1. 24-0113
Ba0.65NbO3
Triklin
Dexp Dcal d(D) h k l
3.5800 3.5831 -.0031 -1 1 1
3.4800 3.4761 .0039 0 -1 1
3.2500 3.2504 -.0004 1 -1 1
3.1400 3.1452 -.0052 0 0 2
3.0400 3.0378 .0022 -2 1 0
2.9600 2.9556 .0044 1 0 2
2.8700 2.8696 .0004 -1 0 2
2.8100 2.8062 .0038 -2 1 1
2.6300 2.6277 .0023 1 1 2
2.3400 2.3422 -.0022 -3 0 1
2.1900 2.1882 .0018 3 1 0
2.1500 2.1513 -.0013 1 2 1
2.0300 2.0310 -.0010 3 0 2
1.9900 1.9901 -.0001 -2 2 1
A= 7.7174 DA= .0006
B= 4.65106 DB= .00008
C= 6.36244 DC= .00001
GAMMA= 92.965 DGAMMA= .007
BETA = 88.046 DBETA = .005
ALPHA= 81.7134 DALPHA= .0003
V=225.5
2. 24-1304
TlNbO3
Triklin
Dexp Dcal d(D) h k l
3.7500 3.7482 .0018 1 1 2
3.0400 3.0401 -.0001 2 0 2
2.8900 2.8894 .0006 1 -1 2
2.6800 2.6798 .0002 0 2 0
2.3600 2.3601 -.0001 2 -1 2
2.0900 2.0902 -.0002 2 1 4
2.0300 2.0300 .0000 2 0 4
1.9320 1.9322 -.0002 -2 2 0
1.8920 1.8921 -.0001 -1 1 4
1.8600 1.8600 -.0000 -3 -2 1
1.7600 1.7599 .0001 4 0 2
1.6400 1.6399 .0001 -1 2 4
A= 7.4819 DA= .0003
B= 5.6155 DB= .0001
C= 9.016 DC= .001
GAMMA= 74.586 DGAMMA= .004
BETA = 76.721 DBETA = .006
ALPHA= 78.875 DALPHA= .008
V=352
3. 24-1305
TlNbO3
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
3.0100 3.0127 -.0027 2 3 0
2.6000 2.6030 -.0030 1 4 0
2.0500 2.0484 .0016 1 4 1
1.8600 1.8590 .0010 3 5 0
1.5850 1.5854 -.0004 0 2 2
1.5400 1.5393 .0007 7 2 0
1.3200 1.3202 -.0002 3 4 2
1.1750 1.1753 -.0003 8 5 0
1.1250 1.1250 -.0000 10 0 0
1.0750 1.0748 .0002 6 5 2
1.0350 1.0350 -.0000 8 7 0
a=11.2502 b=10.7023 c= 3.3198
da= .0009 db= .0006 dc= .0004
V= 399.72
Triklin
Dexp Dcal d(D) h k l
3.0100 3.0103 -.0003 -1 0 1
2.6000 2.5996 .0004 0 1 1
2.0500 2.0502 -.0002 0 -1 1
1.8600 1.8601 -.0001 -2 1 1
1.5850 1.5849 .0001 2 -1 1
1.5400 1.5400 .0000 0 2 1
1.3200 1.3200 .0000 -3 0 2
1.1750 1.1750 .0000 5 1 0
1.1250 1.1250 -.0000 5 1 1
1.0750 1.0749 .0001 -2 0 3
1.0350 1.0350 .0000 -1 -2 2
A= 6.018 DA= .002
B= 3.1981 DB= .00007
C= 3.4930 DC= .0009
GAMMA= 80.715 DGAMMA= .009
BETA = 90.54 DBETA = .04
ALPHA= 76.73 DALPHA= .01
V= 64.49
4. 24-1746
C16H40Cl5NbO
Triklin
Dexp Dcal d(D) h k l
7.9400 7.9218 .0182 -1 0 1
7.4500 7.4757 -.0257 0 1 1
7.0800 7.0869 -.0069 0 -1 1
6.7000 6.6953 .0047 1 0 1
6.3700 6.3731 -.0031 1 1 0
5.8900 5.8977 -.0077 0 0 2
5.3900 5.3986 -.0086 -1 0 2
5.1000 5.0999 .0001 0 1 2
4.8500 4.8518 -.0018 0 -1 2
