1. 30-0720
PbSmSnNbO7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.1300 3.1296 .0004 0 1 2
3.0100 3.0100 .0000 1 0 3
2.6000 2.6003 -.0003 -2 0 1
2.3800 2.3807 -.0007 1 1 3
1.8500 1.8497 .0003 -2 1 3
1.5800 1.5800 .0000 -3 0 3
1.5100 1.5099 .0001 3 1 3
1.3140 1.3168 -.0028 0 0 8
1.2330 1.2329 .0001 -3 0 6
1.2060 1.2060 .0000 2 0 8
1.1770 1.1753 .0017 -3 1 6
1.0750 1.0750 .0000 -5 0 1
1.0140 1.0141 -.0001 5 1 3
a= 5.433 b= 3.8908 c= 10.545 beta= 87.44
da=.002 db=.0005 dc= .001 dbeta=.06
V= 222.7
Triklin
Dexp Dcal d(D) h k l
3.1300 3.1287 .0013 0 1 1
3.0100 3.0112 -.0012 0 -1 1
2.6000 2.6004 -.0004 1 1 1
2.3800 2.3807 -.0007 1 0 2
1.8500 1.8499 .0001 0 -2 1
1.5800 1.5801 -.0001 -2 2 0
1.5100 1.5099 .0001 1 2 2
1.3140 1.3142 -.0002 -2 0 2
1.2330 1.2329 .0001 3 -1 3
1.2060 1.2059 .0001 -2 -1 2
1.1770 1.1771 -.0001 1 -1 4
1.0750 1.0750 -.0000 2 3 1
1.0140 1.0140 .0000 3 1 4
A= 4.3483 DA= .0002
B= 4.16894 DB= .00003
C= 4.9070 DC= .0006
GAMMA= 99.669 DGAMMA= .008
BETA = 70.30 DBETA = .01
ALPHA= 91.20 DALPHA= .01
V= 82.50
2. 30-721
PbSmTiNbO7
Triklin
Dexp Dcal d(D) h k l
3.0900 3.0905 -.0005 0 1 1
2.9700 2.9708 -.0008 0 -1 1
2.5700 2.5701 -.0001 -1 1 1
2.3500 2.3504 -.0004 0 2 1
1.9900 1.9902 -.0002 -1 2 1
1.8200 1.8186 .0014 1 -2 1
1.7300 1.7300 -.0000 -1 0 2
1.5800 1.5803 -.0003 -2 2 1
1.5500 1.5500 .0000 -2 0 2
1.4900 1.4900 .0000 1 4 1
1.4500 1.4501 -.0001 3 0 1
1.3400 1.3399 .0001 4 3 0
A= 5.5959 DA= .0005
B= 6.613 DB= .001
C= 3.5273 DC= .0002
GAMMA= 67.43 DGAMMA= .01
BETA = 97.993 DBETA = .008
ALPHA= 90.662 DALPHA= .006
V= 119.2
3. 30-0756
Li3NbF8
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
4.7600 4.7672 -.0072 0 1 1
4.4100 4.4296 -.0196 2 1 0
3.9600 3.9601 -.0001 2 0 1
3.2000 3.1981 .0019 2 2 0
2.3840 2.3836 .0004 0 2 2
2.2130 2.2131 -.0001 2 3 1
2.1750 2.1751 -.0001 2 2 2
2.0560 2.0557 .0003 5 1 0
1.9670 1.9670 .0000 1 4 0
a=10.64 b= 8.006 c= 5.934
da= .01 db= .001 dc= .001
V= 505.2
4. 30-0757
Li2Nb32O81
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
14.3000 14.3866 -.0866 0 0 1
13.7000 13.7022 -.0022 1 0 0
7.1800 7.1933 -.0133 0 0 2
6.9700 6.9782 -.0082 2 0 1
6.8400 6.8511 -.0111 2 0 0
4.8000 4.7955 .0045 0 0 3
4.7500 4.7476 .0024 3 0 1
3.7760 3.7799 -.0039 -1 2 1
3.7420 3.7416 .0004 1 0 4
3.5930 3.5905 .0025 2 2 1
3.5610 3.5612 -.0002 4 0 1
3.4870 3.4891 -.0021 4 0 2
a= 14.2560 b= 8.375 c= 14.968 beta= 73.97
da=.0006 db= .005 dc=.006 dbeta=.05
V= 1718
5. 30-1229
Na2Nb8O21
Rombik
Groupa 50
Dexp. Dcal. d(D) h k l
8.4000 8.3964 .0036 1 1 0
4.4300 4.4323 -.0023 3 1 0
3.9800 3.9622 .0178 0 0 1
3.7000 3.6902 .0098 4 0 0
3.5900 3.5833 .0067 1 1 1
3.4900 3.4910 -.0010 2 0 1
3.3200 3.3160 .0040 1 3 0
3.1200 3.1300 -.0100 0 2 1
2.9900 2.9906 -.0006 4 2 0
2.8800 2.8815 -.0015 2 2 1
2.8310 2.8360 -.0050 5 1 0
2.7960 2.7988 -.0028 3 3 0
a=14.761 b=10.209 c= 3.962
