0300 3.0296 .0004 0 -3 1
2.9500 2.9493 .0007 0 -2 2
A= 8.588 DA= .001
B= 11.403 DB= .002
C= 9.026 DC= .004
GAMMA= 69.059 DGAMMA= .008
BETA = 63.27 DBETA = .01
ALPHA= 72.784 DALPHA= .007
V= 727.5
2. 1-0126
Ni{PO4}2*8H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.8000 7.7762 .0238 0 1 1
6.6000 6.5749 .0251 -1 1 1
4.8000 4.7905 .0095 -2 1 1
4.4700 4.4715 -.0015 -1 1 2
4.0000 3.9949 .0051 -2 0 2
3.7800 3.7762 .0038 -2 1 2
3.5800 3.5838 -.0038 -3 1 1
3.1300 3.1276 .0024 3 2 1
2.9100 2.9082 .0018 4 1 0
2.6600 2.6617 -.0017 2 2 3
2.5600 2.5600 -.0000 0 1 4
2.4700 2.4706 -.0006 -3 3 2
a= 12.021 b=.001 c= 10.5026 beta= 91.18
da= .001 db=.005 dc=.0006 dbeta=.03
V= 1460.7
Triklin
Dexp Dcal d(D) h k l
7.8000 7.8029 -.0029 1 1 0
6.6000 6.6089 -.0089 0 0 1
4.8000 4.8065 -.0065 0 -2 1
4.4700 4.4659 .0041 -1 1 1
4.0000 3.9988 .0012 2 0 0
3.7800 3.7810 -.0010 -2 -1 1
3.5800 3.5821 -.0021 -2 0 1
3.1300 3.1304 -.0004 2 2 1
2.9100 2.9105 -.0005 -1 1 2
2.6600 2.6596 .0004 1 2 2
2.5600 2.5619 -.0019 -3 0 1
2.4700 2.4705 -.0005 2 4 1
A= 8.429 DA= .001
B= 13.019 DB= .003
C= 6.725 DC= .001
GAMMA= 72.47 DGAMMA= .01
BETA = 98.09 DBETA = .05
ALPHA= 99.03 DALPHA= .05
V= 691.5
3. 1-0200
NiCl2*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5000 5.5040 -.0040 2 0 1
4.8500 4.8415 .0085 -2 0 1
3.5300 3.5232 .0068 -2 0 3
3.0800 3.0806 -.0006 0 1 0
2.9500 2.9480 .0020 1 1 1
2.7000 2.7003 -.0003 0 1 3
2.5400 2.5392 .0008 4 0 4
2.4000 2.4007 -.0007 2 0 7
2.1800 2.1817 -.0017 3 1 4
2.0500 2.0506 -.0006 2 1 6
2.0200 2.0194 .0006 3 0 8
1.9700 1.9691 .0009 -4 1 4
a= 11.067 b= 3.0806 c= 17.250 beta= 77.32
da=.002 db=.0008 dc=.004 dbeta=.004
V= 573.8
Triklin
Dexp Dcal d(D) h k l
5.5000 5.4961 .0039 1 0 0
4.8500 4.8529 -.0029 0 0 1
3.5300 3.5339 -.0039 0 -2 1
3.0800 3.0794 .0006 1 -1 1
2.9500 2.9508 -.0008 -2 1 1
2.7000 2.6996 .0004 -2 2 1
2.5400 2.5394 .0006 0 3 1
2.4000 2.3997 .0003 0 -1 2
2.1800 2.1795 .0005 -1 4 1
2.0500 2.0512 -.0012 0 4 1
2.0200 2.0209 -.0009 -1 -3 2
1.9700 1.9701 -.0001 -3 2 1
A= 6.091 DA= .001
B= 9.608 DB= .003
C= 5.2931 DC= .0005
GAMMA=100.237 DGAMMA= .005
BETA =113.05 DBETA = .01
ALPHA= 90.45 DALPHA= .01
V= 279.5
4. 1-0204
Ni{NO3)2*6H2O
triklin
Dexp Dcal d(D) h k l
