1. 41-0781
Nb3Si2
Triklin
Dexp Dcal d(D) h k l
3.4900 3.4935 -.0035 1 0 0
2.8100 2.8086 .0014 1 2 0
2.4670 2.4666 .0004 -1 0 1
2.4200 2.4195 .0005 -1 3 0
2.3550 2.3543 .0007 1 3 0
2.2270 2.2269 .0001 -1 -2 1
2.2050 2.2047 .0003 1 2 1
2.1800 2.1803 -.0003 -1 2 1
2.0820 2.0810 .0010 1 -3 1
1.7470 1.7467 .0003 2 0 0
1.5100 1.5101 -.0001 1 2 2
1.4770 1.4769 .0001 -2 2 1
A= 3.4971 DA= .0005
B= 9.83 DB= .03
C= 3.6161 DC= .0009
GAMMA= 91.71 DGAMMA= .05
BETA = 87.91 DBETA = .01
ALPHA= 93.89 DALPHA= .02
V= 123.9
2. 41-1225
Fe0.55Nb0.67
Triklin
Dexp Dcal d(D) h k l
4.2336 4.2343 -.0007 -1 -1 1
2.4899 2.4900 -.0001 -2 -1 2
2.3379 2.3367 .0012 3 -2 1
2.2898 2.2908 -.0010 -3 -2 1
2.2567 2.2564 .0003 -4 2 0
2.2245 2.2252 -.0007 0 -2 2
2.1775 2.1788 -.0013 -3 1 2
2.1407 2.1404 .0003 2 2 1
2.0547 2.0562 -.0015 -5 -1 1
2.0303 2.0295 .0008 -1 -3 1
2.0020 2.0027 -.0007 -4 1 2
1.9148 1.9151 -.0003 3 2 1
A= 11.482 DA= .004
B= 6.458 DB= .001
C= 5.436 DC= .001
GAMMA= 96.22 DGAMMA= .01
BETA =100.102 DBETA = .004
ALPHA= 98.84 DALPHA= .01
V= 388.3
3. 42-0622
K4Cu2Nb6O19*9H2O
Triklin
Dexp Dcal d(D) h k l
9.3400 9.3422 -.0022 0 1 0
8.7000 8.6986 .0014 0 1 1
8.0400 8.0401 -.0001 1 0 1
7.8000 7.7986 .0014 0 -1 1
5.7100 5.7061 .0039 1 -1 2
5.2000 5.2014 -.0014 0 1 3
3.5900 3.5899 .0001 -1 2 3
3.2900 3.2899 .0001 2 1 3
3.1300 3.1302 -.0002 2 -2 3
3.0300 3.0299 .0001 -2 0 3
2.8500 2.8501 -.0001 -1 -2 3
2.7400 2.7400 .0000 1 -2 5
2.6800 2.6800 -.0000 3 0 3
2.5900 2.5900 .0000 -1 -3 1
A= 8.54646 DA= .00002
B= 9.6767 DB= .0005
C= 17.6792 DC= .0004
GAMMA=103.184 DGAMMA= .006
BETA = 79.252 DBETA = .002
ALPHA= 85.325 DALPHA= .001
V= 1386.8
4. 42-0623
K16H2Cu7Nb12O38*39H2O
Triklin
Dexp Dcal d(D) h k l
9.3000 9.2407 .0593 0 1 0
8.7500 8.7487 .0013 1 0 0
8.0300 8.0203 .0097 1 1 0
7.7500 7.7402 .0098 1 0 1
5.7100 5.7087 .0013 0 -1 1
5.2100 5.2140 -.0040 -1 0 1
3.5400 3.5391 .0009 3 1 1
3.2900 3.2901 -.0001 2 1 3
3.2700 3.2693 .0007 1 3 2
3.0500 3.0494 .0006 2 -1 2
2.8300 2.8303 -.0003 3 3 3
2.7300 2.7300 -.0000 1 -2 2
2.6700 2.6706 -.0006 2 -2 1
2.5800 2.5801 -.0001 3 0 3
2.4900 2.4902 -.0002 4 3 1
A= 10.89 DA= .01
B= 10.903 DB= .005
C= 10.10 DC= .01
GAMMA= 60.09 DGAMMA= .07
BETA = 59.98 DBETA = .09
ALPHA= 66.00 DALPHA= .08
V= 880.26
5. 42-0624
{NH4}6Cu{NH3}4Cu4Nb12O38*22H2O
Triklin
