1. 31-0044
NH4Co{ClO4}3
Triklin
Dexp Dcal d(D) h k l
6.9900 6.9882 .0018 1 0 0
6.2100 6.2065 .0035 1 1 0
4.2400 4.2423 -.0023 -1 0 1
3.9500 3.9448 .0052 -1 1 0
3.8000 3.8010 -.0010 -1 -1 1
3.4200 3.4210 -.0010 2 1 2
3.3100 3.3117 -.0017 -1 1 1
3.1900 3.1857 .0043 0 2 0
3.1000 3.1018 -.0018 0 2 1
2.8300 2.8302 -.0002 -2 -1 1
2.7400 2.7393 .0007 3 2 1
2.6000 2.5989 .0011 2 -1 1
A= 8.602 DA= .005
B= 7.559 DB= .001
C= 7.673 DC= .009
GAMMA= 58.91 DGAMMA= .02
BETA = 63.91 DBETA = .03
ALPHA= 68.73 DALPHA= .02
V= 377.7
2. 31-0046
{NH4}2{TeMo6O24}*13H2O
Triklin
Dexp Dcal d(D) h k l
8.1900 8.1843 .0057 1 0 0
6.3600 6.3494 .0106 0 1 1
5.7800 5.7737 .0063 0 -1 1
5.0000 5.0105 -.0105 -1 1 0
4.7100 4.7012 .0088 0 0 2
3.7700 3.7668 .0032 0 2 1
3.4100 3.4140 -.0040 2 1 2
3.2100 3.2122 -.0022 -1 2 0
3.1500 3.1447 .0053 2 -1 1
3.0700 3.0694 .0006 -1 2 1
2.8760 2.8741 .0019 -2 -1 2
2.8140 2.8165 -.0025 -1 0 3
A= 8.640 DA= .004
B= 8.301 DB= .003
C= 9.56 DC= .01
GAMMA= 72.58 DGAMMA= .04
BETA = 81.15 DBETA = .02
ALPHA= 82.14 DALPHA= .01
V= 643.4
3. 31-0427
C2H8N4O2*Co{NO3}2*4H2O
Triklin
Dexp Dcal d(D) h k l
11.1000 11.0840 .0161 1 0 0
9.3900 9.3861 .0039 0 1 0
8.8700 8.8419 .0281 -1 0 1
8.3000 8.3153 -.0153 1 0 1
7.8000 7.7904 .0096 0 -1 1
7.1200 7.1194 .0006 1 1 0
6.4600 6.4523 .0077 -1 -1 1
6.1400 6.1531 -.0131 1 1 1
5.9200 5.9322 -.0122 -1 0 2
5.4300 5.4216 .0084 0 1 2
5.0200 5.0178 .0022 2 0 1
4.3400 4.3411 -.0011 -1 2 0
A= 11.106 DA= .001
B= 9.38917 DB= .00009
C= 13.530 DC= .002
GAMMA= 90.6382 DGAMMA= .0006
BETA = 93.57621 DBETA = .00960
ALPHA= 91.275 DALPHA= .008
V=1408.6
4. 31-0428
C6H24N12O6*Co{NO3}2*2H2O
Triklin
Dexp Dcal d(D) h k l
11.1000 11.0712 .0288 1 0 0
9.4200 9.4373 -.0173 0 1 0
8.9300 8.9254 .0046 1 0 1
7.6500 7.6452 .0048 1 -1 1
6.9400 6.9331 .0069 0 1 1
6.3000 6.2872 .0128 -1 -1 1
5.7500 5.7304 .0196 1 1 1
5.4600 5.4597 .0003 -1 0 2
5.1700 5.1647 .0053 2 -1 1
5.0200 5.0120 .0080 -1 -1 2
4.7600 4.7608 -.0008 1 -2 1
4.5900 4.5890 .0010 -1 2 0
A= 11.2964 DA= .0001
B= 9.88 DB= .01
C= 13.786 DC= .009
GAMMA=100.09 DGAMMA= .07
BETA = 82.17 DBETA = .01
ALPHA=105.10 DALPHA= .09
V= 1456.0
5. 31-0429
