53. 31-1298
Na4Hf{SO4}4*3H2O
Triklin
Dexp Dcal d(D) h k l
8.8300 8.8392 -.0092 0 1 0
6.5000 6.4964 .0036 -1 1 1
6.1800 6.1852 -.0052 0 -1 2
6.1000 6.0895 .0105 1 -1 1
5.4000 5.3988 .0012 -1 1 2
4.7400 4.7358 .0042 -1 -1 1
4.3900 4.3885 .0015 1 -2 1
3.9600 3.9604 -.0004 -1 2 2
3.7600 3.7602 -.0002 1 1 2
3.2800 3.2805 -.0005 -2 1 3
3.1900 3.1902 -.0002 1 0 4
3.1300 3.1298 .0002 0 0 5
A= 7.616 DA= .001
B= 9.5220 DB= .0003
C= 15.900 DC= .001
GAMMA=111.05 DGAMMA= .01
BETA = 98.307 DBETA = .002
ALPHA= 92.516 DALPHA= .006
V= 1059.2
54. 32-0234
Cs2Hf2O2{SO4}3*6H2O
Triklin
Dexp Dcal d(D) h k l
11.6000 11.5719 .0281 1 0 0
8.9000 8.9091 -.0091 0 -1 1
8.3000 8.3033 -.0033 -1 0 1
7.1000 7.0979 .0021 0 1 1
6.3000 6.3107 -.0107 -1 1 1
5.7700 5.7860 -.0160 2 0 0
5.0400 5.0390 .0010 -1 0 2
4.8400 4.8473 -.0073 2 0 1
4.6200 4.6166 .0034 1 0 2
4.2500 4.2494 .0006 1 2 1
3.9600 3.9599 .0001 0 -3 1
3.8600 3.8573 .0027 3 0 0
A= 11.650 DA= .006
B= 12.009 DB= .006
C= 10.936 DC= .006
GAMMA= 89.76 DGAMMA= .03
BETA = 96.52 DBETA = .06
ALPHA=102.927 DALPHA= .008
V= 1481.2
55. 32-0236
Cs2Hf{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
8.1000 8.0966 .0034 0 1 1
6.9000 6.8955 .0045 1 0 0
6.3000 6.2957 .0043 0 -1 1
5.6000 5.5959 .0041 1 1 1
4.5900 4.5848 .0052 0 2 1
4.4800 4.4837 -.0037 0 2 0
4.1700 4.1716 -.0016 1 1 2
4.0500 4.0483 .0017 0 2 2
3.8400 3.8424 -.0024 0 1 3
3.3700 3.3697 .0003 2 2 0
3.2000 3.2000 .0000 0 -1 3
3.0700 3.0696 .0004 2 0 1
A= 7.536 DA= .001
B= 9.734 DB= .005
C= 11.958 DC= .002
GAMMA= 72.22 DGAMMA= .01
BETA =101.96 DBETA = .01
ALPHA= 80.07 DALPHA= .01
V= 790.6
56. 32-0422
Hf{ClO4}4
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2921 .0079 1 0 0
6.9400 6.9449 -.0049 -1 1 0
6.5400 6.5355 .0045 -1 0 1
6.1900 6.1868 .0032 -1 -1 1
5.1500 5.1467 .0033 0 1 1
3.7280 3.7282 -.0002 -2 1 1
3.3990 3.3958 .0032 -2 -1 2
3.3050 3.3072 -.0022 2 2 0
3.1340 3.1337 .0003 3 0 1
2.7840 2.7845 -.0005 2 2 1
2.7470 2.7498 -.0028 0 0 3
2.6490 2.6483 .0007 -2 3 0
A= 10.305 DA= .003
B= 9.811 DB= .004
C= 8.989 DC= .004
GAMMA= 92.32 DGAMMA= .05
BETA = 90.705 DBETA = .009
ALPHA=113.36 DALPHA= .01
V= 833.4
57. 32-0916
Rb2Hf2O2{SO4}3*6H2O
Triklin
Dexp Dcal d(D) h k l
11.5000 11.5492 -.0492 1 0 0
8.8000 8.7980 .0020 1 1 1
8.2000 8.2043 -.0043 0 1 1
7.0000 6.9990 .0010 0 -1 1
6.3300 6.3230 .0070 -1 -1 1
5.7000 5.6970 .0030 1 -1 1
4.9800 4.9729 .0071 2 2 1
4.7200 4.7271 -.0071 2 2 0
4.5600 4.5618 -.0018 1 2 2
4.3700 4.3777 -.0077 -2 1 0
4.2200 4.2182 .0018 2 -1 1
3.9300 3.9299 .0001 -1 2 1
A= 12.944 DA= .003
B= 11.1684 DB= .0005
C= 12.0154 DC= .0007
GAMMA= 65.98 DGAMMA= .02
BETA = 72.91 DBETA = .02
ALPHA= 75.04 DALPHA= .01
V=1497.2
58. 32-0917
Rb2Hf{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
7.9000 7.9134 -.0134 0 1 1
6.6000 6.6035 -.0035 0 -1 1
6.1000 6.0915 .0085 -1 -1 1
5.5000 5.5025 -.0025 0 2 1
4.8000 4.7983 .0017 1 2 0
4.4300 4.4300 -.0000 -1 2 2