Dexp Dcal d(D) h k l
27.7600 27.7442 .0158 1 0 0
9.7700 9.7598 .0102 2 1 0
8.6600 8.6593 .0007 1 1 1
7.7900 7.7895 .0005 -2 0 1
6.6000 6.6070 -.0070 -3 0 1
6.3400 6.3395 .0005 -3 1 1
6.1000 6.0979 .0021 -2 -1 1
4.9100 4.9101 -.0001 0 1 2
4.3100 4.3101 -.0001 -3 1 2
4.1600 4.1600 -.0000 3 0 2
4.1200 4.1201 -.0001 3 3 1
3.9800 3.9796 .0004 -4 1 2
A= 27.80 DA= .01
B= 13.582 DB= .007
C= 9.8370 DC= .0001
GAMMA= 86.33 DGAMMA= .04
BETA = 89.35 DBETA = .01
ALPHA= 72.05 DALPHA= .01
V=3526
6. 42-0625
Cu{NH3}Cu5Nb4O16*19H2O
Triklin
Dexp Dcal d(D) h k l
14.7100 14.7154 -.0054 1 0 0
10.3900 10.3988 -.0088 0 1 0
8.9000 8.9047 -.0047 1 1 1
8.5300 8.5279 .0021 -1 0 1
7.5500 7.5544 -.0044 1 -1 1
6.5700 6.5720 -.0020 1 1 2
6.0200 6.0178 .0022 2 1 2
4.9900 4.9894 .0006 0 2 1
4.9200 4.9200 .0000 3 1 2
4.7600 4.7595 .0005 0 -2 1
4.1300 4.1301 -.0001 -3 0 1
3.4000 3.4001 -.0001 4 2 1
A= 16.298 DA= .003
B= 10.553 DB= .005
C= 15.35 DC= .01
GAMMA= 81.11 DGAMMA= .04
BETA = 65.32 DBETA = .01
ALPHA= 82.59 DALPHA= .07
V= 2363.9
7. 42-0768
Co7Nb2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
2.9800 2.9776 .0024 1 1 0
2.6300 2.6286 .0014 3 0 1
2.5700 2.5668 .0032 -1 1 2
2.2900 2.2904 -.0004 2 1 3
2.0400 2.0402 -.0002 3 1 1
1.9960 1.9957 .0003 3 1 0
1.9760 1.9735 .0024 4 0 2
1.9250 1.9253 -.0003 -3 0 3
1.5650 1.5648 .0002 -4 0 3
1.4590 1.4591 -.0001 -2 2 1
1.4370 1.4364 .0006 1 2 4
1.4200 1.4198 .0002 5 1 2
a=7.9020 b= 3.236 c=12.592 beta= 74.26
da=.0002 db=.001 dc=.009 dbeta=.02
V= 309.9
8. 42-0770
NbO2.4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
14.4000 14.4213 -.0213 1 0 0
9.7200 9.6870 .0330 1 1 0
7.2300 7.2107 .0193 2 0 0
5.1800 5.1807 -.0007 -1 0 2
5.1100 5.1144 -.0044 1 2 1
4.8600 4.8582 .0018 1 0 2
4.8100 4.8164 -.0064 -1 1 2
3.7330 3.7302 .0028 2 3 0
3.6010 3.6053 -.0043 4 0 0
3.5620 3.5632 -.0012 0 0 3
3.4780 3.4765 .0015 2 2 2
3.4370 3.4379 -.0009 0 1 3
a= 14.49 b= 13.076 c=10.742 beta=95.64
da= .01 db=.001 dc=.009 dbeta=.02
V= 2026
Triklin
Dexp Dcal d(D) h k l
14.4000 14.1862 .2138 0 0 1
9.7200 9.7198 .0002 1 0 0
7.2300 7.2310 -.0010 0 1 1
5.1800 5.1802 -.0002 -2 -1 1
5.1100 5.1111 -.0011 2 1 1
4.8600 4.8599 .0001 2 0 0
4.8100 4.8107 -.0007 2 0 1
3.7330 3.7332 -.0002 -2 -2 3
3.6010 3.6011 -.0001 0 -3 1
3.5620 3.5619 .0001 1 -2 3