C10H40N20O10*Co{NO3}2*2H2O
Triklin
Dexp Dcal d(D) h k l
11.7000 11.7092 -.0092 -1 0 1
9.6700 9.6687 .0013 0 1 1
8.9700 8.9780 -.0080 0 -1 1
8.6700 8.6733 -.0033 -1 1 0
8.1000 8.0985 .0015 1 0 1
7.3900 7.3905 -.0005 -1 0 2
7.1200 7.0731 .0469 0 0 2
6.5200 6.5068 .0132 -1 1 2
6.3300 6.3456 -.0156 0 1 2
5.9400 5.9494 -.0094 0 -1 2
4.6400 4.6432 -.0032 2 -1 1
5.3900 5.4003 -.0103 -1 -2 1
A= 13.507 DA= .002
B= 12.39 DB= .01
C= 15.1657 DC= .0009
GAMMA= 89.41 DGAMMA= .02
BETA =110.72 DBETA = .09
ALPHA= 86.22 DALPHA= .01
V= 2366.6
6. 31-0433
CoTeMoO6
Triklin
Dexp Dcal d(D) h k l
8.8400 8.8449 -.0049 0 1 0
4.4300 4.4310 -.0010 0 -1 2
3.6500 3.6509 -.0009 -1 0 2
3.3800 3.3798 .0002 0 -2 2
3.3300 3.3305 -.0005 -1 2 0
3.1200 3.1135 .0065 -1 2 1
2.9120 2.9113 .0007 1 2 2
2.8140 2.8152 -.0012 -1 0 3
2.6280 2.6279 .0001 -1 1 3
2.5310 2.5320 -.0010 2 -1 1
2.3000 2.3003 -.0003 -1 2 3
2.2570 2.2573 -.0003 -2 1 2
A= 5.563 DA= .002
B= 8.879 DB= .002
C= 10.027 DC= .001
GAMMA= 85.529 DGAMMA= .008
BETA = 88.12 DBETA = .02
ALPHA= 92.06 DALPHA= .01
V= 493.1
7. 31-0435
Co3{TeMo6O24}*9H2O
Triklin
Dexp Dcal d(D) h k l
8.4200 8.4249 -.0049 1 0 0
7.2500 7.2509 -.0009 1 1 0
6.5600 6.5603 -.0003 0 0 1
5.1700 5.1570 .0130 -1 -2 1
4.8700 4.8739 -.0039 -2 -1 1
4.4100 4.4192 -.0092 1 0 1
3.9300 3.9265 .0035 1 1 1
3.5500 3.5518 -.0018 -1 0 2
3.2600 3.2597 .0003 1 3 0
3.1800 3.1816 -.0016 -3 -2 1
3.0500 3.0521 -.0021 2 0 1
2.7060 2.7064 -.0004 -2 2 1
A= 9.902 DA= .007
B= 10.825 DB= .009
C= 7.7839 DC= .0008
GAMMA= 67.13 DGAMMA= .07
BETA =118.790 DBETA = .003
ALPHA=114.14 DALPHA= .01
V= 647.9
8. 31-0436
Co3{TeMo6O24}*24H2O
Triklin
Dexp Dcal d(D) h k l
8.9900 9.0002 -.0102 -1 0 1
8.3500 8.3771 -.0271 -1 1 0
5.6300 5.6284 .0016 1 -1 2
5.3200 5.3330 -.0130 -2 1 0
3.5000 3.5004 -.0004 1 2 1
5.2300 5.2317 -.0017 -1 -1 2
5.1700 5.1700 .0000 1 1 1
4.7100 4.7048 .0052 2 0 1
4.4700 4.4731 -.0031 -1 0 3
4.1900 4.1905 -.0005 -1 -1 3
3.7800 3.7799 .0001 -1 -2 2
3.7400 3.7402 -.0002 -2 0 3
A= 11.07079 DA= .00001
B= 10.02558 DB= .00002
C= 14.3284 DC= .0001
GAMMA=106.61060 DGAMMA= .00001
BETA = 94.1189 DBETA = .0003
ALPHA=101.6492 DALPHA= .0001
V=1478.4
9. 31-0438
