1. 30-0047
Co2Fe{CN}6
Triklin
Dexp Dcal d(D) h k l
12.5000 12.5588 -.0588 1 0 0
7.3400 7.3250 .0150 1 1 0
6.1500 6.1514 -.0014 0 0 1
4.7100 4.7194 -.0094 1 -1 1
4.5200 4.5168 .0032 1 1 1
4.2000 4.2009 -.0009 -1 1 1
4.0600 4.0615 -.0015 0 -2 0
3.9000 3.8981 .0019 2 -1 1
3.7100 3.7093 .0007 -1 2 0
3.6000 3.5987 .0013 0 -2 1
3.0300 3.0306 -.0006 2 2 1
2.7500 2.7498 .0002 1 1 2
2.6200 2.6200 .0000 4 -1 1
A= 12.697 DA= .006
B= 8.269 DB= .008
C= 6.200 DC= .001
GAMMA= 81.82 DGAMMA= .07
BETA = 88.87 DBETA = .01
ALPHA= 96.83 DALPHA= .07
V= 639.3
2. 30-0122
Ba3Co2WO9
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.6900 4.6902 -.0002 1 1 0
3.3300 3.3297 .0003 1 2 0
2.8600 2.8608 -.0008 2 0 0
2.4400 2.4417 -.0017 1 1 2
2.3400 2.3397 .0003 -2 0 2
2.1700 2.1695 .0005 1 2 2
2.0260 2.0257 .0003 0 1 3
1.8570 1.8575 -.0005 3 1 0
1.7760 1.7764 -.0004 -2 3 2
1.7410 1.7415 -.0005 -3 1 2
1.6540 1.6538 .0002 -2 4 1
1.5600 1.5599 .0001 -1 1 4
1.4320 1.4317 .0003 -4 1 1
1.3700 1.3702 -.0002 -4 2 1
1.2810 1.2815 -.0005 -4 1 3
a= 5.822 b= 8.1889 c= 6.38207 beta=100.64
da=.002 db=.0008 dc=.00007 dbeta=.07
V= 299.0
Triklin
Dexp Dcal d(D) h k l
4.6900 4.6895 .0005 0 1 1
3.3300 3.3297 .0003 -1 1 0
2.8600 2.8599 .0001 0 -1 1
2.4400 2.4405 -.0005 1 1 2
2.3400 2.3400 -.0000 -2 0 2
2.1700 2.1692 .0008 -1 2 2
2.0260 2.0271 -.0011 -1 2 0
1.8570 1.8569 .0001 0 1 3
1.7760 1.7759 .0001 3 0 1
1.7410 1.7411 -.0001 -3 1 0
1.6540 1.6539 .0001 1 -1 2
1.5600 1.5600 .0000 -3 0 3
1.4320 1.4321 -.0001 -3 2 3
1.3700 1.3700 -.0000 0 1 4
1.2810 1.2810 -.0000 1 3 4
A= 6.902 DA= .004
B= 5.5360 DB= .0005
C= 5.7035 DC= .0001
GAMMA= 76.45 DGAMMA= .01
BETA =100.19 DBETA = .01
ALPHA= 66.616 DALPHA= .005
V= 185.34
3. 30-0421
{Co{NH3}4{SO4}8F4
Rombik
Groupa 32,55
Dexp. Dcal. d(D) h k l
6.4100 6.4278 -.0178 0 0 1
5.3000 5.3061 -.0061 1 2 0
4.8700 4.8589 .0111 1 1 1
4.4900 4.4962 -.0062 2 0 0
4.2600 4.2542 .0058 2 1 0
4.0900 4.0920 -.0020 1 2 1
3.9400 3.9388 .0012 1 3 0
3.7100 3.7109 -.0009 2 2 0
a= 8.992 b=13.144 c= 6.43
da= .001 db= .003 dc= .01
V=760.