3.4780 3.4774 .0006 -3 -1 1
3.4370 3.4371 -.0001 -2 1 1
A= 11.045 DA= .003
B= 12.2132 DB= .0007
C= 15.055 DC= .006
GAMMA= 62.744 DGAMMA= .008
BETA = 91.21 DBETA = .04
ALPHA=107.86 DALPHA= .04
V= 1701
9. 43-0787
Ni7Nb12O37*2H2O
Triklin
Dexp Dcal d(D) h k l
4.6600 4.6546 .0054 0 0 1
4.1000 4.0985 .0015 -1 0 1
3.7300 3.7301 -.0001 0 -2 1
3.3100 3.3123 -.0023 -1 -2 1
3.1300 3.1290 .0010 0 -3 1
2.9800 2.9781 .0019 1 2 1
2.8300 2.8293 .0007 -2 1 1
2.7200 2.7198 .0002 -2 2 1
2.4100 2.4098 .0002 1 -4 1
2.3600 2.3605 -.0005 2 0 1
2.2200 2.2203 -.0003 0 2 2
2.0600 2.0605 -.0005 -2 1 2
A= 6.2873 DA= .0008
B= 13.245 DB= .005
C= 4.7497 DC= .00052
GAMMA= 97.37 DGAMMA= .02
BETA =101.286 DBETA = .002
ALPHA= 86.442 DALPHA= .001
V=384.5
10. 44-0468
Nb60WO153
Triklin
Dexp Dcal d(D) h k l
16.2000 15.8663 .3337 0 1 0
13.9300 13.9362 -.0062 1 0 0
10.7300 10.7368 -.0068 0 1 1
8.9600 8.9637 -.0037 0 -1 1
8.1000 8.1039 -.0039 -1 0 1
6.3700 6.3735 -.0035 2 -1 1
5.3600 5.3601 -.0001 -2 1 1
5.1000 5.0978 .0022 -1 0 2
4.7970 4.8005 -.0035 -2 2 1
4.6450 4.6454 -.0004 3 0 0
3.7420 3.7418 .0002 -3 -1 1
3.6380 3.6371 .0009 -3 3 0
A= 14.6123 DA= .0005
B= 16.1484 DB= .0003
C= 13.101 DC= .001
GAMMA= 91.509 DGAMMA= .007
BETA = 73.098 DBETA = .006
ALPHA= 80.296 DALPHA= .009
V=2906.2
11. 44-0531
NaNbOF4
Triklin
Dexp Dcal d(D) h k l
5.6870 5.6808 .0062 0 1 1
5.3270 5.3430 -.0160 1 0 1
5.0790 5.0746 .0044 0 -1 1
4.8680 4.8602 .0078 1 -1 1
4.7190 4.7165 .0025 -1 2 1
4.5420 4.5380 .0040 0 3 0
4.0220 4.0150 .0070 3 1 0
3.9030 3.9055 -.0025 -2 -1 1
3.6860 3.6866 -.0006 2 2 1
3.4660 3.4684 -.0024 2 3 0
3.2360 3.2371 -.0011 -4 2 0
3.1750 3.1765 -.0015 -3 3 1
A= 13.5694 DA= .0008
B= 14.0217 DB= .0006
C= 5.89429 DC= .00007
GAMMA=100.63 DGAMMA= .01
BETA = 91.44 DBETA = .01
ALPHA= 80.95 DALPHA= .01423
V=1089
12. 44-1000
NaNb2{SO4}6*xH2O
Triklin
Dexp Dcal d(D) h k l
4.9800 4.9771 .0029 0 0 1
4.5200 4.5173 .0027 0 -2 1
3.5000 3.4978 .0022 1 -1 1
3.2500 3.2481 .0019 1 3 0
3.1700 3.1678 .0022 1 -3 1
2.8500 2.8467 .0033 -1 1 1
2.7500 2.7521 -.0021 -1 -2 1
2.3200 2.3206 -.0006 1 -2 2
2.0800 2.0797 .0003 1 3 2
2.0100 2.0101 -.0001 2 -2 1
1.9250 1.9251 -.0001 2 2 1
1.8880 1.8877 .0003 0 -9 1
A= 4.1457 DA= .0004
B= 17.8212 DB= .0003
C= 5.097 DC= .001
GAMMA= 94.711 DGAMMA= .006
BETA = 78.683 DBETA = .004