4.6100 4.6099 .0001 1 0 2
4.5200 4.5169 .0031 -1 -1 2
4.1700 4.1700 -.0000 -2 1 0
A= 9.3047 DA= .0006
B= 9.2654 DB= .0002
C= 11.9978 DC= .0009
GAMMA= 92.95 DGAMMA= .04
BETA =100.07 DBETA = .01
ALPHA= 86.394 DALPHA= .005
V=1015
5. 24-1789
C16H30Cl2N3NbS6
Triklin
Dexp Dcal d(D) h k l
11.4000 11.3847 .0153 1 0 0
10.5000 10.5245 -.0245 0 1 0
7.9400 7.9329 .0071 -1 0 1
7.6300 7.5922 .0378 1 -1 1
7.0600 7.0642 -.0042 -1 -1 1
6.3900 6.3950 -.0050 0 1 1
5.8000 5.7930 .0070 -1 1 1
5.2900 5.2823 .0077 1 -2 1
4.9100 4.9123 -.0023 -1 0 2
4.7700 4.7720 -.0020 0 -2 2
4.2300 4.2340 -.0040 2 -2 1
3.9900 3.9895 .0005 -2 -1 2
A= 11.457 DA= .006
B= 11.446 DB= .008
C= 11.602 DC= .005
GAMMA= 96.178 DGAMMA= .004
BETA = 89.32 DBETA = .05
ALPHA=112.306 DALPHA= .002
V=1400
6. 24-1844
C20H40BrN4NbS8
Triklin
Dexp Dcal d(D) h k l
14.1000 14.0586 .0414 1 0 0
10.0000 10.0054 -.0054 -1 1 0
8.7200 8.7152 .0048 0 -1 1
7.6600 7.6614 -.0014 1 1 0
7.3100 7.3092 .0008 -1 -1 1
7.0300 7.0293 .0007 2 0 0
6.9700 6.9667 .0033 0 1 1
6.6500 6.6508 -.0008 -2 0 1
5.5700 5.5712 -.0012 1 1 1
5.2900 5.2896 .0004 2 1 0
5.1800 5.1804 -.0004 -1 -1 2
A= 14.85 DA= .01
B= 11.458 DB= .005
C= 11.358 DC= .007
GAMMA=103.3 DGAMMA= .2
BETA =100.602 DBETA = .005
ALPHA= 99.70 DALPHA= .01
V=1809
7. 25-1743
C15H30N3NbOS6
Triklin
Dexp Dcal d(D) h k l
10.9000 10.9041 -.0041 0 1 1
8.4500 8.4350 .0150 0 -1 1
7.3100 7.3060 .0040 1 -1 0
6.7700 6.7628 .0072 1 1 1
6.6700 6.6533 .0167 -1 -1 1
6.0400 6.0359 .0041 1 -1 1
5.6900 5.6895 .0005 0 0 3
5.3800 5.3855 -.0055 -1 0 3
5.0200 5.0234 -.0034 -1 2 2
4.8200 4.8209 -.0009 1 -1 2
4.7700 4.7750 -.0050 2 0 0
4.6000 4.5985 .0015 -2 1 1
A= 9.765 DA= .003
B= 11.78971 DB= .00004
C= 18.141 DC= .009
GAMMA= 93.431 DGAMMA= .003
BETA =102.060 DBETA = .005
ALPHA= 73.8234 DALPHA= .0005
V= 1961.6
8. 25-1777
C10H12Br12Cl6N2Nb6
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
9.7200 9.6390 .0810 0 1 1
6.9800 6.9789 .0011 1 0 0
6.6500 6.6522 -.0022 0 2 1
5.6600 5.6598 .0002 0 1 2
5.3200 5.3071 .0129 0 3 0
4.8200 4.8195 .0005 0 2 2
4.4000 4.3959 .0041 1 1 2
4.0400 4.0369 .0031 0 0 3
3.7800 3.7813 -.0013 0 4 1
3.3300 3.3261 .0039 0 4 2
3.2800 3.2811 -.0011 2 1 1
3.2100 3.2130 -.0030 0 3 3
a= 6.9789 b=15.92 c=12.111
da= .0007 db= .01 dc= .001
V=1346
Triklin
Dexp Dcal d(D) h k l
9.7200 9.6878 .0322 1 0 0
6.9800 6.9836 -.0036 0 1 1