4.3200 4.3264 -.0064 -1 -2 1
4.1300 4.1292 .0008 1 2 1
4.0300 4.0284 .0016 0 3 0
3.9100 3.9104 -.0004 -1 3 0
3.6200 3.6201 -.0001 2 0 1
3.3600 3.3591 .0009 -1 -2 2
A= 10.672 DA= .001
B= 12.676 DB= .002
C= 10.11229 DC= .00389
GAMMA=103.93 DGAMMA= .02
BETA =116.28 DBETA = .03
ALPHA= 74.364 DALPHA= .002
V=1169.5
59. 33-0059
{NH4}2{SO4}4*2H2O
Triklin
Dexp Dcal d(D) h k l
11.5000 11.5012 -.0012 1 0 0
10.5000 10.4652 .0348 0 1 0
8.5000 8.4972 .0028 0 0 1
7.0000 6.9884 .0116 0 -1 1
6.4000 6.4008 -.0008 1 0 1
5.7000 5.6939 .0061 1 -1 1
5.0000 5.0158 -.0158 2 1 0
4.5000 4.5014 -.0014 -2 1 1
4.2000 4.1899 .0101 -1 0 2
3.7700 3.7699 .0001 -2 -2 1
3.5900 3.5866 .0034 3 1 0
3.5200 3.5171 .0029 2 -2 1
A= 11.627 DA= .005
B= 10.5308 DB= .0001
C= 8.643 DC= .007
GAMMA= 89.71828 DGAMMA= .00002
BETA = 98.41 DBETA = .04
ALPHA= 96.38 DALPHA= .05
V= 1040.4
60. 32-0423
Co6Hf
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
3.3500 3.3514 -.0014 0 1 1
2.8400 2.8384 .0016 2 1 1
2.5300 2.5280 .0020 1 0 2
2.0300 2.0265 .0035 2 2 0
1.8900 1.8884 .0016 2 2 1
1.6000 1.5988 .0012 2 2 2
1.5300 1.5290 .0010 5 2 0
1.4400 1.4404 -.0004 7 1 0
1.3000 1.3010 -.0010 0 0 4
1.2800 1.2811 -.0011 4 3 0
1.2600 1.2602 -.0002 7 1 2
1.2400 1.2399 .0001 8 1 1
1.1700 1.1695 .0005 4 0 4
a=10.677 b= 4.381 c= 5.2039
da= .003 db= .006 dc= .0006
v= 243.4
61. 33-1011
K2Hf{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
10.9000 10.8963 .0037 0 1 1
9.2700 9.2557 .0143 0 -1 1
6.9400 6.9363 .0037 -1 1 0
6.5600 6.5648 -.0048 0 -1 2
6.4000 6.3963 .0037 -1 -1 1
6.3100 6.3036 .0064 -1 1 2
6.0900 6.0876 .0024 0 2 0
5.9300 5.9236 .0064 1 -1 1
5.1800 5.1804 -.0004 -1 1 3
5.1400 5.1411 -.0011 1 1 2
4.9800 4.9836 -.0036 -1 2 0
4.0400 4.0407 -.0007 -2 0 2
A= 8.4127 DA= .0005
B= 12.3947 DB= .0009
C= 18.067 DC= .001
GAMMA= 94.303 DGAMMA= .003
BETA =102.084 DBETA = .004
ALPHA= 79.428 DALPHA= .002
V=1809.5
62. 33-1111
Rb2Hf{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
13.3000 13.3757 -.0757 1 0 0
7.8300 7.8050 .0250 0 1 0
6.6900 6.6879 .0021 2 0 0
6.3400 6.3251 .0149 1 1 1
5.6100 5.6124 -.0024 2 0 2
4.8700 4.8736 -.0036 2 -1 1
4.4600 4.4586 .0014 3 0 0
4.3530 4.3533 -.0003 0 1 2
4.0620 4.0646 -.0026 1 2 0
3.9340 3.9342 -.0002 -1 -1 3
3.6570 3.6559 .0011 1 -2 2
3.6100 3.5992 .0108 2 2 1
A= 14.421 DA= .002
B= 8.357 DB= .002
C= 13.91 DC= .01
GAMMA= 78.281 DGAMMA= .007
BETA = 75.04 DBETA = .07
ALPHA=103.41 DALPHA= .03
V=1535
63. 34-0559
Hf{SeO3}2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.1600 5.1732 -.0132 1 2 0
4.2700 4.2712 -.0012 1 0 2
4.0700 4.0626 .0074 2 1 0
3.5600 3.5688 -.0088 1 2 2
3.2400 3.2478 -.0078 0 4 0
3.1300 3.1351 -.0051 2 1 2
3.0500 3.0430 .0070 2 3 0
2.5900 2.5866 .0034 2 4 0
2.4200 2.4186 .0014 2 2 3
2.3700 2.3685 .0015 1 0 4
2.2200 2.2198 .0002 1 5 2
2.1400 2.1386 .0014 4 0 0
a= 8.554 b=12.991 c= 9.8593
da= .001 db= .004 dc= .0005
V=1095.
