1. 45-0081
Na3Fe{PO4}2
Triklin
Dexp Dcal d(D) h k l
7.1300 7.1120 .0180 0 1 1
6.9400 6.9457 -.0057 0 -1 1
4.4100 4.4147 -.0047 1 1 0
3.7800 3.7839 -.0039 -1 -2 1
3.7500 3.7508 -.0008 0 0 2
3.7300 3.7372 -.0072 -1 3 0
3.6800 3.6703 .0097 1 0 1
3.4700 3.4718 -.0018 1 2 1
3.3700 3.3680 .0020 1 4 0
3.1600 3.1571 .0029 -1 -4 1
3.1000 3.0986 .0014 0 6 1
2.8330 2.8311 .0019 -1 3 2
A= 4.557 DA= .006
B= 20.096 DB= .004
C= 7.56813 DC= .00007
GAMMA= 89.97 DGAMMA= .01
BETA = 97.32 DBETA = .01
ALPHA= 87.96 DALPHA= .03
V= 687.0
2. 45-0981
Al20Cu15Fe65
Triklin
Dexp Dcal d(D) h k l
9.8215 9.8243 -.0028 1 0 0
8.9618 8.9806 -.0188 0 1 1
5.5289 5.5263 .0026 0 -1 1
4.0623 4.0639 -.0016 2 1 0
3.9692 3.9711 -.0019 1 2 1
3.7511 3.7522 -.0011 -3 1 2
3.6980 3.6975 .0005 -1 -1 2
3.5163 3.5151 .0012 -1 3 1
3.4155 3.4139 .0016 -3 2 3
3.3216 3.3218 -.0002 -3 1 3
3.2482 3.2481 .0001 -3 1 0
2.8006 2.8006 .0000 1 0 3
A= 11.428 DA= .001
B= 11.0564 DB= .0004
C= 12.5709 DC= .0001
GAMMA=112.72 DGAMMA= .01
BETA =119.50 DBETA = .01
ALPHA= 56.444 DALPHA= .005
V= 1137.9
3. 45-1017
Al95Fe4Cr
Tetragon
Groupa 76,78,91,95
Dexp. Dcal. d(D) h k l
4.0000 3.9982 .0018 1 0 1
3.4000 3.4028 -.0028 1 1 1
2.1600 2.1604 -.0004 3 0 0
2.0500 2.0496 .0004 3 1 0
1.2700 1.2700 .0000 0 0 4
a= 6.48 c= 5.079
da= .01 dc= .002
V= 213
4. 45-1018
Al91Fe4Cr5
Tetragon
Groupa 90,113
Dexp. Dcal. d(D) h k l
3.9000 3.9051 -.0051 0 0 1
3.4000 3.3960 .0040 1 0 1
2.1700 2.1751 -.0051 3 1 0
2.0600 2.0643 -.0043 2 2 1
1.4990 1.4973 .0017 3 3 1
1.2790 1.2790 .0000 1 0 3
a= 6.8784 c= 3.9051
da= .0007 dc= .0005
V= 184.76
5. 45-1173
B4Fe4Pr1+x
Triklin
Dexp Dcal d(D) h k l
5.0450 5.0406 .0044 1 0 0
3.5710 3.5671 .0039 -1 2 1
3.1330 3.1329 .0001 1 -2 1
3.0840 3.0846 -.0006 1 2 1
2.5260 2.5258 .0002 0 -2 2
2.4704 2.4699 .0005 2 0 1
2.3522 2.3512 .0010 1 0 3
2.2590 2.2595 -.0005 -1 2 3
2.1185 2.1186 -.0001 -1 4 2
1.9662 1.9643 .0019 -2 3 2
1.9545 1.9544 .0001 0 -2 3
1.8813 1.8819 -.0006 2 0 3
A= 5.1590 DA= .0006
B= 9.3013 DB= .0001
C= 7.8774 DC= .0002
GAMMA=100.74 DGAMMA= .02
BETA = 87.173 DBETA = .005
ALPHA= 74.37 DALPHA= .01
V=355.6
6. 45-1174
B4Fe4Pr1+x
Triklin