6.6500 6.6457 .0043 0 -1 1
5.6600 5.6602 -.0002 -1 -1 1
5.3200 5.3164 .0036 1 -1 1
4.8200 4.8177 .0023 0 2 0
4.4000 4.3990 .0010 -1 0 2
4.0400 4.0390 .0010 -1 1 2
3.7800 3.7810 -.0010 1 -1 2
3.3300 3.3296 .0004 2 0 2
3.2800 3.2813 -.0013 1 2 2
3.2100 3.2099 .0001 -1 -2 2
A= 9.7098 DA= .0001
B= 9.657 DB= .002
C= 9.645 DC= .002
GAMMA= 87.49 DGAMMA= .01
BETA = 92.803 DBETA = .003
ALPHA= 87.2948 DALPHA= .0009
V= 901.3
9. 26-1380
NaNbO3
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
4.8000 4.7966 .0034 1 1 1
3.7900 3.8091 -.0191 1 2 0
3.3600 3.3600 .0000 0 2 2
3.2900 3.2934 -.0034 0 0 3
3.0600 3.0511 .0089 2 1 1
2.9700 2.9681 .0019 1 0 3
2.7900 2.7905 -.0005 1 3 0
2.6900 2.6904 -.0004 2 1 2
2.6000 2.5987 .0013 0 3 2
2.4700 2.4701 -.0001 0 0 4
2.3900 2.3850 .0050 0 1 4
2.3000 2.2979 .0021 2 1 3
a= 6.849 b= 9.167 c= 9.880
da= .003 db= .004 dc= .003
v= 620.3
10. 27-1277
Na11Nb9O28*24H2O
Triklin
Dexp Dcal d(D) h k l
13.2000 13.1915 .0085 1 0 0
12.0000 12.0081 -.0081 0 1 0
11.2000 11.1895 .0105 1 0 1
10.6000 10.5701 .0299 0 -1 1
9.4400 9.4639 -.0239 1 1 0
7.2500 7.2481 .0019 -1 0 1
6.4800 6.4654 .0146 2 -1 1
5.8300 5.8367 -.0067 2 1 1
3.5900 3.5895 .0005 4 0 1
5.2800 5.2850 -.0050 0 -2 2
4.5300 4.5338 -.0038 3 -1 1
4.2500 4.2512 -.0012 1 -2 3
A= 14.506 DA= .007
B= 13.0674 DB= .0001
C= 13.466 DC= .006
GAMMA= 92.87 DGAMMA= .01
BETA = 66.35 DBETA = .03
ALPHA=112.24 DALPHA= .03
V= 2148.6
11. 28-0326
CsNbO{SO4}2
Triklin
Dexp Dcal d(D) h k l
8.8000 8.8007 -.0007 -1 0 1
4.8700 4.8690 .0010 3 0 3
4.5300 4.5339 -.0039 0 -1 1
4.2600 4.2605 -.0005 -1 0 3
3.9300 3.9325 -.0025 0 -1 2
3.7400 3.7389 .0011 3 1 3
3.6800 3.6807 -.0007 -2 -1 1
3.5300 3.5312 -.0012 3 1 0
3.3500 3.3488 .0012 0 -1 3
3.0400 3.0401 -.0001 3 1 5
2.9600 2.9597 .0003 1 1 5
2.9000 2.9003 -.0003 4 1 5
A= 16.836 DA= .005
B= 4.99161 DB= .00008
C= 17.572 DC= .001
GAMMA= 84.68 DGAMMA= .01
BETA = 61.69 DBETA = .01
ALPHA= 81.205 DALPHA= .007
V=1284
12. 28-0469
InNbO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.6900 3.6895 .0005 2 -1 0
2.9930 2.9931 -.0001 2 0 2
2.5640 2.5645 -.0005 1 -1 3
2.5160 2.5160 -.0000 0 3 0
2.4110 2.4114 -.0004 1 -3 0
2.2320 2.2318 .0002 3 -1 2
2.1150 2.1151 -.0001 4 0 0
2.0910 2.0909 .0001 2 -3 1
1.9170 1.9166 .0004 2 0 4
1.8420 1.8419 .0001 1 4 0
1.7430 1.7430 -.0000 -2 2 4
