1. 34-0668
AlNb6As
Triklin
Dexp Dcal d(D) h k l
2.8570 2.8571 -.0001 1 -1 1
2.5520 2.5519 .0001 -1 -1 2
2.5010 2.5013 -.0003 1 -1 3
2.4400 2.4400 .0000 0 -2 3
2.3600 2.3599 .0001 1 1 2
2.2370 2.2371 -.0001 -1 -1 4
2.2030 2.2028 .0002 -1 0 5
2.0770 2.0770 .0000 0 -2 5
1.9800 1.9777 .0023 0 2 4
1.6010 1.6001 .0009 -1 0 8
1.5790 1.5782 .0008 1 -3 3
1.4770 1.4770 -.0000 -1 -3 1
A= 3.2512 DA= .0001
B= 5.3150 DB= .0005
C= 14.39 DC= .02
GAMMA= 96.3952 DGAMMA= .0006
BETA = 92.65 DBETA = .02
ALPHA= 97.77 DALPHA= .01
V= 244.4
2. 34-0685
SbInNb6
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.6750 3.6738 .0012 1 3 0
2.9710 2.9749 -.0039 4 2 0
2.8630 2.8640 -.0010 2 0 1
2.7110 2.7083 .0027 5 1 0
2.5080 2.5054 .0026 5 2 0
2.4240 2.4234 .0006 0 3 1
2.3670 2.3683 -.0013 3 2 1
2.3340 2.3333 .0007 4 0 1
2.2100 2.2091 .0009 4 4 0
2.0860 2.0852 .0008 5 0 1
1.9840 1.9833 .0007 6 3 0
1.5860 1.5857 .0003 2 6 1
a=13.939 b=11.4253 c= 3.1415
da= .001 db= .0007 dc= .000396
V=500.3
Triklin
Dexp Dcal d(D) h k l
3.6750 3.6700 .0050 -1 1 1
2.9710 2.9706 .0004 1 2 0
2.8630 2.8661 -.0031 1 1 1
2.7110 2.7111 -.0001 0 3 0
2.5080 2.5093 -.0013 -1 0 2
2.4240 2.4230 .0010 0 3 1
2.3670 2.3669 .0001 0 -3 1
2.3340 2.3345 -.0005 2 0 0
2.2100 2.2097 .0003 -2 -1 1
2.0860 2.0852 .0008 -2 2 0
1.9840 1.9835 .0005 1 -1 2
1.5860 1.5860 .0000 0 2 3
A= 4.82505 DA= .00007
B= 8.15986 DB= .00003
C= 5.26670 DC= .00001
GAMMA= 94.3311 DGAMMA= .0006
BETA =104.1251 DBETA = .0004
ALPHA= 87.38557 DALPHA= .00001
V=200.4
3. 34-1029
alfa-RbNb3F16
Triklin
Dexp Dcal d(D) h k l
7.2400 7.2445 -.0045 1 1 0
6.0800 6.0692 .0108 -1 0 1
5.6700 5.6660 .0040 -1 -2 1
5.0900 5.0932 -.0032 1 0 1
4.9000 4.9029 -.0029 -1 -3 1
4.4300 4.4306 -.0006 1 2 1
4.1600 4.1635 -.0035 -1 -4 1
4.0700 4.0722 -.0022 0 0 2
3.9800 3.9784 .0016 0 -2 2
3.9070 3.9047 .0023 1 3 1
3.8730 3.8727 .0003 -1 0 2
3.7670 3.7682 -.0012 0 5 0
A= 7.6938 DA= .0009
B= 19.281 DB= .006
C= 8.414 DC= .001
GAMMA= 81.93 DGAMMA= .02
BETA =101.27 DBETA = .01
ALPHA=100.59 DALPHA= .09
V= 1196.2
4. 34-1172
TlNb3F16
Triklin
Dexp Dcal d(D) h k l
7.2500 7.2486 .0014 1 0 1
4.4400 4.4428 -.0028 0 1 0
4.1500 4.1505 -.0005 0 -1 2
