1. 37-0230
Zn2.5Co0.5{PO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
7.0830 7.0770 .0060 1 0 0
5.2280 5.2330 -.0050 1 1 1
4.8160 4.8197 -.0037 1 -1 1
4.2700 4.2718 -.0018 -1 -1 1
3.9160 3.9152 .0008 -1 2 0
3.6240 3.6245 -.0005 1 -2 1
3.5120 3.5113 .0007 2 0 1
3.2000 3.2096 -.0096 2 -1 1
3.0180 3.0224 -.0044 1 3 1
2.9380 2.9382 -.0002 0 -2 2
2.6160 2.6165 -.0005 2 2 2
2.5100 2.5081 .0019 0 4 0
A= 7.303 DA= .007
B= 10.090 DB= .006
C= 7.547 DC= .009
GAMMA= 83.98 DGAMMA= .05
BETA = 76.85 DBETA = .09
ALPHA= 87.61 DALPHA= .07
V= 538.4
2. 37-0231
gammaZn2.5Co0.5{PO4}2
Triklin
Dexp Dcal d(D) h k l
5.0390 5.0315 .0075 -1 0 3
4.3360 4.3395 -.0035 0 1 0
4.0150 4.0149 .0001 0 -1 2
3.8530 3.8519 .0011 -1 1 0
3.6630 3.6631 -.0001 -1 1 2
3.4270 3.4275 -.0005 -1 1 3
3.2270 3.2236 .0034 1 1 2
3.0200 3.0216 -.0016 1 1 3
2.8990 2.8989 .0001 2 0 3
2.8000 2.8004 -.0004 1 1 4
2.7220 2.7225 -.0005 -2 0 5
2.6260 2.6257 .0003 -1 1 6
A= 6.750 DA= .001
B= 4.3700 DB= .0001
C= 20.742 DC= .007
GAMMA= 96.764 DGAMMA= .002
BETA = 95.314 DBETA = .006
ALPHA= 89.95 DALPHA= .01126
V=605
3. 37-0530
C4H10CoN4O8*3H2O
Triklin
Dexp Dcal d(D) h k l
7.6180 7.6120 .0060 1 0 0
7.1440 7.1290 .0150 0 1 0
5.9650 5.9523 .0127 0 -1 1
5.7530 5.7700 -.0170 1 1 0
3.9350 3.9304 .0046 -2 -1 1
3.8070 3.8060 .0010 2 0 0
3.7800 3.7766 .0034 -2 0 1
3.6520 3.6536 -.0016 2 1 0
3.6140 3.6181 -.0041 0 -1 2
3.5560 3.5525 .0035 0 0 2
3.2570 3.2587 -.0017 -2 -1 2
3.0530 3.0489 .0041 2 0 1
A= 8.196 DA= .002
B= 7.747 DB= .004
C= 7.840 DC= .003
GAMMA= 73.76 DGAMMA= .02
BETA =109.014 DBETA = .009
ALPHA=110.49 DALPHA= .01
V=433.5
4. C2CoO4*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9600 5.9346 .0254 1 1 0
5.4900 5.4884 .0016 -1 1 1
4.4900 4.5170 -.0270 0 0 2
3.6900 3.6890 .0010 0 2 1
3.0100 3.0113 -.0013 0 0 3
2.8500 2.8515 -.0015 -3 1 1
2.7400 2.7396 .0004 -2 1 3
2.7000 2.6978 .0022 -3 1 2
2.6200 2.6197 .0003 1 0 3
2.4200 2.4214 -.0014 1 3 1
2.2400 2.2428 -.0028 -4 0 2
1.7780 1.7776 .0004 -2 4 2
1.4310 1.4310 .0000 -6 0 4
1.4280 1.4280 -.0000 -3 5 1
a= 9.146 b= 8.08256 c= 9.458 beta= 107.10
da=.0043 db=.000025 dc=.0092 dbeta=.09
V= 668
Triklin
Dexp Dcal d(D) h k l
5.9600 5.9579 .0021 0 1 1
4.4900 4.4909 -.0009 0 -1 1
3.6900 3.6867 .0033 2 1 1
3.0100 3.0096 .0004 1 -2 1
2.8500 2.8502 -.0002 -1 1 2
2.7400 2.7401 -.0001 0 3 1
2.7000 2.6998 .0002 -1 -2 1
2.6200 2.6199 .0001 -2 2 1
2.4200 2.4204 -.0004 3 1 2
2.2400 2.2401 -.0001 2 3 2
1.7780 1.7779 .0001 1 1 4
1.4310 1.4310 -.0000 1 -2 4
1.4280 1.4280 .0000 -2 1 4
A= 8.216 DA= .004
B= 8.294 DB= .001
C= 7.1445 DC= .0004
GAMMA= 87.65 DGAMMA= .02
BETA = 73.730 DBETA = .006