da= .006 db= .002 dc= .003
V= 597.1
6. 30-1230
Na2Nb14O36
Triklin
Dexp Dcal d(D) h k l
11.3000 11.2955 .0045 1 0 0
7.5300 7.5389 -.0089 1 1 0
6.5900 6.5949 -.0049 0 1 1
6.3000 6.3003 -.0003 1 1 1
4.8600 4.8681 -.0081 -2 0 1
3.8200 3.8156 .0044 -1 1 2
3.7300 3.7320 -.0020 2 2 1
3.5400 3.5425 -.0025 2 1 2
3.4600 3.4686 -.0086 -3 -1 1
3.3600 3.3608 -.0008 1 2 2
3.2400 3.2382 .0018 3 2 0
3.1500 3.1501 -.0001 2 2 2
2.9530 2.9526 .0004 3 1 2
A= 11.88 DA= .01
B= 8.34 DB= .01
C= 8.801 DC= .001
GAMMA= 72.5 DGAMMA= .1
BETA = 89.57 DBETA = .04
ALPHA= 76.04 DALPHA= .01
V= 805.0
7. 30-1481
Zn{Li,Nb}O4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.0900 6.0832 .0068 1 1 0
4.9100 4.9109 -.0009 -1 1 1
4.2900 4.2990 -.0090 0 2 0
3.5200 3.5168 .0032 2 1 1
3.4500 3.4491 .0009 -1 1 2
3.0300 3.0314 -.0014 2 0 2
3.0100 3.0094 .0006 0 2 2
2.8500 2.8493 .0007 1 2 2
2.7200 2.7192 .0008 1 3 0
2.5800 2.5806 -.0006 -3 1 1
2.5400 2.5416 -.0016 -1 1 3
2.4600 2.4554 .0046 -2 2 2
a= 8.609 b= 8.598 c= 8.429 beta= 89.2
da=.01 db=.003 dc= .002 dbeta=.1
V= 623.9
Triklin
Dexp Dcal d(D) h k l
6.0900 6.0877 .0023 1 1 0
4.9100 4.9183 -.0083 0 1 1
4.2900 4.2943 -.0043 0 -1 1
3.5200 3.5225 -.0025 2 -1 1
3.4500 3.4500 .0000 1 2 0
3.0300 3.0301 -.0001 1 0 2
3.0100 3.0122 -.0022 2 2 1
2.8500 2.8514 -.0014 2 0 2
2.7200 2.7211 -.0011 -1 0 2
2.5800 2.5783 .0017 -3 -1 1
2.5400 2.5385 .0015 3 0 2
2.4600 2.4592 .0008 0 2 2
A= 10.78 DA= .02
B= 7.251 DB= .002
C= 6.152 DC= .004
GAMMA= 84.75 DGAMMA= .09
BETA = 77.58 DBETA = .02
ALPHA= 81.20 DALPHA= .04
V= 463.38
8. 30-1846
C5H12Br5N2NbO
Rombik
Groupa 52
Dexp. Dcal. d(D) h k l
6.8100 6.8410 -.0310 1 0 1
4.9400 4.9409 -.0009 0 1 1
4.0400 4.0373 .0027 2 1 1
3.4270 3.4205 .0065 2 0 2
3.1870 3.1819 .0051 0 2 0
2.7150 2.7151 -.0001 3 1 2
2.6380 2.6380 .0000 5 0 1
2.4310 2.4329 -.0019 1 2 2
2.2550 2.2554 -.0004 4 2 1
a=14.007 b= 6.364 c= 7.840
da= .001 db= .002 dc= .001
V= 698.8
9. 30-1847
C5H10Cl5N2NbS
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
7.0400 7.0773 -.0373 0 1 0
6.3800 6.4008 -.0208 1 1 0
5.6500 5.6357 .0143 1 0 1
5.0200 5.0010 .0190 3 0 0
4.4200 4.4087 .0113 1 1 1
3.8690 3.8626 .0064 3 0 1
3.5370 3.5386 -.0016 0 2 0
2.7980 2.7936 .0044 0 1 2
2.5930 2.5980 -.0050 3 0 2
2.3620 2.3591 .0029 0 3 0
a=15.002940 b= 7.077255 c= 6.081019
da= .039425 db= .007814 dc= .017015
V=645.7
10. 30-1848
C5H12Cl5N2NbO
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
7.1000 7.1320 -.0320 1 0 0
5.0700 5.0594 .0106 -1 1 1
4.3400 4.3502 -.0102 1 0 2
4.1400 4.1430 -.0030 1 2 0
3.3640 3.3655 -.0015 2 1 0
3.1340 3.1369 -.0029 -1 0 3
2.8420 2.8390 .0030 2 2 1
2.6760 2.6756 .0004 1 3 2
2.4690 2.4687 .0003 -1 0 4
2.1270 2.1271 -.0001 2 1 4
2.0360 2.0359 .0001 0 5 0
1.9140 1.9141 -.0001 1 2 5
1.7430 1.7430 -.0000 -3 0 4
1.7430 1.7432 -.0002 4 1 1
1.6290 1.6291 -.0001 -1 6 1
1.5780 1.5780 .0000 3 4 3