Triklin
Dexp Dcal d(D) h k l
5.1600 5.1594 .0006 -1 0 1
4.2700 4.2718 -.0018 0 1 1
4.0700 4.0715 -.0015 0 -1 1
3.5600 3.5604 -.0004 1 -1 1
3.2400 3.2420 -.0020 1 1 1
3.1300 3.1303 -.0003 1 1 2
3.0500 3.0486 .0014 -1 1 3
2.5900 2.5914 -.0014 2 0 3
2.4200 2.4191 .0009 2 -1 2
2.3700 2.3685 .0015 -1 -1 4
2.2200 2.2179 .0021 2 0 5
2.1400 2.1397 .0003 -1 -1 5
A= 5.69953 DA= .00003
B= 4.3715 DB= .0007
C= 16.096 DC= .001
GAMMA= 97.159 DGAMMA= .002
BETA = 85.2619 DBETA = .0004
ALPHA= 85.197 DALPHA= .004
V=394.7
64. 34-0791
Cs4Hf{SO4}4*2H2O
Triklin
Dexp Dcal d(D) h k l
8.0100 7.9978 .0122 -1 0 1
6.9000 6.9183 -.0183 1 1 0
6.7900 6.7700 .0200 1 0 1
6.7600 6.7700 -.0100 1 0 1
6.2300 6.2522 -.0222 0 -1 1
5.0300 5.0274 .0026 1 1 2
4.5850 4.5785 .0065 0 -1 2
4.4230 4.4255 -.0025 0 0 3
4.1920 4.1920 .0000 1 2 1
4.1410 4.1400 .0010 1 2 0
4.0880 4.0879 .0001 2 1 1
3.9510 3.9507 .0003 2 0 1
A= 9.1051 DA= .0005
B= 8.7559 DB= .0002
C= 13.92053 DC= .00005
GAMMA= 77.75 DGAMMA= .01
BETA = 96.80 DBETA = .02
ALPHA= 75.822 DALPHA= .004
V=1036.4
65. 34-0868
Cs2Hf{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
6.8400 6.8318 .0082 1 0 1
6.2600 6.2609 -.0009 0 1 1
5.2800 5.2769 .0031 0 -1 1
4.6100 4.6091 .0009 2 1 1
4.4570 4.4560 .0010 1 2 1
4.1370 4.1338 .0032 1 0 2
4.0400 4.0396 .0004 -1 1 1
3.8630 3.8608 .0022 0 1 2
3.4640 3.4690 -.0050 2 2 2
3.4190 3.4159 .0031 2 0 2
3.3710 3.3731 -.0021 0 -1 2
3.2200 3.2240 -.0040 -2 -1 1
A= 9.331 DA= .001
B= 9.115 DB= .001
C= 8.865 DC= .003
GAMMA= 64.875 DGAMMA= .008
BETA = 66.45 DBETA = .01
ALPHA= 71.93 DALPHA= .01
V=616.6
66. 34-0989
K4Hf2{SO4}5*SeO4*6H2O
Triklin
Dexp Dcal d(D) h k l
7.6300 7.6291 .0009 1 0 0
6.8100 6.7977 .0123 1 1 0
6.0600 6.0673 -.0073 0 -1 1
5.8100 5.7878 .0222 0 2 1
5.4800 5.4778 .0022 1 2 0
4.6700 4.6615 .0085 1 1 1
4.3400 4.3300 .0100 -1 -2 1
4.1700 4.1594 .0106 0 4 0
3.8400 3.8414 -.0014 0 4 1
3.7400 3.7374 .0026 -1 4 0
3.6500 3.6524 -.0024 -1 -3 1
3.6200 3.6217 -.0017 -2 1 1
A= 7.76174 DA= .00001
B= 16.90207 DB= .00001
C= 7.12596 DC= .00001
GAMMA= 94.69922 DGAMMA= .00001
BETA =100.16040 DBETA = .00001
ALPHA= 80.33275 DALPHA= .00001
V=905.8
67. 34-1073
K3Hf2OH{SeO4}5*7H2O
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
13.6000 13.6938 -.0938 0 0 1
7.8700 7.9172 -.0472 0 1 0
6.8500 6.8541 -.0041 0 1 1
5.1800 5.1789 .0011 0 1 2
5.0800 5.0788 .0012 1 1 1
4.2700 4.2731 -.0031 1 1 2
3.9600 3.9586 .0014 0 2 0
3.9100 3.9080 .0020 1 0 3
3.8000 3.8029 -.0029 0 2 1
3.4300 3.4270 .0030 0 2 2
3.3100 3.3111 -.0011 2 1 1
3.1400 3.1423 -.0023 0 1 4
a= 7.5633 b= 7.917 c=13.694
da= .0001 db= .001 dc= .002
V= 820.0
68. 34-1306
HfBr3
Triklin
Dexp Dcal d(D) h k l
8.5600 8.5579 .0021 1 0 0
6.3000 6.2913 .0087 1 1 1
4.1190 4.1199 -.0009 -1 -1 1
3.4100 3.4065 .0035 3 1 1
3.2630 3.2615 .0015 0 -2 1
3.1800 3.1822 -.0022 -1 -2 1
3.1120 3.1116 .0004 0 1 2
3.0760 3.0781 -.0021 3 1 0
3.0360 3.0370 -.0010 1 2 2
2.8940 2.8909 .0031 3 2 0
2.6820 2.6824 -.0004 3 0 2
2.4590 2.4603 -.0013 3 3 0
A= 10.2551 DA= .0004
B= 8.93755 DB= .00004
C= 7.2403 DC= .0001
GAMMA= 63.6839 DGAMMA= .0009
BETA = 64.247 DBETA = .001
ALPHA= 74.36 DALPHA= .001
V=533.3
69. 34-1371
Hf{NH4}4{SO4}4*4H2O
Triklin
Dexp Dcal d(D) h k l
8.9000 8.8968 .0032 -1 1 0
7.4000 7.4077 -.0077 0 1 1
6.7000 6.6973 .0027 0 -1 1
5.7000 5.7067 -.0067 -1 1 1