Dexp Dcal d(D) h k l
3.5620 3.5619 .0001 0 1 1
3.2270 3.2272 -.0002 -1 0 1
3.0760 3.0734 .0026 -1 1 1
2.5250 2.5254 -.0004 -2 0 1
2.4658 2.4670 -.0012 -2 1 1
2.3940 2.3931 .0009 2 2 0
2.2578 2.2593 -.0015 0 -2 1
2.1165 2.1175 -.0010 -2 2 1
1.9870 1.9871 -.0001 1 3 0
1.9510 1.9502 .0008 4 0 1
1.8739 1.8748 -.0009 4 1 1
1.7624 1.7616 .0008 2 -1 2
A= 8.17036 DA= .00009
B= 6.33446 DB= .00002
C= 4.01194 DC= .00008
GAMMA= 91.4375 DGAMMA= .0004
BETA = 78.152 DBETA = .001
ALPHA= 81.1604 DALPHA= .0002
V=200.4
7. 45-1175
B4Fe4Pr1+x
Triklin
Dexp Dcal d(D) h k l
3.5790 3.5796 -.0006 1 1 0
3.1320 3.1322 -.0002 -1 0 2
2.5300 2.5301 -.0001 -1 -2 1
2.4717 2.4713 .0004 -1 0 3
2.3558 2.3559 -.0001 -1 -2 2
2.2599 2.2605 -.0006 -2 0 1
2.1201 2.1210 -.0009 0 1 4
1.9654 1.9654 -.0000 -1 2 3
1.8798 1.8797 .0001 -1 1 4
1.7654 1.7658 -.0004 3 -2 3
1.7231 1.7232 -.0001 3 -1 3
1.6400 1.6399 .0001 -2 3 2
A= 5.3951 DA= .0002
B= 8.052 DB= .002
C= 10.72376 DC= .00000
GAMMA=112.042 DGAMMA= .005
BETA = 71.2382 DBETA = .0007
ALPHA=112.01 DALPHA= .017
V=391.4
8. 45-1176
Al86Fe14
Tetragon
Groupa 75
Dexp. Dcal. d(D) h k l
3.9150 3.9188 -.0038 1 1 1
2.1728 2.1730 -.0002 1 0 3
2.0684 2.0682 .0002 1 1 3
1.5070 1.5070 .0000 4 2 0
a= 6.7394 c= 6.8868
da= .0001 dc= .0007
V= 312.80
9. 45-1177
Al82Fe18
Tetragon
Groupa 100,117,127
Dexp. Dcal. d(D) h k l
3.7983 3.7929 .0054 1 1 0
2.1633 2.1631 .0002 0 0 3
2.0667 2.0672 -.0005 2 0 2
1.4877 1.4877 .0000 3 2 0
a= 5.3640 c= 6.489
da= .0004 dc= .002
V= 186.71
10. 45-1308
Al65Cr10Fe10Ge15
Geksagon
Groupa 144,145,151 152,153,154,171,
172,180,181
Dexp. Dcal. d(D) h k l
3.3050 3.3053 -.0003 1 1 1
2.1460 2.1439 .0021 0 0 3
2.0400 2.0411 -.0011 1 0 3
1.4810 1.4810 .0000 4 0 2
1.2630 1.2631 -.0001 1 0 5
a= 7.706 c= 6.431564
da= .0092 dc= .001
V=330.7
11. 45-1358
Ca2Fe3+3{AsO4}4{OH}*12H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
14.0600 14.2261 -.1661 1 0 0
5.5820 5.5702 .0118 2 0 1
4.2850 4.2718 .0132 1 0 2
3.2550 3.2559 -.0009 3 0 2
2.7890 2.7896 -.0006 2 1 0
2.2360 2.2346 .0014 4 1 1
2.1380 2.1359 .0021 2 0 4
1.7590 1.7596 -.0006 5 0 4
1.6280 1.6280 .0000 6 0 4