a= 7.137 b= 10.1797 c= 10.6779 beta= 87.87
da=.002 db=.0001 dc=.0008 dbet=.01
V=775.0
11. 30-1849
C10H24Cl3N4NbO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.1000 7.0921 .0079 1 1 0
6.1100 6.1005 .0095 1 1 1
5.0700 5.0640 .0060 1 0 2
4.5600 4.5578 .0022 2 1 0
4.1400 4.1431 -.0031 1 2 1
3.4930 3.4913 .0017 -1 0 3
3.1340 3.1318 .0022 0 3 1
2.7550 2.7541 .0009 2 3 0
2.6000 2.6002 -.0002 -1 1 4
2.1760 2.1761 -.0001 4 0 3
1.9140 1.9139 .0001 4 1 4
1.7430 1.7430 -.0000 -4 4 1
1.6560 1.6562 -.0002 2 5 3
a= 10.315 b= 9.777 c= 11.336 beta= 87.28
da=.003 db=.001 dc=.002 dbeta=.02
V= 1142
12. 30-1850
C27H19N3Nb3O7
Triklin
Dexp Dcal d(D) h k l
8.5100 8.4991 .0109 0 1 1
8.2100 8.2937 -.0837 -1 1 0
7.8100 7.7649 .0451 0 -1 1
7.4200 7.4334 -.0134 0 2 0
6.7400 6.7600 -.0200 1 1 0
6.4300 6.3968 .0332 -1 2 0
6.2500 6.2362 .0138 -1 0 1
5.8000 5.7865 .0135 1 1 1
5.2300 5.2319 -.0019 1 -2 1
5.0600 5.0553 .0047 1 2 0
4.9500 4.9556 -.0056 0 3 0
4.8300 4.8359 -.0059 0 0 2
A= 8.79552 DA= .00003
B= 15.3488 DB= .0001
C= 9.72450 DC= .00002
GAMMA=103.2682 DGAMMA= .0003
BETA = 88.0956 DBETA = .0004
ALPHA= 84.94492 DALPHA= .00005
V=1275
13. 30-1851
C28H93N7Nb12O38*H2O
Triklin
Dexp Dcal d(D) h k l
13.1000 13.4113 -.3113 0 0 1
12.0000 12.0321 -.0321 1 0 0
9.9100 9.9083 .0017 0 1 0
8.5500 8.5439 .0061 0 -1 1
8.3600 8.3632 -.0032 1 0 1
8.0600 8.0577 .0023 -1 -1 1
5.8100 5.8193 -.0093 -2 0 1
4.5400 4.5403 -.0003 -2 1 1
4.0700 4.0739 -.0039 -3 -1 1
3.7290 3.7239 .0051 1 -2 2
3.6440 3.6435 .0005 3 1 1
3.3170 3.3158 .0012 0 -1 4
A= 12.488 DA= .005
B= 10.2663 DB= .0009
C= 13.76 DC= .01
GAMMA= 76.958 DGAMMA= .005
BETA =100.40 DBETA = .02
ALPHA= 99.85 DALPHA= .08
V= 1675
14. 30-1852
C5H12Cl5N2NbS
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
8.3100 8.3174 -.0074 2 0 1
7.1000 7.1185 -.0185 3 0 0
6.2500 6.2722 -.0222 3 0 1
5.6500 5.6336 .0164 2 0 2
5.0700 5.0792 -.0092 1 1 0
4.7500 4.7433 .0067 1 1 1
4.4400 4.4270 .0130 2 1 1
4.3400 4.3294 .0106 1 0 3
4.0800 4.0849 -.0049 2 0 3
3.7570 3.7558 .0012 3 0 3
3.4040 3.4052 -.0012 4 0 3
3.1660 3.1667 -.0007 2 0 4
a=21.355370 b= 5.229270 c=13.263580
da= .036754 db= .003635 dc= .005223
V=1481
Triklin
Dexp Dcal d(D) h k l
8.3100 8.3094 .0006 0 0 1
7.1000 7.1112 -.0112 1 0 0
6.2500 6.2411 .0089 0 -2 1
5.6500 5.6470 .0030 1 -2 1
5.0700 5.0770 -.0070 -1 0 1
4.7500 4.7419 .0081 -1 1 1
4.4400 4.4401 -.0001 1 2 0
4.3400 4.3407 -.0007 0 -1 2
4.0800 4.0803 -.0003 1 -2 2
3.7570 3.7562 .0008 1 2 1
3.4040 3.4047 -.0007 -1 4 0
3.1660 3.1663 -.0003 0 2 2
A= 7.48823 DA= .00004
B= 14.90744 DB= .00004
C= 8.89291 DC= .00001
GAMMA=106.6123 DGAMMA= .0003
BETA = 77.5127 DBETA = .0002
ALPHA=109.4636 DALPHA= .0003
V=887.9
15. 30-1853
C20H64N5Nb9O27*6H2O
Triklin
Dexp Dcal d(D) h k l
12.3000 12.3307 -.0307 1 0 0
10.2000 10.1897 .0103 0 1 0
10.0000 10.0226 -.0226 0 1 1
8.4800 8.4999 -.0199 1 0 1