4.0110 4.0105 .0005 2 0 0
3.9310 3.9313 -.0003 1 0 4
3.8870 3.8861 .0009 2 0 1
3.7380 3.7349 .0031 -2 0 2
3.6130 3.6120 .0010 1 -1 2
3.4240 3.4251 -.0011 -2 0 3
2.9470 2.9467 .0003 2 1 1
2.7230 2.7229 .0001 0 1 5
2.6730 2.6736 -.0006 3 0 0
A= 8.034 DA= .001
B= 4.4639 DB= .0007
C= 18.555 DC= .009
GAMMA= 87.80 DGAMMA= .05
BETA = 92.55 DBETA = .02
ALPHA= 95.21 DALPHA= .04
V=660.9
5. 34-1361
Nb2P6O20*4H2O
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
5.3700 5.4067 -.0367 0 2 0
4.2300 4.2360 -.0060 0 0 1
3.8200 3.8090 .0110 1 1 1
3.6200 3.6278 -.0078 3 2 0
3.3300 3.3345 -.0045 0 2 1
3.2300 3.2353 -.0053 2 3 0
3.0400 3.0363 .0037 4 2 0
2.7700 2.7736 -.0036 4 0 1
2.6600 2.6587 .0013 1 4 0
2.4700 2.4678 .0022 4 2 1
2.1400 2.1396 .0004 1 5 0
2.0580 2.0580 .0000 1 1 2
a=14.68 b=10.813 c= 4.2359
da= .02 db= .009 dc= .0007
v= 672
Triklin
Dexp Dcal d(D) h k l
5.3700 5.3719 -.0019 0 1 1
4.2300 4.2358 -.0058 1 1 1
3.8200 3.8211 -.0011 0 -1 1
3.6200 3.6220 -.0020 0 2 0
3.3300 3.3352 -.0052 1 -1 1
3.2300 3.2305 -.0005 1 2 1
3.0400 3.0415 -.0015 -1 1 1
2.7700 2.7728 -.0028 0 0 2
2.6600 2.6574 .0026 -1 -1 1
2.4700 2.4682 .0018 1 -2 1
2.1400 2.1404 -.0004 1 3 0
2.0580 2.0574 .0006 1 2 3
A= 4.9179 DA= .0001
B= 7.7685 DB= .0005
C= 6.3044 DC= .0003
GAMMA= 82.526 DGAMMA= .005
BETA = 69.283 DBETA = .005
ALPHA= 68.831 DALPHA= .00480
V=210.0
6. 34-1386
As4Nb2O15
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.2800 5.2579 .0221 4 0 0
4.9000 4.8756 .0244 1 0 1
4.1100 4.1214 -.0114 1 1 1
3.7900 3.7938 -.0038 1 2 0
3.6900 3.6930 -.0030 5 1 0
3.3900 3.3794 .0106 3 2 0
3.2900 3.2829 .0071 4 1 1
2.9700 2.9731 -.0031 5 1 1
2.8000 2.7997 .0003 7 1 0
2.4700 2.4728 -.0028 5 2 1
2.3600 2.3598 .0002 3 0 2
2.3100 2.3099 .0001 4 3 0
a=21.03 b= 7.7142 c= 5.012
da= .02 db= .0006 dc= .001
V= 813
Triklin
Dexp Dcal d(D) h k l
5.2800 5.2761 .0039 1 0 0
4.9000 4.9002 -.0002 1 1 1
4.1100 4.1044 .0056 1 -1 1
3.7900 3.7794 .0106 0 -2 1
3.6900 3.6829 .0071 -1 2 0
3.3900 3.3908 -.0008 -1 1 1
3.2900 3.2945 -.0045 1 -2 1
2.9700 2.9677 .0023 0 2 2
2.8000 2.7999 .0001 0 4 0
2.4700 2.4711 -.0011 2 2 0
2.3600 2.3588 .0012 -1 1 2
2.3100 2.3100 .0000 -2 2 0
A= 5.647 DA= .005