ALPHA= 96.06 DALPHA= .01
V= 366.47
13. 45-0161
LiNbOF4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.9400 4.9365 .0035 1 1 0
4.2700 4.2701 -.0001 1 0 2
3.8800 3.8850 -.0050 2 0 0
3.5500 3.5508 -.0008 1 1 2
3.4600 3.4550 .0050 2 1 1
3.2000 3.1962 .0038 0 2 0
3.1100 3.1104 -.0004 -2 0 1
2.7600 2.7618 -.0018 3 0 1
2.6700 2.6674 .0026 -1 2 1
2.1300 2.1308 -.0008 0 3 0
2.0900 2.0897 .0003 3 2 1
1.9500 1.9503 -.0003 -1 3 1
1.7700 1.7701 -.0001 -1 3 2
a= 8.290 b= 6.392 c= 8.689 beta= 69.59
da=.005 db=.002 dc=.006 dbeta=.06
V= 431.6
14. 45-0162
LiNbOF4
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
4.2600 4.2646 -.0046 1 2 0
3.8700 3.8782 -.0082 2 1 1
3.5500 3.5478 .0022 3 1 0
3.1000 3.1004 -.0004 3 1 1
2.7600 2.7587 .0013 0 3 1
2.6700 2.6704 -.0004 2 1 2
2.1400 2.1394 .0006 4 0 2
2.0900 2.0908 -.0008 1 0 3
1.9500 1.9494 .0006 2 1 3
1.7700 1.7702 -.0002 5 3 1
a=11.540 b= 9.1790 c= 6.378
da= .003 db= .0001 dc= .001
V= 675.6
15. 45-1083
Li19KNb20O60
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
3.7430 3.7475 -.0045 0 1 2
2.7310 2.7344 -.0034 0 1 4
2.5690 2.5716 -.0026 1 0 0
2.2450 2.2467 -.0017 1 0 3
2.1210 2.1210 -.0000 0 2 2
1.8730 1.8733 -.0003 1 1 4
1.7180 1.7179 .0001 1 0 6
1.6370 1.6363 .0007 1 2 2
1.6140 1.6139 .0001 0 1 8
1.5150 1.5144 .0006 1 2 4
1.4850 1.4854 -.0004 0 3 0
a= 2.5716 b= 4.456 c=13.852
da= .0009 db= .001 dc= .002
V= 158.7
16. 45-1084
Li9KNb10O30
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
3.7420 3.7472 -.0052 0 1 2
2.7320 2.7343 -.0023 0 1 4
2.5720 2.5721 -.0001 1 0 0
2.2470 2.2470 -.0000 1 0 3
2.1200 2.1206 -.0006 1 1 2
1.8740 1.8736 .0004 0 2 4
1.7180 1.7182 -.0002 1 0 6
1.6360 1.6363 -.0003 1 2 2
1.6140 1.6140 .0000 0 1 8
1.5150 1.5144 .0006 1 2 4
1.4850 1.4851 -.0001 0 3 0
a= 2.5721 b= 4.4554 c=13.853
da= .0009 db= .0008 dc= .002
V= 158.7
17. 45-1085
Li4KNb5O15
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
3.7670 3.7572 .0098 2 1 0
2.7440 2.7415 .0025 4 1 0
2.5820 2.5800 .0020 0 0 1
2.2540 2.2536 .0004 3 0 1
2.1280 2.1265 .0015 2 2 0
1.8790 1.8786 .0004 4 2 0
1.7230 1.7229 .0001 6 0 1
1.6410 1.6409 .0001 2 2 1
1.6180 1.6182 -.0002 8 1 0
1.5180 1.5186 -.0006 4 2 1
1.4890 1.4892 -.0002 0 3 0
a=13.888 b= 4.4675 c= 2.580
da= .001 db= .0007 dc= .001
V=160.1
18. 45-1198
BiNbS3
Geksag.