8.0400 8.0147 .0253 -1 1 1
7.9200 7.9093 .0107 -1 1 0
7.8100 7.8013 .0087 1 1 0
7.5700 7.5602 .0098 1 1 1
6.5400 6.5479 -.0079 0 1 2
6.1600 6.1653 -.0053 2 0 0
5.6300 5.6249 .0051 1 1 2
5.5300 5.5343 -.0043 0 2 1
A= 12.3600 DA= .0002
B= 11.080 DB= .002
C= 13.484 DC= .004
GAMMA= 92.26 DGAMMA= .01
BETA = 93.87 DBETA = .01
ALPHA= 66.89 DALPHA= .01
V=1696
16. 30-1853
C20H64N5Nb9O27*6H2O
Triklin
Dexp Dcal d(D) h k l
12.3000 12.3133 -.0133 0 0 1
10.2000 10.1785 .0215 0 1 0
10.0000 10.0212 -.0212 0 -1 1
8.4800 8.4847 -.0047 2 0 1
8.0400 7.9977 .0423 -2 -1 1
7.9200 7.8915 .0285 2 1 0
7.8100 7.8135 -.0035 -2 1 0
7.5700 7.5779 -.0079 2 -1 1
6.5400 6.5376 .0024 -3 -1 1
6.1600 6.1567 .0033 0 0 2
5.6300 5.6352 -.0052 -2 0 2
5.5300 5.5364 -.0064 0 -2 1
A= 24.73 DA= .05
B= 11.082 DB= .001
C= 13.4261 DC= .0003
GAMMA= 88.01 DGAMMA= .01
BETA = 93.71 DBETA = .09
ALPHA=113.30 DALPHA= .05
V= 3373
17. 31-0469
C4{NbO3}2*4H2O
Triklin
Dexp Dcal d(D) h k l
3.6480 3.6454 .0026 0 1 1
2.9440 2.9435 .0005 2 1 0
2.7420 2.7418 .0002 -2 -1 1
2.5200 2.5200 -.0000 2 1 1
2.3240 2.3231 .0009 3 1 0
2.2900 2.2892 .0008 -3 -1 1
2.2350 2.2333 .0017 0 -1 2
2.1800 2.1807 -.0007 -2 -1 2
2.0700 2.0705 -.0005 -1 2 1
1.8790 1.8797 -.0007 0 -2 1
1.8630 1.8627 .0003 -1 -2 1
1.7940 1.7940 .0000 -3 2 1
1.7130 1.7126 .0004 -3 2 0
1.5030 1.5046 -.0016 -4 -1 3
A= 9.01 DA= .02
B= 4.234 DB= .001
C= 6.1494 DC= .0006
GAMMA= 94.61 DGAMMA= .09
BETA =107.92 DBETA = .06
ALPHA= 80.72 DALPHA= .02
V= 220.2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.6480 3.6491 -.0011 2 1 0
2.9440 2.9421 .0019 1 0 3
2.7420 2.7396 .0024 1 1 3
2.5200 2.5207 -.0007 3 1 1
2.3240 2.3260 -.0020 1 3 1
2.2900 2.2906 -.0006 3 1 2
2.2350 2.2362 -.0012 3 2 0
2.1800 2.1794 .0006 3 2 1
2.0700 2.0700 .0000 -3 0 3
1.8790 1.8791 -.0001 0 0 5
1.8630 1.8617 .0013 3 3 0
1.7940 1.7940 -.0000 4 2 1
1.7130 1.7130 .0000 2 4 0
1.5030 1.5031 -.0001 0 3 5
a= 8.349 b= 7.51365 c=9.396 beta=89.41
da=.002 db=.00001 dc=.007 dbeta=.08
V= 589.4
18. 31-0903
Ni8NbB3O15
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8400 5.8255 .0145 1 0 1
5.3000 5.2911 .0089 0 2 0
5.1200 5.1033 .0167 1 1 1
4.8900 4.8745 .0155 2 0 1
3.5300 3.5274 .0026 0 3 0
3.0400 3.0374 .0026 0 3 1
2.9150 2.9127 .0023 2 0 2
2.6480 2.6457 .0023 -4 1 1
2.6110 2.6131 -.0021 3 1 2
2.5340 2.5327 .0013 5 1 1
2.4600 2.4602 -.0002 2 4 0
2.4280 2.4278 .0002 -4 2 1
2.3110 2.3115 -.0005 -3 0 2
2.2300 2.2301 -.0001 6 0 0
2.1860 2.1887 -.0027 3 4 1
a= 13.6 b= 10.582 c= 6.057 beta= 80.5
da=.1 db=.008 dc=.002 dbeta=.1
V= 857.7
Triklin
Dexp Dcal d(D) h k l
5.8400 5.8302 .0098 1 0 0
5.3000 5.2961 .0039 -1 1 0
5.1200 5.1239 -.0039 0 0 1
4.8900 4.8603 .0297 0 -1 1
3.5300 3.5296 .0004 0 1 1
3.0400 3.0415 -.0015 2 -1 1
2.9150 2.9151 -.0001 2 0 0
2.6480 2.6481 -.0001 -2 2 0
2.6110 2.6096 .0014 1 -2 2
2.5340 2.5301 .0039 1 2 0
2.4600 2.4592 .0008 -1 -2 1