C4H16Br2CoN8S4
Triklin
Dexp Dcal d(D) h k l
6.7300 6.7232 .0068 0 1 0
5.5300 5.5554 -.0254 2 1 0
5.1700 5.1455 .0245 1 1 1
4.9300 4.9347 -.0047 1 0 2
4.6100 4.6272 -.0172 -3 0 1
4.4700 4.4779 -.0079 -1 0 2
4.3300 4.3143 .0157 1 -1 2
4.1300 4.1334 -.0034 3 0 2
3.9500 3.9490 .0010 -2 0 2
3.6700 3.6749 -.0049 3 -1 2
3.6300 3.6241 .0059 4 1 1
3.5300 3.5272 .0028 -4 1 0
A= 17.79 DA= .02
B= 6.842 DB= .005
C= 10.052 DC= .002
GAMMA= 87.0 DGAMMA= .1
BETA = 79.90 DBETA = .01
ALPHA= 99.57 DALPHA= .05
V=1183
10. 31-0439
C4H16Cl2CoN8S4
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
6.7100 6.7541 -.0441 0 2 0
6.1100 6.1622 -.0522 1 2 0
4.5100 4.5027 .0073 0 3 0
3.8500 3.8640 -.0140 2 3 0
3.6200 3.6249 -.0049 4 1 0
3.0100 3.0088 .0012 0 1 2
2.8850 2.8874 -.0024 4 3 0
2.7060 2.7016 .0044 0 5 0
2.3800 2.3787 .0013 3 5 0
2.1910 2.1915 -.0005 6 3 0
2.1510 2.1503 .0007 7 0 0
2.0480 2.0489 -.0009 7 2 0
a=15.052 b=13.508 c= 6.173
da= .004 db= .004 dc= .002
V=1255
Triklin
Dexp Dcal d(D) h k l
6.7100 6.7128 -.0028 0 -1 1
6.1100 6.1068 .0032 1 0 0
4.5100 4.5094 .0006 0 -1 3
3.8500 3.8484 .0016 -1 1 0
3.6200 3.6187 .0013 -1 1 1
3.0100 3.0094 .0006 2 0 1
2.8850 2.8849 .0001 -1 1 3
2.7060 2.7053 .0007 1 2 3
2.3800 2.3812 -.0012 -2 1 1
2.1910 2.1904 .0006 -3 -1 1
2.1510 2.1510 .0000 2 -1 4
2.0480 2.0477 .0003 -1 -2 7
A= 6.651 DA= .001
B= 7.5358 DB= .0003
C= 15.504 DC= .002
GAMMA= 66.7213 DGAMMA= .0008
BETA = 93.27 DBETA = .01
ALPHA=101.923 DALPHA= .007
V= 698.1
11. 31-0440
C2H8Cl2CoN4S2
Triklin
Dexp Dcal d(D) h k l
6.5100 6.5267 -.0167 0 1 1
6.1100 6.1182 -.0082 -1 1 0
5.8700 5.8609 .0091 0 -1 1
5.2100 5.2150 -.0050 1 -1 1
5.1000 5.1063 -.0063 1 1 0
4.5500 4.5597 -.0097 1 0 2
3.9200 3.9199 .0001 1 -1 2
3.7300 3.7228 .0072 0 2 1
3.5900 3.5858 .0042 -1 2 1
3.4900 3.4890 .0010 0 0 3
3.4400 3.4446 -.0046 -1 -1 2
3.3300 3.3283 .0017 2 1 0
A= 8.2147 DA= .0007
B= 7.797 DB= .005
C= 10.554 DC= .008
GAMMA= 99.90 DGAMMA= .08
BETA = 86.51 DBETA = .02
ALPHA= 84.25 DALPHA= .02
V= 660.5
12. 31-0999
K2Co{IO3}4*2H2O
Triklin
Dexp Dcal d(D) h k l
6.2300 6.2645 -.0345 1 1 1
6.1500 6.1475 .0025 0 -1 1
4.1000 4.1014 -.0014 -1 1 1