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
11.5500 11.5049 .0451 0 0 1
5.7600 5.7525 .0075 0 0 2
3.8390 3.8350 .0040 0 0 3
2.8780 2.8762 .0018 0 0 4
2.3010 2.3010 .0000 0 0 5
1.9180 1.9175 .0005 0 0 6
1.6394 1.6394 .0000 2 0 4
1.4379 1.4381 -.0002 0 0 8
a= 4.6078 c= 11.505
da=.0005 dc=.002
V= 211.54
Rombik
Groupa 39,67
Dexp. Dcal. d(D) h k l
11.5500 11.5037 .0463 1 0 0
5.7600 5.7519 .0081 2 0 0
3.8390 3.8362 .0028 0 2 0
2.8780 2.8759 .0021 4 0 0
2.3010 2.3011 -.0001 4 2 0
1.9180 1.9181 -.0001 0 4 0
1.6394 1.6394 .0000 2 3 1
1.4379 1.4380 -.0001 8 0 0
a=11.504 b= 7.6723 c= 2.3005
da= .003 db= .0006 dc= .0002
V=203.05
19. 46-0092
Li8Nb2O9
Triklin
Dexp Dcal d(D) h k l
8.2400 8.2291 .0109 1 0 0
6.3200 6.3277 -.0077 0 1 1
4.9700 4.9738 -.0038 0 -1 1
4.5500 4.5498 .0002 0 2 0
4.2700 4.2631 .0069 -2 0 1
4.1100 4.1146 -.0046 2 0 0
4.0100 4.0084 .0016 2 1 0
3.8250 3.8268 -.0018 -2 1 1
3.7320 3.7352 -.0032 1 2 1
3.3420 3.3414 .0006 2 2 0
3.2900 3.2929 -.0029 -2 0 2
2.8010 2.8011 -.0001 -2 2 2
A= 8.831 DA= .005
B= 9.422 DB= .001
C= 7.600 DC= .001
GAMMA= 84.93 DGAMMA= .01
BETA =109.09 DBETA = .01
ALPHA= 78.385 DALPHA= .007
V= 577.1
20. 46-1084
NbRbF4O
Triklin
Dexp Dcal d(D) h k l
5.6260 5.6102 .0158 0 1 1
5.4980 5.4988 -.0008 0 -1 1
4.4840 4.4833 .0007 1 0 1
3.9510 3.9527 -.0017 1 0 2
3.5420 3.5399 .0021 1 -1 1
3.4770 3.4710 .0060 -1 1 1
3.3880 3.3875 .0005 1 1 2
3.2550 3.2495 .0055 1 -1 2
3.1780 3.1822 -.0042 -1 -1 2
2.8190 2.8225 -.0035 1 0 4
2.7510 2.7494 .0016 0 -2 2
2.5890 2.5887 .0003 1 2 0
A= 4.65209 DA= .00001
B= 6.10119 DB= .00001
C= 13.52103 DC= .00001
GAMMA= 87.88368 DGAMMA= .00002
BETA = 85.91257 DBETA = .00006
ALPHA= 88.32980 DALPHA= .00003
V=382.4
21. 47-0366
Na2.6Cu1.0Nb11.0O30
Triklin
Dexp Dcal d(D) h k l
11.8210 11.8240 -.0030 1 0 0
11.6420 11.6398 .0022 -1 1 0
10.3220 10.3145 .0075 1 0 1
9.3410 9.3398 .0012 0 2 0
8.8910 8.8888 .0022 1 1 0
8.5650 8.5921 -.0271 0 2 1
7.4460 7.4325 .0135 -1 0 1
7.4180 7.4325 -.0145 -1 0 1
7.1060 7.1113 -.0053 -1 2 1
6.3750 6.3574 .0176 0 1 2
6.1370 6.1422 -.0052 2 0 1
5.5420 5.5428 -.0008 1 2 2
A= 12.8036 DA= .0008
B= 19.8673 DB= .0005
C= 13.2057 DC= .0009
GAMMA=103.202 DGAMMA= .009
BETA = 74.880 DBETA = .006
ALPHA= 79.376 DALPHA= .004
V=3050
22. 47-1385
Nb2SnSe5
Tetrag.
