1. 33-0411
{Co{NH3}6}}2{Pu{SO4}5}*3H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.1800 6.1905 -.0105 1 1 0
5.0700 5.0613 .0087 1 1 1
4.3800 4.3900 -.0100 2 0 0
4.1500 4.1560 -.0060 2 0 1
3.9100 3.9084 .0016 1 2 0
3.5700 3.5713 -.0013 1 2 1
3.2900 3.2920 -.0020 -1 2 1
3.0700 3.0665 .0035 -1 0 2
2.9100 2.9098 .0002 0 3 0
2.7600 2.7619 -.0019 1 2 2
2.6400 2.6351 .0049 1 3 1
2.5100 2.5091 .0009 -1 2 2
a= 8.99 b= 8.729 c= 7.26 beta= 77.52
da=.01 db=.002 dc=.01 dbeta=.06
V= 557
2. 33-0412
{Co{NH3}6}2{Th{SO4}5}*2H2O
Triklin
Dexp Dcal d(D) h k l
8.8200 8.8409 -.0209 1 0 0
8.3200 8.3116 .0084 0 1 0
6.2400 6.2381 .0019 1 -1 1
5.0800 5.0697 .0103 0 1 1
4.3500 4.3554 -.0054 2 0 1
4.1600 4.1558 .0042 0 2 0
3.9500 3.9511 -.0011 2 -2 1
3.8900 3.8915 -.0015 -1 -1 1
3.5900 3.5959 -.0059 1 -1 2
3.3100 3.3139 -.0039 1 2 0
3.2100 3.2061 .0039 2 0 2
3.0900 3.0898 .0002 1 -2 2
A= 10.214 DA= .001
B= 9.18902 DB= .00007
C= 7.330 DC= .003
GAMMA=114.83 DGAMMA= .03
BETA = 68.959 DBETA = .008
ALPHA=102.76 DALPHA= .03
V= 580.8
3. 33-0426
C6CoLaO12*9H2O
Triklin
Dexp Dcal d(D) h k l
10.3000 10.3288 -.0288 1 0 0
9.9200 9.9034 .0166 0 1 1
8.6800 8.6836 -.0036 -1 0 1
7.8200 7.8079 .0121 0 0 2
7.4900 7.5006 -.0106 1 1 1
7.0100 6.9929 .0171 -1 -1 1
6.9100 6.9091 .0009 0 1 2
5.9000 5.8987 .0013 1 1 2
5.4000 5.4161 -.0161 -1 -1 2
4.6800 4.6807 -.0007 -1 0 3
4.5700 4.5688 .0012 1 1 3
4.0300 4.0289 .0011 -2 1 2
A= 10.40 DA= .01
B= 11.63 DB= .01
C= 15.768 DC= .002
GAMMA= 83.27 DGAMMA= .09
BETA = 90.05 DBETA = .05
ALPHA= 82.111 DALPHA= .007
V= 1875.8
4. 33-0440
Co3TeO6
Triklin
Dexp Dcal d(D) h k l
4.4300 4.4200 .0100 0 2 0
4.3000 4.2986 .0014 2 0 0
4.0700 4.0714 -.0014 0 0 2
3.8600 3.8629 -.0029 2 1 1
3.6000 3.5998 .0002 2 2 0
3.3600 3.3630 -.0030 -1 2 1
3.1300 3.1301 -.0001 0 2 2
2.9950 2.9941 .0009 -2 0 2
2.7830 2.7838 -.0008 -1 -3 1
2.7640 2.7655 -.0015 3 2 0
2.6820 2.6820 .0000 3 0 1
2.5840 2.5837 .0003 -1 3 0
A= 8.9218 DA= .0001
B= 9.204 DB= .001
C= 8.172 DC= .004
GAMMA= 74.57 DGAMMA= .01
BETA = 90.16 DBETA = .04
ALPHA= 85.35 DALPHA= .04
V=645.3
5. 33-0441
CoTeO4*0.5H2O
Triklin
Dexp Dcal d(D) h k l
3.2900 3.2911 -.0011 -1 0 1
2.5800 2.5802 -.0002 0 1 1