5.4000 5.4000 -.0000 2 -1 1
5.0800 5.0792 .0008 2 0 0
4.9000 4.9028 -.0028 1 0 2
4.4600 4.4520 .0080 2 -2 1
4.0700 4.0692 .0008 0 -1 2
3.9900 3.9978 -.0078 -2 1 1
3.8700 3.8646 .0054 -2 0 1
3.6600 3.6598 .0002 -2 2 1
A= 11.4119 DA= .0004
B= 11.5364 DB= .0005
C= 9.8374 DC= .0003
GAMMA=106.251 DGAMMA= .002
BETA = 68.756 DBETA = .004
ALPHA= 90.572 DALPHA= .004
V=1152.9
70. 35-0831
{NH4}2Hf{SO4}3*2H2O
Triklin
Dexp Dcal d(D) h k l
12.7000 12.7197 -.0197 1 0 0
7.7000 7.7166 -.0166 1 1 1
6.5000 6.4794 .0206 -1 0 1
6.0000 5.9954 .0046 2 1 0
5.3000 5.3026 -.0026 -1 -1 1
4.8000 4.8132 -.0132 1 2 1
4.5000 4.4968 .0032 2 1 2
4.2600 4.2611 -.0011 2 0 2
4.0400 4.0341 .0059 -1 2 0
3.8300 3.8341 -.0041 0 -2 1
3.6300 3.6291 .0009 3 0 2
3.5500 3.5477 .0023 3 2 2
A= 14.014 DA= .006
B= 9.938 DB= .002
C= 9.65 DC= .01
GAMMA= 71.23 DGAMMA= .04
BETA = 69.73 DBETA = .04
ALPHA= 74.27 DALPHA= .03
V=1174
71. 35-0889
HfCl4*2OP{Hcs}3
Triklin
Dexp Dcal d(D) h k l
6.9200 6.8914 .0286 1 1 1
4.9300 4.9343 -.0043 -1 -1 1
4.5300 4.5341 -.0041 2 0 1
4.3100 4.3064 .0036 1 1 2
4.1900 4.1824 .0076 0 0 2
4.0400 4.0418 -.0018 0 -2 1
3.8700 3.8684 .0016 0 1 2
3.7100 3.7093 .0007 1 -1 2
3.4900 3.4908 -.0008 -2 -1 1
3.4500 3.4457 .0043 2 2 2
3.2500 3.2533 -.0033 1 3 1
3.3000 3.2994 .0006 1 3 0
A= 9.86 DA= .01
B= 10.029 DB= .004
C= 8.984 DC= .002
GAMMA= 69.69 DGAMMA= .07
BETA = 68.69 DBETA = .02
ALPHA= 81.11 DALPHA= .04
V=774.5
72. 36-0589
CsHf{ClO4}5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.4488 4.4531 -.0043 1 1 0
4.0615 4.0616 -.0001 0 0 3
3.6142 3.6185 -.0043 -3 0 1
3.4485 3.4454 .0031 -2 1 2
3.3663 3.3659 .0004 1 1 2
3.2158 3.2154 .0004 2 1 1
2.7888 2.7910 -.0022 -3 0 4
2.7081 2.7076 .0005 -1 1 4
2.5995 2.5985 .0010 -4 0 3
2.4366 2.4370 -.0004 0 0 5
2.3492 2.3480 .0012 4 0 1
2.2704 2.2720 -.0016 4 1 0
2.2074 2.2077 -.0003 1 0 5
2.1647 2.1641 .0006 -3 1 5
2.1162 2.1158 .0004 4 0 2
a= 10.877 b= 4.946 c= 12.954 beta= 109.84
da=.003 db=.002 dc= .001 dbeta=.01
V= 655.5
73. 36-0590
Cs2Hf{ClO4}6
Triklin
Dexp Dcal d(D) h k l
8.4010 8.4031 -.0021 -1 0 1
7.5419 7.5315 .0104 1 -1 1
6.3076 6.3157 -.0081 -1 0 2
6.1502 6.1495 .0007 0 -1 2
5.6425 5.6336 .0089 1 -1 2
5.5233 5.5123 .0110 -1 -1 1
5.1111 5.1137 -.0026 -2 1 1
4.6819 4.6835 -.0016 2 0 0
4.5392 4.5489 -.0097 -2 2 1
4.1866 4.1805 .0061 -2 2 2
4.1023 4.1042 -.0019 2 -1 2
3.9646 3.9658 -.0012 -1 -1 3
A= 10.457 DA= .004
B= 11.439 DB= .003
C= 15.792 DC= .003
GAMMA=115.87 DGAMMA= .01
BETA = 96.90 DBETA = .01
ALPHA= 85.536 DALPHA= .009
V=1686.5
74. 36-0591
Cs3Hf{ClO4}7
Triklin
Dexp Dcal d(D) h k l
5.4222 5.4190 .0032 2 1 0
4.5762 4.5731 .0031 2 0 1
4.0872 4.0860 .0012 0 -2 1
3.7779 3.7763 .0016 2 -1 1
3.6434 3.6414 .0020 3 1 0
3.4750 3.4749 .0001 -2 2 0
3.3764 3.3749 .0015 -2 -2 1
3.2249 3.2273 -.0024 2 3 2
3.1336 3.1340 -.0004 -2 2 1
2.9413 2.9428 -.0015 -1 2 2
2.8956 2.8963 -.0007 -3 0 1
2.7161 2.7167 -.0006 -1 4 0
A= 11.3855 DA= .0006
B= 13.594 DB= .002
C= 7.436 DC= .001
GAMMA= 68.395 DGAMMA= .007
BETA = 73.680 DBETA = .009
ALPHA= 70.662 DALPHA= .008
V=992.9
75. 36-0592
RbHf{ClO4}5
Triklin
Dexp Dcal d(D) h k l
8.9408 8.9079 .0329 0 1 1
8.4814 8.4421 .0393 0 -1 1
7.6726 7.6866 -.0140 1 0 0
7.4156 7.4044 .0112 -1 1 0
6.6579 6.6607 -.0028 1 -1 1
6.4922 6.4934 -.0012 0 0 2
6.3076 6.2997 .0079 -1 0 1
6.2192 6.2260 -.0068 -1 1 1
5.7372 5.7367 .0005 1 1 0