B= 11.598 DB= .001
C= 6.713 DC= .009
GAMMA= 80.53 DGAMMA= .03
BETA = 69.71 DBETA = .08
ALPHA= 75.79 DALPHA= .03
V= 398.2
7. 34-1599
C2H8o2*Nb6Cl12{OH}2*6H2O
Rombik
Grupa 30,53
Dexp. Dcal. d(D) h k l
8.6000 8.5719 .0281 0 1 1
7.3500 7.3471 .0029 1 0 0
4.2800 4.2836 -.0036 1 1 2
3.6800 3.6781 .0019 1 3 0
3.3000 3.3010 -.0010 1 1 3
3.0100 3.0119 -.0019 1 2 3
2.8350 2.8346 .0004 1 4 1
2.4900 2.4897 .0003 0 5 1
2.4500 2.4490 .0010 3 0 0
2.3300 2.3307 -.0007 1 4 3
2.2400 2.2387 .0013 2 1 4
2.2200 2.2211 -.0011 3 1 2
a= 7.347 b=12.746 c=11.582
da= .003 db= .002 dc= .007
V=1085
Triklin
Dexp Dcal d(D) h k l
8.6000 8.5026 .0974 0 0 1
7.3500 7.3428 .0072 -1 0 1
4.2800 4.2805 -.0005 -1 1 1
3.6800 3.6802 -.0002 1 -1 1
3.3000 3.2999 .0001 2 1 0
3.0100 3.0089 .0011 -1 0 3
2.8350 2.8342 .0008 0 0 3
2.4900 2.4902 -.0002 0 -1 3
2.4500 2.4492 .0008 1 0 3
2.3300 2.3303 -.0003 2 1 2
2.2400 2.2398 .0002 2 2 0
2.2200 2.2201 -.0001 -3 -1 3
A= 8.944 DA= .001
B= 5.26952 DB= .00003
C= 9.0266 DC= .0004
GAMMA= 89.759 DGAMMA= .007
BETA =109.63 DBETA = .05
ALPHA= 89.784 DALPHA= .001
V= 400.7
8. 35-1934
Cl2H30LiNbO6
Triklin
Dexp Dcal d(D) h k l
10.5700 10.5706 -.0006 -1 1 0
10.2100 10.2235 -.0135 0 1 1
9.1000 9.0739 .0261 0 -1 1
8.9200 8.9077 .0123 1 -1 1
8.3800 8.3589 .0211 1 1 0
8.0600 8.0615 -.0015 1 1 1
7.6300 7.6228 .0072 -1 0 1
7.4900 7.4891 .0009 -1 1 1
7.0600 7.0643 -.0043 -1 2 0
6.4100 6.4146 -.0046 1 0 2
6.2200 6.2294 -.0094 -1 -1 1
6.0800 6.0770 .0030 0 1 2
A= 12.7555 DA= .0007
B= 15.2115 DB= .0005
C= 13.2352 DC= .0001
GAMMA=102.207 DGAMMA= .001
BETA = 74.0382 DBETA = .0009
ALPHA= 86.8654 DALPHA= .0009
V=2392
9. 36-0917
Nb6Br12Cl2*xH2O
Triklin
Dexp Dcal d(D) h k l
8.9300 8.9330 -.0030 1 0 0
8.3900 8.3758 .0142 0 1 0
7.9700 7.9746 -.0046 0 0 1
7.3300 7.3235 .0065 -1 0 1
6.1300 6.1268 .0032 1 1 0
5.1500 5.1459 .0041 1 1 1
4.6200 4.6145 .0055 -2 1 1
4.2000 4.2007 -.0007 -1 2 2
3.9830 3.9819 .0011 0 2 2
3.9340 3.9322 .0018 -2 1 0
3.8800 3.8784 .0016 1 -1 1
3.7820 3.7839 -.0019 -1 2 0
A= 9.684 DA= .001
B= 9.692 DB= .007
C= 9.821 DC= .003
GAMMA=100.952 DGAMMA= .002
BETA =112.714 DBETA = .005
ALPHA= 59.79 DALPHA= .02
V= 734.8
10. 36-0918