7.2000 7.1982 .0018 1 0 0
5.5000 5.5021 -.0021 0 1 1
5.1000 5.0960 .0040 0 -1 1
4.4000 4.3989 .0011 1 0 1
4.1400 4.1377 .0023 -1 0 2
3.7800 3.7802 -.0002 -1 2 0
3.4000 3.4016 -.0016 -2 2 1
3.1200 3.1197 .0003 -2 2 2
2.9000 2.9011 -.0011 2 1 0
2.7400 2.7394 .0006 -2 -1 2
2.6200 2.6189 .0011 -3 0 1
2.5500 2.5508 -.0008 -2 2 3
A= 8.5126 DA= .0001
B= 7.9539 DB= .0003
C= 8.580 DC= .001
GAMMA=111.86840 DGAMMA= .00003
BETA =117.336 DBETA = .007
ALPHA= 76.47 DALPHA= .01
V= 477.6
5. 1-0230
C4H4NiO6
Triklin
Dexp Dcal d(D) h k l
6.4000 6.3995 .0005 0 1 1
5.9000 5.9012 -.0012 0 -1 1
5.6000 5.6040 -.0040 1 0 1
5.2000 5.2079 -.0079 1 1 1
4.5300 4.5213 .0087 -1 1 1
4.0400 4.0402 -.0002 1 2 0
3.7000 3.7065 -.0065 1 1 2
3.4800 3.4750 .0050 -1 1 2
3.1300 3.1281 .0019 -2 1 0
3.0100 3.0100 .0000 -2 1 1
2.8500 2.8489 .0011 2 1 2
2.6400 2.6421 -.0021 -2 1 2
A= 7.538 DA= .002
B= 8.617 DB= .003
C= 9.029 DC= .002
GAMMA= 77.58 DGAMMA= .02
BETA = 90.95 DBETA = .01
ALPHA= 85.67 DALPHA= .05
V= 570.7
6. 1-0267
NiF2*4H2O
Triklin
Dexp Dcal d(D) h k l
4.8500 4.8454 .0046 1 1 0
4.1000 4.1003 -.0003 0 1 1
3.7800 3.7806 -.0006 0 -1 1
3.1100 3.1127 -.0027 0 0 2
2.9800 2.9788 .0012 -1 1 1
2.7500 2.7561 -.0061 0 1 2
2.5300 2.5345 -.0045 0 2 0
2.4400 2.4406 -.0006 2 2 1
2.3100 2.3079 .0021 3 1 1
2.2200 2.2170 .0030 1 2 2
2.1500 2.1519 -.0019 3 0 0
2.0000 2.0012 -.0012 3 2 0
A= 7.0166 DA= .0002
B= 5.4389 DB= .0008
C= 6.403 DC= .001
GAMMA= 69.261 DGAMMA= .007
BETA = 77.32 DBETA = .02
ALPHA= 81.19 DALPHA= .02
V=222.3
7. 1-0299
C2Ni6O4*2H2O
Rombik
Groupa 56
Dexp. Dcal. d(D) h k l
4.7200 4.7127 .0073 1 1 0
3.9000 3.9077 -.0077 0 2 0
2.9600 2.9538 .0062 2 0 0
2.5200 2.5179 .0021 0 1 2
2.1800 2.1752 .0048 1 3 1
2.0600 2.0606 -.0006 1 2 2
1.9100 1.9095 .0005 3 1 0
1.8600 1.8611 -.0011 0 3 2
1.5700 1.5709 -.0009 3 3 0
a= 5.908 b= 7.815 c= 5.319
da= .004 db= .002 dc= .001
V= 245.6
8. 1-0419
{NH4}2Ni{SO4}2*6H2O
Triklin
Dexp Dcal d(D) h k l
7.2000 7.1992 .0008 0 1 1
6.2000 6.2103 -.0103 1 0 1
5.4000 5.3915 .0085 0 -1 1
5.1000 5.0983 .0017 0 2 0
4.1600 4.1660 -.0060 -1 2 0
3.7600 3.7579 .0021 0 -2 1
3.5800 3.5875 -.0075 2 0 1
3.2900 3.2883 .0017 2 -1 1
3.1100 3.1052 .0048 2 0 2
3.0200 3.0205 -.0005 1 3 2