5.2006 5.2052 -.0046 0 -2 1
4.3282 4.3289 -.0007 0 0 3
4.2181 4.2176 .0005 1 -2 2
A= 8.0323 DA= .0004
B= 12.092 DB= .002
C= 13.0801 DC= .0005
GAMMA=105.522 DGAMMA= .005
BETA = 83.90 DBETA = .01
ALPHA= 88.675 DALPHA= .002
V=1215.4
76. 36-0593
Rb2Hf{ClO4}6
Triklin
Dexp Dcal d(D) h k l
8.6814 8.6831 -.0017 -1 0 1
8.1985 8.2076 -.0091 0 1 1
7.8915 7.8900 .0015 0 -1 1
7.3175 7.3028 .0147 -1 1 1
6.2631 6.2547 .0084 1 0 1
5.8199 5.8281 -.0082 -2 -1 1
5.7372 5.7237 .0135 2 0 0
5.5579 5.5669 -.0090 1 -1 1
5.3069 5.3062 .0007 2 2 0
5.1228 5.1353 -.0125 -2 1 1
4.9521 4.9464 .0057 -1 -3 1
4.5952 4.5962 -.0010 -1 1 2
A= 12.424 DA= .001
B= 16.959 DB= .001
C= 9.7437 DC= .0002
GAMMA= 76.918 DGAMMA= .008
BETA =108.826 DBETA = .007
ALPHA= 91.744 DALPHA= .005
V=1890.6
77. 36-0632
C2H4F5HfKO2
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
6.0500 6.0372 .0128 1 0 1
4.9800 4.9829 -.0029 1 1 0
3.7500 3.7466 .0034 0 2 0
3.2500 3.2473 .0027 2 0 1
3.1800 3.1834 -.0034 1 2 1
3.0300 3.0475 -.0175 2 1 0
2.8000 2.8000 .0000 2 1 2
2.7300 2.7257 .0043 2 0 3
2.5800 2.5753 .0047 0 2 4
2.5000 2.4977 .0023 0 3 0
2.4300 2.4297 .0003 2 0 4
2.3400 2.3392 .0008 1 3 0
a= 6.67 b= 7.4932 c=14.1834
da= .01 db= .0008 dc= .0009
V= 709
Triklin
Dexp Dcal d(D) h k l
6.0500 6.0535 -.0035 1 0 0
4.9800 4.9731 .0069 1 -1 0
3.7500 3.7427 .0073 0 -1 2
3.2500 3.2520 -.0020 1 1 0
3.1800 3.1827 -.0027 2 -1 1
3.0300 3.0268 .0032 2 0 0
2.8000 2.7997 .0003 2 0 1
2.7300 2.7319 -.0019 -1 2 0
2.5800 2.5796 .0004 2 -2 1
2.5000 2.5005 -.0005 -1 0 3
2.4300 2.4300 -.0000 2 -2 2
2.3400 2.3415 -.0015 -1 -1 3
A= 6.6636 DA= .0009
B= 5.753 DB= .001
C= 8.529 DC= .002
GAMMA=114.62 DGAMMA= .06
BETA = 84.43 DBETA = .04
ALPHA=108.27 DALPHA= .07
V= 282.1
78. 37-0037
K2HfF6
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
6.4820 6.5260 -.0440 1 1 0
5.9460 5.9386 .0074 2 0 0
4.7450 4.7274 .0176 2 1 0
3.4180 3.4154 .0026 1 0 1
3.9520 3.9591 -.0071 3 0 0
3.4140 3.4154 -.0014 1 0 1
3.2430 3.2440 -.0010 0 1 1
2.7760 2.7755 .0005 4 1 0
a=11.877 b= 7.81 c= 3.56606
da= .008 db= .05 dc= .00006
V=331
79. 37-0038
K2HfF6
Triklin
Dexp Dcal d(D) h k l
7.2550 7.2542 .0008 0 1 1
5.6620 5.6601 .0019 -1 0 1
5.0970 5.1018 -.0048 0 -1 1
4.5990 4.5981 .0009 -1 1 1
4.5290 4.5296 -.0006 -1 1 0
4.2100 4.2033 .0067 0 0 2
3.8420 3.8410 .0010 -1 0 2
3.6190 3.6271 -.0081 0 2 2
3.4530 3.4526 .0004 2 1 0
3.0840 3.0844 -.0004 2 2 0
2.7720 2.7690 .0030 1 3 2
2.7060 2.7064 -.0004 1 -1 2
2.5180 2.5182 -.0002 -1 -3 1
2.3740 2.3746 -.0006 2 3 2
2.2650 2.2648 .0002 -2 2 0
A= 6.9520 DA= .0001
B= 9.1494 DB= .0001
C= 8.9526 DC= .0001
GAMMA= 74.257 DGAMMA= .001
BETA = 93.807 DBETA = .003
ALPHA= 72.141 DALPHA= .001
V=514.8
Dexp Dcal d(D) h k l
7.2550 7.2651 -.0101 0 1 0
5.6620 5.6577 .0043 1 1 0
5.3560 5.3519 .0041 0 -1 2
5.0970 5.0915 .0055 1 1 1
4.5990 4.6175 -.0185 1 -1 2
4.5290 4.5327 -.0037 2 0 0
4.2100 4.2205 -.0105 1 1 2
3.8420 3.8384 .0036 2 1 0
3.6190 3.6177 .0013 0 -2 1
3.4530 3.4517 .0013 1 1 3
3.0840 3.0827 .0013 0 2 2
2.7720 2.7704 .0016 2 0 4
A= 9.0654 DA= .0007
B= 7.3129 DB= .0001
C= 14.0743 DC= .0006
GAMMA= 90.258 DGAMMA= .001
BETA = 89.880 DBETA = .001
ALPHA= 96.5593 DALPHA= .0005
V=927.4
80. 37-0154
Hf{OH}PO4
Triklin
Dexp Dcal d(D) h k l
5.9300 5.9250 .0050 0 1 0
5.5000 5.4982 .0018 1 0 1
5.0700 5.0636 .0064 0 1 1