Nb6Br12{OH}2*8H2O
Rombik
Groupa 56
Dexp. Dcal. d(D) h k l
9.0600 9.1345 -.0745 0 0 2
8.4300 8.4053 .0247 0 2 0
8.0400 8.0261 .0139 0 1 2
4.2000 4.2027 -.0027 0 4 0
3.1910 3.1929 -.0019 1 3 0
3.1440 3.1452 -.0012 1 3 1
3.0150 3.0141 .0009 1 3 2
2.8200 2.8188 .0012 1 4 1
2.6170 2.6168 .0002 1 3 4
a= 3.885 b=16.81 c=18.269
da= .007 db= .04 dc= .002
V=1193
11. 36-0920
Nb6Cl12{Oh}2*8H2O
Triklin
Dexp Dcal d(D) h k l
8.4600 8.4647 -.0047 1 0 0
7.9000 7.8509 .0491 0 1 0
7.6800 7.6946 -.0146 0 0 1
7.5800 7.5924 -.0124 0 1 1
7.1000 7.0724 .0276 1 0 1
6.8600 6.8298 .0302 1 1 1
5.8400 5.8528 -.0128 -1 1 0
5.6700 5.6643 .0057 1 1 0
4.4300 4.4283 .0017 1 -1 1
4.3100 4.3258 -.0158 2 1 1
4.2500 4.2512 -.0012 1 2 1
4.0900 4.0890 .0010 1 0 2
A= 9.17 DA= .01
B= 9.052 DB= .008
C= 9.48 DC= .01
GAMMA= 80.52 DGAMMA= .09
BETA = 67.40 DBETA = .08
ALPHA= 60.21 DALPHA= .07
V=628.6
12. 36-1175
Te4Nb2O13
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.9800 4.9818 -.0018 0 2 0
4.8300 4.8400 -.0100 0 2 1
4.5300 4.5454 -.0154 0 1 4
4.1800 4.1917 -.0117 1 1 0
4.0900 4.0863 .0037 0 0 5
3.7800 3.7807 -.0007 0 1 5
3.5700 3.5698 .0002 1 1 3
3.4300 3.4266 .0034 1 0 4
3.3900 3.3877 .0023 1 2 0
3.3800 3.3877 -.0077 1 2 0
3.3500 3.3421 .0079 1 2 1
3.2800 3.2782 .0018 0 3 1
a= 4.621 b= 9.964 c=20.431
da= .001 db= .008 dc= .001
V= 941
Triklin
Dexp Dcal d(D) h k l
4.9800 4.9756 .0044 -1 1 1
4.8300 4.8293 .0007 -1 -1 1
4.5300 4.5300 .0000 -2 1 1
4.1800 4.1778 .0022 0 -2 1
4.0900 4.0911 -.0011 -1 -2 1
3.7800 3.7810 -.0010 2 1 1
3.5700 3.5713 -.0013 -3 2 1
3.4300 3.4293 .0007 -4 2 0
3.3900 3.3896 .0004 -1 -3 1
3.3800 3.3797 .0003 2 2 1
3.3500 3.3505 -.0005 1 -3 1
3.2800 3.2796 .0004 2 -4 0
A= 15.132 DA= .004
B= 13.944 DB= .004
C= 5.337 DC= .00116
GAMMA= 96.47 DGAMMA= .02
BETA = 99.62 DBETA = .01
ALPHA= 88.579 DALPHA= .001
V=1102
13. 37-0675
BaNb2O5CO3O5
Triklin
Dexp Dcal d(D) h k l
4.2183 4.2198 -.0015 2 1 0
4.1140 4.1138 .0002 0 2 0
3.9515 3.9514 .0001 1 0 1
3.7354 3.7376 -.0022 -1 1 1
3.6420 3.6390 .0030 1 2 0
3.3386 3.3378 .0008 2 0 1
3.3022 3.3015 .0007 -2 1 1
3.1339 3.1340 -.0001 3 1 0
3.0339 3.0348 -.0009 2 2 0
2.9980 2.9973 .0007 -2 -1 1