1.5070 1.5073 -.0003 2 1 5
1.4050 1.4050 .0000 10 0 1
a=14.226 b= 3.033 c= 8.957
da= .002 db= .002 dc= .006
V= 386.4
12. 45-1358
Ca2Fe3+3{AsO4}4{OH}*12H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
14.0600 14.2234 -.1634 1 0 0
5.5820 5.5832 -.0012 1 1 0
4.2850 4.2745 .0105 1 0 2
3.2550 3.2569 -.0019 3 0 2
2.7890 2.7916 -.0026 2 2 0
2.2360 2.2356 .0004 4 2 1
2.1380 2.1372 .0008 2 0 4
1.7590 1.7587 .0003 4 3 0
1.6280 1.6284 -.0004 6 0 4
1.5070 1.5076 -.0006 9 1 1
1.4050 1.4048 .0002 10 0 1
a=14.223 b= 6.070 c= 8.963
da= .006 db= .005 dc= .004
V= 773.9
13. 45-1510
C3H9FeO3*CH3OH
Triklin
Dexp Dcal d(D) h k l
10.3100 10.3180 -.0080 -1 1 0
9.8300 9.8245 .0055 1 1 0
8.9300 8.9285 .0015 0 0 1
7.0400 7.0390 .0010 1 -1 1
6.6400 6.6417 -.0017 0 2 1
5.0300 5.0086 .0214 0 3 1
4.5500 4.5562 -.0062 0 1 2
4.2900 4.2877 .0023 2 0 2
3.6900 3.6899 .0001 3 1 2
3.5600 3.5590 .0010 -3 1 1
3.3400 3.3398 .0002 -2 1 2
3.1500 3.1504 -.0004 4 2 1
A= 13.637 DA= .006
B= 16.0939 DB= .0004
C= 9.504 DC= .006
GAMMA= 89.43 DGAMMA= .04
BETA = 74.02 DBETA = .01
ALPHA= 78.07 DALPHA= .04
V=1958
1. 46-0015
FeYGe2O7
Triklin
Dexp Dcal d(D) h k l
5.9200 5.9301 -.0101 0 1 1
5.1900 5.1839 .0061 0 -1 1
4.9700 4.9808 -.0108 -1 1 0
4.2600 4.2589 .0011 -1 0 1
3.4600 3.4618 -.0018 1 1 1
3.2700 3.2763 -.0063 -1 2 1
3.1700 3.1637 .0063 1 -2 1
3.0800 3.0828 -.0028 1 1 2
3.0400 3.0358 .0042 0 -2 1
2.9700 2.9651 .0049 0 2 2
2.7700 2.7718 -.0018 0 -1 3
2.7200 2.7232 -.0032 1 -2 2
A= 5.4311 DA= .0005
B= 7.211 DB= .003
C= 9.8891 DC= .0003
GAMMA=110.25 DGAMMA= .09
BETA = 84.94 DBETA = .05
ALPHA= 84.08 DALPHA= .01
V= 358.2
2. 46-0198
FeH6P3O12
Triklin
Dexp Dcal d(D) h k l
11.1800 11.1698 .0102 1 0 0
9.0700 9.0597 .0103 0 1 0
8.8300 8.8311 -.0011 -1 0 1
7.7600 7.7625 -.0025 1 1 0
5.7700 5.7739 -.0039 -2 0 1
4.7150 4.7066 .0084 -2 -1 1
4.6270 4.6267 .0003 0 0 2
4.5800 4.5761 .0039 1 2 1
4.2010 4.1990 .0020 1 1 2
4.1700 4.1709 -.0009 2 0 1
3.8750 3.8813 -.0063 2 2 0
3.8020 3.7980 .0040 1 2 2
A= 11.957 DA= .001
B= 10.022 DB= .001
C= 10.766 DC= .001
GAMMA= 87.91 DGAMMA= .02
BETA =108.18 DBETA = .03
ALPHA= 66.84 DALPHA= .01
М=1109.4
3. 46-0832