4.8500 4.8454 .0046 -1 1 1
4.5400 4.5367 .0033 0 0 2
4.4000 4.4114 -.0114 1 1 0
3.9700 3.9767 -.0067 2 0 0
3.6600 3.6602 -.0002 1 0 2
3.5300 3.5282 .0018 0 -1 2
3.3100 3.3091 .0009 -2 0 2
3.1400 3.1379 .0021 2 -1 1
3.1300 3.1256 .0044 -2 1 2
A= 8.2250 DA= .0009
B= 6.0274 DB= .0002
C= 9.260 DC= .001
GAMMA=100.288 DGAMMA= .002
BETA =101.261 DBETA = .002
ALPHA= 85.5818 DALPHA= .0004
V=442.7
81. 37-0156
Hf2O{PO4}2
Triklin
Dexp Dcal d(D) h k l
4.4300 4.4368 -.0068 0 0 1
3.8300 3.8312 -.0012 0 -2 1
3.1500 3.1512 -.0012 -1 0 1
3.1100 3.1113 -.0013 -1 -1 1
2.8800 2.8805 -.0005 -1 -2 1
2.6200 2.6228 -.0028 2 0 0
2.5400 2.5387 .0013 2 1 0
2.3400 2.3393 .0007 0 5 0
2.2000 2.2002 -.0002 1 -1 2
2.1200 2.1204 -.0004 0 1 2
1.9750 1.9754 -.0004 0 2 2
1.9610 1.9606 .0004 2 3 1
A= 5.3232 DA= .0001
B= 11.86296 DB= .00007
C= 4.55379 DC= .00001
GAMMA= 93.682 DGAMMA= .001
BETA = 80.458 DBETA = .001
ALPHA= 99.370 DALPHA= .001
V=279.5
82. 37-0705
{NH4}4Hf{SO4}4*2H2O
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
6.7800 6.7762 .0038 0 2 0
4.9200 4.9414 -.0214 2 2 0
3.6200 3.6107 .0093 4 0 0
3.4800 3.4890 -.0090 4 1 0
3.2200 3.2212 -.0012 1 1 1
2.7700 2.7707 -.0007 3 4 0
2.7200 2.7203 -.0003 0 3 1
2.4400 2.4377 .0023 4 1 1
2.0400 2.0397 .0003 7 1 0
1.9410 1.9411 -.0001 3 5 1
1.8880 1.8881 -.0001 6 2 1
1.7500 1.7501 -.0001 7 1 1
a=14.443 b=13.552 c= 3.4073
da= .002 db= .004 dc= .0003
V=666.9
Triklin
Dexp Dcal d(D) h k l
6.7800 6.7801 -.0001 1 0 0
4.9200 4.9263 -.0063 1 1 1
3.6200 3.6194 .0006 -1 -1 1
3.4800 3.4825 -.0025 2 0 1
3.2200 3.2201 -.0001 1 2 0
2.7700 2.7694 .0006 2 2 1
2.7200 2.7197 .0003 -1 2 0
2.4400 2.4391 .0009 -1 1 2
2.0400 2.0390 .0010 2 3 0
1.9410 1.9417 -.0007 3 -1 2
1.8880 1.8877 .0003 0 2 3
1.7500 1.7500 .0000 0 -3 2
A= 7.366 DA= .003
B= 6.759 DB= .005
C= 6.990 DC= .001
GAMMA= 75.43 DGAMMA= .05
BETA = 70.46 DBETA = .02
ALPHA= 81.02 DALPHA= .03
V= 316.4
83. 37-0707
{NH4}4Hf{SO4}4*H2O
Triklin
Dexp Dcal d(D) h k l
6.2400 6.2352 .0048 0 -1 1
5.8500 5.8530 -.0030 -1 1 1
4.8000 4.8008 -.0008 1 -1 1
4.5900 4.5940 -.0040 -1 -1 1
4.2900 4.2906 -.0006 0 0 2
4.1900 4.1916 -.0016 -1 2 0
3.7500 3.7488 .0012 -2 0 1
3.3300 3.3293 .0007 -2 2 1
3.1200 3.1176 .0024 0 -2 2
2.9700 2.9707 -.0007 2 0 1
2.8000 2.8008 -.0008 0 -1 3
2.6700 2.6704 -.0004 0 3 0
A= 8.0122 DA= .0001
B= 8.580 DB= .001
C= 9.0655 DC= .0004
GAMMA=109.909 DGAMMA= .007
BETA =107.594 DBETA = .003
ALPHA= 90.19 DALPHA= .01
V=557.8
84. 37-0708
{NH4}4Hf{SO4}4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.3700 6.3788 -.0088 2 0 0
4.2600 4.2525 .0075 3 0 0
3.6800 3.6824 -.0024 -2 1 1
3.4000 3.4031 -.0031 3 1 0
3.0400 3.0354 .0046 3 1 1
2.8700 2.8712 -.0012 4 0 1
2.7600 2.7592 .0008 -2 1 2
2.6800 2.6808 -.0008 3 0 2
2.4200 2.4198 .0002 -4 0 2
2.3600 2.3602 -.0002 3 2 0
1.9380 1.9380 -.0000 -4 0 3
a=12.77 b= 5.6748 c= 7.12 beta= 92.11
da=.01 db=.0008 dc=.01 dbeta=.1
V= 515.6
Triklin
Dexp Dcal d(D) h k l
6.3700 6.3718 -.0018 0 1 0
4.2600 4.2591 .0009 1 0 2
3.6800 3.6807 -.0007 2 -1 2
3.4000 3.4002 -.0002 -1 2 0
3.0400 3.0402 -.0002 2 -2 2
2.8700 2.8702 -.0002 -2 0 1
2.7600 2.7599 .0001 3 -1 2
2.6800 2.6798 .0002 2 0 3
2.4200 2.4201 -.0001 1 1 3
2.3600 2.3600 .0000 3 -2 3
1.9380 1.9380 .0000 2 2 2
A= 8.4622 DA= .0009
B= 7.0920 DB= .0003
C= 9.0359 DC= .0008
GAMMA=115.494 DGAMMA= .007
BETA = 63.793 DBETA = .006