2.7800 2.7799 .0001 2 2 0
2.5400 2.5394 .0006 0 0 3
A= 7.2413 DA= .0002
B= 10.687 DB= .002
C= 8.4612 DC= .0006
GAMMA= 86.431 DGAMMA= .006
BETA = 70.364 DBETA = .003
ALPHA= 72.743 DALPHA= .008
V=588.5
9. 1-0489
Ni{BF4}2*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.6000 6.6171 -.0171 1 1 0
5.9000 5.8988 .0012 0 1 1
4.8900 4.8803 .0097 2 0 0
4.0900 4.0872 .0028 1 2 0
3.8000 3.7903 .0097 1 1 2
3.6000 3.5989 .0011 -2 0 1
3.3400 3.3417 -.0017 -2 1 1
3.0000 3.0005 -.0005 0 3 0
2.7700 2.7752 -.0052 1 0 3
2.6800 2.6812 -.0012 -3 0 1
2.6100 2.6109 -.0009 4 0 1
2.5200 2.5210 -.0010 3 0 3
a= 10.456 b= 9.001 c= 8.366 beta= 68.97
da=.001 db= .001 dc=.001 dbeta=.01
V= 735.0
Triklin
Dexp Dcal d(D) h k l
6.6000 6.5904 .0096 0 1 1
5.9000 5.8959 .0041 1 1 0
4.8900 4.8943 -.0043 0 -1 1
4.0900 4.0894 .0006 -1 -1 1
3.8000 3.8005 -.0005 -1 2 1
3.6000 3.6039 -.0039 2 0 1
3.3400 3.3368 .0032 0 -2 1
3.0000 2.9995 .0005 -1 2 2
2.7700 2.7692 .0008 -1 3 0
2.6800 2.6800 .0000 3 0 0
2.6100 2.6098 .0002 2 2 2
2.5200 2.5186 .0014 -2 -2 1
A= 8.056 DA= .002
B= 9.215 DB= .004
C= 7.513 DC= .004
GAMMA= 89.73 DGAMMA= .03
BETA = 86.48 DBETA = .02
ALPHA= 72.85 DALPHA= .01
V= 531.8
10. 1-0659
NiSO4*H2O
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
4.7700 4.7517 .0183 2 0 1
3.7900 3.7997 -.0097 0 0 4
3.3300 3.3350 -.0050 3 0 0
3.0200 3.0258 -.0058 2 0 4
2.5300 2.5331 -.0031 0 0 6
2.4800 2.4813 -.0013 0 2 2
2.3300 2.3308 -.0008 0 2 3
2.1700 2.1713 -.0013 0 0 7
2.0800 2.0758 .0042 2 1 6
2.0100 2.0064 .0036 0 1 7
1.9500 1.9488 .0012 1 2 5
1.8700 1.8698 .0002 5 1 0
a=10.00499 b= 5.250 c=15.199
da= .00005 db= .001 dc= .001
V= 798.4
Triklin
Dexp Dcal d(D) h k l
4.7700 4.7717 -.0017 1 0 0
3.7900 3.7870 .0030 -1 1 1
3.3300 3.3316 -.0016 1 -1 1
3.0200 3.0223 -.0023 1 0 2
2.5300 2.5307 -.0007 -1 -1 1
2.4800 2.4822 -.0022 -2 1 0
2.3300 2.3317 -.0017 -1 2 1
2.1700 2.1679 .0021 -1 2 2
2.0800 2.0793 .0007 0 -1 3
2.0100 2.0125 -.0025 0 -2 1
1.9500 1.9497 .0003 0 0 4
1.8700 1.8706 -.0006 -1 1 4
A= 5.0897 DA= .0004
B= 4.7296 DB= .0002
C= 7.93707 DC= .00009
GAMMA=110.368 DGAMMA= .001
BETA = 93.610 DBETA = .004
ALPHA= 79.3016 DALPHA= .0004
V=176.0
11. 1-1102
NiSO4
Monoklin
Dexp Dcal d(D) h k l
