1. 22-0040
{NH4}4{CoMo6H6O24}*5H2O
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
10.9000 10.9516 -.0516 0 1 0
7.9600 7.9441 .0159 0 1 1
5.7300 5.7704 -.0404 0 0 2
5.1200 5.1051 .0149 0 1 2
3.7300 3.7302 -.0002 1 1 0
3.1300 3.1340 -.0040 -1 0 2
3.0300 3.0357 -.0057 -1 2 1
2.7900 2.7900 .0000 0 1 4
2.7200 2.7200 .0000 -1 2 2
2.6400 2.6400 .0000 -1 0 3
a= 3.986 b= 10.95 c= 11.593 beta= 84.57
da=.004 db=.02 dc=.002 dbet=.06
V=503
2. 22-0042
NH4CoPO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.9000 8.8898 .0102 0 1 0
4.4300 4.4306 -.0006 -1 0 2
3.5000 3.5017 -.0017 0 0 3
3.3100 3.3085 .0015 1 2 2
3.1800 3.1814 -.0014 -1 0 3
2.9200 2.9199 .0001 2 1 3
2.7200 2.7193 .0007 -2 0 3
2.5300 2.5300 -.0000 2 3 1
2.4300 2.4299 .0001 4 0 2
1.9400 1.9401 -.0001 -4 0 3
1.6900 1.6901 -.0001 5 3 1
a= 10.306 b= 8.890 c= 10.605 beta= 82.13
da=.003 db=.005 dc=.002 dbeta=.01
V= 962
3. 22-0043
NH4CoPO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.3000 6.3217 -.0217 0 1 1
4.6600 4.6624 -.0024 2 1 0
4.5200 4.5228 -.0028 2 0 2
4.3900 4.3862 .0038 2 1 1
3.4800 3.4833 -.0033 3 0 2
3.4300 3.4280 .0020 0 0 4
3.2300 3.2302 -.0002 2 1 3
3.1900 3.1915 -.0015 -3 1 2
3.1600 3.1608 -.0008 0 2 2
3.1300 3.1293 .0007 3 1 2
3.0000 3.0003 -.0003 2 2 1
2.7900 2.7899 .0001 -2 1 4
2.7300 2.7293 .0007 1 2 3
2.5000 2.4997 .0003 -3 1 4
a= 12.338 b= 7.124 c= 13.717 beta= 91.58
da=.008 db=.003 dc=.02 dbeta=.04
V= 1205
Triklin
Dexp Dcal d(D) h k l
6.3000 6.3166 -.0166 1 1 0
4.6600 4.6561 .0039 -1 1 1
4.5200 4.5102 .0098 -1 -1 1
4.3900 4.3893 .0007 1 1 1
3.4800 3.4824 -.0024 1 3 0
3.4300 3.4312 -.0012 2 0 0
3.2300 3.2324 -.0024 -2 0 1
3.1900 3.1909 -.0009 0 1 2
3.1600 3.1583 .0017 2 2 0
3.1300 3.1288 .0012 -2 1 0
3.0000 2.9998 .0002 0 2 2
2.7900 2.7900 .0000 2 2 1
2.7300 2.7297 .0003 0 4 1
2.5000 2.5001 -.0001 1 -3 1
A= 7.0193 DA= .0004
B= 11.3350 DB= .0003
C= 6.456 DC= .003
GAMMA= 81.94 DGAMMA= .05
BETA = 97.36 DBETA = .07
ALPHA= 79.40 DALPHA= .01
V=493.4
4. 22-0222
CoHPO4*1.5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.8000 7.7789 .0211 0 1 0
6.7000 6.6676 .0324 1 1 0
5.2600 5.2673 -.0073 0 1 1
4.3300 4.3149 .0151 3 0 0
3.8100 3.8000 .0100 2 1 1
3.7700 3.7733 -.0033 3 1 0
3.7200 3.7249 -.0049 1 2 0
3.6600 3.6587 .0013 -1 0 2
3.4700 3.4654 .0046 -2 0 2
3.2800 3.2725 .0075 1 0 2
3.1000 3.1043 -.0043 -3 0 2
3.0200 3.0165 .0035 1 1 2