3.8300 3.8277 .0023 0 1 2
3.4300 3.4312 -.0012 -1 0 2
3.3000 3.2939 .0061 -2 0 1
3.1400 3.1411 -.0011 2 0 2
2.8000 2.7980 .0020 1 1 3
2.7400 2.7408 -.0008 1 3 2
2.5700 2.5706 -.0006 3 2 2
2.5600 2.5607 -.0007 1 -1 3
2.5200 2.5193 .0007 -1 3 0
A= 8.651 DA= .005
B= 10.0879 DB= .0003
C= 8.5536 DC= .0004
GAMMA= 65.55 DGAMMA= .03
BETA = 78.22 DBETA = .01
ALPHA= 84.49 DALPHA= .01
V= 665.1
13. 31-1000
K2CoFe{CN}6
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
5.0400 5.0396 .0004 1 0 0
3.5700 3.5783 -.0083 0 1 0
2.8900 2.8916 -.0016 1 0 1
2.5200 2.5198 .0002 2 0 0
2.2500 2.2491 .0009 1 1 1
2.0500 2.0510 -.0010 2 0 1
1.7800 1.7794 .0006 2 1 1
a= 5.0396 b= 3.578 c= 3.53
da= .0004 db= .008 dc= .01
V=63.7
14. 31-1176
RbCo{ClO4}3
Triklin
Dexp Dcal d(D) h k l
6.1000 6.1008 -.0008 -1 1 0
4.4500 4.4466 .0034 1 3 0
4.2200 4.2157 .0043 1 3 1
3.9500 3.9571 -.0071 -1 1 1
3.8500 3.8460 .0040 -1 3 0
3.7800 3.7764 .0036 0 4 0
3.5500 3.5543 -.0043 1 -1 2
3.3000 3.3012 -.0012 0 4 1
3.1700 3.1690 .0010 2 0 2
3.0900 3.0876 .0024 -1 3 1
2.8200 2.8171 .0029 2 4 0
2.6000 2.6002 -.0002 1 -5 1
A= 7.8471 DA= .0003
B= 15.310 DB= .001
C= 7.493 DC= .002
GAMMA= 80.64 DGAMMA= .02
BETA = 66.93 DBETA = .01
ALPHA= 86.75 DALPHA= .03
V=817.3
15. 32-0225
CsCo{ClO4}3
Triklin
Dexp Dcal d(D) h k l
4.4700 4.4728 -.0028 1 0 1
3.6700 3.6687 .0013 -1 2 0
3.3800 3.3808 -.0008 1 -2 1
3.1800 3.1812 -.0012 2 -1 1
2.6000 2.6002 -.0002 1 0 2
2.4200 2.4215 -.0015 -2 0 2
2.3300 2.3294 .0006 -3 2 0
2.2600 2.2604 -.0004 2 -3 1
2.1900 2.1898 .0002 -2 -3 1
2.1400 2.1400 .0000 -1 -3 2
2.0700 2.0697 .0003 0 2 2
2.0200 2.0196 .0004 -4 1 0
A= 8.236 DA= .007
B= 8.166 DB= .002
C= 5.832 DC= .001
GAMMA= 93.18 DGAMMA= .02
BETA = 93.97 DBETA = .05
ALPHA=103.86 DALPHA= .02
V= 378.8
16. 32-0290
{Co{NH3}6{TiOF4}3
Triklin
Dexp Dcal d(D) h k l
6.6600 6.6570 .0030 -1 1 0
4.9200 4.9192 .0008 0 0 1
4.0800 4.0791 .0009 0 -2 1
3.8320 3.8332 -.0012 1 1 1
3.4340 3.4350 -.0010 -1 -2 1
3.3060 3.3057 .0003 1 4 0
3.2250 3.2251 -.0001 1 -3 1
2.8780 2.8782 -.0002 -2 1 1
2.5680 2.5678 .0002 -2 -2 1
2.3100 2.3099 .0001 -1 2 2
2.2010 2.2010 .0000 1 -2 2
1.8180 1.8180 -.0000 1 -8 1