ALPHA=105.587 DALPHA= .005
V= 437.11
85. 39-0521
betaHf7O8N4
Rombik
Groupa 37,66
Dexp. Dcal. d(D) h k l
2.9260 2.9250 .0010 0 1 1
2.5290 2.5298 -.0008 0 2 0
1.9953 1.9953 .0000 2 0 0
1.7923 1.7924 -.0001 0 0 2
1.5261 1.5261 .0000 0 3 1
a= 3.9906 b= 5.0597 c= 3.585
da= .0001 db= .0008 dc= .002
v= 72.38
86. 40-0690
N2H5HfF5
Triklin
Dexp Dcal d(D) h k l
7.1783 7.1865 -.0082 1 0 0
5.0532 5.0498 .0034 1 1 1
4.3073 4.3062 .0011 -1 -1 1
3.9882 3.9919 -.0037 0 0 2
3.6274 3.6305 -.0031 1 0 2
3.2479 3.2473 .0006 0 2 1
2.9688 2.9684 .0004 -1 -2 1
2.8810 2.8822 -.0012 2 1 2
2.7336 2.7339 -.0003 2 -1 1
2.4244 2.4259 -.0015 -1 0 3
2.1699 2.1704 -.0005 2 3 0
2.1010 2.1005 .0005 3 2 2
A= 7.48331 DA= .003
B= 7.05375 DB= .004
C= 8.09801 DC= .004
GAMMA= 74.63 DGAMMA= .05
BETA = 82.93 DBETA = .01
ALPHA= 81.85 DALPHA= .01
V= 406.3
87. 43-1123
BaHfH6
Triklin
Dexp Dcal d(D) h k l
8.6200 8.6074 .0126 -1 1 1
6.5500 6.5468 .0032 1 1 0
6.2200 6.2243 -.0043 0 2 1
6.0200 6.0195 .0005 -1 1 2
5.4250 5.4169 .0081 -2 1 0
5.1730 5.1751 -.0021 -1 -1 1
4.9830 4.9901 -.0071 2 0 1
4.7050 4.7048 .0002 1 2 1
4.3360 4.3345 .0015 -1 3 1
3.9720 3.9691 .0029 -1 -1 2
3.9000 3.8989 .0011 1 2 3
3.7820 3.7827 -.0007 -2 0 2
A= 10.922 DA= .002
B= 13.134 DB= .003
C= 14.2522 DC= .0007
GAMMA=108.60 DGAMMA= .02
BETA = 91.40 DBETA = .01
ALPHA= 65.264 DALPHA= .003
V=1748
88. 44-1089
BaHfF6
Triklin
Dexp Dcal d(D) h k l
7.4600 7.4589 .0011 1 0 0
4.7200 4.7170 .0030 0 1 1
4.3000 4.3028 -.0028 1 -1 1
3.9760 3.9766 -.0006 0 -2 1
3.7300 3.7295 .0005 2 0 0
3.5150 3.5201 -.0051 1 1 1
3.0500 3.0486 .0014 2 -1 1
3.0340 3.0296 .0044 -2 -1 1
3.0100 3.0099 .0001 1 -3 1
2.6250 2.6264 -.0014 -3 1 0
2.6000 2.6007 -.0007 -1 4 0
2.1740 2.1740 .0000 2 -1 2
A= 8.005 DA= .001
B= 10.424 DB= .005
C= 5.862 DC= .001
GAMMA=108.48 DGAMMA= .04
BETA = 99.031 DBETA = .006
ALPHA= 93.65 DALPHA= .06
V= 454.9
89. 45-1258
K1.75Hf5.75*0.5H2O
Triklin
Dexp Dcal d(D) h k l
10.1000 10.1154 -.0154 1 0 0
6.8000 6.7751 .0249 0 1 0
6.4000 6.3967 .0033 -1 0 1
5.1500 5.1466 .0034 1 -1 1
4.8500 4.8390 .0110 2 1 0
4.6900 4.6966 -.0066 0 -1 2
4.2500 4.2489 .0011 1 -1 2
4.0000 3.9983 .0017 2 0 2
3.9500 3.9508 -.0008 -1 1 1
3.6300 3.6299 .0001 -1 -2 1
3.4800 3.4819 -.0019 3 1 0
3.2900 3.2900 .0000 0 0 3
A= 10.753 DA= .001
B= 7.3479 DB= .0003
C= 10.427 DC= .002
GAMMA= 74.65 DGAMMA= .03
BETA = 81.87 DBETA = .03
ALPHA=104.01 DALPHA= .06
V= 752.0
90. 45-1259
K1.5HfF3.5SO4*H2O
Triklin
Dexp Dcal d(D) h k l
7.6000 7.6014 -.0014 0 0 1
7.0300 7.0295 .0005 -1 1 0
6.2700 6.2556 .0144 0 -2 1
5.7000 5.6982 .0018 -1 2 0
4.7400 4.7388 .0012 -1 2 1
4.5900 4.5907 -.0007 1 3 0
4.0300 4.0296 .0004 0 -4 1
3.8600 3.8617 -.0017 0 -1 2
3.7000 3.7002 -.0002 -2 -2 1
3.5400 3.5397 .0003 2 2 0
3.4600 3.4596 .0004 0 -3 2
3.3700 3.3711 -.0011 1 -4 1
A= 8.075 DA= .004
B= 17.291 DB= .006
C= 8.048 DC= .002
GAMMA= 86.443 DGAMMA= .002
BETA =106.15 DBETA = .01
ALPHA=101.063 DALPHA= .008
V= 1059.3
91. 45-1260
HHfF{SO4}2*4.5H2O
Triklin
Dexp Dcal d(D) h k l
8.9000 8.9031 -.0031 0 1 1
8.2500 8.2407 .0093 0 -1 1
7.6000 7.6040 -.0040 1 0 0
6.2000 6.2027 -.0027 -1 -1 1
5.7000 5.7058 -.0058 0 2 1
5.2000 5.2011 -.0011 1 2 1
4.4600 4.4516 .0084 0 2 2
4.1900 4.1867 .0033 1 2 2
4.1200 4.1203 -.0003 0 -2 2
3.9600 3.9544 .0056 1 -2 1
3.7500 3.7506 -.0006 2 1 1
3.6000 3.6005 -.0005 2 0 1