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
9.2810 9.2812 -.0002 0 0 1
6.1510 6.1758 -.0248 1 0 0
4.6330 4.6406 -.0076 0 0 2
3.7110 3.7100 .0010 1 0 2
3.0890 3.0879 .0011 2 0 0
2.6470 2.6472 -.0002 2 1 1
2.3170 2.3203 -.0033 0 0 4
2.0600 2.0603 -.0003 2 1 3
1.8530 1.8550 -.0020 2 0 4
1.6850 1.6844 .0006 3 2 1
1.5480 1.5469 .0011 0 0 6
a= 6.1758 c= 9.28
da= .00085 dc= .01
v= 353.99
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
9.2810 9.2672 .0138 0 2 0
6.1510 6.1781 -.0271 0 3 0
4.6330 4.6336 -.0006 0 4 0
3.7110 3.7069 .0041 0 5 0
3.0890 3.0891 -.0001 0 6 0
2.6470 2.6478 -.0008 0 7 0
2.3170 2.3168 .0002 0 8 0
2.0600 2.0594 .0006 0 9 0
1.8530 1.8534 -.0004 0 10 0
1.6850 1.6849 .0001 0 11 0
1.5480 1.5480 .0000 0 0 3
a= 3.133 b=18.5344 c= 4.644
da= .001 db= .0003 dc= .001
V= 269.7
23. 47-1453
Nb12Pb5Se33
Tetragon.
Groupa 85,118,129
Dexp. Dcal. d(D) h k l
6.2220 6.2200 .0020 1 1 0
4.6630 4.6735 -.0105 0 0 2
3.7300 3.7363 -.0063 1 1 2
3.1110 3.1100 .0010 2 2 0
2.6680 2.6661 .0019 3 1 1
2.3340 2.3367 -.0027 0 0 4
2.0800 2.0800 .0000 4 1 1
1.7190 1.7204 -.0014 2 0 5
1.5590 1.5578 .0012 0 0 6
a= 8.796 c= 9.35
da= .003 dc= .01
V= 723.2
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
6.2220 6.2202 .0018 0 1 0
4.6630 4.6490 .0140 2 1 0
3.7300 3.7321 -.0021 3 1 0
3.1110 3.1101 .0009 0 2 0
2.6680 2.6683 -.0003 4 0 1
2.3340 2.3325 .0015 6 0 0
2.0800 2.0805 -.0005 5 2 0
1.7190 1.7189 .0001 0 2 2
1.5590 1.5592 -.0002 8 1 1
a=13.995 b= 6.220 c= 4.125
da= .003 db= .002 dc= .002
V=359.1
24. 47-1934
C6H24Br14Nb6O6
Triklin
Dexp Dcal d(D) h k l
9.4100 9.4274 -.0174 1 0 0
8.8100 8.8140 -.0040 0 1 0
6.5400 6.5227 .0173 0 0 1
4.4700 4.4580 .0120 1 -1 1
4.4100 4.4070 .0030 0 2 0
4.1600 4.1690 -.0090 -1 2 0
3.9860 3.9815 .0045 2 1 0
3.4610 3.4651 -.0041 2 -1 1
3.3400 3.3369 .0031 1 -2 1
3.2180 3.2176 .0004 -1 -2 1
3.1430 3.1425 .0005 3 0 0
3.0870 3.0867 .0003 -1 1 2
A= 9.505 DA= .002
B= 8.917 DB= .001
C= 6.5704 DC= .0003
GAMMA= 96.58 DGAMMA= .01
BETA = 93.865 DBETA = .002
ALPHA= 83.88 DALPHA= .07492
V=549.3
25. 48-0190
Ba2NbCuO5.5
(Áåç î÷.î÷. ñëàáûõ)
Triklin
Dexp Dcal d(D) h k l
4.0903 4.0967 -.0064 0 -1 2
3.5308 3.5282 .0026 -2 1 0
3.3611 3.3585 .0026 0 1 2