2.4280 2.4302 -.0022 0 -2 2
A= 6.394 DA= .003
B= 7.526 DB= .009
C= 5.607 DC= .008
GAMMA=113.0515 DGAMMA= .0003
BETA = 74.63 DBETA = .03
ALPHA=112.76 DALPHA= .02
V=227.1
19. 31-0904
Ni2NbBO6
Triklin
Dexp Dcal d(D) h k l
5.0500 5.0506 -.0006 1 -1 1
4.3400 4.3352 .0048 1 1 0
3.7000 3.7007 -.0007 1 -1 2
3.2700 3.2710 -.0010 2 -1 2
3.1300 3.1297 .0003 2 0 2
2.6860 2.6847 .0013 3 -1 2
2.5640 2.5635 .0005 3 0 2
2.4110 2.4113 -.0002 0 0 3
2.3520 2.3521 -.0001 3 1 1
2.2760 2.2760 .0000 4 -1 1
2.2440 2.2435 .0005 4 0 0
A= 9.3250 DA= .0001
B= 5.699 DB= .001
C= 7.92281 DC= .00006
GAMMA=101.144 DGAMMA= .004
BETA = 75.61 DBETA = .01
ALPHA=111.44 DALPHA= .01
V=377.3
20. 31-0905
Ni3Nb2O8
Triklin
Dexp Dcal d(D) h k l
5.4000 5.4098 -.0098 0 0 1
4.4600 4.4600 -.0000 -1 0 1
3.8300 3.8258 .0042 0 -2 1
3.7000 3.6950 .0050 -1 2 0
3.2100 3.2154 -.0054 1 0 1
3.1400 3.1382 .0018 1 1 1
3.0500 3.0508 -.0008 1 -1 1
2.7780 2.7783 -.0003 -1 0 2
2.7340 2.7348 -.0008 1 -2 1
2.6630 2.6595 .0035 0 1 2
2.5620 2.5619 .0001 0 4 1
2.5170 2.5173 -.0003 1 3 1
2.4830 2.4827 .0003 2 1 0
2.3660 2.3655 .0005 -2 2 1
2.2660 2.2672 -.0012 -1 3 2
A= 5.318 DA= .001
B= 11.361 DB= .002
C= 5.707 DC= .004
GAMMA= 88.46 DGAMMA= .03
BETA =108.40 DBETA = .04
ALPHA= 87.936 DALPHA= .002
V= 326.7
21. 31-0905
KNbO3
Triklin
Dexp Dcal d(D) h k l
8.5700 8.5648 .0052 0 1 1
8.1900 8.1781 .0119 1 1 0
7.6900 7.6913 -.0013 0 -1 1
7.2000 7.2001 -.0001 -1 -1 1
6.8400 6.8304 .0096 1 1 1
5.9700 5.9779 -.0079 -1 0 2
3.8670 3.8674 -.0004 1 1 3
3.8180 3.8183 -.0003 -2 1 1
3.4310 3.4328 -.0018 1 2 3
3.3820 3.3808 .0012 -1 0 4
3.2530 3.2509 .0021 -3 -1 1
3.1920 3.1923 -.0003 1 -2 2
A= 9.798 DA= .008
B= 10.613 DB= .006
C= 13.824 DC= .001
GAMMA= 72.75 DGAMMA= .06
BETA = 98.23 DBETA = .01
ALPHA= 86.368 DALPHA= .002
V= 1350.2
22. 31-1060
K2Nb8O21
Triklin
Dexp Dcal d(D) h k l
11.8000 11.8248 -.0248 1 0 0
10.6000 10.5993 .0007 1 1 0
9.3600 9.3410 .0190 0 1 1
8.8000 8.7854 .0146 -1 0 1
7.4700 7.4740 -.0040 0 -1 1
6.4200 6.4194 .0006 -1 1 1
6.1500 6.1824 -.0324 0 0 2
5.5800 5.5744 .0056 1 -1 1
5.1900 5.1863 .0037 2 2 1
4.4100 4.4118 -.0018 -2 1 1
4.1300 4.1316 -.0016 3 2 0
4.0700 4.0718 -.0018 1 1 3
A= 13.03 DA= .01
B= 12.51 DB= .01
C= 12.69 DC= .01
GAMMA= 65.31 DGAMMA= .05
BETA = 87.51 DBETA = .07
ALPHA= 77.38 DALPHA= .08
V= 1831.4
23. 31-1061
K2Nb16O41
Triklin
Dexp Dcal d(D) h k l
19.5000 19.4374 .0626 1 0 0
13.7000 13.7264 -.0264 0 1 0
12.2000 12.1962 .0038 0 0 1
9.6700 9.6690 .0010 1 1 1
8.6500 8.6619 -.0119 -1 1 1
7.6000 7.5972 .0028 1 -1 1
6.6600 6.6554 .0046 1 2 0
5.3900 5.3903 -.0003 -2 2 0
5.1000 5.0985 .0015 3 -1 1
4.8500 4.8450 .0050 -2 -2 1
4.7100 4.7111 -.0011 4 1 0
4.5200 4.5198 .0002 -3 2 0
A= 19.6116 DA= .0003
B= 14.163 DB= .001
C= 12.576 DC= .005
GAMMA= 83.84 DGAMMA= .02
BETA = 84.20 DBETA = .04
ALPHA= 76.62 DALPHA= .02
V=3366
24. 31-1062
K2Nb24O61
Geksag.