FeAu3{CN}6
Triklin
Dexp Dcal d(D) h k l
10.2200 10.2197 .0003 1 0 0
5.1500 5.1536 -.0036 1 0 1
3.4400 3.4421 -.0021 1 -2 1
3.0930 3.0934 -.0004 -3 -2 1
2.9610 2.9611 -.0001 1 2 1
2.6530 2.6526 .0004 2 3 0
2.5820 2.5820 .0000 -3 1 1
2.3010 2.3007 .0003 4 0 1
2.0670 2.0633 .0037 -4 0 2
1.9830 1.9830 -.0000 1 -4 1
1.7920 1.7919 .0001 -3 -4 3
1.7630 1.7630 -.0000 2 4 1
A= 10.6891 DA= .0003
B= 8.9104 DB= .0001
C= 6.7426 DC= .0007
GAMMA= 73.597 DGAMMA= .003
BETA =100.127 DBETA = .005
ALPHA=111.356 DALPHA= .003
V=571.9
4. 46-0973
FeMgCl4*8H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.4330 8.3890 .0440 -1 0 1
8.3370 8.3166 .0204 1 1 0
6.0520 6.0591 -.0071 2 0 0
5.6710 5.6673 .0037 1 1 1
4.6880 4.6785 .0095 -1 0 2
4.5420 4.5383 .0037 2 0 1
4.2240 4.2182 .0058 2 1 1
4.1490 4.1583 -.0093 2 2 0
4.0690 4.0624 .0066 -2 2 1
3.5020 3.5005 .0015 -3 0 2
3.0330 3.0305 .0025 -1 1 3
2.8620 2.8586 .0034 0 4 0
a= 12.536 b= 11.434 c= 9.43 beta= 104.84
da=.002 db=.005 dc=.01 dbeta=.04
V= 1306
Triklin
Dexp Dcal d(D) h k l
8.4330 8.4569 -.0239 1 0 0
8.3370 8.3065 .0305 0 1 0
6.0520 6.0382 .0138 0 0 1
5.6710 5.6471 .0239 1 1 0
4.6880 4.6868 .0012 -1 1 1
4.5420 4.5369 .0051 0 -1 1
4.2240 4.2284 -.0044 2 0 0
4.1490 4.1533 -.0043 0 2 0
4.0690 4.0650 .0040 1 -1 1
3.5020 3.4988 .0032 -2 0 1
3.0330 3.0343 -.0013 -2 -1 1
2.8620 2.8627 -.0007 -1 0 2
A= 8.50702 DA= .00007
B= 8.473 DB= .001
C= 6.129 DC= .002
GAMMA= 96.11 DGAMMA= .02
BETA = 92.24 DBETA = .03
ALPHA= 80.21 DALPHA= .03
М=434.4
5. 46-0974
FeZnCl4*6H2O
Triklin
Dexp Dcal d(D) h k l
7.0010 6.9872 .0138 0 1 1
6.1890 6.2002 -.0112 1 0 1
5.1460 5.1489 -.0029 0 -1 1
4.8230 4.8276 -.0046 1 1 0
4.6990 4.6904 .0086 0 0 2
4.4420 4.4428 -.0008 1 0 2
4.3530 4.3464 .0066 -1 1 1
3.5250 3.5261 -.0011 0 -1 2
3.3170 3.3149 .0021 1 1 3
3.2560 3.2590 -.0030 0 1 3
3.2210 3.2214 -.0004 2 0 0
3.1600 3.1604 -.0004 2 1 1
A= 6.73705 DA= .00000
B= 7.8976 DB= .0001
C= 10.29135 DC= .00003
GAMMA= 86.2095 DGAMMA= .0004
BETA = 73.0754 DBETA = .0001
ALPHA= 72.0057 DALPHA= .0007
V=498.0
6. 46-1058
Cu40Fe60
Triklin
Dexp Dcal d(D) h k l
5.1502 5.1508 -.0006 0 1 0
3.0501 3.0493 .0008 2 1 0