4. 30-0422
{Co{NH3}4{H2O]{SO4}2PtCl6*2H2O
Triklin
Dexp Dcal d(D) h k l
9.1100 9.1095 .0005 1 1 0
6.4300 6.4301 -.0001 0 1 1
5.6400 5.6401 -.0001 0 -1 1
5.2000 5.2001 -.0001 -1 -1 1
4.8800 4.8800 .0000 1 -1 1
4.5700 4.5700 -.0000 2 2 1
4.1300 4.1300 .0000 -2 -1 1
4.0400 4.0400 .0000 1 1 2
A= 12.575 DA= .002
B= 10.476 DB= .003
C= 8.1844 DC= .0005
GAMMA= 64.98 DGAMMA= .02
BETA = 73.603 DBETA = .008
ALPHA= 76.42 DALPHA= .01
V= 928.9
5. 30-0423
Co2{NH3}8{H2O}4{SeO4}2*3H2O
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
10.4000 10.5033 -.1033 1 0 1
6.1900 6.1885 .0015 1 0 2
5.7100 5.7316 -.0216 3 0 0
4.6500 4.6562 -.0062 0 1 1
4.5000 4.4944 .0056 1 1 1
4.3500 4.3368 .0132 3 0 2
3.9300 3.9323 -.0023 2 0 3
3.5000 3.5011 -.0011 3 0 3
a=17.195 b= 4.973 c=13.266
da= .009 db= .002 dc= .009
V=1134
Triklin
Dexp Dcal d(D) h k l
10.4000 10.3769 .0231 1 0 0
6.1900 6.1903 -.0003 -1 1 0
5.7100 5.7100 .0000 -1 0 1
4.6500 4.6498 .0002 1 -1 1
4.5000 4.5001 -.0001 -2 1 0
4.3500 4.3499 .0001 -1 1 1
3.9300 3.9301 -.0001 2 0 1
3.5000 3.5000 -.0000 -2 -1 1
A= 10.531 DA= .002
B= 6.9725 DB= .0004
C= 6.586 DC= .002
GAMMA= 98.95 DGAMMA= .02
BETA = 92.97 DBETA = .02
ALPHA= 96.33 DALPHA= .01
V= 474
6. 30-0424
{Co{NH3}4{H2O}{SO4}}ClO4
Rombik
Groupa 39,67
Dexp. Dcal. d(D) h k l
6.3400 6.3708 -.0308 2 0 0
4.4600 4.4494 .0106 0 2 0
4.2500 4.2472 .0028 3 0 0
4.0000 3.9859 .0141 0 0 2
3.6400 3.6478 -.0078 2 2 0
3.4700 3.4544 .0156 3 1 1
2.9000 2.9064 -.0064 3 0 2
2.6900 2.6910 -.0010 2 2 2
a=12.74 b= 8.899 c= 7.97
da= .03 db= .005 dc= .01
V= 903.9
Triklin
Dexp Dcal d(D) h k l
6.3400 6.3400 .0000 0 1 1
4.4600 4.4600 -.0000 -1 2 0
4.2500 4.2500 -.0000 0 -1 1
4.0000 4.0000 .0000 -2 2 2
3.6400 3.6400 -.0000 -2 2 0
3.4700 3.4700 .0000 0 1 2
2.9000 2.9000 .0000 1 2 1
2.6900 2.6900 .0000 -3 2 0
A= 9.9674 DA= .0006
B= 11.3364 DB= .0004
C= 8.4450 DC= .0002
GAMMA=130.051 DGAMMA= .003
BETA =124.740 DBETA = .002
ALPHA= 52.302 DALPHA= .001
V= 553
7. 30-0425
{Co{NH3}4{H2O} {SO4}*3H2O
Triklin
Dexp Dcal d(D) h k l
8.9800 8.9798 .0002 1 0 0
8.5800 8.5806 -.0006 -1 1 0
6.8000 6.7998 .0002 1 -1 1
5.9600 5.9597 .0003 1 1 0
5.1400 5.1401 -.0001 1 1 1
4.6900 4.6901 -.0001 0 -2 1
4.4300 4.4300 .0000 -1 2 1
4.2200 4.2200 .0000 1 -1 2
A= 9.80046 DA= .00006
B= 11.6956 DB= .0001
C= 8.8719 DC= .0003
GAMMA=111.591 DGAMMA= .004
BETA = 78.620 DBETA = .001
ALPHA= 96.213 DALPHA= .006
V= 926.3
8. 30-0426
{Co{NH3}4{H2O}22SO4}3*3H2O
Tetrag.