1.4650 1.4651 -.0001 3 0 5
A= 8.4642 DA= .0001
B= 7.54814 DB= .00008
C= 8.7379 DC= .0007
GAMMA= 89.983 DGAMMA= .001
BETA = 91.754 DBETA = .007
ALPHA= 89.97 DALPHA= .01
V=558.0
Triklin
Dexp Dcal d(D) h k l
3.6900 3.6887 .0013 -1 0 1
2.9930 2.9931 -.0001 -1 1 1
2.5640 2.5638 .0002 -1 0 2
2.5160 2.5190 -.0030 1 1 0
2.4110 2.4106 .0004 -1 1 2
2.2320 2.2313 .0007 -1 -1 1
2.1150 2.1147 .0003 -2 1 0
2.0910 2.0908 .0002 -2 1 1
1.9170 1.9172 -.0002 2 -1 1
1.8420 1.8420 -.0000 1 0 3
1.7430 1.7426 .0004 2 1 0
1.4650 1.4650 .0000 -2 -1 2
A= 4.657 DA= .001
B= 3.630 DB= .001
C= 6.241 DC= .002
GAMMA=102.57 DGAMMA= .02
BETA = 93.85 DBETA = .03
ALPHA= 78.31 DALPHA= .02
V= 100.8
13. 28-0533
PbNb4F22
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
9.8000 9.7759 .0241 2 0 0
8.9000 8.8545 .0455 2 0 1
5.5700 5.5921 -.0221 -1 0 3
5.1100 5.0941 .0159 -3 0 2
4.9100 4.9195 -.0095 0 1 1
4.4300 4.4302 -.0002 2 1 1
4.1900 4.1845 .0055 2 0 4
4.1000 4.1000 .0000 2 1 2
3.9600 3.9599 .0001 -2 0 4
3.9100 3.9104 -.0004 5 0 0
3.8800 3.8796 .0004 5 0 1
3.8200 3.8201 -.0001 3 0 4
a= 19.604 b= 5.117 c= 17.9402 beta= 85.82
da=.005 db=.002 dc= .0004 dbet=.01
V=1790
Triklin
Dexp Dcal d(D) h k l
9.8000 9.7802 .0198 0 0 1
8.9000 8.8945 .0055 1 0 0
5.5700 5.5669 .0031 0 -2 1
5.1100 5.1078 .0022 1 -1 1
4.9100 4.9104 -.0004 0 -1 2
4.4300 4.4293 .0007 -2 -1 2
4.1900 4.1909 -.0009 0 1 2
4.1000 4.0990 .0010 1 -2 1
3.9600 3.9610 -.0010 -2 1 0
3.9100 3.9123 -.0023 0 -3 1
3.8800 3.8785 .0015 0 3 0
3.8200 3.8200 -.0000 2 2 0
A= 9.974 DA= .001
B= 12.352 DB= .001
C= 11.116 DC= .002
GAMMA= 74.941 DGAMMA= .004
BETA =115.59 DBETA = .01
ALPHA=107.693 DALPHA= .007
V=1164
14. 28-0534
PbNb4F22
Triklin
Dexp Dcal d(D) h k l
9.1000 9.0957 .0043 -1 0 1
7.6000 7.6024 -.0024 1 1 1
6.1000 6.1026 -.0026 -1 -1 1
5.1000 5.0972 .0028 -1 1 2
4.5200 4.5225 -.0025 -2 1 0
4.2200 4.2198 .0002 0 -1 2
4.1800 4.1797 .0003 1 2 2
4.0400 4.0409 -.0009 0 1 3
3.8900 3.8889 .0011 2 -1 1
3.8200 3.8203 -.0003 -1 -2 1
3.7700 3.7701 -.0001 -1 2 0
3.6400 3.6397 .0003 -2 -2 1
A= 13.130 DA= .001
B= 9.4167 DB= .0004
C= 12.23742 DC= .00008
GAMMA= 75.243 DGAMMA= .002
BETA = 92.023 DBETA = .002
ALPHA= 72.4412 DALPHA= .0006
V=1385
15. 28-0535
Pb3NbF11
Triklin
Dexp Dcal d(D) h k l
3.8000 3.7999 .0001 1 1 1
3.7300 3.7276 .0024 1 -1 1
3.6900 3.6917 -.0017 1 3 0
3.6400 3.6388 .0012 0 -2 1