2.6624 2.6636 -.0012 -2 0 1
2.3890 2.3900 -.0010 -2 -1 1
2.0074 2.0076 -.0002 2 1 1
1.9156 1.9157 -.0001 -4 0 1
1.8534 1.8531 .0003 -4 1 1
1.7309 1.7311 -.0002 -5 2 0
1.5708 1.5707 .0001 -1 -3 1
1.4280 1.4272 .0008 -2 3 1
1.3719 1.3722 -.0003 6 1 0
1.2296 1.2304 -.0008 7 -2 1
A= 9.5435 DA= .0004
B= 5.4511 DB= .0004
C= 3.170 DC= .00009
GAMMA=104.955 DGAMMA= .001
BETA = 91.124 DBETA = .007
ALPHA=101.3403 DALPHA= .0009
V=155.8
7. 46-1089
C*xFeCl3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
21.7000 21.7799 -.0799 0 0 1
7.3100 7.3082 .0018 1 1 0
5.4500 5.4514 -.0014 1 1 3
3.6300 3.6300 .0000 0 0 6
3.1400 3.1400 .0000 3 1 0
2.7300 2.7300 .0000 0 4 0
2.4200 2.4200 .0000 0 0 9
1.8200 1.8200 .0000 0 6 0
1.6800 1.6800 .0000 3 5 6
1.5600 1.5600 .0000 0 7 0
A= 9.93981 DA= .00008
B= 10.92000 DB= .00001
C= 22.0111 DC= .0003
BETA = 81.694 DBETA = .005
V=2364
8. 46-1103
Al65Cr10Fe10Ge15
Geksagon
Groupa 158,165,173,176,182
Dexp. Dcal. d(D) h k l
3.2860 3.2788 .0072 0 0 2
2.1640 2.1610 .0030 2 0 1
2.0560 2.0577 -.0017 1 1 2
1.4850 1.4862 -.0012 3 0 1
1.2700 1.2696 .0004 3 1 0
a= 5.286 c= 6.56
da=.001 dc= .01
V= 158.7
9. 46-1450
{Fe,Al,M}6{Si,Al}4O10{OH}4*H2O
Triklin
Dexp Dcal d(D) h k l
16.0400 16.0698 -.0298 0 1 0
8.0300 8.0349 -.0049 0 2 0
5.4000 5.3566 .0434 0 3 0
4.0700 4.0716 -.0016 2 1 0
3.3200 3.3163 .0037 1 3 1
3.2100 3.2140 -.0040 0 5 0
2.9100 2.9094 .0006 1 4 1
2.7500 2.7491 .0009 0 -1 2
2.6000 2.5999 .0001 -2 0 2
2.5600 2.5602 -.0002 2 5 0
2.4800 2.4806 -.0006 0 -3 2
2.3700 2.3697 .0003 -1 6 1
A= 8.61575 DA= .00001
B= 16.071 DB= .001
C= 5.7117 DC= .0001
GAMMA= 89.552 DGAMMA= .005
BETA =102.69810 DBETA = .00004
ALPHA= 90.5970 DALPHA= .0004
V=770.8
10. 46-1680
C10H8AgClFe
Triklin
Dexp Dcal d(D) h k l
12.6700 12.6660 .0040 1 0 0
11.2100 11.2341 -.0241 0 1 0
8.6300 8.6615 -.0315 0 1 1
8.4200 8.4360 -.0160 -1 1 1
6.7240 6.7211 .0029 -1 -1 1
5.9510 5.9478 .0032 1 -1 1
5.7210 5.7204 .0006 -1 0 2
5.6280 5.6236 .0044 -1 1 2
5.3950 5.4010 -.0060 0 2 1
4.6370 4.6391 -.0021 0 -1 2
4.4700 4.4707 -.0007 2 -1 1
4.2180 4.2180 .0000 -2 2 2
A= 13.423 DA= .006
B= 11.54 DB= .01
C= 11.82 DC= .01