4.3000 4.3039 -.0039 -1 0 2
3.9200 3.9144 .0056 1 0 2
3.5800 3.5753 .0047 -2 0 2
3.3300 3.3289 .0011 1 1 2
3.1500 3.1499 .0001 2 0 2
2.5500 2.5492 .0008 -1 2 2
2.3300 2.3291 .0009 4 1 0
2.0000 2.0001 -.0001 1 3 1
1.9600 1.9596 .0004 -4 2 1
1.8700 1.8698 .0002 2 1 4
1.7800 1.7794 .0006 -2 2 4
1.6700 1.6699 .0001 6 0 0
a= 10.101 b= 6.32778 c= 9.047 beta= 97.28
da= 4.285812E-03 db=.00009 dc=.002 dbeta=.01
V= 573.6
Triklin
Dexp Dcal d(D) h k l
4.3000 4.3008 -.0008 1 0 0
3.9200 3.9182 .0018 -1 1 0
3.5800 3.5803 -.0003 -1 0 1
3.3300 3.3328 -.0028 1 1 0
3.1500 3.1467 .0033 0 -1 2
2.5500 2.5466 .0034 1 -1 2
2.3300 2.3312 -.0012 0 1 2
2.0000 1.9997 .0003 1 2 1
1.9600 1.9597 .0003 2 -2 1
1.8700 1.8700 -.0000 -1 -3 2
1.7800 1.7802 -.0002 2 -1 2
1.6700 1.6704 -.0004 2 0 2
A= 4.3679 DA= .0003
B= 7.180 DB= .003
C= 6.304 DC= .002
GAMMA= 99.17 DGAMMA= .04
BETA = 90.25 DBETA = .01
ALPHA=112.75 DALPHA= .02
V= 179.5
12. 2-0060
{Ni,Mg}3Si2O5{OH}
Groupa 27
Dexp. Dcal. d(D) h k l
9.8000 9.9331 -.1331 1 0 0
6.9000 6.9698 -.0698 0 1 0
4.5000 4.4677 .0323 1 1 1
3.5900 3.5918 -.0018 0 0 2
3.1900 3.1928 -.0028 0 1 2
2.8600 2.8527 .0073 2 2 0
2.6500 2.6513 -.0013 2 2 1
2.4000 2.4004 -.0004 3 2 0
1.6800 1.6807 -.0007 3 3 2
1.5200 1.5198 .0002 2 2 4
1.3100 1.3100 .0000 5 4 0
a= 9.93 b= 6.970 c= 7.184
da= .02 db= .009 dc= .005
V= 497
13. 2-0125
NiAs2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.4000 6.4400 -.0400 2 0 0
3.5400 3.5503 -.0103 0 0 3
3.1700 3.1745 -.0045 1 1 0
2.8200 2.8158 .0042 2 1 1
2.7500 2.7555 -.0055 4 0 2
2.5300 2.5297 .0003 3 1 1
2.4600 2.4607 -.0007 2 0 4
2.3200 2.3190 .0010 5 0 2
2.1300 2.1302 -.0002 0 0 5
1.9700 1.9674 .0026 2 1 4
1.9100 1.9082 .0018 3 0 5
1.7800 1.7766 .0034 4 0 5
a=12.8801 b= 3.2756 c=10.651
da= .0009 db= .0006 dc= .003
V= 449.4
Triklin
Dexp Dcal d(D) h k l
6.4000 6.4014 -.0014 1 0 0
3.5400 3.5391 .0009 -1 1 1
3.1700 3.1673 .0027 -1 -1 1
2.8200 2.8210 -.0010 -2 1 0
2.7500 2.7508 -.0008 0 -1 2
2.5300 2.5293 .0007 1 1 1
2.4600 2.4610 -.0010 0 1 2
2.3200 2.3201 -.0001 -2 -1 2
2.1300 2.1338 -.0038 3 0 0
1.9700 1.9708 -.0008 0 2 0
1.9100 1.9102 -.0002 -2 0 4
1.7800 1.7796 .0004 -3 0 4
A= 7.2888 DA= .0009
B= 4.0495 DB= .0001
C= 7.684 DC= .003