a= 13.26 b= 7.779 c=7.331 beta= 102.484
da=.02 db=.003 dc=.007 dbeta=.001
V= 738
Triklin
Dexp Dcal d(D) h k l
7.8000 7.8066 -.0066 0 1 1
6.7000 6.7044 -.0044 0 -1 1
5.2600 5.2587 .0013 1 1 0
4.3300 4.3324 -.0024 1 1 1
3.8100 3.8101 -.0001 -1 0 2
3.7700 3.7710 -.0010 1 2 1
3.7200 3.7176 .0024 -1 3 0
3.6600 3.6636 -.0036 0 -3 1
3.4700 3.4693 .0007 -1 -1 2
3.2800 3.2820 -.0020 0 4 0
3.1000 3.1007 -.0007 1 -1 2
3.0200 3.0222 -.0022 -2 1 1
A= 6.1372 DA= .0001
B= 13.427 DB= .001
C= 8.876 DC= .003
GAMMA= 97.59 DGAMMA= .01
BETA =100.84 DBETA = .01
ALPHA= 79.33 DALPHA= .02
V= 702.4
5. 22-0244
C10H30Co6O21
Triklin
Dexp Dcal d(D) h k l
10.9000 10.9318 -.0318 0 1 1
10.4000 10.3946 .0054 1 1 1
10.1000 10.0918 .0082 1 1 0
9.8100 9.8263 -.0163 0 -1 1
9.5900 9.5800 .0100 -1 1 0
9.3500 9.3799 -.0299 1 0 2
9.0200 9.0090 .0110 1 -1 1
8.3500 8.3475 .0025 2 0 1
8.1200 8.1565 -.0365 1 1 2
7.7300 7.7331 -.0031 -1 -1 1
7.3800 7.3756 .0044 2 0 2
7.0500 7.0559 -.0059 1 -1 2
A= 16.819 DA= .008
B= 12.86 DB= .01
C= 19.37 DC= .01
GAMMA= 84.06 DGAMMA= .03
BETA = 67.308 DBETA = .009
ALPHA= 81.79 DALPHA= .08
V=3824
6. 22-0582
C10H16Co3O11
Triklin
Dexp Dcal d(D) h k l
11.9000 11.8810 .0190 1 0 0
10.4000 10.3988 .0012 0 -1 0
7.8300 7.8334 -.0034 0 -1 1
6.5300 6.5264 .0036 2 1 0
5.9200 5.9228 -.0028 0 0 2
5.7100 5.7056 .0044 -2 -1 1
5.2900 5.2864 .0036 -1 0 2
5.2000 5.1994 .0006 0 -2 0
4.3800 4.3763 .0037 -2 -1 2
4.1400 4.1396 .0004 -1 -2 2
4.1100 4.1106 -.0006 -3 -1 1
3.7400 3.7395 .0005 -1 0 3
A= 13.200 DA= .007
B= 11.553 DB= .003
C= 11.846 DC= .003
GAMMA= 64.17 DGAMMA= .02
BETA = 89.71 DBETA = .02
ALPHA= 90.12 DALPHA= .04
V= 1626.0
7. 22-0583
C14H22Co4O15*2H2O
Triklin
Dexp Dcal d(D) h k l
10.7000 10.6750 .0250 1 0 0
10.3000 10.3038 -.0038 0 1 1
8.6400 8.6281 .0119 0 -1 1
7.3000 7.3083 -.0083 1 1 0
7.1800 7.1738 .0062 -1 1 1
6.6000 6.5941 .0059 0 -1 2
6.5500 6.5360 .0140 -1 0 2
6.0600 6.0567 .0033 -1 1 2
4.9900 4.9920 -.0020 -1 1 3
4.8700 4.8703 -.0003 0 -2 1
4.6500 4.6494 .0006 0 2 3
4.5200 4.5210 -.0010 -1 2 2
A= 11.003 DA= .003
B= 10.8425 DB= .0007
C= 20.97 DC= .01
GAMMA= 90.46 DGAMMA= .04
BETA = 76.39 DBETA = .02
ALPHA= 78.24 DALPHA= .03
V=2377
8. 22-0584
{Co{NH3}4CO3}2SO4*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6500 5.6492 .0008 2 0 0
5.1200 5.1147 .0053 0 1 0
4.4700 4.4645 .0055 0 1 1
3.9200 3.9159 .0041 -3 0 1
3.4800 3.4847 -.0047 -1 1 2