1.6090 1.6090 .0000 3 -3 2
A= 6.9439 DA= .0007
B= 16.3952 DB= .0002
C= 4.9338 DC= .0006
GAMMA= 97.70 DGAMMA= .01
BETA = 91.731 DBETA = .003
ALPHA= 85.760 DALPHA= .005
V= 555.0
17. 32-0292
CoF3*3.5H2O
Tetragon
Groupa 105,112,131
Dexp. Dcal. d(D) h k l
4.5800 4.5703 .0097 0 0 1
4.0000 3.9941 .0059 2 0 0
3.0100 3.0075 .0025 2 0 1
2.5240 2.5261 -.0021 3 1 0
1.8310 1.8300 .0010 4 0 1
1.7310 1.7341 -.0031 3 0 2
1.6930 1.6946 -.0016 3 1 2
1.5990 1.5976 .0014 5 0 0
1.5280 1.5234 .0046 0 0 3
1.4680 1.4709 -.0029 1 1 3
a= 7.988 c= 4.570
da= .005 dc= .002
V=291.6
Triklin
Dexp Dcal d(D) h k l
4.5800 4.5801 -.0001 1 0 0
4.0000 3.9993 .0007 -1 0 1
3.0100 3.0099 .0001 -1 -2 1
2.5240 2.5239 .0001 1 -1 1
1.8310 1.8310 -.0000 -1 3 0
1.7310 1.7310 -.0000 1 -1 2
1.6930 1.6930 .0000 -3 -1 1
1.5990 1.5990 .0000 1 4 0
1.5280 1.5280 .0000 2 -2 1
1.4680 1.4680 .0000 -2 -3 3
A= 5.09368 DA= .00004
B= 6.77240 DB= .00002
C= 4.9389 DC= .0001
GAMMA= 75.2903 DGAMMA= .0003
BETA =114.357 DBETA = .001
ALPHA=105.908 DALPHA= .003
V= 147.3
18. 32-0308
Co{ReO4}2
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.8600 3.8511 .0089 2 1 0
2.8600 2.8610 -.0010 0 2 0
2.6100 2.6035 .0065 4 0 0
2.3000 2.2990 .0010 3 0 1
2.0900 2.0828 .0072 5 0 0
1.9900 1.9852 .0048 4 0 1
1.9300 1.9256 .0044 4 2 0
1.8800 1.8761 .0039 1 3 0
1.7900 1.7910 -.0010 2 3 0
1.6500 1.6501 -.0001 5 1 1
1.6000 1.6006 -.0006 1 3 1
1.4600 1.4607 -.0007 6 1 1
a=10.41 b= 5.722 c= 3.068
da= .02 db= .001 dc= .001
V= 182.8
Triklin
Dexp Dcal d(D) h k l
3.8600 3.8604 -.0004 1 0 0
2.8600 2.8619 -.0019 1 1 1
2.6100 2.6100 -.0000 -1 -1 1
2.3000 2.2996 .0004 -1 1 1
2.0900 2.0912 -.0012 0 0 2
1.9900 1.9884 .0016 1 0 2
1.9300 1.9302 -.0002 2 0 0
1.8800 1.8807 -.0007 2 0 1
1.7900 1.7899 .0001 1 -3 1
1.6500 1.6503 -.0003 -1 -2 2
1.6000 1.5993 .0007 -2 -2 1
1.4600 1.4602 -.0002 -2 -3 1
A= 3.9571 DA= .0001
B= 6.82311 DB= .00008
C= 4.26909 DC= .00001
GAMMA= 82.104 DGAMMA= .002
BETA = 81.0154 DBETA = .0004
ALPHA= 95.9189 DALPHA= .0007
V=111.65
19. 32-0309
Co{ReO4}2*4H2O
Triklin
Dexp Dcal d(D) h k l
3.8100 3.8100 .0000 1 0 0
3.5900 3.5910 -.0010 1 1 0
3.4700 3.4700 -.0000 1 0 1
3.1900 3.1896 .0004 1 1 1