GAMMA=101.6340 DGAMMA= .0004
BETA =115.55 DBETA = .09
ALPHA= 90.69 DALPHA= .01
V= 199.2
14. 2-0354
Ni3Si2{OH}4
Triklin
Dexp Dcal d(D) h k l
4.3500 4.3503 -.0003 1 0 1
3.8300 3.8275 .0025 0 -1 1
3.6300 3.6297 .0003 1 0 2
2.6300 2.6285 .0015 1 -1 3
2.4300 2.4265 .0035 -1 -1 1
2.2500 2.2502 -.0002 1 -2 1
2.1500 2.1497 .0003 -1 -1 2
1.9000 1.9002 -.0002 1 -2 3
1.7700 1.7701 -.0001 0 1 5
1.7300 1.7296 .0004 0 -2 3
1.6900 1.6901 -.0001 1 -2 4
1.6300 1.6300 -.0000 -1 -1 4
A= 4.8203 DA= .0004
B= 4.6141 DB= .0003
C= 9.70 DC= .01
GAMMA=111.42 DGAMMA= .05
BETA = 77.91 DBETA = .08
ALPHA= 91.47 DALPHA= .04
V= 196.2
15. 2-0622
{Pt,Pd,Ni}5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.4500 3.4484 .0016 -2 0 1
3.0300 3.0275 .0025 2 1 0
2.8900 2.8942 -.0042 0 2 0
2.4700 2.4701 -.0001 1 2 1
1.9300 1.9295 .0005 0 3 0
1.7700 1.7701 -.0001 0 1 4
1.7400 1.7400 .0000 -3 2 2
1.5400 1.5402 -.0002 2 0 4
1.5100 1.5097 .0003 -1 0 5
1.3100 1.3098 .0002 1 4 2
1.2400 1.2400 .0000 -3 2 5
1.1600 1.1600 .0000 6 1 0
a= 7.2154 b= 5.7884 c=7.553 beta=100.07
da=.0004 db=.0004 dc=.001 dbeta=.01
V= 310.6
Triklin
Dexp Dcal d(D) h k l
3.4500 3.4500 .0000 1 1 0
3.0300 3.0302 -.0002 1 2 0
2.8900 2.8903 -.0003 -1 0 1
2.4700 2.4700 .0000 -1 -2 1
1.9300 1.9301 -.0001 -1 0 2
1.7700 1.7699 .0001 2 1 0
1.7400 1.7399 .0001 0 4 2
1.5400 1.5400 -.0000 -2 -3 1
1.5100 1.5107 -.0007 2 3 1
1.3100 1.3099 .0001 1 6 2
1.2400 1.2400 .0000 0 -7 1
1.1600 1.1600 .0000 0 6 3
A= 3.5630 DA= .0001
B= 9.75 DB= .01
C= 4.346 DC= .001
GAMMA= 83.29 DGAMMA= .09
BETA = 95.91 DBETA = .03
ALPHA= 81.23 DALPHA= .02
V= 147.0
16. 2-0810
Ni2Te3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.3300 3.3304 -.0004 2 1 1
2.8200 2.8204 -.0004 1 2 1
2.6300 2.6304 -.0004 3 0 1
2.3500 2.3504 -.0004 0 0 3
2.0800 2.0803 -.0003 0 3 0
2.0300 2.0293 .0007 -3 0 1
1.9300 1.9298 .0002 -3 1 1
1.5900 1.5898 .0002 4 2 3
1.5600 1.5602 -.0002 0 4 0
1.4400 1.4402 -.0002 5 0 0
1.4100 1.4102 -.0002 0 0 5
1.3200 1.3184 .0016 5 0 5
a= 7.918 b= 6.2409 c= 7.7539 beta= 65.41
da=.001 db=.0006 dc=.002 dbeta=.01
V= 348.5
Triklin
Dexp Dcal d(D) h k l
3.3300 3.3319 -.0019 0 1 0
2.8200 2.8198 .0002 0 -1 2
2.6300 2.6307 -.0007 -1 1 0
2.3500 2.3468 .0032 1 -1 2