Groupa 90,113
Dexp. Dcal. d(D) h k l
10.3000 10.3261 -.0261 0 0 1
6.0000 6.0140 -.0140 2 0 1
5.6000 5.5714 .0286 2 1 1
4.6400 4.6300 .0100 1 1 2
4.2600 4.2619 -.0019 3 1 1
4.1000 4.1038 -.0038 3 2 0
3.8200 3.8137 .0063 3 2 1
3.5600 3.5664 -.0064 3 0 2
a= 14.80 c= 10.33
da= .01 dc= .01
v=2261
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2965 .0035 1 0 0
6.0000 5.9987 .0013 0 1 0
5.6000 5.5989 .0011 0 0 1
4.6400 4.6400 -.0000 -1 0 1
4.2600 4.2602 -.0002 0 -1 1
4.1000 4.1000 .0000 1 -1 1
3.8200 3.8201 -.0001 1 1 1
3.5600 3.5601 -.0001 -1 1 1
A= 10.411 DA= .001
B= 6.0169 DB= .0002
C= 5.6779 DC= .0003
GAMMA= 90.5368 DGAMMA= .0004
BETA = 81.5119 DBETA = .0008
ALPHA= 94.4590 DALPHA= .0001
V= 350.7
9. 30-0427
{Co{NH3}4{H2O}{SO4}}NO3
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
6.7000 6.6814 .0186 1 0 2
5.1000 5.1084 -.0084 3 0 0
4.8400 4.8305 .0095 3 0 1
4.4400 4.4504 -.0104 2 1 2
4.2100 4.2084 .0016 3 0 2
4.0400 4.0404 -.0004 0 2 0
3.7800 3.7783 .0017 1 2 1
3.1300 3.1299 .0001 0 2 3
a=15.325 b= 8.0807 c=14.84838
da= .005 db= .0007 dc= .00008
V=1838.8
Triklin
Dexp Dcal d(D) h k l
6.7000 6.6993 .0007 -1 0 1
5.1000 5.0998 .0002 0 1 1
4.8400 4.8398 .0002 0 -1 1
4.4400 4.4401 -.0001 -1 1 1
4.2100 4.2100 .0000 -2 -1 1
4.0400 4.0400 -.0000 1 1 1
3.7800 3.7800 -.0000 -1 0 2
3.1300 3.1300 -.0000 0 -2 1
A= 8.8418 DA= .0001
B= 7.6589 DB= .0001
C= 7.59771 DC= .00008
GAMMA= 71.159 DGAMMA= .003
BETA =115.957 DBETA = .005
ALPHA= 95.5609 DALPHA= .0009
V= 437
10. 30-0428
{Co{NH3}4{H2O}{SO4}2SeO4*4H2O
Triklin
Dexp Dcal d(D) h k l
9.1100 9.1100 .0000 1 0 0
8.6200 8.6191 .0009 -1 1 0
6.8000 6.7997 .0003 -1 1 1
5.9800 5.9801 -.0001 0 -1 1
5.0900 5.0899 .0001 -2 1 0
4.7300 4.7300 .0000 1 1 1
4.4500 4.4500 .0000 -1 -1 1
4.1500 4.1500 -.0000 -2 2 1
A= 10.2480 DA= .00006
B= 10.1906 DB= .0004
C= 9.2167 DC= .0003
GAMMA=117.2406 DGAMMA= .0002
BETA = 95.490 DBETA = .001
ALPHA= 80.377 DALPHA= .004
V= 844
11. 30-0430
{Co{NH3}4{SO4}}BF4
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
7.6900 7.6552 .0348 0 0 2
6.5200 6.4985 .0215 1 1 0
5.6000 5.5835 .0165 1 0 2
4.4900 4.4865 .0035 1 2 0
4.3000 4.3055 -.0055 1 2 1
3.8700 3.8707 -.0007 1 2 2
3.6100 3.6011 .0089 2 0 2
3.4600 3.4654 -.0054 1 0 4
a= 8.16 b=10.74 c=15.31
da= .08 db= .07 dc= .02
V=1342
Triklin
Dexp Dcal d(D) h k l
7.6900 7.6884 .0016 1 0 0
6.5200 6.5202 -.0002 0 -1 1
5.6000 5.5999 .0001 -1 0 1
4.4900 4.4900 .0000 1 2 0