3.1300 3.1297 .0003 2 0 2
3.0300 3.0327 -.0027 3 1 0
2.4200 2.4197 .0003 1 1 3
2.3300 2.3298 .0002 2 2 0
a= 11.832010 b= 5.11 c= 9.58 beta= 107.3
da=.05 db= .001 dc=.09 dbeta=.1
V= 554
22-0585
Co{NH3}4Cl3
Tetragon
Groupa 94
Dexp. Dcal. d(D) h k l
5.8100 5.7766 .0334 1 1 0
5.6500 5.6094 .0406 1 0 1
4.6300 4.6242 .0058 1 1 1
3.8300 3.8579 -.0279 0 0 2
3.6700 3.6534 .0166 2 1 0
3.6100 3.6100 -.0000 2 0 1
2.8700 2.8883 -.0183 2 2 0
2.1500 2.1466 .0034 3 1 2
1.8700 1.8698 .0002 3 0 3
a= 8.17 c= 7.72
da= .01 dc= .01
V= 514.9
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
5.8100 5.7953 .0147 1 0 1
5.6500 5.6482 .0018 1 1 0
4.6300 4.6250 .0050 1 1 1
3.8300 3.8246 .0054 1 0 2
3.6700 3.6647 .0053 2 1 0
3.6100 3.6108 -.0008 2 0 1
2.8700 2.8712 -.0012 0 1 3
2.1500 2.1500 .0000 -3 1 3
1.8700 1.8700 .0000 1 4 0
a= 8.4342 b= 7.675 c= 9.3909 beta= 98.49
da=.0002 db=.006 dc=.0004 dbet= .02
V=602.0
9. 22-0586
{Co{NH3}4CO3}Cl3
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
5.7600 5.7706 -.0106 2 0 0
3.5300 3.5181 .0119 0 1 0
3.0000 3.0039 -.0039 2 1 0
2.8800 2.8853 -.0053 4 0 0
2.4900 2.4880 .0020 3 0 2
2.4200 2.4122 .0078 3 1 1
2.0300 2.0313 -.0013 3 1 2
1.9300 1.9299 .0001 5 1 0
1.7600 1.7591 .0009 0 2 0
1.6800 1.6803 -.0003 1 2 1
1.5700 1.5695 .0005 2 0 4
a=11.54 b= 3.518 c= 6.524
da= .01 db= .005 dc= .003
V= 264.9
10. 22-0587
Co{NH3}4Cl3*H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
6.2200 6.2486 -.0286 0 2 0
5.1700 5.1455 .0245 1 2 0
4.5500 4.5345 .0155 2 0 0
4.2600 4.2626 -.0026 2 1 0
3.5900 3.5864 .0036 0 0 1
3.3400 3.3351 .0049 1 0 1
2.7400 2.7443 -.0043 2 1 1
a= 9.07 b=12.497 c= 3.59
da= .01 db= .002 dc= .01
v= 406
11. 22-0588
Co{NH3}4PO4
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
7.1100 7.1463 -.0363 1 1 0
4.9300 4.9290 .0010 2 1 0
4.1700 4.1692 .0008 0 1 1
3.6100 3.6008 .0092 3 1 0
3.5700 3.5732 -.0032 2 2 0
3.3900 3.4040 -.0140 2 1 1
3.1400 3.1329 .0071 1 2 1
2.5000 2.4982 .0018 4 0 1
2.2800 2.2809 -.0009 5 1 0
1.9500 1.9502 -.0002 3 4 0
a=11.791 b= 8.985 c= 4.707
da= .004 db= .007 dc= .004
V= 498.6
12. 22-0589
Co0.5Cd0.5GeO3
Triklin
Dexp Dcal d(D) h k l
4.8500 4.8531 -.0031 0 1 1
4.4300 4.4248 .0052 0 -1 1
3.8100 3.8044 .0056 -1 1 1
3.4300 3.4277 .0023 1 1 1
3.3200 3.3272 -.0072 1 2 0
3.0200 3.0212 -.0012 1 -2 1
2.9100 2.9070 .0030 0 3 1
2.6100 2.6103 -.0003 0 1 2
2.5800 2.5832 -.0032 1 3 0