GAMMA= 98.53 DGAMMA= .06
BETA =108.72 DBETA = .05
ALPHA= 77.82 DALPHA= .09
V= 1688.7
11. 46-1681
C10H8AgClFe
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.6600 11.5816 .0784 1 0 0
9.0100 8.9656 .0444 1 1 0
7.6100 7.6072 .0028 0 0 1
5.6700 5.6591 .0109 1 0 1
5.4230 5.4135 .0095 -2 0 1
5.2580 5.2551 .0029 1 1 1
4.6990 4.7210 -.0220 0 3 0
4.4700 4.4828 -.0128 2 2 0
4.3770 4.3718 .0052 1 3 0
3.7000 3.7015 -.0015 -2 0 2
3.5390 3.5408 -.0018 0 4 0
3.3490 3.3508 -.0018 0 2 2
a= 12.09 b= 14.163 c=7.938 beta= 106.61
da=.01 db= .005 dc=.001 dbeta=.04
V= 1302.1
Triklin
Dexp Dcal d(D) h k l
11.6600 11.6630 -.0030 1 0 0
9.0100 9.0213 -.0113 1 1 0
7.6100 7.6081 .0019 -1 0 1
5.6700 5.6590 .0110 2 1 0
5.4230 5.4210 .0020 2 0 1
5.2580 5.2579 .0001 0 1 2
4.6990 4.7043 -.0053 0 -1 2
4.4700 4.4643 .0057 -1 1 2
4.3770 4.3803 -.0033 1 -1 2
3.7000 3.7028 -.0028 -1 2 2
3.5390 3.5427 -.0037 3 2 0
3.3490 3.3490 -.0000 -1 3 0
A= 12.03999 DA= .00009
B= 11.5418 DB= .0006
C= 11.3030 DC= .0003
GAMMA= 77.184 DGAMMA= .003
BETA = 81.57 DBETA = .01
ALPHA= 80.412 DALPHA= .003
V=1500.4
12. 46-1682
C10H8AgBrFe
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
11.6600 11.6915 -.0315 1 0 0
9.0900 9.0950 -.0050 0 1 0
5.8640 5.8458 .0182 2 0 0
4.5480 4.5475 .0005 0 2 0
3.5750 3.5822 -.0072 3 1 0
3.2270 3.2282 -.0012 3 1 2
2.9040 2.9025 .0015 3 2 1
2.5810 2.5816 -.0006 3 1 4
2.5200 2.5188 .0012 4 0 3
2.3660 2.3661 -.0001 2 3 3
2.0418 2.0418 .0000 2 2 6
a=11.692 b= 9.095 c=14.896
da= .005 db= .001 dc= .004
v=1583.9
13. 46-1683
C10H8BrCuFe
Triklin
Dexp Dcal d(D) h k l
10.1600 10.1654 -.0054 0 1 1
9.4200 9.4200 .0000 1 0 0
7.3900 7.3981 -.0081 0 -1 1
7.0150 7.0168 -.0018 1 0 1
6.6540 6.6608 -.0068 -1 1 1
6.2530 6.2517 .0013 -1 0 2
5.6900 5.6979 -.0079 -1 1 2
5.1640 5.1626 .0014 -1 -1 2
4.5480 4.5506 -.0026 0 -2 1
4.4140 4.4036 .0104 2 1 1
3.9190 3.9179 .0011 -2 -2 1
3.5870 3.5855 .0015 0 1 4
A= 9.90563 DA= .00008
B= 11.63801 DB= .00005
C= 14.53712 DC= .00011
GAMMA= 77.95966 DGAMMA= .00005
BETA = 99.4040 DBETA = .0002
ALPHA= 74.3073 DALPHA= .0002
V=1534.3
14. 46-1684
C11H11AgFeO
Triklin
Dexp Dcal d(D) h k l