3.0439 3.0444 -.0005 3 0 0
2.9037 2.9036 .0001 2 1 2
2.8843 2.8859 -.0016 3 -1 1
2.6479 2.6470 .0009 2 -1 4
2.5331 2.5330 .0001 0 2 0
2.3790 2.3790 .0000 -3 -1 1
2.3581 2.3576 .0005 -3 0 2
2.2351 2.2343 .0008 1 -1 5
2.1887 2.1892 -.0005 0 1 4
A= 9.6732 DA= .0008
B= 5.2211 DB= .0001
C= 11.488 DC= .001
GAMMA= 98.30 DGAMMA= .01
BETA = 71.26 DBETA = .02
ALPHA=103.33 DALPHA= .01
V=532.9
26. 49-0701
HfNb2O17
Triklin
Dexp Dcal d(D) h k l
4.0257 4.0250 .0007 1 1 1
3.6245 3.6260 -.0015 1 -1 1
3.4012 3.4017 -.0005 2 1 1
3.0685 3.0673 .0012 2 -1 1
2.8774 2.8778 -.0004 1 -2 1
2.7598 2.7619 -.0021 2 3 0
2.5523 2.5524 -.0001 3 2 1
2.4853 2.4857 -.0004 -1 3 1
2.2913 2.2914 -.0001 1 -3 1
2.1669 2.1661 .0008 2 4 0
1.9608 1.9607 .0001 -2 2 2
1.8186 1.8186 .0000 5 -1 1
A= 10.766 DA= .001
B= 9.056 DB= .001
C= 4.6582 DC= .0002
GAMMA= 82.53 DGAMMA= .01
BETA = 90.91 DBETA = .02
ALPHA= 84.94 DALPHA= .01
V=448.0
27. 49-0823
Na{Bi,Nb}O3-x
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9060 3.9074 -.0014 2 1 0
3.5940 3.5936 .0004 -1 0 3
3.4570 3.4584 -.0014 1 0 3
3.2410 3.2390 .0020 3 0 1
2.9520 2.9513 .0007 2 0 3
2.7530 2.7550 -.0020 -1 0 4
2.6730 2.6728 .0002 1 0 4
2.5440 2.5440 .0000 0 1 4
2.3960 2.3957 .0003 -3 1 3
1.9920 1.9918 .0002 1 2 4
1.8750 1.8755 -.0005 2 2 4
1.7420 1.7418 .0002 -1 3 3
a= 10.349 b= 5.97418 c=11.267 beta= 93.42
da=.003 db= .00001 dc=.004 dbeta=.002
V= 695.4
Triklin
Dexp Dcal d(D) h k l
3.9060 3.9012 .0048 0 1 0
3.5940 3.5919 .0021 0 -1 2
3.4570 3.4566 .0004 1 0 3
3.2410 3.2403 .0007 0 -1 3
2.9520 2.9520 -.0000 1 0 4
2.7530 2.7547 -.0017 -1 1 2
2.6730 2.6725 .0005 1 1 3
2.5440 2.5451 -.0011 0 -1 5
2.3960 2.3955 .0005 0 1 5
1.9920 1.9919 .0001 -2 0 6
1.8750 1.8748 .0002 2 0 5
1.7420 1.7423 -.0003 2 1 5
A= 5.2636 DA= .0002
B= 3.9627 DB= .0001
C= 16.1418 DC= .0003
GAMMA= 80.530 DGAMMA= .005
BETA = 98.789 DBETA = .003
ALPHA= 94.9021 DALPHA= .0007
V=327.4
28. 49-0824
KNbO3
Triklin
Dexp Dcal d(D) h k l
9.0700 9.0946 -.0246 0 1 0
7.6940 7.6811 .0129 -1 0 1
6.8090 6.8104 -.0014 1 -1 1
5.3720 5.3682 .0038 0 -1 2
4.5520 4.5473 .0047 0 2 0
4.0400 4.0417 -.0017 0 -2 2
3.4260 3.4251 .0009 -2 -1 2
3.2430 3.2422 .0008 1 2 1
3.0790 3.0796 -.0006 -2 2 2