2.3200 2.3184 .0016 0 -1 1
1.7300 1.7302 -.0002 -1 2 1
1.6500 1.6500 .0000 -2 2 0
1.5500 1.5500 .0000 2 1 1
1.4800 1.4799 .0001 0 -2 1
1.4000 1.3998 .0002 1 2 1
1.2900 1.2901 -.0001 0 2 2
1.1900 1.1900 .0000 -1 3 0
1.1300 1.1301 -.0001 -1 -2 2
1.1000 1.1000 .0000 -3 3 0
1.0600 1.0599 .0001 2 -2 2
1.0400 1.0401 -.0001 2 -3 1
.9300 .9300 -.0000 2 -1 3
Param.:
A= 5.628 DA= .001
B= 3.63801 DB= .00006
C= 3.6376 DC= .0003
GAMMA=107.71 DGAMMA= .02
BETA =107.37 DBETA = .02
ALPHA= 79.191 DALPHA= .002
V= 67.34
6. 33-0442
beta-Co3Te2MoO10
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
9.0100 9.0479 -.0379 0 0 1
5.1700 5.1794 -.0094 0 1 0
3.3280 3.3281 -.0001 3 1 1
2.9680 2.9708 -.0028 5 0 0
2.7920 2.7944 -.0024 2 0 3
2.5500 2.5512 -.0012 1 2 0
2.5150 2.5106 .0044 4 1 2
2.4590 2.4593 -.0003 2 1 3
2.2400 2.2392 .0008 5 1 2
1.9120 1.9121 -.0001 3 1 4
1.7930 1.7924 .0006 5 2 2
1.7550 1.7555 -.0005 6 2 1
1.5810 1.5811 -.0001 8 0 3
a=14.8539 b= 5.179 c= 9.0479
da= .0008 db= .002 dc= .0002
V= 696.1
7. 33-0443
alfa-Co3Te2MoO10
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.9000 3.9017 -.0017 2 0 0
3.6500 3.6473 .0027 -1 1 1
3.0700 3.0694 .0006 0 0 2
2.9500 2.9537 -.0037 1 1 2
2.6660 2.6653 .0007 2 2 1
2.6020 2.6012 .0008 3 0 0
2.5550 2.5565 -.0015 3 1 1
2.3980 2.4000 -.0020 3 0 2
2.2800 2.2795 .0005 3 1 2
1.9500 1.9509 -.0009 4 0 0
1.9050 1.9048 .0002 0 3 2
1.8740 1.8733 .0007 3 1 3
1.6420 1.6424 -.0004 -1 2 3
1.5690 1.5689 .0001 1 1 4
1.5610 1.5607 .0003 5 0 0
a=8.24 b= 7.288 c= 6.481 beta= 71.29
da=.02 db=.004 dc=.002 dbeta=.06
V= 368.6
8. 33-1073
C6CoO12Pr*8H2O
Triklin
Dexp Dcal d(D) h k l
9.9200 9.9348 -.0148 1 0 1
7.7500 7.7321 .0179 0 1 1
7.4900 7.4941 -.0041 0 -1 1
6.4100 6.4241 -.0141 0 0 2
5.9800 5.9648 .0152 -1 1 0
5.8200 5.8371 -.0171 1 -1 1
5.5000 5.4998 .0002 2 0 1
5.3000 5.2914 .0086 2 1 2
5.2400 5.2329 .0071 0 -1 2
5.1500 5.1496 .0004 2 0 0
4.9700 4.9674 .0026 2 0 2
4.8400 4.8388 .0012 1 -1 2
A= 12.0231 DA= .0003
B= 10.3172 DB= .0005
C= 13.9811 DC= .0005
GAMMA= 66.354 DGAMMA= .006
BETA = 66.853 DBETA = .006
ALPHA= 79.327 DALPHA= .005
V=1459.9
9. 33-1238
beta-NaCoPO4
Triklin
Dexp Dcal d(D) h k l