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
11.2000 11.3173 -.1173 0 0 1
9.1200 9.0815 .0385 1 0 1
8.9800 9.0815 -.1015 1 0 1
6.2800 6.3147 -.0347 2 0 1
5.6200 5.6586 -.0386 0 0 2
5.3100 5.3039 .0061 1 0 2
4.6200 4.6291 -.0091 3 0 1
3.7790 3.7773 .0017 3 0 2
3.6630 3.6616 .0014 1 0 3
3.6070 3.6063 .0007 4 0 1
3.3910 3.3833 .0077 3 1 2
3.3330 3.3363 -.0033 3 2 1
a= 17.573 c= 11.32
da=.001 dc= .03
V=3026
Triklin
Dexp Dcal d(D) h k l
11.2000 11.2043 -.0043 1 0 0
9.1200 9.1437 -.0237 1 1 0
8.9800 8.9764 .0036 0 0 1
6.2800 6.2861 -.0061 -1 -2 1
5.6200 5.6022 .0178 2 0 0
5.3100 5.3102 -.0002 -1 1 1
4.6200 4.6219 -.0019 -3 -1 1
3.7790 3.7806 -.0016 -2 -2 3
3.6630 3.6639 -.0009 -2 -1 3
3.6070 3.6063 .0007 0 -3 1
3.3910 3.3911 -.0001 -2 1 2
3.3330 3.3313 .0017 2 2 1
A= 14.142 DA= .005
B= 12.645 DB= .008
C= 11.398 DC= .003
GAMMA= 58.92 DGAMMA= .03
BETA =123.22 DBETA = .01
ALPHA=121.66 DALPHA= .01
V= 1374.6
25. 31-1062
K4Nb6O17
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.0200 8.0350 -.0150 0 0 1
5.4300 5.4338 -.0038 1 1 0
4.0900 4.1006 -.0106 0 2 0
3.2780 3.2772 .0008 2 1 1
2.7360 2.7338 .0022 0 3 0
2.3480 2.3473 .0007 3 1 1
2.2470 2.2473 -.0003 1 2 3
2.0530 2.0509 .0021 -1 2 3
1.9860 1.9867 -.0007 0 4 1
1.9510 1.9511 -.0001 0 1 4
1.8270 1.8264 .0006 1 2 4
1.7780 1.7786 -.0006 2 4 1
1.6440 1.6439 .0001 -3 0 3
1.4940 1.4945 -.0005 2 5 0
1.3720 1.3720 -.0000 -1 4 4
a= 7.394 b= 8.201 c= 8.189 beta= 78.86
da=.005 db=.003 dc=.006 dbeta=.04
V= 487.2
26. 31-1064
K4NbO17
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
16.4000 16.5468 -.1468 0 0 2
8.2800 8.2734 .0066 0 0 4
7.0600 7.0539 .0061 0 1 2
5.6800 5.6746 .0054 0 1 4
5.6000 5.5769 .0231 1 0 3
5.1000 5.0936 .0064 1 0 4
4.6300 4.6244 .0056 1 0 5
4.5400 4.5362 .0038 1 1 3
4.2700 4.2645 .0055 1 1 4
4.2000 4.1957 .0043 1 0 6
3.7980 3.7951 .0029 0 2 2
3.5250 3.5270 -.0020 0 2 4
a= 6.46 b= 7.798 c=33.09
da= .01 db= .003 dc= .01
v=1668
27. 31-1065
K8Nb18O49
Triklin
Dexp Dcal d(D) h k l
9.3800 9.3631 .0169 1 0 1
8.4500 8.4708 -.0208 0 1 1
7.2400 7.2491 -.0091 0 -1 1
6.9300 6.9105 .0195 1 1 0
6.0600 6.0678 -.0078 1 0 2
5.4600 5.4590 .0010 0 1 2
5.1800 5.1786 .0014 -1 -1 1
4.6900 4.6869 .0031 1 2 1
7.4400 7.4311 .0089 -1 1 0
4.2500 4.2488 .0012 -1 1 2
3.9040 3.9028 .0012 -2 1 1
3.8180 3.8199 -.0019 -1 -2 1
A= 10.519 DA= .004
B= 10.62 DB= .01
C= 12.6188 DC= .0001
GAMMA= 91.00 DGAMMA= .04
BETA = 68.95 DBETA = .07
ALPHA= 82.03 DALPHA= .02
V= 1299
28. 31-1402
TiNbO7