4.3000 4.3000 .0000 -2 -1 1
3.8700 3.8700 .0000 -1 -1 2
3.6100 3.6101 -.0001 -2 0 1
3.4600 3.4600 .0000 0 0 2
A= 8.945 DA= .003
B= 10.152 DB= .002
C= 7.835 DC= .002
GAMMA= 60.50 DGAMMA= .02
BETA =110.05 DBETA = .03
ALPHA=116.58 DALPHA= .06
V= 546.9
12. 30-0520
{Co{NH3}4{SO4}Br}
Rombik
Groupa 52
Dexp. Dcal. d(D) h k l
6.6300 6.6169 .0131 1 0 1
5.3700 5.3673 .0027 1 1 1
4.3000 4.2947 .0053 1 1 2
3.9100 3.9117 -.0017 2 0 0
3.7700 3.7693 .0007 0 1 3
3.1000 3.1006 -.0006 0 0 4
2.9700 2.9701 -.0001 0 3 1
2.7500 2.7500 .0000 1 1 4
a= 7.82 b= 9.177 c=12.402
da= .01 db= .002 dc= .002
v= 890.5
13. 30-0672
{Co{NH3}4{SO4}Cl}
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
7.3700 7.3722 -.0022 1 0 1
6.4800 6.4564 .0236 1 1 0
5.2100 5.2013 .0087 0 0 3
4.8200 4.8283 -.0083 0 2 1
4.2600 4.2556 .0044 0 2 2
3.8700 3.8672 .0028 2 1 0
3.7500 3.7536 -.0036 2 1 1
3.1200 3.1208 -.0008 0 0 5
a= 8.365 b=10.155 c=15.60
da= .004 db= .004 dc= .02
V=1325
14. 30-0685
{Co{NH3}4{SO4}{NO3}}
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.8800 6.9122 -.0322 0 0 1
6.2800 6.2634 .0166 1 0 1
5.3000 5.2957 .0043 2 1 0
5.0900 5.1069 -.0169 0 1 1
4.8400 4.8278 .0122 1 1 1
4.1300 4.1358 -.0058 3 1 0
4.0200 4.0168 .0032 3 0 1
3.7900 3.7890 .0010 0 2 0
a=14.807 b= 7.58 c= 6.9122
da= .008 db= .01 dc= .0001
V=775.6
15. 30-0803
{Co{NH3}4{SO4}2PtCl6
Tetragon.
Groupa 90,113
Dexp. Dcal. d(D) h k l
8.8400 8.9698 -.1298 0 0 1
6.2300 6.2064 .0236 1 1 1
5.4500 5.4368 .0132 2 1 0
5.0200 5.0320 -.0120 2 0 1
4.2900 4.2982 -.0082 2 2 0
3.8900 3.8761 .0139 2 2 1
3.7000 3.6930 .0070 3 0 1
3.1500 3.1561 -.0061 3 2 1
a= 12.16 c=8.97
da= .05 dc= .09
v=1326
Triklin
Dexp Dcal d(D) h k l
8.8400 8.8403 -.0003 0 0 1
6.2300 6.2300 .0000 -1 1 1
5.4500 5.4500 .0000 0 -2 1
5.0200 5.0200 .0000 -1 -1 2
4.2900 4.2900 .0000 0 -2 2
3.8900 3.8900 .0000 1 1 1
3.7000 3.7000 .0000 0 -3 1
3.1500 3.1500 .0000 -2 3 0
A= 9.46075 DA= .00002
B= 11.23957 DB= .00003
C= 10.47548 DC= .00001
GAMMA= 98.9985 DGAMMA= .0001
BETA =113.0534 DBETA = .0002
ALPHA=107.5368 DALPHA= .0002
V= 928.478
16. 30-0812
C12H48Cl12CoMn5N24O12
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
7.4600 7.4038 .0562 0 2 0
4.6400 4.6599 -.0199 2 2 0
3.7900 3.8109 -.0209 2 3 0
3.7200 3.7019 .0181 0 4 0
3.2800 3.2715 .0085 1 2 1
3.1600 3.1500 .0100 2 4 0
2.8600 2.8752 -.0152 1 5 0
2.6000 2.5980 .0020 1 4 1
2.4100 2.4122 -.0022 3 3 1
2.3000 2.2990 .0010 1 5 1