5.2900 5.2894 .0006 0 -2 1
3.9930 3.9924 .0006 0 -4 1
3.7410 3.7384 .0026 1 0 0
3.5440 3.5431 .0009 1 2 0
3.4900 3.4881 .0019 -1 2 0
3.3060 3.3042 .0018 -1 -3 1
2.7150 2.7148 .0002 -1 1 2
2.6880 2.6883 -.0003 0 -7 1
2.5710 2.5711 -.0001 -1 -6 1
2.4920 2.4907 .0013 1 4 1
2.2520 2.2518 .0002 -1 7 1
2.1490 2.1495 -.0005 1 8 0
A= 3.898 DA= .001
B= 20.686 DB= .001
C= 6.291 DC= .002
GAMMA= 87.96 DGAMMA= .01
BETA =106.42 DBETA = .01
ALPHA= 92.498 DALPHA= .002
V=486.1
10. 33-1587
C15H20Cl3CoN4O4
Triklin
Dexp Dcal d(D) h k l
11.4000 11.3978 .0022 1 0 0
10.7000 10.7039 -.0039 1 1 0
8.6300 8.6226 .0074 0 0 1
7.6400 7.6253 .0147 0 1 1
6.9900 7.0003 -.0103 1 1 1
6.4000 6.3909 .0091 2 1 0
5.3500 5.3520 -.0020 2 2 0
5.2100 5.2088 .0012 -2 -1 1
5.0900 5.0935 -.0035 -2 0 1
4.1900 4.1897 .0003 -2 1 1
3.3100 3.3100 -.0000 3 0 1
2.8700 2.8700 .0000 4 3 1
A= 12.829 DA= .005
B= 12.483 DB= .002
C= 8.844 DC= .007
GAMMA= 63.81 DGAMMA= .05
BETA = 92.68 DBETA = .06
ALPHA= 79.95 DALPHA= .05
V= 1239
11. 33-1588
C15H20ClCoN6O8
Triklin
Dexp Dcal d(D) h k l
11.8000 11.8453 -.0453 1 0 0
10.5000 10.5078 -.0078 1 1 0
7.9600 7.9739 -.0139 0 0 1
7.7500 7.7527 -.0027 0 -1 1
7.1700 7.1635 .0065 1 0 1
6.6700 6.6692 .0008 1 -1 1
6.3200 6.3187 .0013 -1 -1 1
5.2600 5.2603 -.0003 0 3 0
5.1300 5.1299 .0001 0 2 1
4.4300 4.4293 .0007 -2 0 1
4.3800 4.3797 .0003 2 3 0
A= 12.174 DA= .005
B= 16.33 DB= .01
C= 8.196 DC= .005
GAMMA= 80.26 DGAMMA= .05
BETA = 82.783 DBETA = .002
ALPHA= 99.78 DALPHA= .01
V= 1562
12. 33-1589
C15H20ClCoN6O8
Triklin
Dexp Dcal d(D) h k l
11.8000 11.8161 -.0161 1 0 0
10.5000 10.4837 .0163 1 1 0
7.8500 7.8429 .0071 1 1 1
7.1700 7.1642 .0058 -1 0 1
6.3300 6.3289 .0011 2 1 0
6.1300 6.1282 .0018 0 -1 1
5.2400 5.2419 -.0019 2 2 0
5.1400 5.1393 .0007 2 2 1
4.4100 4.4107 -.0007 0 0 2
3.6900 3.6901 -.0001 1 3 2
3.5600 3.5601 -.0001 3 0 1
3.1700 3.1700 .0000 0 -3 1
A= 12.8579 DA= .0004
B= 13.1883 DB= .0004
C= 9.3495 DC= .0002
GAMMA= 66.833 DGAMMA= .005
BETA = 83.92 DBETA = .01
ALPHA= 70.718 DALPHA= .006
V=1374.6
13. 33-1590
C6H4CoN6O4*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.9300 4.9298 .0002 0 0 2
3.5700 3.5685 .0015 -2 0 1
3.4500 3.4561 -.0061 2 0 1