2.9177 2.9183 -.0006 0 -2 1
A= 11.1541 DA= .0004
B= 8.373 DB= .001
C= 4.2680 DC= .0001
GAMMA=100.5751 DGAMMA= .0003
BETA = 91.345 DBETA = .001
ALPHA= 88.10 DALPHA= .04
V=391.8
14. 38-0088
Li4Nb2TiO9
Triklin
Dexp Dcal d(D) h k l
4.8236 4.8175 .0061 -1 0 1
3.9585 3.9585 .0000 -1 1 1
3.8003 3.8016 -.0013 1 0 1
3.6472 3.6505 -.0033 -1 1 0
3.4832 3.4823 .0009 -1 1 2
2.6951 2.6948 .0003 -1 2 2
2.5726 2.5733 -.0007 0 2 3
2.4205 2.4217 -.0012 -2 -1 1
2.3128 2.3119 .0009 1 -1 2
2.2492 2.2500 -.0008 0 -1 3
2.1325 2.1322 .0003 2 2 0
2.0949 2.0945 .0004 -1 0 4
A= 5.1209 DA= .0006
B= 6.9316 DB= .0004
C= 8.9546 DC= .0002
GAMMA= 85.655 DGAMMA= .004
BETA =102.960 DBETA = .006
ALPHA= 71.302 DALPHA= .002
V=289.4
15. 38-0276
Li13TiNb5O21
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
6.5240 6.5083 .0157 0 1 0
6.1590 6.1424 .0166 3 0 0
4.4770 4.4762 .0008 1 0 1
3.7610 3.7602 .0008 4 1 0
3.6910 3.6893 .0017 3 0 1
3.4870 3.4847 .0023 2 1 1
3.2610 3.2602 .0008 4 0 1
2.8820 2.8797 .0023 5 0 1
2.7810 2.7775 .0035 6 1 0
2.6320 2.6321 -.0001 1 2 1
2.4390 2.4393 -.0003 5 2 0
2.3810 2.3797 .0013 6 1 1
a=18.427 b= 6.51 c= 4.6144
da= .005 db= .01 dc= .0002
V= 553
16. 38-0456
NbTi{OH}9
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
3.7000 3.6900 .0100 0 2 0
3.1800 3.1840 -.0040 0 2 1
2.1000 2.1000 .0000 0 0 3
1.8900 1.8896 .0004 1 2 0
1.6400 1.6399 .0001 1 3 0
a= 2.200 b= 7.380 c= 6.300
da= .001 db= .001 dc= .001
V=102.29
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
3.7000 3.6983 .0017 1 2 0
3.1800 3.1796 .0004 3 1 0
2.1000 2.1002 -.0002 3 3 0
1.8900 1.8890 .0010 1 0 1
1.6400 1.6400 .0000 2 2 1
a=10.417 b= 7.912 c= 1.9210
da= .001 db= .001 dc= .001
V=158.31
17. 38-0480
{Nd,Ce,Ca,Th}{Ti,Nb}2{OH}6
Triklin
Dexp Dcal d(D) h k l
5.4500 5.4461 .0039 1 0 0
4.7200 4.7222 -.0022 -1 1 1
4.4000 4.4001 -.0001 -1 -1 1
4.0000 3.9963 .0037 1 -1 1
3.1600 3.1598 .0002 1 -3 1
3.0700 3.0697 .0003 0 4 0
3.0000 3.0000 -.0000 0 2 2
2.9300 2.9308 -.0008 -1 -2 2
2.7700 2.7700 .0000 -2 1 0
2.6400 2.6401 -.0001 -1 3 2
2.5600 2.5594 .0006 2 1 0
2.4300 2.4307 -.0007 2 -1 1
A= 5.6641 DA= .0005
B= 12.5201 DB= .0008
C= 7.4547 DC= .0006
GAMMA= 99.812 DGAMMA= .007