2.1100 2.1070 .0030 4 5 0
2.0400 2.0439 -.0039 1 6 1
a=11.993 b=14.81 c= 3.828
da= .001 db= .01 dc= .003
V= 679.8
Triklin
Dexp Dcal d(D) h k l
7.4600 7.4584 .0016 1 0 0
4.6400 4.6371 .0029 -1 0 1
3.7900 3.7890 .0010 -1 -2 1
3.7200 3.7208 -.0008 -1 1 1
3.2800 3.2814 -.0014 2 0 1
3.1600 3.1627 -.0027 2 -1 1
2.8600 2.8640 -.0040 1 3 0
2.6000 2.5992 .0008 1 1 2
2.4100 2.4121 -.0021 -2 -1 2
2.3000 2.2990 .0010 -3 -1 1
2.1100 2.1100 -.0000 3 -2 1
2.0400 2.0404 -.0004 -1 -2 3
A= 7.492 DA= .001
B= 9.41485 DB= .00008
C= 6.495 DC= .003
GAMMA= 85.706 DGAMMA= .005
BETA = 88.08 DBETA = .03
ALPHA=107.00 DALPHA= .02
V= 436.2
17. 30-0930
KCoW3.3O11.4*7.6H2O
Triklin
Dexp Dcal d(D) h k l
3.4200 3.4209 -.0009 0 1 1
3.2200 3.2196 .0004 -2 0 1
3.0300 3.0303 -.0003 -2 -1 1
2.9150 2.9147 .0003 0 2 0
2.4900 2.4892 .0008 -3 0 1
2.3410 2.3408 .0002 1 0 2
1.9690 1.9693 -.0003 3 -2 1
1.8650 1.8650 -.0000 -2 1 2
1.6950 1.6950 .0000 1 2 2
1.5480 1.5479 .0001 2 -3 2
1.3500 1.3500 -.0000 -5 -2 2
1.2600 1.2600 .0000 -4 -2 3
A= 8.8736 DA= .0004
B= 5.936 DB= .002
C= 4.902 DC= .001
GAMMA= 87.254 DGAMMA= .007
BETA = 89.03 DBETA = .03
ALPHA=100.443 DALPHA= .004
V= 253.5
18. 30-0941
C10H40Cl2CoN20O10
Triklin
Dexp Dcal d(D) h k l
9.7600 9.7314 .0286 0 0 1
5.7400 5.7331 .0069 0 -2 1
5.3900 5.3978 -.0078 1 1 0
5.2400 5.2301 .0099 1 -1 2
4.8900 4.8936 -.0036 1 -2 1
4.7600 4.7701 -.0101 -1 -1 1
4.5700 4.5809 -.0109 1 0 2
3.9200 3.9174 .0026 -1 -2 1
3.7400 3.7381 .0019 0 1 2
3.5400 3.5409 -.0009 1 -3 1
3.4300 3.4283 .0017 2 0 1
3.4000 3.3998 .0002 1 2 1
A= 7.036 DA= .001
B= 11.76 DB= .02
C= 11.818 DC= .004
GAMMA=102.55 DGAMMA= .04
BETA = 69.6333 DBETA = .0001
ALPHA=120.87 DALPHA= .08
V=788.2
19. 30-1022
{Co,Mn}OOH
Geksagon.
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
9.7500 9.7249 .0251 0 0 1
4.8600 4.8625 -.0025 0 0 2
2.4500 2.4498 .0002 1 0 2
1.4180 1.4180 -.0000 2 0 0
a= 3.2748 c= 9.725
da= .0009 dc=.003
V=90.32
20. 30-1184
C8H8CoNa2O8S2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.7800 7.7772 .0028 1 1 0
6.4300 6.4296 .0004 2 0 0
5.5900 5.6002 -.0102 2 0 1
4.4500 4.4537 -.0037 0 2 1
4.2000 4.1941 .0059 -1 2 1
3.9500 3.9509 -.0009 -3 0 1
3.4100 3.4103 -.0003 3 0 2
3.1900 3.1926 -.0026 2 0 3
2.9100 2.9088 .0012 0 2 3
2.8000 2.8001 -.0001 4 0 2
2.6200 2.6205 -.0005 4 2 1
2.5200 2.5180 .0020 5 0 1
a= 12.864 b= 9.7657 c= 10.868 beta= 88.44
da=.003 db=.0002 dc=.006 dbeta=.03
V= 1365
Triklin