3.2800 3.2823 -.0023 0 2 0
3.1400 3.1352 .0048 -2 1 1
2.9600 2.9594 .0006 1 0 3
2.7000 2.6979 .0021 1 1 3
2.5900 2.5899 .0001 -1 2 2
2.3800 2.3800 .0000 2 2 1
2.3400 2.3402 -.0002 3 1 0
2.3100 2.3095 .0005 1 0 4
2.2400 2.2404 -.0004 -1 2 3
a= 7.523 b= 6.56 c= 9.871 beta= 92.75
da=.003 db=.01 dc=.008 dbeta=.07
V= 486.9
Triklin
Dexp Dcal d(D) h k l
4.9300 4.9387 -.0087 0 1 0
3.5700 3.5708 -.0008 -1 0 1
3.4500 3.4538 -.0038 0 -1 2
3.2800 3.2851 -.0051 1 0 1
3.1400 3.1387 .0013 -1 0 2
2.9600 2.9625 -.0025 -1 -1 2
2.7000 2.6989 .0011 1 1 2
2.5900 2.5883 .0017 -1 1 1
2.3800 2.3794 .0006 0 -2 1
2.3400 2.3393 .0007 -1 -2 1
2.3100 2.3098 .0002 1 0 3
2.2400 2.2409 -.0009 0 2 2
A= 3.821 DA= .002
B= 5.144 DB= .002
C= 10.051 DC= .001
GAMMA= 73.855 DGAMMA= .003
BETA = 97.21 DBETA = .01
ALPHA= 90.282 DALPHA= .004
V= 188.2
14. 33-1591
C6H4CoN6O4
Triklin
Dexp Dcal d(D) h k l
11.0000 11.0000 -.0000 1 0 0
8.6900 8.6959 -.0059 1 1 0
7.5200 7.4856 .0344 0 1 1
6.1900 6.1889 .0011 0 -1 1
5.8700 5.8734 -.0034 1 0 1
4.8800 4.8850 -.0050 1 2 1
4.5200 4.5143 .0057 -2 -1 1
3.6700 3.6667 .0033 3 0 0
3.5100 3.5113 -.0013 -3 1 1
3.3400 3.3405 -.0005 -2 2 2
3.3100 3.3100 .0000 0 3 2
3.2800 3.2813 -.0013 3 2 0
3.2700 3.2705 -.0005 -2 -1 2
3.2600 3.2605 -.0005 1 -3 1
2.9400 2.9408 -.0008 3 -1 1
2.7900 2.7896 .0004 -2 4 0
2.4400 2.4397 .0003 3 2 2
A= 11.201 DA= .001
B= 13.648 DB= .001
C= 8.146 DC= .003
GAMMA= 89.49 DGAMMA= .01
BETA =100.51 DBETA = .02
ALPHA= 77.88 DALPHA= .02
V= 1196
15. 33-1593
C46H36Cl2CoN4O4S2
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
11.2000 11.2200 -.0200 0 1 0
9.3000 9.2800 .0200 1 0 0
8.3100 8.3354 -.0254 1 0 1
7.1500 7.1510 -.0010 1 1 0
6.3200 6.3210 -.0010 0 0 3
5.7100 5.7092 .0008 1 1 2
a= 9.280 b=11.220 c=18.963
da= .001 db= .001 dc= .001
V=1974.5
16. 33-1594
C24H17CoN8O10*2H2O
Triklin
Dexp Dcal d(D) h k l
10.5000 10.4992 .0008 1 0 0
8.4900 8.5043 -.0143 0 1 0
7.6700 7.6804 -.0104 0 0 1
7.3400 7.3418 -.0018 0 -1 1
7.0900 7.0906 -.0006 -1 1 0
6.2000 6.2129 -.0129 1 1 0
4.7800 4.7817 -.0017 2 -1 1
4.5500 4.5494 .0006 1 -2 1
3.9100 3.9092 .0008 -1 -2 1
3.4600 3.4598 .0002 3 -1 1
2.6900 2.6897 .0003 2 1 2