3.5200 3.5186 .0014 1 -2 1
3.3500 3.3499 .0001 0 -3 1
3.3000 3.2970 .0030 -1 4 0
3.2500 3.2523 -.0023 1 -3 1
3.1900 3.1907 -.0007 0 4 1
2.9710 2.9713 -.0003 1 -4 1
2.8680 2.8676 .0004 0 7 0
2.6530 2.6539 -.0009 -1 6 0
A= 4.8269 DA= .0002
B= 20.10461 DB= .00003
C= 4.3638 DC= .0004
GAMMA= 88.303 DGAMMA= .003
BETA = 65.83 DBETA = .01
ALPHA= 86.847 DALPHA= .003
V=385
16. 28-0788
K2Nb6O16
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.5600 5.5579 .0021 2 1 0
3.9600 3.9588 .0012 0 1 2
3.4600 3.4608 -.0008 0 2 2
3.2300 3.2292 .0008 3 1 1
3.0200 3.0178 .0022 4 1 0
2.9410 2.9414 -.0004 3 2 1
2.7860 2.7864 -.0004 0 0 3
2.6050 2.6049 .0001 -5 0 1
2.4510 2.4514 -.0004 4 2 1
2.4000 2.4000 .0000 -5 2 1
2.1680 2.1683 -.0003 -6 0 1
2.1340 2.1345 -.0005 -3 5 1
a= 13.025 b= 12.344 c= 8.746 beta= 107.09
da=.006 db= 8.541 dc= .005 dbeta=.01
V= 1344.0
Triklin
Dexp Dcal d(D) h k l
5.5600 5.5648 -.0048 1 0 0
3.9600 3.9600 .0000 1 1 0
3.4600 3.4618 -.0018 -1 0 1
3.2300 3.2283 .0017 -1 1 1
3.0200 3.0235 -.0035 1 1 1
2.9410 2.9437 -.0027 1 -1 1
2.7860 2.7824 .0036 2 0 0
2.6050 2.6033 .0017 1 2 0
2.4510 2.4546 -.0036 2 1 0
2.4000 2.3985 .0015 0 -2 1
2.1680 2.1668 .0012 2 1 1
2.1340 2.1334 .0006 0 1 2
A= 5.590 DA= .003
B= 6.250 DB= .005
C= 4.392 DC= .003
GAMMA= 95.40 DGAMMA= .09
BETA = 91.58 DBETA = .05
ALPHA= 83.44 DALPHA= .04
V= 151.7
17. 28-0789
K10Nb4O5{SO4}10
Tetragon
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
7.6300 7.5589 .0711 1 0 0
5.3600 5.3450 .0150 1 1 0
4.4000 4.3537 .0463 0 0 1
3.3900 3.3805 .0095 2 1 0
2.8500 2.8541 -.0041 2 0 1
2.5200 2.5196 .0004 3 0 0
2.3910 2.3903 .0007 3 1 0
2.2780 2.2776 .0004 2 2 1
2.1780 2.1769 .0011 0 0 2
2.0970 2.0965 .0005 3 2 0
2.0970 2.0953 .0017 3 1 1
1.8300 1.8302 -.0002 2 1 2
a= 7.559 c= 4.354
da= .004 dc= .005
V= 248.7
18. 28-1118
Na4NbO4
Triklin
Dexp Dcal d(D) h k l
4.4600 4.4592 .0008 0 1 1
4.3400 4.3474 -.0074 -1 0 1
3.7700 3.7682 .0018 0 -1 1
2.9500 2.9521 -.0021 -1 1 1
2.8100 2.8121 -.0021 1 2 0
2.6700 2.6714 -.0014 -2 -1 1
2.6300 2.6305 -.0005 0 -1 2
2.5200 2.5216 -.0016 0 2 1
2.3600 2.3594 .0006 2 2 1
2.2500 2.2500 .0000 0 -2 1
2.1600 2.1595 .0005 -1 0 3
1.9700 1.9687 .0013 -1 2 0
A= 5.848 DA= .009
B= 5.699 DB= .003
C= 6.9519 DC= .0009
GAMMA= 64.45 DGAMMA= .02
BETA = 90.43 DBETA = .01
ALPHA= 81.138 DALPHA= .004
V= 205.8