BETA =101.85 DBETA = .01
ALPHA= 93.376 DALPHA= .004
V= 507.4
18. 38-0612
NbOCl2
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
6.1700 6.1805 -.0105 0 1 1
3.7300 3.7347 -.0047 -1 0 1
3.2300 3.2290 .0010 0 3 1
2.6100 2.6138 -.0038 -1 1 2
2.3600 2.3563 .0037 1 4 0
2.0300 2.0324 -.0024 -2 2 1
1.9680 1.9666 .0014 1 5 0
1.9520 1.9520 .0000 1 5 1
1.8630 1.8630 .0000 0 1 4
1.6800 1.6800 .0000 3 0 2
a= 5.129 b= 10.711 c=7.83 beta= 75.23
da=.006 db=.004 dc=.03 dbet=.03
V=413.3
19. 38-0613
Cs{Nb{ClO4}6}
Triklin
Dexp Dcal d(D) h k l
5.2870 5.2930 -.0060 0 -1 1
5.1885 5.1875 .0010 -2 0 1
4.1174 4.1193 -.0019 -2 1 0
3.7779 3.7788 -.0009 0 -1 2
3.5912 3.5931 -.0019 2 -1 1
3.3966 3.3946 .0020 -2 -1 2
3.2928 3.2933 -.0005 3 1 0
3.1909 3.1904 .0005 -3 0 2
3.0826 3.0820 .0006 -1 2 0
2.9895 2.9899 -.0004 3 1 1
2.9076 2.9089 -.0013 2 -1 2
2.7939 2.7938 .0001 -4 0 1
A= 11.276 DA= .003
B= 6.526 DB= .004
C= 9.631 DC= .007
GAMMA= 87.25 DGAMMA= .05
BETA = 99.62 DBETA = .08
ALPHA= 88.67 DALPHA= .07
V= 697.5
20. 38-0614
NbO2ClO4
Triklin
Dexp Dcal d(D) h k l
8.8198 8.8186 .0012 1 0 0
4.1945 4.1928 .0017 0 1 1
4.0799 4.0797 .0002 0 -1 1
3.8557 3.8524 .0033 -1 2 1
3.6791 3.6792 -.0001 1 0 1
3.4670 3.4650 .0020 -2 1 1
2.8442 2.8435 .0007 -3 3 0
2.4637 2.4636 .0001 3 2 0
2.3915 2.3921 -.0006 2 4 0
2.3351 2.3357 -.0006 -3 5 0
2.2616 2.2611 .0005 0 6 0
2.0636 2.0638 -.0002 -1 3 2
1.8855 1.8855 -.0000 -1 -3 2
1.8579 1.8578 .0001 4 -3 1
1.8094 1.8095 -.0001 2 -2 2
1.6932 1.6933 -.0001 -5 5 1
A= 9.30317 DA= .00001
B= 14.161 DB= .003
C= 4.4122 DC= .0002
GAMMA=106.4458 DGAMMA= .0002
BETA = 99.909 DBETA = .001
ALPHA= 84.661 DALPHA= .007
V= 548.58
21. 38-0615
NbO{ClO4}3
Triklin
Dexp Dcal d(D) h k l
3.9964 3.9985 -.0021 1 1 1
3.6671 3.6683 -.0012 2 1 1
3.5266 3.5260 .0006 -1 -1 1
3.2786 3.2776 .0010 0 0 2
3.1642 3.1639 .0003 3 1 1
3.0152 3.0133 .0019 -2 1 1
2.7537 2.7538 -.0001 2 1 2
2.6292 2.6302 -.0010 3 -1 1
2.5064 2.5060 .0004 -1 -1 2
2.3865 2.3869 -.0004 -3 0 2
2.1450 2.1467 -.0017 2 0 3
2.0362 2.0352 .0010 3 0 3
A= 12.3160 DA= .0002
B= 4.70222 DB= .00005
C= 6.64996 DC= .00007
GAMMA= 80.3069 DGAMMA= .0001
BETA = 81.4811 DBETA = .0007
ALPHA= 83.8532 DALPHA= .0005