Dexp Dcal d(D) h k l
7.7800 7.7710 .0090 1 0 0
6.4300 6.4284 .0016 0 0 1
5.5900 5.5900 .0000 0 -2 1
4.4500 4.4483 .0017 -1 2 1
4.2000 4.1974 .0026 1 1 1
3.9500 3.9524 -.0024 -2 -1 1
3.4100 3.4095 .0005 -1 -1 2
3.1900 3.1906 -.0006 -1 -3 2
2.9100 2.9099 .0001 -2 -5 1
2.8000 2.8002 -.0002 -2 1 2
2.6200 2.6192 .0008 2 -3 1
2.5200 2.5207 -.0007 -3 1 0
A= 8.252 DA= .001
B= 17.9805 DB= .0003
C= 6.855 DC= .001
GAMMA= 80.317 DGAMMA= .001
BETA =108.564 DBETA = .006
ALPHA=101.004 DALPHA= .005
V= 940.3
21. 30-1606
C12H30Br2CoN2O2
Triklin
Dexp Dcal d(D) h k l
8.4800 8.4799 .0001 1 0 0
7.6900 7.6895 .0005 0 1 1
6.6900 6.6893 .0007 0 -1 1
5.6200 5.6201 -.0001 1 1 1
4.4500 4.4500 -.0000 1 -2 1
4.2400 4.2400 .0000 2 0 0
3.7900 3.7900 .0000 -1 1 2
3.6800 3.6800 .0000 1 -1 2
3.4200 3.4200 -.0000 -1 -1 2
A= 8.56698 DA= .00006
B= 13.0970 DB= .0004
C= 8.6911 DC= .0001
GAMMA= 97.414 DGAMMA= .001
BETA = 87.661 DBETA = .0002
ALPHA= 81.7745 DALPHA= .0001
V= 955.3
22. 30-1608
C22H18CoN8
Triklin
Dexp Dcal d(D) h k l
8.4600 8.4632 -.0032 1 0 0
6.0000 5.9991 .0009 1 1 1
5.2700 5.2681 .0019 -1 -1 1
4.5000 4.5013 -.0013 2 0 1
4.3100 4.3080 .0020 1 2 0
4.0300 4.0297 .0003 2 1 1
3.8600 3.8477 .0123 -2 1 0
3.5600 3.5601 -.0001 -1 2 1
2.7400 2.7400 -.0000 -1 -3 2
2.5500 2.5501 -.0001 2 -3 3
2.4100 2.4098 .0002 0 -4 2
2.1400 2.1398 .0002 3 -1 5
A= 9.017 DA= .007
B= 10.006 DB= .002
C= 11.8697 DC= .0009
GAMMA= 92.00 DGAMMA= .05
BETA = 69.88 DBETA = .01
ALPHA=100.26 DALPHA= .04
V= 989.1
23. 30-1609
C4H12Cl12Cl2CoO2
Rombik
Groupa 16,25,47
Dexp. Dcal. d(D) h k l
7.5500 7.5243 .0257 0 0 1
6.9200 7.0080 -.0880 0 1 0
4.5100 4.5190 -.0090 2 1 0
3.9300 3.9416 -.0116 3 0 0
3.5100 3.5040 .0060 0 2 0
2.9600 2.9562 .0038 4 0 0
2.7500 2.7514 -.0014 4 0 1
2.5600 2.5611 -.0011 4 1 1
1.9600 1.9602 -.0002 5 2 0
1.9070 1.9065 .0005 6 0 1
a=11.825 b= 7.008 c= 7.52
da= .003 db= .001 dc= .01
V= 623.5
Triklin
Dexp Dcal d(D) h k l
7.5500 7.5526 -.0026 1 0 0
6.9200 6.9189 .0011 0 1 1
4.5100 4.5096 .0004 0 -1 1
3.9300 3.9301 -.0001 -1 2 0
3.5100 3.5101 -.0001 -1 -1 1
2.9600 2.9600 .0000 2 1 2
2.7500 2.7500 .0000 -1 3 0
2.5600 2.5600 -.0000 1 1 3
1.9600 1.9600 .0000 -3 2 2
1.9070 1.9070 .0000 3 -3 1
A= 7.7988 DA= .0005
B= 9.1001 DB= .0004
C= 7.7987 DC= .0004
GAMMA= 95.248 DGAMMA= .005
BETA = 79.695 DBETA = .002
ALPHA= 67.383 DALPHA= .001
V= 494.8
24. 30-1611
C12H30Cl2CoN2O2
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