2.0800 2.0805 -.0005 -1 0 3
2.0300 2.0307 -.0007 1 1 0
1.9300 1.9296 .0004 1 1 1
1.5900 1.5903 -.0003 0 -1 5
1.5600 1.5606 -.0006 2 -1 1
1.4400 1.4395 .0005 -2 1 2
1.4100 1.4099 .0001 0 -2 4
1.3200 1.3198 .0002 -1 -2 2
A= 3.216 DA= .001
B= 3.4870 DB= .0002
C= 8.43332 DC= .00008
GAMMA=104.810 DGAMMA= .01
BETA = 88.22 DBETA = .01
ALPHA= 98.93 DALPHA= .01
V= 90.3
17. 2-0962
{Co,Ni}As2
Triklin
Dexp Dcal d(D) h k l
6.0000 6.0003 -.0003 1 1 0
4.2000 4.2011 -.0011 -1 -1 1
3.4000 3.4006 -.0006 -1 -3 1
2.9000 2.9006 -.0006 -1 -4 1
2.6400 2.6400 -.0000 1 -3 1
2.2200 2.2196 .0004 2 2 1
2.0700 2.0702 -.0002 3 0 0
1.9500 1.9501 -.0001 -2 -4 2
1.8700 1.8701 -.0001 -1 -7 1
1.7700 1.7697 .0003 -2 -7 1
1.6900 1.6902 -.0002 2 -5 1
1.6300 1.6303 -.0003 2 1 2
A= 6.5123 DA= .0003
B= 13.48052 DB= .00003
C= 4.67245 DC= .00003
GAMMA= 78.5469 DGAMMA= .0007
BETA =104.896 DBETA = .002
ALPHA=100.026 DALPHA= .008
V= 385.2
18. 2-0971
Ni{Sb,Bi}S
Triklin
Dexp Dcal d(D) h k l
4.1500 4.1565 -.0065 0 1 1
3.4100 3.4102 -.0002 0 -1 1
2.9300 2.9307 -.0007 -1 0 1
2.6200 2.6236 -.0036 -1 1 1
2.4000 2.4014 -.0014 0 0 2
2.3200 2.3200 .0000 0 -2 1
2.0800 2.0793 .0007 -1 2 1
1.9800 1.9811 -.0011 -1 0 2
1.8700 1.8706 -.0006 2 0 1
1.7800 1.7786 .0014 2 2 0
1.7000 1.6992 .0008 0 3 2
1.6300 1.6296 .0004 0 1 3
A= 4.01186 DA= .00006
B= 6.1438 DB= .0002
C= 4.93455 DC= .00001
GAMMA= 79.267 DGAMMA= .004
BETA = 83.371 DBETA = .005
ALPHA= 77.513 DALPHA= .002
V=116.3
19. 2-1028
{Ni,Fe}AsS
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
2.8500 2.8544 -.0044 0 2 0
2.5500 2.5568 -.0068 1 2 0
2.3300 2.3315 -.0015 1 2 1
2.0100 2.0133 -.0033 0 2 2
1.9000 1.9002 -.0002 1 2 2
1.7200 1.7216 -.0016 1 3 1
1.6500 1.6492 .0008 2 2 2
1.5800 1.5814 -.0014 2 0 3
1.5300 1.5284 .0016 2 3 1
1.2700 1.2714 -.0014 0 2 4
1.2400 1.2414 -.0014 1 2 4
1.2200 1.2197 .0003 3 3 2
a= 5.751 b= 5.709 c= 5.680
da= .006 db= .001 dc= .007
v= 186.5
Triklin
Dexp Dcal d(D) h k l
2.8500 2.8526 -.0026 -1 1 1
2.5500 2.5488 .0012 -1 0 1
2.3300 2.3289 .0011 1 -1 1
2.0100 2.0113 -.0013 -1 2 0
1.9000 1.8995 .0005 -1 1 2
1.7200 1.7183 .0017 -1 -1 1
1.6500 1.6501 -.0001 -1 2 2
1.5800 1.5809 -.0009 1 -1 2
1.5300 1.5301 -.0001 -2 0 1
1.2700 1.2696 .0004 1 -2 2