V=374.0
22. 38-0616
Nb{ClO4}5
Triklin
Dexp Dcal d(D) h k l
8.3376 8.3452 -.0076 -1 1 0
7.7076 7.6946 .0130 1 1 0
7.3540 7.3593 -.0053 0 1 1
7.0051 7.0060 -.0009 1 1 1
5.7669 5.7640 .0029 1 -1 1
5.6211 5.6193 .0018 0 2 0
5.2558 5.2548 .0010 -2 1 0
4.0615 4.0622 -.0007 0 -2 1
3.9294 3.9268 .0026 3 0 1
3.9265 3.9268 -.0003 3 0 1
3.8723 3.8720 .0003 0 0 2
3.5826 3.5828 -.0002 -1 -2 1
A= 11.98723 DA= .00007
B= 11.6610 DB= .0002
C= 8.42799 DC= .00007
GAMMA= 89.8765 DGAMMA= .0009
BETA = 72.4382 DBETA = .0003
ALPHA= 75.237 DALPHA= .002
V=1082.1
23. 38-1067
NbHx
Triklin
Dexp Dcal d(D) h k l
2.4900 2.4899 .0001 -1 0 1
2.1500 2.1512 -.0012 0 -2 1
1.9200 1.9208 -.0008 1 -2 1
1.7500 1.7498 .0002 0 3 1
1.5100 1.5098 .0002 -2 0 1
1.4200 1.4204 -.0004 1 2 3
1.3400 1.3396 .0004 -2 2 1
1.2800 1.2802 -.0002 -1 1 3
1.2300 1.2299 .0001 0 -2 3
1.1300 1.1298 .0002 1 2 4
1.0600 1.0600 .0000 -3 2 0
.9990 .9991 -.0001 -3 2 1
A= 3.5822 DA= .0001
B= 5.4034 DB= .0001
C= 4.705 DC= .001
GAMMA= 87.27 DGAMMA= .01
BETA = 76.286 DBETA = .006
ALPHA= 80.55 DALPHA= .04
V=87.2
24. 38-1214
C6.5NbCr0.6F8O1.2
Geksag.
Grupa 143
Dexp. Dcal. d(D) h k l
8.3800 8.3601 .0199 0 0 1
4.1800 4.1800 -.0000 0 0 2
2.7740 2.7740 .0000 1 0 0
2.0900 2.0900 -.0000 0 0 4
a= 3.20314 c= 8.36007
da= .000000 dc= .00007
V= 85.78
25. 40-0032
Cs5Nb13O35
Triklin
Dexp Dcal d(D) h k l
3.7600 3.7650 -.0050 0 0 1
3.6500 3.6472 .0028 -1 3 0
3.5800 3.5824 -.0024 0 -2 1
3.3500 3.3508 -.0008 -1 0 1
3.2500 3.2503 -.0003 -1 2 1
3.1200 3.1192 .0008 -1 3 1
3.0500 3.0521 -.0021 -1 -3 1
2.9570 2.9572 -.0002 0 5 1
2.8710 2.8714 -.0004 -1 6 0
2.7860 2.7856 .0004 1 6 0
2.0850 2.0847 .0003 -2 1 1
1.8815 1.8817 -.0002 -2 5 0
1.7915 1.7912 .0003 0 -4 2
A= 4.280 DA= .001
B= 23.73 DB= .02
C= 3.9804 DC= .0004
GAMMA= 91.96 DGAMMA= .07
BETA =108.941 DBETA = .002
ALPHA= 89.06 DALPHA= .02
V= 382.1
26. 40-0033
Cu2K5Nb11O31
Rombik
Grupa 33,49,62
Dexp. Dcal. d(D) h k l
5.6000 5.6386 -.0386 2 1 0
4.0000 4.0007 -.0007 1 3 0
3.5100 3.5053 .0047 2 3 0
3.2600 3.2599 .0001 1 2 1
3.1600 3.1644 -.0044 0 4 0
3.0700 3.0690 .0010 1 4 0
2.9760 2.9761 -.0001 3 3 0
2.8250 2.8249 .0001 1 3 1
2.6310 2.6305 .0005 3 2 1