2.4000 2.4001 -.0001 2 0 3
A= 10.7553 DA= .0006
B= 9.452 DB= .004
C= 8.5038 DC= .0003
GAMMA=101.09 DGAMMA= .01
BETA = 80.108 DBETA = .007
ALPHA=114.78 DALPHA= .01
V= 766.2
17. 33-1595
C24H16ClCoN6O4*3H2O
Triklin
Dexp Dcal d(D) h k l
11.2000 11.2043 -.0043 1 0 0
10.4000 10.3801 .0199 0 1 0
8.2200 8.2179 .0021 -1 0 1
7.9700 7.9753 -.0053 1 1 0
7.0900 7.1017 -.0117 -1 -1 1
6.3100 6.3125 -.0025 1 -1 1
4.8000 4.7996 .0004 -1 -2 1
4.3100 4.3103 -.0003 -1 1 2
4.0600 4.0595 .0005 -1 -2 2
3.6200 3.6199 .0001 -3 0 1
3.5400 3.5399 .0001 2 1 2
3.4600 3.4600 -.0000 0 3 0
A= 11.290 DA= .002
B= 10.569 DB= .001
C= 11.402 DC= .003
GAMMA= 84.19 DGAMMA= .03
BETA = 94.90 DBETA = .01
ALPHA= 99.59 DALPHA= .01
V= 1331.3
18. 33-1596
C40H32Co2N14O12*8H2O
Triklin
Dexp Dcal d(D) h k l
14.7000 14.7036 -.0036 1 0 0
7.9100 7.9078 .0022 1 1 0
6.8600 6.8595 .0005 1 1 1
6.6000 6.6004 -.0004 -1 1 1
6.1300 6.1298 .0002 -2 0 1
5.5100 5.5096 .0004 -1 -1 1
4.9600 4.9609 -.0009 1 -1 1
4.5500 4.5502 -.0002 3 1 0
4.1400 4.1397 .0003 2 -1 1
A= 14.8967 DA= .0004
B= 9.0121 DB= .0001
C= 9.959 DC= .001
GAMMA= 82.969 DGAMMA= .001
BETA = 93.686 DBETA = .007
ALPHA= 73.34 DALPHA= .01
V= 1264.3
19. 33-1597
c20H16ClCoN6O8
Triklin
Dexp Dcal d(D) h k l
9.8800 9.8535 .0265 1 0 0
8.4900 8.5002 -.0102 0 1 0
8.2100 8.2036 .0064 0 -1 1
7.3400 7.3419 -.0019 1 0 1
6.6800 6.6794 .0006 -1 -1 1
6.0900 6.0913 -.0013 -1 1 0
5.8300 5.8261 .0039 0 1 1
5.4800 5.4817 -.0017 0 0 2
4.3100 4.3104 -.0004 -1 -2 1
4.2500 4.2501 -.0001 0 2 0
4.0600 4.0601 -.0001 -2 1 0
A= 9.930 DA= .002
B= 9.109 DB= .003
C= 11.67 DC= .01
GAMMA= 82.8885 DGAMMA= .0004
BETA = 92.24 DBETA = .07
ALPHA=110.02 DALPHA= .09
V= 984.1
20. 33-1598
C20H16ClCoN6O8
Triklin
Dexp Dcal d(D) h k l
13.5000 13.4987 .0013 1 0 0
9.3400 9.3548 -.0148 1 1 0
8.0600 8.0778 -.0178 -1 0 1
7.3700 7.3722 -.0022 -1 -1 1
6.8100 6.8113 -.0013 0 1 1
6.4300 6.4247 .0053 1 -1 1
6.1600 6.1589 .0011 -1 1 1
5.6400 5.6364 .0036 1 2 0
5.4100 5.4131 -.0031 0 -2 1
4.2400 4.2402 -.0002 1 0 2
4.0700 4.0691 .0009 -2 -1 2
A= 13.667 DA= .009
B= 12.13 DB= .01
C= 9.4680 DC= .0009
GAMMA= 83.72 DGAMMA= .05
BETA = 97.40 DBETA = .05
ALPHA= 99.79 DALPHA= .06