9.3300 9.3565 -.0265 0 1 1
8.4900 8.4902 -.0002 0 -1 1
6.2450 6.2426 .0024 1 1 0
5.7030 5.7020 .0010 1 0 1
4.6990 4.6997 -.0007 1 -1 1
4.5480 4.5497 -.0017 -1 -2 1
4.3770 4.3785 -.0015 -1 1 2
4.0400 4.0380 .0020 1 2 2
3.5200 3.5200 -.0000 0 3 2
3.1980 3.1984 -.0004 -2 0 1
3.0180 3.0182 -.0002 1 1 4
2.8380 2.8377 .0003 1 -2 3
A= 6.626 DA= .001
B= 11.876 DB= .001
C= 14.016 DC= .001
GAMMA= 77.840 DGAMMA= .003
BETA = 93.09 DBETA = .02
ALPHA= 85.14 DALPHA= .01
V= 1071.3
15. 46-1685
C11H11CuFeO
Triklin
Dexp Dcal d(D) h k l
12.2800 12.2485 .0315 1 0 0
11.8500 11.8467 .0033 0 1 1
11.1600 11.1383 .0217 0 -1 1
8.9600 8.9616 -.0016 -1 -1 1
5.3500 5.3517 -.0017 1 1 3
8.6300 8.6898 -.0598 -1 1 0
7.7200 7.7045 .0155 -1 0 2
6.9240 6.9332 -.0092 -1 -1 2
6.5950 6.6044 -.0094 0 -2 1
6.3680 6.3677 .0003 1 2 1
5.9850 5.9862 -.0012 2 1 0
5.8440 5.8302 .0138 -1 2 0
A= 12.4171 DA= .0008
B= 14.639 DB= .001
C= 18.981 DC= .007
GAMMA= 81.14 DGAMMA= .01
BETA = 92.769 DBETA = .008
ALPHA= 86.82 DALPHA= .01
V=3404.9
16. 46-1686
C10H9CuFe
Rombik
Grupa 16
Dexp. Dcal. d(D) h k l
12.2200 12.2545 .0345 0 1 1
8.3500 8.3224 -.0276 0 0 2
6.0550 6.0362 -.0188 0 3 0
5.9170 5.9345 .0175 1 0 1
5.5380 5.5482 .0102 0 0 3
5.2060 5.1999 -.0061 1 2 0
4.9580 4.9634 .0054 1 2 1
4.7330 4.7307 -.0023 0 2 3
4.1680 4.1612 -.0068 0 0 4
2.4470 2.4467 -.0003 1 6 3
2.4470 2.4476 .0006 1 2 6
2.3292 2.3291 -.0001 2 3 4
2.3292 2.3291 -.0001 2 3 4
a= 6.3519 b= 18.11 c= 16.645
da=.0003 db= .02 dc=.004
V= 1914
17. 46-1687
C10H9AgFe
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
12.7000 12.7031 -.0031 0 1 0
8.3500 8.3877 -.0377 1 1 0
5.1140 5.1121 .0019 2 1 0
3.5750 3.5726 .0024 3 1 0
3.2100 3.2118 -.0018 3 2 0
3.0300 3.0298 .0002 0 2 2
2.8580 2.8582 -.0002 2 1 2
2.5630 2.5628 .0002 2 4 1
a=11.168 b=12.70 c= 6.895
da= .003 db= .02 dc= .002
V= 978
18. 46-1688
C10H8Cu2Fe
Tetragon
Groupa 77,84,93
Dexp. Dcal. d(D) h k l
9.9700 9.9319 .0381 0 0 2
9.1700 9.1727 -.0027 1 0 0
3.0270 3.0220 .0050 3 0 1
2.4640 2.4645 -.0005 3 2 2
2.1356 2.1356 .0000 2 2 7
1.5083 1.5080 .0003 6 1 0
1.2862 1.2863 -.0001 7 1 2
a= 9.173 c= 19.86
da= .002 dc= .03
V=1671