ALPHA= 73.72 DALPHA= .01
V= 448.2
5. 37-0537
Na2CoP4O8N4H4*6H2O
Triklin
Dexp Dcal d(D) h k l
8.7900 8.7932 -.0032 1 0 0
7.7900 7.7933 -.0033 0 1 1
6.2400 6.2570 -.0170 0 -1 1
5.4000 5.3992 .0008 1 -1 1
4.9300 4.9299 .0001 0 1 2
4.6800 4.6769 .0031 0 2 1
4.4400 4.4380 .0020 -2 1 1
3.9700 3.9568 .0132 0 -2 1
3.8800 3.8869 -.0069 1 -2 1
3.6300 3.6302 -.0002 2 1 0
3.5000 3.5004 -.0004 -2 0 2
3.2000 3.2026 -.0026 0 3 1
A= 9.257 DA= .001
B= 10.109 DB= .009
C= 10.530 DC= .003
GAMMA=107.31 DGAMMA= .01
BETA = 99.734 DBETA = .002
ALPHA= 75.28 DALPHA= .03
V= 905
6. 37-0668
Ca2Co2O5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.3670 5.3634 .0036 2 0 0
3.5750 3.5756 -.0006 3 0 0
3.0700 3.0732 -.0032 0 1 0
2.9520 2.9544 -.0024 1 1 0
2.6930 2.6909 .0021 -2 0 3
2.6880 2.6909 -.0029 -2 0 3
2.5560 2.5551 .0009 4 0 4
2.4100 2.4094 .0006 3 1 1
2.2770 2.2767 .0003 4 0 5
2.1460 2.1454 .0006 5 0 0
2.0790 2.0795 -.0005 1 0 6
a= 11.708 b= 3.073 c= 12.83 beta= 66.36
da=.005 db=.001 dc=.01 dbeta=.05
V= 422.8
Triklin
Dexp Dcal d(D) h k l
5.3670 5.3742 -.0072 0 1 0
3.5750 3.5764 -.0014 0 -1 2
3.0700 3.0696 .0004 -1 0 2
2.9520 2.9510 .0010 -1 1 2
2.6930 2.6941 -.0011 0 -1 3
2.6880 2.6871 .0009 0 2 0
2.5560 2.5555 .0005 1 -2 2
2.4100 2.4097 .0003 -1 0 3
2.2770 2.2776 -.0006 -1 2 2
2.2270 2.2267 .0003 0 0 4
2.1460 2.1461 -.0001 -2 0 1
2.0790 2.0790 .0000 0 -2 3
A= 4.914 DA= .001
B= 5.891 DB= .002
C= 8.984 DC= .001
GAMMA=113.75 DGAMMA= .02
BETA = 84.14 DBETA = .01
ALPHA= 96.663 DALPHA= .009
V=236.0
7. 37-0669
CaCo2O4
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
5.4320 5.4290 .0030 0 1 1
3.7130 3.7139 -.0009 1 0 3
3.4580 3.4506 .0074 0 1 3
2.7420 2.7407 .0013 1 2 1
2.7150 2.7145 .0005 0 2 2
2.4160 2.4203 -.0043 3 0 2
2.3590 2.3596 -.0006 3 1 1
2.3430 2.3461 -.0031 2 2 1
2.2330 2.2335 -.0005 2 2 2
2.1060 2.1070 -.0010 0 0 6
2.0790 2.0773 .0017 2 2 3
1.9720 1.9750 -.0030 3 2 0
a= 7.860 b= 6.012 c=12.64
da= .004 db= .002 dc= .01
V= 597.3
Triklin
Dexp Dcal d(D) h k l
5.4320 5.4315 .0005 -1 1 0
3.7130 3.7146 -.0016 -1 2 0
3.4580 3.4589 -.0009 1 -2 2
2.7420 2.7424 -.0004 -1 1 2
2.7150 2.7145 .0005 -2 1 1
2.4160 2.4152 .0008 -2 0 2
2.3590 2.3599 -.0009 2 -3 2
2.3430 2.3429 .0001 -2 2 1
2.2330 2.2325 .0005 -2 -2 2
2.1060 2.1058 .0002 -3 1 0
2.0790 2.0793 -.0003 3 0 0
1.9720 1.9730 -.0010 -3 1 1
A= 6.3600 DA= .0003
B= 9.298 DB= .001
C= 8.527 DC= .004
GAMMA=101.24 DGAMMA= .05
BETA = 85.23 DBETA = .03
ALPHA=117.55 DALPHA= .04
V= 438.5
8. 37-0670
Ca3Mn1.5Co1.5O8-x
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6000 5.5997 .0003 -2 0 3
4.7600 4.7589 .0011 0 1 0
4.6000 4.6014 -.0014 0 1 1