V= 1527.7
21. 33-1599
C46H36CoI4N4O2S2
Triklin
Dexp Dcal d(D) h k l
12.6000 12.5884 .0116 1 0 0
11.0000 10.9838 .0162 0 1 0
9.0600 9.0444 .0156 1 0 1
8.4100 8.4031 .0069 1 -1 1
6.1000 6.1010 -.0010 1 1 1
5.5300 5.5320 -.0020 1 -2 1
4.9600 4.9527 .0073 -2 2 0
4.1100 4.1097 .0003 -1 -2 1
3.6900 3.6911 -.0011 -2 3 0
3.4400 3.4400 .0000 -2 0 2
3.3000 3.3001 -.0001 2 0 3
3.1800 3.1795 .0005 1 -2 3
A= 13.972 DA= .001
B= 11.78517 DB= .00005
C= 10.4409 DC= .0006
GAMMA=110.43 DGAMMA= .01
BETA = 71.0854 DBETA = .0007
ALPHA=101.902 DALPHA= .006
V=1515
22. 33-1601
C12H36CoN6O2P2*2SeCN
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.8000 10.8239 -.0239 1 0 0
7.6300 7.6132 .0168 1 1 1
5.9000 5.9050 -.0050 -1 0 1
5.5300 5.5493 -.0193 1 2 1
5.4000 5.4119 -.0119 2 0 0
4.4800 4.4797 .0003 2 2 1
3.8000 3.8059 -.0059 3 1 1
3.5900 3.5879 .0021 -1 1 2
3.4500 3.4450 .0050 3 2 1
3.2800 3.2808 -.0008 -1 2 2
3.2100 3.2089 .0011 3 2 0
3.0400 3.0402 -.0002 -2 3 1
3.0000 2.9998 .0002 1 2 3
2.5500 2.5500 -.0000 -1 4 2
2.2900 2.2900 -.0000 -2 0 3
a=11.86 b= 14.04 c=10.05 beta= 65.83
da=.01 db=.01 dc= .01 dbeta=.09
V= 1527
Triklin
Dexp Dcal d(D) h k l
10.8000 10.8145 -.0145 1 0 0
7.6300 7.6351 -.0051 1 1 0
5.9000 5.8996 .0004 0 1 1
5.5300 5.5397 -.0097 1 0 1
5.4000 5.3976 .0024 2 1 0
4.4800 4.4817 -.0017 -1 -1 1
3.8000 3.7992 .0008 1 -1 1
3.5900 3.5951 -.0051 -2 1 1
3.4500 3.4497 .0003 3 1 1
3.2800 3.2771 .0029 -1 2 1
3.2100 3.2090 .0010 -1 0 2
3.0400 3.0399 .0001 2 1 2
3.0000 3.0000 .0000 -2 -2 1
2.5500 2.5501 -.0001 0 -3 0
2.2900 2.2899 .0001 -2 -3 1
A= 11.569 DA= .009
B= 8.52 DB= .01
C= 6.92 DC= .01
GAMMA= 69.35 DGAMMA= .07
BETA = 86.58 DBETA = .09
ALPHA= 73.49 DALPHA= .09
V= 611.4
23. 33-1812
C33H38Co3O8P
Triklin
Dexp Dcal d(D) h k l
10.0000 9.9820 .0180 1 0 0
8.5000 8.5129 -.0129 0 1 0
8.0000 7.9976 .0024 0 0 1
7.7000 7.6998 .0002 -1 1 0
6.2000 6.1889 .0111 -1 0 1
5.9000 5.8940 .0060 0 -1 1
5.7000 5.6978 .0022 1 1 0
4.6500 4.6510 -.0010 -1 -1 1
4.2000 4.2013 -.0013 -2 0 1
3.6500 3.6505 -.0005 0 -1 2
A= 10.4538 DA= .0002
B= 8.916 DB= .006
C= 8.0021 DC= .0005
GAMMA=107.26 DGAMMA= .01
BETA = 88.57 DBETA = .05
ALPHA= 91.639 DALPHA= .009
V= 711.9