3.0700 3.0718 -.0018 -1 -1 1
2.8600 2.8625 -.0025 -1 -2 1
2.5200 2.5187 .0013 0 -4 2
2.3900 2.3907 -.0007 0 5 0
2.2600 2.2578 .0022 -1 -4 1
2.2000 2.2000 -.0000 -1 1 2
2.0600 2.0602 -.0002 -1 4 1
2.0100 2.0114 -.0014 1 -5 2
A= 3.8511 DA= .0006
B= 12.381 DB= .006
C= 6.6548 DC= .0002
GAMMA= 94.16 DGAMMA= .02
BETA = 81.913 DBETA = .007
ALPHA=104.97 DALPHA= .02
V= 303.3
20. 32-0315
Co{TcO4}2*3H2O
Triklin
Dexp Dcal d(D) h k l
4.2200 4.2199 .0001 -1 1 0
3.7700 3.7691 .0009 -1 -1 2
3.1400 3.1403 -.0003 -1 -2 2
3.0300 3.0304 -.0004 -2 0 1
2.8500 2.8497 .0003 -1 2 0
2.5900 2.5934 -.0034 -2 -2 2
2.4400 2.4395 .0005 0 -3 1
2.2700 2.2680 .0020 0 -2 3
2.1100 2.1100 .0000 -2 2 0
2.0700 2.0700 .0000 -1 1 3
1.9700 1.9697 .0003 1 -1 3
1.8700 1.8701 -.0001 1 -2 3
A= 6.248 DA= .005
B= 7.521 DB= .005
C= 7.866 DC= .001
GAMMA= 76.78 DGAMMA= .07
BETA =112.82 DBETA = .01
ALPHA=111.54 DALPHA= .01
V= 315.3
21. 32-0316
Co{TcO4}*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8000 3.7984 .0016 -1 1 1
3.5700 3.5674 .0026 0 2 0
3.1600 3.1576 .0024 0 1 2
3.0400 3.0386 .0014 -1 0 2
2.8200 2.8239 -.0039 2 0 0
2.4900 2.4883 .0017 -2 1 1
2.0700 2.0713 -.0013 2 1 2
1.9000 1.8992 .0008 -2 2 2
1.8500 1.8505 -.0005 2 2 2
1.7800 1.7805 -.0005 -2 1 3
1.7100 1.7093 .0007 0 1 4
1.6500 1.6492 .0008 1 4 1
a= 5.652 b= 7.135 c= 7.047 beta= 92.10
da=.001 db= .007 dc=.009 dbeta=.04
V= 284.0
Triklin
Dexp Dcal d(D) h k l
3.8000 3.8008 -.0008 1 1 0
3.5700 3.5718 -.0018 -1 1 1
3.1600 3.1600 -.0000 -1 -1 1
3.0400 3.0391 .0009 -1 0 2
2.8200 2.8220 -.0020 1 -1 1
2.4900 2.4909 -.0009 0 2 1
2.0700 2.0703 -.0003 2 -1 1
1.9000 1.9004 -.0004 2 2 0
1.8500 1.8502 -.0002 -2 1 3
1.7800 1.7799 .0001 -2 -2 1
1.7100 1.7100 .0000 -3 1 0
1.6500 1.6499 .0001 2 1 3
A= 5.682 DA= .001
B= 5.021 DB= .001
C= 6.861 DC= .002
GAMMA= 88.25 DGAMMA= .03
BETA = 97.69 DBETA = .01
ALPHA= 75.84 DALPHA= .01
V= 187.7
22. 32-0317
Co3TeO6
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
4.2900 4.3047 -.0147 2 1 0
4.0900 4.1639 -.0739 3 0 0
3.1100 3.1230 -.0130 4 0 0
2.9700 2.9705 -.0005 0 2 0
2.7600 2.7643 -.0043 4 1 0
2.6700 2.6683 .0017 4 0 1
2.5200 2.5185 .0015 1 2 1