19. 28-1119
Na6Nb8O23*9H2O
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
16.3000 16.5261 -.2261 1 0 0
12.8000 12.8742 -.0742 0 1 1
12.0000 11.9611 .0389 1 1 0
10.2000 10.1561 .0439 1 1 1
9.5400 9.6132 -.0732 0 0 2
8.6600 8.6670 -.0070 0 2 0
8.3400 8.3096 .0304 1 0 2
7.6900 7.6755 .0145 1 2 0
7.1300 7.1284 .0016 1 2 1
6.2800 6.2663 .0137 2 0 2
4.9200 4.9194 .0006 1 2 3
3.9500 3.9506 -.0006 0 4 2
a=16.53 b=17.33394 c=19.23
da= .02 db= .0009 dc= .01
v=5527
Triklin
Dexp Dcal d(D) h k l
16.3000 16.3099 -.0099 1 0 0
12.8000 12.7839 .0161 1 1 0
12.0000 11.9969 .0031 -1 0 1
10.2000 10.2078 -.0078 0 -1 1
9.5400 9.5385 .0015 0 0 2
8.6600 8.6600 .0000 -1 1 0
8.3400 8.3149 .0251 1 1 2
7.6900 7.6917 -.0017 2 0 1
7.1300 7.1146 .0154 -1 -1 2
6.2800 6.2788 .0012 -1 -2 1
4.9200 4.9227 -.0027 2 2 3
3.9500 3.9491 .0009 3 1 4
A= 17.767 DA= .004
B= 14.153 DB= .002
C= 19.3303 DC= .0003
GAMMA= 66.953 DGAMMA= .001
BETA = 83.127 DBETA = .001
ALPHA= 81.588 DALPHA= .002
V=4414
20. 28-1318
TiNb3O9
Triklin
Dexp Dcal d(D) h k l
7.6300 7.6231 .0069 0 1 1
5.8300 5.8360 -.0060 0 -1 1
4.6000 4.5876 .0124 1 1 0
4.4000 4.3996 .0004 1 0 1
4.1100 4.1164 -.0064 -1 0 1
3.8300 3.8296 .0004 0 -2 1
3.7900 3.7895 .0005 -1 -1 1
3.6700 3.6788 -.0088 1 2 0
3.4300 3.4281 .0019 1 0 2
3.2900 3.2901 -.0001 0 3 1
3.1900 3.1905 -.0005 0 3 0
3.1000 3.1008 -.0008 0 1 3
A= 4.91501 DA= .00003
B= 10.0709 DB= .0003
C= 9.388 DC= .001
GAMMA= 79.9537 DGAMMA= .0009
BETA = 82.894 DBETA = .002
ALPHA= 73.919 DALPHA= .002
V=438.09
21. 28-1319
Ti14Nb6O21
Triklin
Dexp Dcal d(D) h k l
6.4600 6.4599 .0001 1 0 0
3.3000 3.2996 .0004 2 1 1
3.2100 3.2075 .0025 1 -1 1
3.1400 3.1399 .0001 2 1 0
2.7100 2.7102 -.0002 -2 -1 1
2.4800 2.4829 -.0029 0 2 0
2.2200 2.2195 .0005 1 -1 3
2.1900 2.1889 .0011 3 0 1
2.0800 2.0811 -.0011 3 1 3
1.9960 1.9959 .0001 -1 -2 2
1.9140 1.9140 -.0000 3 2 0
1.7710 1.7707 .0003 1 3 2
A= 6.969 DA= .001
B= 5.373 DB= .001
C= 9.432 DC= .005
GAMMA= 70.68 DGAMMA= .03
BETA = 74.95 DBETA = .04
ALPHA= 74.32 DALPHA= .04
V= 315.2
22. 28-1398
TiNb{PO}3Cl18
Triklin
Dexp Dcal d(D) h k l
6.2400 6.2458 -.0058 1 1 1
5.9400 5.9404 -.0004 -1 1 0
5.3600 5.3628 -.0028 -1 -1 1
5.0900 5.0914 -.0014 0 -1 1
4.8600 4.8681 -.0081 -1 0 2
4.6600 4.6626 -.0026 0 0 2
4.4900 4.4945 -.0045 -3 0 1
3.7200 3.7203 -.0003 3 1 1
3.3600 3.3602 -.0002 2 0 2