1.2400 1.2395 .0005 -1 0 3
1.2200 1.2203 -.0003 -3 2 1
A= 3.749 DA= .001
B= 4.1860 DB= .0009
C= 4.1695 DC= .0005
GAMMA=117.53 DGAMMA= .01
BETA = 96.28 DBETA = .04
ALPHA= 75.002 DALPHA= .005
V=56.05
20. 2-1029
Ni{As,Sb}S
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
2.8500 2.8495 .0005 0 0 3
2.5500 2.5427 .0073 1 1 1
2.3300 2.3309 -.0009 2 1 1
2.0200 2.0207 -.0007 5 0 0
1.9100 1.9101 -.0001 3 1 2
1.7100 1.7097 .0003 0 0 5
1.6500 1.6483 .0017 5 0 3
1.5700 1.5667 .0033 6 0 2
1.5100 1.5105 -.0005 3 1 4
1.4000 1.3969 .0031 2 1 5
1.2400 1.2410 -.0010 4 0 6
1.2100 1.2112 -.0012 8 0 2
a=10.104 b= 2.761 c= 8.548
da= .003 db= .002 dc= .001
V= 238.5
Triklin
Dexp Dcal d(D) h k l
2.8500 2.8482 .0018 1 1 0
2.5500 2.5486 .0014 0 1 1
2.3300 2.3322 -.0022 0 -1 1
2.0200 2.0203 -.0003 1 2 0
1.9100 1.9095 .0005 0 2 1
1.7100 1.7103 -.0003 -1 -1 1
1.6500 1.6511 -.0011 2 0 0
1.5700 1.5698 .0002 0 3 0
1.5100 1.5094 .0006 -2 1 0
1.4000 1.3996 .0004 0 1 2
1.2400 1.2401 -.0001 -2 0 1
1.2100 1.2098 .0002 -2 -1 1
A= 3.605 DA= .001
B= 4.791 DB= .001
C= 3.101 DC= .001
GAMMA= 81.12 DGAMMA= .01
BETA = 67.11 DBETA = .02
ALPHA= 81.31 DALPHA= .02
V= 48.5
21. 2-1037
NiAs2
Triklin
Dexp Dcal d(D) h k l
3.6700 3.6689 .0011 -1 -1 1
2.9900 2.9915 -.0015 -1 1 0
2.8890 2.8883 .0007 -1 -1 2
2.8100 2.8105 -.0005 1 -1 1
2.5300 2.5289 .0011 -1 -2 1
2.4600 2.4630 -.0030 0 1 4
2.3800 2.3779 .0021 0 2 3
2.2100 2.2109 -.0009 -2 0 1
2.0700 2.0713 -.0013 -1 0 4
2.0200 2.0171 .0029 -2 0 2
1.8800 1.8793 .0007 1 0 5
1.8000 1.8011 -.0011 -2 -1 3
A= 5.1973 DA= .0005
B= 6.145 DB= .001
C= 10.36236 DC= .00002
GAMMA= 64.43 DGAMMA= .01
BETA = 76.637 DBETA = .005
ALPHA= 71.699 DALPHA= .004
V=281.6
22. 2-1348
Ni3Se2
Triklin
Dexp Dcal d(D) h k l
4.2600 4.2614 -.0014 -1 0 1
3.0200 3.0200 -.0000 1 2 0
2.9800 2.9802 -.0002 -1 -2 1
2.7300 2.7308 -.0008 0 0 2
2.4600 2.4600 .0000 -2 -1 1
2.4200 2.4178 .0022 1 -1 2
2.1200 2.1204 -.0004 0 -4 1
1.9000 1.8998 .0002 -2 2 2
1.8800 1.8805 -.0005 0 -4 2
1.8300 1.8298 .0002 0 -2 3
1.7300 1.7288 .0012 -1 -4 2
1.7100 1.7107 -.0007 1 -2 3
A= 5.790 DA= .003
B= 8.7801 DB= .0009
C= 5.6463 DC= .0007
GAMMA=102.09 DGAMMA= .01
BETA = 96.39 DBETA = .04
ALPHA=101.525 DALPHA= .001
V= 271.5