2.4720 2.4718 .0002 4 0 1
2.4327 2.4325 .0002 1 4 1
2.3500 2.3488 .0012 2 5 0
a=12.596 b=12.6574 c= 3.989
da= .003 db= .0009 dc= .001
V= 636.1
Triklin
Dexp Dcal d(D) h k l
5.6000 5.6036 -.0036 0 1 0
4.0000 3.9968 .0032 -1 0 1
3.5100 3.5118 -.0018 0 -1 2
3.2600 3.2613 -.0013 0 0 2
3.1600 3.1595 .0005 2 -1 1
3.0700 3.0699 .0001 0 -2 1
2.9760 2.9749 .0011 2 -1 2
2.8250 2.8260 -.0010 -1 1 1
2.6310 2.6300 .0010 -2 0 1
2.4720 2.4730 -.0010 3 0 1
2.4327 2.4322 .0005 2 1 2
2.3500 2.3500 -.0000 3 0 2
A= 7.427 DA= .001
B= 6.14128 DB= .00007
C= 7.674 DC= .001
GAMMA= 90.0470 DGAMMA= .0006
BETA = 68.675 DBETA = .008
ALPHA=112.429 DALPHA= .002
V=297.6
27. 41-0781
Nb3Si2
Triklin
Dexp Dcal d(D) h k l
3.4900 3.4935 -.0035 1 0 0
2.8100 2.8086 .0014 1 2 0
2.4670 2.4666 .0004 -1 0 1
2.4200 2.4195 .0005 -1 3 0
2.3550 2.3543 .0007 1 3 0
2.2270 2.2269 .0001 -1 -2 1
2.2050 2.2047 .0003 1 2 1
2.1800 2.1803 -.0003 -1 2 1
2.0820 2.0810 .0010 1 -3 1
1.7470 1.7467 .0003 2 0 0
1.5100 1.5101 -.0001 1 2 2
1.4770 1.4769 .0001 -2 2 1
A= 3.4971 DA= .0005
B= 9.83 DB= .03
C= 3.6161 DC= .0009
GAMMA= 91.71 DGAMMA= .05
BETA = 87.91 DBETA = .01
ALPHA= 93.89 DALPHA= .02
V= 123.9
28. 40-0032
Cs5Nb13O35
Triklin
Dexp Dcal d(D) h k l
3.7600 3.7635 -.0035 0 1 1
3.6500 3.6501 -.0001 -1 1 0
3.5800 3.5824 -.0024 -1 1 1
3.3500 3.3499 .0001 -1 -1 1
3.2500 3.2509 -.0009 -3 0 1
3.1200 3.1197 .0003 -2 0 2
3.0500 3.0510 -.0010 -2 1 1
2.9570 2.9556 .0014 -2 1 0
2.8710 2.8725 -.0015 1 -1 1
2.7860 2.7851 .0009 1 0 2
2.0850 2.0845 .0005 1 2 0
1.8815 1.8817 -.0002 0 2 2
1.7915 1.7912 .0003 -2 2 2
A= 9.98 DA= .01
B= 4.223 DB= .001
C= 6.752 DC= .003
GAMMA= 85.49 DGAMMA= .04
BETA =106.70 DBETA = .08
ALPHA= 82.761 DALPHA= .007
V= 268.5
29. 40-0033
Cu2K5Nb11O31
Rombik
Grupa 33,49,62
Dexp. Dcal. d(D) h k l
5.6000 5.6386 -.0386 2 1 0
4.0000 4.0007 -.0007 1 3 0
3.5100 3.5053 .0047 2 3 0
3.2600 3.2599 .0001 1 2 1
3.1600 3.1644 -.0044 0 4 0
3.0700 3.0690 .0010 1 4 0
2.9760 2.9761 -.0001 3 3 0
2.8250 2.8249 .0001 1 3 1
2.6310 2.6305 .0005 3 2 1
2.4720 2.4718 .0002 4 0 1
2.4327 2.4325 .0002 1 4 1
2.3500 2.3488 .0012 2 5 0
a=12.596 b=12.6574 c= 3.989
da= .003 db= .0009 dc= .001
V= 636.1