2.5500 2.5488 .0012 -2 2 0
2.5000 2.5004 -.0004 1 -3 1
2.4600 2.4617 -.0017 -2 1 1
A= 5.461 DA= .006
B= 9.951 DB= .007
C= 5.2916 DC= .0005
GAMMA=100.31 DGAMMA= .09
BETA = 92.21 DBETA = .06
ALPHA= 83.39 DALPHA= .02
V= 281.0
13. 22-0589
Co0.5Cd0.5GeO3
Triklin
Dexp Dcal d(D) h k l
4.8500 4.8447 .0053 0 1 0
4.4300 4.4357 -.0057 -1 0 1
3.8100 3.8166 -.0066 0 -1 2
3.4300 3.4286 .0014 1 1 0
3.3200 3.3206 -.0006 -1 1 1
3.0200 3.0239 -.0039 0 0 3
2.9100 2.9096 .0004 0 -1 3
2.6100 2.6137 -.0037 -2 0 1
2.5800 2.5804 -.0004 1 -2 1
2.5500 2.5495 .0005 1 -2 2
2.5000 2.4999 .0001 0 -2 1
2.4600 2.4589 .0011 1 -1 4
A= 6.444 DA= .009
B= 5.224 DB= .002
C= 9.967 DC= .002
GAMMA=106.83 DGAMMA= .09
BETA = 69.967 DBETA = .007
ALPHA=108.80 DALPHA= .9
V= 292
14. 22-0595
C8H12Co3)9
triklin
Dexp Dcal d(D) h k l
11.6000 11.5487 .0513 1 0 0
8.6100 8.5924 .0176 1 1 0
6.2800 6.2812 -.0012 0 0 1
5.9200 5.9312 -.0112 1 1 1
5.7800 5.7743 .0057 2 0 0
4.9800 4.9796 .0004 1 2 0
4.8400 4.8472 -.0072 -1 1 1
4.2900 4.2962 -.0062 2 2 0
4.1300 4.1311 -.0011 2 2 1
3.9200 3.9258 -.0058 3 1 0
3.8500 3.8496 .0004 3 0 0
3.7700 3.7722 -.0022 -2 -1 1
A= 12.08 DA= .02
B= 10.53 DB= .02
C= 6.560 DC= .004
GAMMA= 73.9 DGAMMA= .1
BETA = 80.35 DBETA = .06
ALPHA= 74.22 DALPHA= .05
V= 767
15. 22-1080
C4H6CoO4*2H2O
Triklin
Dexp Dcal d(D) h k l
8.6400 8.6335 .0065 1 0 0
6.5500 6.5391 .0109 0 1 0
6.3100 6.3093 .0007 -1 0 1
5.1500 5.1483 .0017 1 -1 1
4.5100 4.5054 .0046 -1 1 1
4.2900 4.2873 .0027 -1 0 2
3.7000 3.7020 -.0020 2 -1 1
3.6000 3.6002 -.0002 2 0 2
3.5500 3.5557 -.0057 0 0 3
3.4600 3.4552 .0048 1 0 3
3.2600 3.2629 -.0029 0 -1 3
3.2200 3.2191 .0009 1 -1 3
A= 8.736 DA= .002
B= 6.589 DB= .001
C= 10.828 DC= .009
GAMMA= 94.22 DGAMMA= .03
BETA = 81.893 DBETA = .009
ALPHA= 96.24 DALPHA= .01
V= 612.4
16. 22-1220
K3Co{CN}5
Triklin
Dexp Dcal d(D) h k l
7.8500 7.8515 -.0015 1 0 0
7.0400 7.0372 .0028 -1 1 0
3.9000 3.9043 -.0043 1 -1 1
3.7800 3.7796 .0004 -1 0 1
3.6900 3.6909 -.0009 2 1 0
3.4900 3.4884 .0016 -1 -1 1
3.1900 3.1886 .0014 2 0 1
3.0700 3.0718 -.0018 2 -1 1
2.9370 2.9357 .0013 2 2 1
2.8540 2.8546 -.0006 -2 1 1
2.7610 2.7623 -.0013 -1 4 1
2.6760 2.6779 -.0019 -1 -3 1
A= 7.9264 DA= .0005
B= 13.704 DB= .003
C= 4.702 DC= .006
GAMMA= 93.556 DGAMMA= .008
BETA = 83.61 DBETA = .01
ALPHA= 81.219 DALPHA= .005
V= 500.0
17. 22-1578
C8H12BaCoN4O6*6H2O
Triklin
Dexp Dcal d(D) h k l