3.1400 3.1389 .0011 3 2 1
2.9900 2.9906 -.0006 3 1 2
2.9300 2.9284 .0016 -3 1 3
A= 13.87 DA= .01
B= 8.059 DB= .002
C= 10.160 DC= .004
GAMMA= 81.05 DGAMMA= .04
BETA =103.6 DBETA = .1
ALPHA= 73.80 DALPHA= .06
V= 1030
23. 28-1434
PbNbF7
Triklin
Dexp Dcal d(D) h k l
5.6200 5.6214 -.0014 2 1 0
4.9500 4.9481 .0019 2 1 1
3.8200 3.8198 .0002 0 -1 1
3.7400 3.7400 .0000 2 2 0
3.7100 3.7095 .0005 1 -1 1
3.6200 3.6208 -.0008 -1 -1 1
3.2900 3.2911 -.0011 4 1 1
2.8810 2.8806 .0004 -2 2 1
2.6680 2.6681 -.0001 1 -2 1
2.3710 2.3726 -.0015 3 3 2
2.4680 2.4685 -.0005 -3 2 1
2.4040 2.4035 .0005 -1 2 2
A= 13.851 DA= .008
B= 8.758 DB= .005
C= 5.765 DC= .004
GAMMA= 72.93 DGAMMA= .05
BETA = 73.31 DBETA = .06
ALPHA= 67.44 DALPHA= .04
V= 605.1
24. 28-1477
beta-Nb2ZnO6
Triklin
Dexp Dcal d(D) h k l
7.1400 7.1394 .0006 -1 0 1
7.0700 7.0699 .0001 -1 1 1
5.2900 5.2900 .0000 -1 0 2
4.0300 4.0283 .0017 0 -2 1
3.9300 3.9299 .0001 -1 0 3
3.6000 3.5998 .0002 -2 2 0
3.5200 3.5226 -.0026 -1 2 3
3.2600 3.2600 -.0000 -1 -2 1
3.1500 3.1497 .0003 -2 2 3
2.9160 2.9171 -.0011 1 -3 1
2.8480 2.8486 -.0006 0 -2 3
2.5510 2.5507 .0003 0 -3 2
A= 8.50 DA= .01
B= 9.691 DB= .001
C= 12.89 DC= .02
GAMMA=111.50 DGAMMA= .06
BETA =102.64 DBETA = .09
ALPHA= 78.09 DALPHA= .04
V= 954.2
25. 28-1478
Nb34Zn2O87
Triklin
Dexp Dcal d(D) h k l
14.3000 14.3221 -.0221 1 0 0
10.3000 10.3118 -.0118 0 1 0
9.7200 9.7212 -.0012 1 1 0
7.1660 7.1617 .0043 -2 -1 1
6.3090 6.3092 -.0002 0 1 1
5.7590 5.7675 -.0085 1 1 1
5.1550 5.1543 .0007 2 0 1
4.7730 4.7740 -.0010 3 0 0
4.4770 4.4772 -.0002 -1 2 0
4.1370 4.1367 .0003 0 2 1
3.9600 3.9603 -.0003 -3 0 2
3.7600 3.7589 .0011 1 1 2
A= 15.932 DA= .001
B= 11.452 DB= .001
C= 10.743 DC= .004
GAMMA= 68.650 DGAMMA= .002
BETA =110.871 DBETA = .007
ALPHA=110.612 DALPHA= .005
V= 1649
26. 28-1875
C16H40Br5NbO
Triklin
Dexp Dcal d(D) h k l
7.9800 7.9851 -.0051 0 0 1
7.6600 7.6463 .0137 0 1 1
6.9400 6.9571 -.0171 0 -1 1
5.4700 5.4801 -.0101 -1 -1 1
4.9500 4.9520 -.0020 1 0 1
4.7100 4.7148 -.0048 1 3 0
4.4900 4.4806 .0094 0 -3 1
4.2200 4.2238 -.0038 -1 3 1
4.0500 4.0480 .0020 1 3 1
3.8800 3.8834 -.0034 1 4 0
3.7400 3.7409 -.0009 -1 1 2
3.6500 3.6548 -.0048 -1 4 0
A= 7.28549 DA= .00000
B= 17.8422 DB= .0001
C= 8.14893 DC= .00009
GAMMA= 87.2333 DGAMMA= .0005
BETA = 98.9991 DBETA = .0004
ALPHA= 83.3280 DALPHA= .0005
V=1036