2.9000 2.8999 .0001 4 0 2
2.8800 2.8809 -.0009 -4 1 1
2.6460 2.6460 -.0000 4 1 1
2.4750 2.4756 -.0006 4 1 2
2.1670 2.1676 -.0006 -6 1 2
2.1340 2.1342 -.0002 -3 2 2
2.0530 2.0530 .0000 -7 0 5
1.9580 1.9579 .0001 4 2 0
1.9400 1.9414 -.0014 -4 2 4
A= 14.684 DA= .001
B= 4.759 DB= .001
C= 19.280 DC= .008
BETA =110.322 DBETA = .008
V=1262
Triklin
Dexp Dcal d(D) h k l
5.6000 5.6022 -.0022 1 0 1
4.7600 4.7611 -.0011 0 1 1
4.6000 4.6014 -.0014 0 -1 1
2.9000 2.9018 -.0018 0 0 2
2.8800 2.8794 .0006 1 -1 2
2.6460 2.6465 -.0005 1 2 2
2.4750 2.4751 -.0002 2 2 2
2.1670 2.1668 .0002 3 0 2
2.1340 2.1340 .0000 1 0 3
2.0530 2.0529 .0001 -1 3 1
1.9580 1.9579 .0001 1 4 0
1.9400 1.9401 -.0001 1 -3 2
A= 6.8585 DA= .0004
B= 8.0237 DB= .0001
C= 6.4956 DC= .0002
GAMMA= 80.553 DGAMMA= .003
BETA = 63.392 DBETA = .003
ALPHA= 83.973 DALPHA= .003
V=315.0
9. 37-0681
KFe0.5Co0.5Cl3*2H2O
Triklin
Dexp Dcal d(D) h k l
5.7900 5.7991 -.0091 0 1 1
5.0300 5.0374 -.0074 0 -1 1
4.8000 4.8001 -.0001 -1 -1 1
4.3400 4.3416 -.0016 -1 2 0
4.1400 4.1429 -.0029 0 2 1
3.1100 3.1093 .0007 2 1 1
3.0400 3.0382 .0018 -1 -1 2
2.9600 2.9607 -.0007 -2 -2 1
2.8900 2.8896 .0004 -2 2 2
2.6800 2.6801 -.0001 -3 1 2
2.6400 2.6403 -.0003 -3 0 2
2.5400 2.5402 -.0002 1 -3 1
A= 9.521 DA= .004
B= 9.6772 DB= .0005
C= 6.966 DC= .001
GAMMA= 97.68 DGAMMA= .07
BETA =108.5 DBETA = .1
ALPHA= 79.45 DALPHA= .02
V= 596.3
10. 37-0974
Co6Mo12Fe4Bi1.5Ox
Triklin
Dexp Dcal d(D) h k l
6.2500 6.2480 .0020 1 1 0
4.8700 4.8773 -.0073 1 2 0
4.7100 4.7165 -.0065 0 2 1
4.3300 4.3339 -.0039 1 0 1
4.0700 4.0646 .0054 -1 3 1
3.9000 3.9002 -.0002 -2 1 0
3.8600 3.8599 .0001 -1 4 0
3.7300 3.7267 .0033 -2 2 1
3.5100 3.5071 .0029 -1 0 2
3.4600 3.4558 .0042 1 2 1
3.3630 3.3660 -.0030 -1 4 1
3.2830 3.2844 -.0014 -2 -2 1
A= 8.202 DA= .005
B= 16.097 DB= .001
C= 7.08 DC= .01
GAMMA=101.688 DGAMMA= .003
BETA =108.02 DBETA = .05
ALPHA= 94.57 DALPHA= .02
V=859.2
11. 37-0975
Co6Mo12Fe4Bi1.5SbOx
Triklin
Dexp Dcal d(D) h k l
6.2500 6.2499 .0001 1 0 0
4.8700 4.8741 -.0041 -1 1 1
4.7100 4.7083 .0017 -1 -1 1
4.3300 4.3281 .0019 1 1 0
4.0800 4.0838 -.0038 0 -2 1
3.8200 3.8212 -.0012 0 2 0
3.7400 3.7349 .0051 -1 1 2
3.5100 3.5089 .0011 1 1 1
3.3680 3.3703 -.0023 0 0 3
3.2780 3.2776 .0004 1 -2 2
3.2550 3.2551 -.0001 -2 0 1
3.1710 3.1729 -.0019 -2 1 1
A= 6.61236 DA= .00002
B= 8.2951 DB= .0001
C= 11.05934 DC= .00006
GAMMA= 99.96027 DGAMMA= .00005
BETA =102.213 DBETA = .003
ALPHA=107.6985 DALPHA= .0009
V=546.4
12. 37-1238
CoAs6Se10
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
4.2480 4.2524 -.0044 1 2 0
3.3256 3.3315 -.0059 2 0 0
3.1996 3.2018 -.0022 0 1 2