Triklin
Dexp Dcal d(D) h k l
5.1500 5.1490 .0010 -1 0 1
3.7000 3.6904 .0096 -1 1 1
3.6100 3.6085 .0015 1 -1 1
3.4600 3.4537 .0063 0 -1 1
3.3900 3.3899 .0001 -1 0 2
3.3100 3.3092 .0008 -2 0 1
3.1500 3.1500 .0000 1 0 3
2.9400 2.9386 .0014 -2 1 1
2.8800 2.8808 -.0008 3 0 2
2.7800 2.7829 -.0029 2 -1 2
2.6700 2.6711 -.0011 0 1 3
2.5900 2.5872 .0028 3 -1 1
A= 9.041 DA= .004
B= 4.253 DB= .005
C= 9.573 DC= .002
GAMMA= 97.1 DGAMMA= .1
BETA = 69.69 DBETA = .02
ALPHA= 80.91 DALPHA= .07
V= 334.5
29. 31-1812
C10H28Cl3N3NbO3P
Triklin
Dexp Dcal d(D) h k l
6.8200 6.8149 .0051 1 0 0
5.6200 5.6248 -.0048 -1 1 1
5.1600 5.1599 .0001 -1 -1 1
4.6200 4.6163 .0037 1 0 1
4.3400 4.3426 -.0026 -1 2 1
4.0800 4.0858 -.0058 -1 2 0
3.7890 3.7915 -.0025 0 2 2
3.5220 3.5234 -.0014 0 -1 2
3.2090 3.2093 -.0003 1 -2 1
3.0400 3.0394 .0006 -1 3 2
2.8240 2.8230 .0010 1 -1 2
2.6300 2.6293 .0007 -1 4 1
A= 7.111 DA= .001
B= 11.511 DB= .004
C= 8.738 DC= .004
GAMMA= 87.83 DGAMMA= .03
BETA =105.38 DBETA = .09
ALPHA= 75.77 DALPHA= .05
V= 664.4
30. 31-1813
C16H20Cl3NbO3S
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
7.9900 7.9542 .0358 1 1 0
6.6600 6.6633 -.0033 0 0 1
5.7600 5.7375 .0225 2 0 1
4.9900 4.9878 .0022 3 0 1
4.3000 4.3018 -.0018 3 1 1
3.8350 3.8409 -.0059 4 1 1
3.4410 3.4393 .0017 6 1 0
2.6080 2.6073 .0007 0 3 1
2.4630 2.4635 -.0005 3 3 1
a=22.57 b= 8.4997 c= 6.66
da= .01 db= .0004 dc= .01
V=1278
31. 31-1814
C22H25AsCl3NbO3
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
9.2100 9.2377 -.0277 1 2 0
7.0400 7.0186 .0214 1 3 0
6.1500 6.1687 -.0187 2 2 0
4.9900 5.0024 -.0124 1 1 1
4.3600 4.3517 .0083 2 0 1
3.5480 3.5495 -.0015 4 1 0
3.3520 3.3529 -.0009 1 7 0
3.0190 3.0173 .0017 0 8 0
2.7800 2.7815 -.0015 2 8 0
2.5930 2.5924 .0006 5 4 0
2.4140 2.4138 .0002 0 10 0
2.3130 2.3130 -.0000 3 8 1
a=14.354 b=24.138 c= 5.472
da= .009 db= .001 dc= .008
v=1896
Triklin
Dexp Dcal d(D) h k l
9.2100 9.3150 -.1050 0 0 1
7.0400 7.0369 .0031 -1 0 1
6.1500 6.1512 -.0012 0 1 1
4.9900 4.9886 .0014 0 -1 1
4.3600 4.3583 .0017 2 0 0
3.5480 3.5488 -.0008 -1 2 0
3.3520 3.3518 .0002 -1 2 2
3.0190 3.0194 -.0004 -2 1 3
2.7800 2.7797 .0003 -2 0 3
2.5930 2.5929 .0001 1 2 2
2.4140 2.4143 -.0003 3 1 0
2.3130 2.3129 .0001 0 3 1
A= 9.512 DA= .001
B= 7.4477 DB= .0004
C= 9.9060 DC= .0003
GAMMA=111.261 DGAMMA= .007
BETA =105.58 DBETA = .01
ALPHA= 73.019 DALPHA= .002
V= 615.0
32. 31-1815
C22H25Cl3NbO3P
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
8.2200 8.2188 .0012 1 0 2