2.8400 2.8407 -.0007 2 2 0
2.4940 2.4939 .0001 3 -3 2
2.3680 2.3680 .0000 -2 4 0
A= 9.9384 DA= .0007
B= 9.846 DB= .001
C= 11.4881 DC= .0008
GAMMA=107.624 DGAMMA= .001
BETA = 93.116 DBETA = .002
ALPHA=102.612 DALPHA= .001
V=1037.1
29. 49-0825
K{Bi,Nb}O3-x
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.0400 4.0285 .0115 3 1 0
3.5970 3.6020 -.0050 0 1 1
3.4590 3.4603 -.0013 2 0 1
3.1860 3.1901 -.0041 4 1 0
2.8840 2.8799 .0041 0 2 1
2.8180 2.8193 -.0013 1 2 1
2.7140 2.7143 -.0003 1 3 0
2.0140 2.0143 -.0003 6 2 0
1.9430 1.9433 -.0003 0 1 2
1.7430 1.7428 .0002 2 2 2
1.6490 1.6490 -.0000 1 5 0
a=13.821 b= 8.3046 c= 3.9976
da= .006 db= .0009 dc= .0004
V= 458.8
Triklin
Dexp Dcal d(D) h k l
4.0400 4.0417 -.0017 0 1 0
3.5970 3.5990 -.0020 1 0 0
3.4590 3.4583 .0007 0 -1 2
3.1860 3.1843 .0017 1 0 2
2.8840 2.8836 .0004 0 -1 3
2.8180 2.8176 .0004 1 1 1
2.7140 2.7143 -.0003 0 0 4
2.0140 2.0141 -.0001 1 -1 4
1.9430 1.9430 .0000 0 2 1
1.7430 1.7431 -.0001 2 1 0
1.6490 1.6489 .0001 -2 0 2
A= 3.6599 DA= .0006
B= 4.1123 DB= .0001
C= 11.007 DC= .001
GAMMA= 82.225 DGAMMA= .009
BETA = 83.953 DBETA = .009
ALPHA= 96.346 DALPHA= .005
V= 161.9
30. 49-1101
Na3NbP3Ox
Triklin
Dexp Dcal d(D) h k l
8.8600 8.8469 .0131 1 0 0
7.3100 7.3261 -.0161 0 1 1
6.4700 6.4827 -.0127 0 -1 1
5.6500 5.6520 -.0020 1 -2 0
4.8800 4.8812 -.0012 1 -1 1
4.5300 4.5255 .0045 -2 1 2
4.3100 4.3060 .0040 0 0 2
4.2800 4.2850 -.0050 -2 2 2
4.1800 4.1798 .0002 -2 2 0
4.1300 4.1290 .0010 -2 0 2
3.8690 3.8684 .0006 0 -1 2
3.6420 3.6439 -.0019 0 3 1
A= 10.828 DA= .005
B= 12.590 DB= .002
C= 10.096 DC= .002
GAMMA=114.41 DGAMMA= .02
BETA =120.71 DBETA = .02
ALPHA= 71.953 DALPHA= .008
V=1069.3
31. 50-0819
KNbF5
Triklin
Dexp Dcal d(D) h k l
5.4000 5.3969 .0031 -1 0 1
5.0000 5.0031 -.0031 0 -1 1
4.7800 4.7695 .0105 1 -1 1
3.7300 3.7309 -.0009 0 2 0
3.6600 3.6657 -.0057 -2 1 1
3.5700 3.5689 .0011 -2 0 1
3.3700 3.3692 .0008 0 1 2
3.2900 3.2921 -.0021 -1 0 2
3.0700 3.0679 .0021 -2 2 1
2.6300 2.6308 -.0008 -3 2 0
2.5700 2.5687 .0013 -3 0 1
2.3800 2.3804 -.0004 3 1 0
A= 8.7153 DA= .0003
B= 7.83521 DB= .00004
C= 7.2748 DC= .0007
GAMMA=107.179 DGAMMA= .002
BETA = 89.839 DBETA = .006
ALPHA= 85.652 DALPHA= .001
V=473.5