2.9043 2.9036 .0007 1 3 1
2.8580 2.8615 -.0035 0 2 2
2.3625 2.3607 .0018 2 0 2
2.1776 2.1775 .0001 3 1 0
2.1305 2.1298 .0007 0 4 2
1.7746 1.7747 -.0001 1 6 0
a= 6.663 b=11.0471 c= 6.691
da= .005 db= .0008 dc= .006
V= 492.5
13. 37-1606
C36H78Cl2CoN6O14
Triklin
Dexp Dcal d(D) h k l
12.4700 12.4415 .0285 1 0 0
11.7700 11.8092 -.0392 -1 1 0
9.8400 9.8211 .0189 0 -1 1
9.3000 9.2916 .0084 1 0 1
8.7000 8.7455 -.0455 -1 2 0
7.5200 7.5169 .0031 0 -2 1
7.2600 7.2605 -.0005 -1 1 1
6.3600 6.3673 -.0073 -2 1 0
5.9100 5.9046 .0054 -2 2 0
5.8200 5.7951 .0249 2 -2 1
5.7500 5.7523 -.0023 0 -3 1
5.5700 5.5718 -.0018 2 1 0
A= 13.14 DA= .01
B= 20.28 DB= .03
C= 11.3430 DC= .0008
GAMMA=104.30 DGAMMA= .05
BETA = 76.64 DBETA = .02
ALPHA= 95.97 DALPHA= .09
V=2312
14. 37-1609
C24H52Cl2CoN4O12
Triklin
Dexp Dcal d(D) h k l
10.0600 10.0676 -.0076 0 1 1
9.6000 9.6394 -.0394 0 -1 1
7.1200 7.1077 .0123 1 0 1
6.9800 6.9998 -.0198 0 2 0
6.7800 6.7860 -.0060 1 -1 1
5.6400 5.6376 .0024 -1 0 2
5.2200 5.2163 .0037 1 0 2
4.8200 4.8197 .0003 0 -2 2
4.4800 4.4816 -.0016 0 3 1
4.3300 4.3293 .0007 0 -1 3
4.1200 4.1192 .0008 -2 2 0
4.0600 4.0620 -.0020 -2 2 1
A= 8.9408 DA= .0002
B= 14.3815 DB= .0006
C= 13.923 DC= .005
GAMMA=103.01 DGAMMA= .02
BETA = 95.253 DBETA = .009
ALPHA= 86.41 DALPHA= .01
V= 1735.4
15. 37-1630
C14H10CoO6
Triklin
Dexp Dcal d(D) h k l
12.0000 11.9809 .0191 1 0 0
11.7000 11.6677 .0323 0 1 0
10.8500 10.8091 .0409 0 0 1
8.7600 8.7683 -.0083 1 1 0
7.3700 7.3914 -.0214 1 1 1
6.3600 6.3465 .0135 -1 -1 1
5.9900 5.9905 -.0005 2 0 0
5.9000 5.8960 .0040 1 0 2
5.5500 5.5384 .0116 2 1 0
5.4100 5.4046 .0054 0 0 2
5.1800 5.1826 -.0026 2 0 2
4.8800 4.8800 .0000 1 2 1
4.5700 4.5702 -.0002 2 1 2
4.4400 4.4438 -.0038 -2 -1 1
4.3100 4.3127 -.0027 -1 -1 2
A= 13.091 DA= .003
B= 11.8777 DB= .0003
C= 11.971 DC= .001
GAMMA= 88.97 DGAMMA= .03
BETA = 66.793 DBETA = .008
ALPHA= 99.46 DALPHA= .03
V=1681
16. 37-1868
C28H21CoNdO13*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9900 5.9986 -.0086 1 1 0
5.3200 5.3250 -.0050 1 1 1
4.8900 4.8926 -.0026 0 1 2
4.1700 4.1745 -.0045 1 1 2
3.3100 3.3131 -.0031 2 0 2
3.1100 3.1069 .0031 2 1 2
2.8900 2.8900 .0000 0 3 1
2.4000 2.4000 .0000 2 3 0
2.3600 2.3598 .0002 2 0 4
2.0100 2.0100 .0000 -1 2 5
a= 8.085 b=8.948 c= 11.687 beta= 90.41
da=.008 db=.002 dc=.003 dbeta=.02
V= 845.4
17. 37-1869
C28H21CoO13Pr*4H2O
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
4.9300 4.9275 .0025 0 0 2
4.2500 4.2550 -.0050 0 1 0
3.3400 3.3372 .0028 1 1 1
3.0600 3.0522 .0078 2 0 1
2.8700 2.8786 -.0086 1 1 2
2.0200 2.0195 .0005 1 2 0
a= 6.420 b= 4.255 c= 9.855
da= .001 db= .001 dc= .001
V=269.2