A= 7.899 DA= .001
B= 13.038 DB= .001
C= 11.751 DC= .002
GAMMA= 74.314 DGAMMA= .006
BETA = 89.65 DBETA = .03
ALPHA= 85.64 DALPHA= .01
V=1161.1
92. 48-1683
Hf3Pd4
Triklin
Dexp Dcal d(D) h k l
3.6600 3.6738 -.0138 0 -1 1
3.3370 3.3408 -.0038 1 -1 1
3.2730 3.2718 .0012 -1 -2 1
3.1520 3.1512 .0008 -2 -1 1
3.1230 3.1226 .0004 -2 1 1
2.9020 2.9016 .0004 -2 -2 1
2.7900 2.7875 .0025 2 0 1
2.6470 2.6461 .0009 -3 -1 1
2.5860 2.5862 -.0002 -2 -3 1
2.5040 2.5046 -.0006 -4 2 0
2.4800 2.4794 .0006 -1 -4 1
2.3880 2.3873 .0007 2 2 1
A= 10.433 DA= .002
B= 12.805 DB= .001
C= 3.757 DC= .001
GAMMA= 97.98 DGAMMA= .01
BETA = 97.989 DBETA = .002
ALPHA= 96.495 DALPHA= .002
V=487.7
93. 48-1684
HfPd2
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
4.2820 4.2963 -.0143 0 2 1
3.6340 3.6252 .0088 2 2 0
3.3100 3.3095 .0005 2 1 1
3.1270 3.1230 .0040 1 4 0
2.8060 2.8097 -.0037 3 1 0
2.6460 2.6454 .0006 2 4 0
2.5860 2.5828 .0032 0 2 2
2.5130 2.5112 .0018 3 1 1
2.3900 2.3886 .0014 3 2 1
2.3280 2.3278 .0002 1 5 1
2.2890 2.2870 .0020 1 3 2
2.2150 2.2155 -.0005 2 2 2
a= 8.62073 b=13.40 c= 5.598
da= .00005 db= .01 dc= .002
V= 646.8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.2820 4.2831 -.0011 3 0 1
3.6340 3.6350 -.0010 -3 0 2
3.3100 3.3060 .0040 -2 0 3
3.1270 3.1316 -.0046 1 1 1
2.8060 2.8072 -.0012 1 1 2
2.6460 2.6454 .0006 3 1 1
2.5860 2.5863 -.0003 -4 0 3
2.5130 2.5116 .0014 4 0 3
2.3900 2.3876 .0024 -4 1 1
2.3280 2.3288 -.0008 2 1 3
2.2890 2.2868 .0022 6 0 1
2.2150 2.2148 .0002 -3 1 3
a= 14.12 b= 3.364 c= 11.058 beta= 91.67
da=.01 db= .004 dc=.003 dbeta=.07
V= 524.9
Triklin
Dexp Dcal d(D) h k l
4.2820 4.2789 .0031 -1 0 1
3.6340 3.6364 -.0024 1 1 1
3.3100 3.3110 -.0010 -1 -1 1
3.1270 3.1260 .0010 -1 1 2
2.8060 2.8069 -.0009 -1 -1 2
2.6460 2.6435 .0025 2 -1 2
2.5860 2.5879 -.0019 2 0 2
2.5130 2.5130 -.0000 -1 1 3
2.3900 2.3915 -.0015 2 -2 1
2.3280 2.3279 .0001 -2 2 0
2.2890 2.2882 .0008 2 1 1
2.2150 2.2146 .0004 1 -3 1
A= 5.551 DA= .001
B= 6.751 DB= .005
C= 10.706 DC= .005
GAMMA=104.63 DGAMMA= .04
BETA = 75.641 DBETA = .009
ALPHA= 95.14 DALPHA= .01
V=375.6
94. 49-0186
PbHfO3
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
2.8280 2.8237 .0043 2 0 0
2.7610 2.7617 -.0007 2 1 0
2.6500 2.6506 -.0006 0 5 0
1.9290 1.9286 .0004 0 0 2
1.6360 1.6367 -.0007 3 4 0
1.5810 1.5812 -.0002 2 1 2
1.4250 1.4249 .0001 1 9 0
1.3810 1.3808 .0002 4 2 0
a= 5.6473 b=13.2528 c= 3.857
da= .0008 db= .0008 dc= .001
V= 288.7
Rombik
Groupa 26,28,51
romb.
Dexp. Dcal. d(D) h k l
2.8280 2.8237 .0043 0 0 2
2.7610 2.7617 -.0007 1 0 2
2.6500 2.6506 -.0006 5 0 0
1.9290 1.9286 .0004 0 1 0
1.6360 1.6367 -.0007 4 0 3
1.5810 1.5812 -.0002 1 1 2
1.4250 1.4249 .0001 9 0 1
1.3810 1.3808 .0002 2 0 4
a=13.2528 b= 1.9286 c= 5.6473
da= .0008 db= .0005 dc= .000826
V= 144.34
95. 49-1489
HfPd
Triklin
Dexp Dcal d(D) h k l
5.0590 5.0588 .0002 0 3 1
4.6020 4.5995 .0025 -1 0 1
4.3650 4.3674 -.0024 -1 -2 1
4.0450 4.0456 -.0006 -1 -3 1
3.7000 3.6987 .0013 0 6 0
3.6340 3.6339 .0001 1 2 1
3.4170 3.4162 .0008 -1 4 1
3.3370 3.3358 .0012 0 2 2
3.2940 3.2923 .0017 0 -6 1
3.1370 3.1382 -.0012 -1 -2 2
3.0400 3.0401 -.0001 -1 2 2
2.9950 2.9951 -.0001 -1 -6 1
A= 5.2339 DA= .0002
B= 22.2626 DB= .0006
C= 7.17856 DC= .00001
GAMMA= 85.521 DGAMMA= .001
BETA =101.7911 DBETA = .0004
ALPHA= 91.7162 DALPHA= .0003
V=816.5