2.3800 2.3777 .0023 2 2 1
1.9700 1.9648 .0052 6 1 0
1.8800 1.8814 -.0014 4 1 2
1.8500 1.8477 .0023 0 3 1
1.7600 1.7604 -.0004 3 2 2
a=12.49 b= 5.941 c= 5.136
da= .01 db= .002 dc= .003
V= 381.1
Triklin
Dexp Dcal d(D) h k l
4.2900 4.2898 .0002 1 0 0
4.0900 4.0936 -.0036 1 1 0
3.1100 3.1092 .0008 -1 -1 2
2.9700 2.9713 -.0013 1 0 2
2.7600 2.7597 .0003 -1 0 2
2.6700 2.6677 .0023 0 1 2
2.5200 2.5198 .0002 0 2 0
2.3800 2.3817 -.0017 -1 -1 3
1.9700 1.9676 .0024 -2 -2 2
1.8800 1.8794 .0006 -1 -1 4
1.8500 1.8511 -.0011 0 2 2
1.7600 1.7603 -.0003 0 -3 2
A= 4.619 DA= .004
B= 5.714 DB= .006
C= 8.111 DC= .001
GAMMA= 68.64 DGAMMA= .07
BETA = 92.861 DBETA = .009
ALPHA=108.465 DALPHA= .008
V= 188.6
23. 32-0765
K3{Co{NO3}6}
Triklin
Dexp Dcal d(D) h k l
12.7000 12.7186 -.0186 1 0 0
9.1800 9.1655 .0145 -1 1 0
6.6500 6.6513 -.0013 -1 1 1
5.5300 5.5281 .0019 0 2 0
5.1700 5.1698 .0002 2 0 1
4.6800 4.6813 -.0013 -2 0 1
4.3700 4.3761 -.0061 -2 2 1
4.1100 4.1147 -.0047 0 1 2
3.6110 3.6131 -.0021 2 -2 1
3.4600 3.4586 .0014 -2 3 0
3.1540 3.1538 .0002 3 -2 1
3.0190 3.0185 .0005 3 1 2
A= 12.9256 DA= .0003
B= 11.92 DB= .01
C= 8.24 DC= .01
GAMMA= 98.50 DGAMMA= .07
BETA = 87.48 DBETA = .02
ALPHA= 70.31 DALPHA= .09
V= 1176
24. 32-1066
Na2CoFe{CN6}6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.9500 5.9468 .0032 1 1 0
5.3100 5.3191 -.0091 1 0 1
5.1100 5.1006 .0094 -1 1 1
4.7800 4.7817 -.0017 1 1 1
4.4200 4.4178 .0022 0 0 2
4.0900 4.0952 -.0052 0 1 2
3.6200 3.6174 .0026 1 0 2
2.6600 2.6598 .0002 -1 3 2
2.5500 2.5503 -.0003 -2 2 2
a= 7.116 b= 10.92 c= 8.87 beta= 94.754
da=.007 db=.01 dc=.01 dbeta=.001
V= 686.4
25. 32-1073
C6CoO12Pr*8H2O
Triklin
Dexp Dcal d(D) h k l
9.9200 9.9348 -.0148 1 0 1
7.7500 7.7321 .0179 0 1 1
7.4900 7.4941 -.0041 0 -1 1
6.4100 6.4241 -.0141 0 0 2
5.9800 5.9648 .0152 -1 1 0
5.8200 5.8371 -.0171 1 -1 1
5.5000 5.4998 .0002 2 0 1
5.3000 5.2914 .0086 2 1 2
5.2400 5.2329 .0071 0 -1 2
5.1500 5.1496 .0004 2 0 0
4.9700 4.9674 .0026 2 0 2
4.8400 4.8388 .0012 1 -1 2
A= 12.0231 DA= .0003
B= 10.3172 DB= .0005
C= 13.9811 DC= .0005
GAMMA= 66.354 DGAMMA= .006
BETA = 66.853 DBETA = .006
ALPHA= 79.327 DALPHA= .005
V=1460