7.1000 7.1299 -.0299 2 0 2
6.0000 5.9994 .0006 3 0 2
5.5100 5.4941 .0159 0 1 0
5.0200 5.0240 -.0040 2 1 0
4.7700 4.7751 -.0051 5 0 1
4.3600 4.3550 .0050 0 0 4
4.0200 4.0257 -.0057 6 0 1
3.7390 3.7374 .0016 6 0 2
3.5480 3.5466 .0014 7 0 0
3.3900 3.3928 -.0028 5 1 2
3.0590 3.0552 .0038 8 0 1
a=24.826 b= 5.4941 c=17.420
da= .005 db= .0006 dc= .003
v=2376
Triklin
Dexp Dcal d(D) h k l
8.2200 8.2264 -.0064 0 1 1
7.1000 7.0979 .0021 1 0 0
6.0000 5.9997 .0003 1 1 0
5.5100 5.5108 -.0008 0 2 1
5.0200 5.0095 .0105 1 -1 1
4.7700 4.7697 .0003 1 2 1
4.3600 4.3683 -.0083 0 0 2
4.0200 4.0186 .0014 1 2 2
3.7390 3.7415 -.0025 1 -2 1
3.5480 3.5489 -.0009 2 0 0
3.3900 3.3899 .0001 2 1 0
3.0590 3.0580 .0010 0 -3 1
A= 7.377 DA= .005
B= 11.671 DB= .005
C= 9.57 DC= .01
GAMMA= 84.23 DGAMMA= .07
BETA = 74.2 DBETA = .1
ALPHA= 70.75 DALPHA= .04051
V= 748.4
33. 31-1816
C24H20Cl3NbO3S2
Triklin
Dexp Dcal d(D) h k l
7.5600 7.5597 .0003 0 0 1
6.7600 6.7487 .0113 1 0 0
5.9800 5.9772 .0028 0 -2 1
5.5100 5.5099 .0001 0 2 1
5.1900 5.1864 .0036 -1 2 0
4.4200 4.4176 .0024 1 0 1
3.8350 3.8345 .0005 -1 -1 2
3.5330 3.5336 -.0006 1 -3 1
3.2900 3.2906 -.0006 0 -5 1
2.9890 2.9886 .0004 0 -4 2
2.8850 2.8854 -.0004 1 1 2
2.6740 2.6742 -.0002 2 2 1
A= 7.1092 DA= .0007
B= 17.7053 DB= .0004
C= 7.9727 DC= .0009
GAMMA= 84.485 DGAMMA= .006
BETA =107.94 DBETA = .01
ALPHA= 96.173 DALPHA= .00722
V= 947.1
34. 31-1817
C36H30Cl3NbO3P2
Triklin
Dexp Dcal d(D) h k l
8.8400 8.8524 -.0124 1 0 0
7.3800 7.3757 .0043 0 1 1
6.3400 6.3372 .0028 0 -1 1
5.5500 5.5532 -.0032 1 1 1
4.9400 4.9366 .0034 0 2 1
4.4400 4.4358 .0042 1 0 2
4.0400 4.0422 -.0022 1 1 2
3.8690 3.8674 .0016 -2 1 1
3.5640 3.5638 .0002 -1 0 2
2.8850 2.8860 -.0010 3 -3 1
2.5640 2.5639 .0001 -2 -2 1
2.3100 2.3102 -.0002 1 -5 0
A= 9.898 DA= .001
B= 11.7213 DB= .0007
C= 9.123 DC= .001
GAMMA=111.720 DGAMMA= .007
BETA = 76.6163 DBETA = .0003
ALPHA= 86.951 DALPHA= .009
V= 945.2
35. 31-1818
C32H96N8Nb6O19*33H2O
Triklin
Dexp Dcal d(D) h k l
14.0000 14.0041 -.0041 0 1 1
13.3000 13.2410 .0590 0 -1 1
12.0000 11.9955 .0045 1 1 0
10.8000 10.7824 .0176 -1 -1 1
9.8600 9.8728 -.0128 0 0 2
8.6700 8.6691 .0009 0 2 1
8.5500 8.5434 .0066 0 -1 2
8.4000 8.3951 .0049 -1 2 0
8.3000 8.3001 -.0001 0 -2 1
8.1900 8.1943 -.0043 -2 0 1
7.4800 7.4876 -.0076 -1 -2 1
7.2800 7.2781 .0019 -2 -1 1
A= 16.8454 DA= .0004
B= 18.8635 DB= .0007
C= 20.1928 DC= .0006
GAMMA= 94.491 DGAMMA= .002
BETA =101.660 DBETA = .001
ALPHA= 85.963 DALPHA= .003
V=6293