8.6400 8.3753 .2647 1 0 1
7.6000 7.5911 .0089 1 1 0
6.6000 6.5905 .0095 1 1 1
5.8200 5.8167 .0033 -1 0 1
5.4000 5.3958 .0042 2 0 0
4.5000 4.5027 -.0027 1 2 1
3.9000 3.8987 .0013 2 1 2
3.5000 3.5000 .0000 1 2 2
a= 11.556 b= 10.6800 c= 9.2786 beta= 69.03
da=.009 db=.0007 dc=.0002 dbet=.01
V=1070
25. 30-1612
C24H60Cl2CoN4O12
Rombik
Groupa 61
Dexp. Dcal. d(D) h k l
8.7800 8.8331 -.0531 0 0 2
7.6000 7.5424 .0576 1 0 2
5.5800 5.6021 -.0221 2 0 2
4.4200 4.4165 .0035 0 0 4
4.2400 4.2381 .0019 3 0 2
3.7200 3.7174 .0026 2 1 0
3.3900 3.3920 -.0020 1 1 3
a=14.491 b= 4.331 c=17.67
da= .008 db= .005 dc= .07
V=1108.7
26. 30-1614
C20H16ClCoN6O4*7H2O
Triklin
Dexp Dcal d(D) h k l
13.1000 13.1105 -.0105 1 0 0
12.1000 12.1104 -.0104 0 1 0
8.8800 8.8757 .0043 0 0 1
7.1200 7.1256 -.0056 0 -1 1
6.8000 6.7988 .0012 -1 0 1
6.1600 6.1596 .0004 1 2 0
5.7900 5.8005 -.0105 2 0 1
4.8000 4.7970 .0030 2 -1 1
4.1800 4.1802 -.0002 0 1 2
4.0400 4.0397 .0003 2 1 2
3.9400 3.9395 .0005 2 3 0
3.7700 3.7706 -.0006 2 3 1
3.3200 3.3196 .0004 3 2 2
A= 13.86 DA= .01
B= 12.59 DB= .01
C= 9.0430 DC= .0001
GAMMA= 74.12 DGAMMA= .08
BETA = 78.98 DBETA = .02
ALPHA= 86.47 DALPHA= .02
V= 1490.0
27. 30-1615
C20H16CoN7O7*3H2O
Triklin
Dexp Dcal d(D) h k l
9.8300 9.8196 .0104 1 0 0
8.6700 8.6746 -.0046 -1 1 0
6.9700 6.9700 .0000 -1 1 1
6.5100 6.5102 -.0002 -1 0 1
5.8500 5.8508 -.0008 1 0 1
5.5700 5.5704 -.0004 0 2 0
5.0500 5.0467 .0033 -2 1 0
4.9100 4.9098 .0002 2 0 0
4.7800 4.7810 -.0010 -2 1 1
4.3900 4.3896 .0004 -2 0 1
3.8600 3.8599 .0001 -1 2 2
3.4100 3.4104 -.0004 -3 1 0
A= 10.436 DA= .003
B= 12.192 DB= .009
C= 8.344 DC= .002
GAMMA=108.82 DGAMMA= .05
BETA =101.35 DBETA = .02
ALPHA= 72.22 DALPHA= .03
V= 951.1
28. 30-1616
C20H16CoN7*3H2O
Triklin
Dexp Dcal d(D) h k l
13.0000 13.0155 -.0155 1 0 0
9.2100 9.2103 -.0003 0 1 0
8.6700 8.6710 -.0010 -1 0 1
7.2900 7.2931 -.0031 1 1 0
6.8800 6.8779 .0021 0 1 1
6.1600 6.1620 -.0020 -1 -1 1
5.8800 5.8805 -.0005 -2 0 1
4.8200 4.8189 .0011 -2 -1 1
4.3500 4.3499 .0001 -1 -1 2
4.0600 4.0601 -.0001 1 1 2
3.8100 3.8099 .0001 3 0 1
A= 13.175 DA= .001
B= 9.2319 DB= .0006
C= 10.369 DC= .004
GAMMA= 93.91 DGAMMA= .02
BETA = 98.08 DBETA = .07
ALPHA= 89.089 DALPHA= .003
V= 1245.7
29. 30-1617
c24H16CoN7*2H2O
Triklin
Dexp Dcal d(D) h k l
11.4000 11.4468 -.0468 1 0 0
10.4000 10.3810 .0190 0 1 0
8.4200 8.3908 .0292 0 0 1
8.0600 8.1193 -.0593 -1 0 1
7.6600 7.6599 .0001 1 1 0
7.0900 7.0879 .0021 0 -1 1
5.0300 5.0288 .0012 -2 1 0
4.7700 4.7678 .0022 -2 1 1
4.3300 4.3287 .0013 -1 -1 2
4.0200 4.0197 .0003 -2 -2 1
3.5400 3.5406 -.0006 1 -1 2
3.4600 3.4603 -.0003 0 3 0
A= 12.0949 DA= .0008
B= 10.5200 DB= .0003
C= 8.975 DC= .001
GAMMA= 87.431 DGAMMA= .006
BETA =108.84 DBETA = .04
ALPHA= 99.32 DALPHA= .02
V= 1066.6
30. 30-1618
c24H16ClCoN6O8*H2O
Triklin
Dexp Dcal d(D) h k l
9.4200 9.4191 .0009 1 0 0
8.9300 8.9346 -.0046 1 1 0
7.6200 7.6261 -.0061 0 0 1
6.4300 6.4277 .0023 0 -1 1
6.0200 6.0077 .0123 -1 0 1
5.7900 5.7909 -.0009 -1 1 0
5.4800 5.4739 .0061 1 1 1
5.1500 5.1506 -.0006 2 1 0
4.4500 4.4509 -.0009 -2 -1 1
3.8300 3.8300 .0000 -1 2 0
3.4400 3.4408 -.0008 0 1 2
A= 10.36 DA= .01
B= 11.11 DB= .01
C= 7.698 DC= .003
GAMMA= 65.49 DGAMMA= .09
BETA = 94.601 DBETA = .009
ALPHA= 97.69 DALPHA= .01
V= 798.6
31. 30-1620
C12H30CoI2N2O2
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
8.7800 8.7370 .0430 0 0 1
7.5900 7.5932 -.0032 1 0 1
6.6400 6.6219 .0181 1 1 0
5.6100 5.6200 -.0100 0 1 1
3.6700 3.6700 .0000 0 2 0
3.4000 3.4008 -.0008 4 1 0
a=15.350 b= 7.3400 c= 8.737
da= .001 db= .0005 dc= .001
V= 984.4
32. 30-1621
C12H8CoN2O6*4H2O
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
8.5000 8.5167 -.0167 0 2 0
7.1900 7.2077 -.0177 0 2 1
6.2800 6.2873 -.0073 0 1 2
5.6800 5.6778 .0022 0 3 0
4.1900 4.2017 -.0117 1 3 0
4.0200 4.0127 .0073 1 3 1
3.5700 3.5693 .0007 1 3 2
3.5200 3.5187 .0013 1 4 0
3.3600 3.3600 -.0000 1 2 3
a= 6.25 b=17.03 c=13.53
da= .03 db= .05 dc= .02
V=1440
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
8.5000 8.5300 -.0300 1 1 0
7.1900 7.2046 -.0146 -1 0 1
6.2800 6.2913 -.0113 -1 1 1
5.6800 5.6818 -.0018 2 0 0
4.1900 4.1993 -.0093 -1 0 2
4.0200 4.0246 -.0046 1 3 0
3.5700 3.5728 -.0028 -3 0 1
3.5200 3.5200 .0000 -1 2 2
3.3600 3.3600 .0000 2 0 2
a= 11.393 b=12.910 c= 8.8065 beta= 94.113
da=.002 db=.001 dc=.0001 dbet=.006
V=1290
33. 30-1623
C11H22CoN2O8P
Triklin
Dexp Dcal d(D) h k l
9.8300 9.8016 .0284 0 1 1
9.2300 9.2462 -.0162 -1 0 1
8.9900 8.9858 .0042 0 -1 1
7.9400 7.9230 .0170 1 0 1
7.7600 7.7523 .0077 -1 1 1
6.6700 6.6771 -.0071 0 2 0
6.6100 6.6157 -.0057 1 -1 1
6.0900 6.0916 -.0016 -1 0 2
5.7900 5.7920 -.0020 1 2 0
5.4500 5.4511 -.0011 -2 0 1
5.4100 5.4066 .0034 -1 -1 2
5.0700 5.0690 .0010 -2 1 1
A= 11.301 DA= .006
B= 13.405 DB= .005
C= 13.351 DC= .009
GAMMA= 89.39 DGAMMA= .03
BETA = 98.85 DBETA = .05
ALPHA= 85.19 DALPHA= .01
V= 1991