10.6000 10.5613 .0387 1 0 0
8.3400 8.3580 -.0180 1 1 0
7.2300 7.2397 -.0097 -1 0 1
6.5100 6.5132 -.0032 0 -1 1
5.8700 5.8719 -.0019 -1 1 1
5.3700 5.3769 -.0069 1 2 0
5.0600 5.0573 .0027 2 1 0
4.7700 4.7670 .0030 -1 -2 1
4.3100 4.3093 .0007 -1 2 1
4.1500 4.1490 .0010 1 2 1
3.8700 3.8702 -.0002 -1 -1 2
3.5200 3.5204 -.0004 3 0 0
A= 11.0468 DA= .0002
B= 11.69 DB= .02
C= 8.0857 DC= .0007
GAMMA= 82.07 DGAMMA= .07
BETA =105.40 DBETA = .09
ALPHA= 92.97 DALPHA= .09
V= 996.9
18. 22-1649
C12H22CoO6
Triklin
Dexp Dcal d(D) h k l
10.5000 10.5135 -.0135 1 0 0
9.7200 9.6214 .0986 0 1 0
5.9500 5.9845 -.0345 0 0 1
5.4000 5.4091 -.0091 1 0 1
4.8200 4.8250 -.0050 -1 1 1
4.6000 4.5870 .0130 1 1 1
4.1500 4.1462 .0038 -1 -1 1
3.7900 3.7880 .0020 -2 0 1
3.4800 3.4819 -.0019 1 2 1
3.4000 3.4004 -.0004 2 -2 1
3.0500 3.0505 -.0005 3 1 0
2.9600 2.9597 .0003 -1 3 1
A= 10.9065 DA= .0005
B= 9.96894 DB= .00009
C= 6.0159 DC= .0002
GAMMA=104.608 DGAMMA= .002
BETA = 85.896 DBETA = .002
ALPHA= 87.0114 DALPHA= .0007
V=629.6
19. 22-1651
C20H16Cl3CoN4*2H2O
Triklin
Dexp Dcal d(D) h k l
13.0000 12.9583 .0417 1 0 0
12.1000 12.1245 -.0245 0 1 0
9.0000 9.0192 -.0192 -1 1 0
8.7000 8.6964 .0036 1 1 0
6.8800 6.8825 -.0025 0 1 1
5.9900 5.9887 .0013 -1 1 1
5.8000 5.8031 -.0031 -2 1 0
5.5600 5.5697 -.0097 -1 2 0
5.2400 5.2459 -.0059 -2 0 1
4.6700 4.6690 .0010 0 2 1
4.4900 4.4896 .0004 0 -2 2
4.3200 4.3194 .0006 3 0 0
A= 13.028 DA= .003
B= 12.596 DB= .001
C= 10.4419 DC= .0002
GAMMA= 93.498 DGAMMA= .007
BETA = 84.48 DBETA = .03
ALPHA=105.59 DALPHA= .08
V= 1641.6
20. 22-1652
C20H16Cl3CoN4O4
Triklin
Dexp Dcal d(D) h k l
9.7100 9.7153 -.0053 1 0 0
9.1100 9.1197 -.0097 -1 1 0
7.2500 7.2604 -.0104 0 1 1
5.8300 5.8293 .0007 -1 2 0
5.4700 5.4694 .0006 1 1 1
5.1800 5.1813 -.0013 -2 1 0
4.2500 4.2499 .0001 2 0 1
3.9900 3.9902 -.0002 -1 3 0
3.5700 3.5698 .0002 1 1 2
3.1200 3.1199 .0001 -3 1 1
2.6600 2.6599 .0001 -3 4 1
A= 10.399 DA= .001
B= 12.5178 DB= .0009
C= 7.7469 DC= .0008
GAMMA=110.190 DGAMMA= .006
BETA = 90.79 DBETA = .01
ALPHA= 73.080 DALPHA= .004
V= 901.3
21. 22-1653
C20H21Cl4CoN4O2
Triklin
Dexp Dcal d(D) h k l
9.6000 9.5866 .0134 1 0 0
7.8100 7.8226 -.0126 0 1 0
7.3200 7.3473 -.0273 -1 0 1
6.9700 6.9480 .0220 1 0 1
6.1600 6.1477 .0123 0 1 1
5.8300 5.8375 -.0075 -1 1 1
5.3400 5.3487 -.0087 0 0 2
4.9900 4.9760 .0140 -1 -1 1
4.5400 4.5390 .0010 0 -1 2
4.4700 4.4689 .0011 -2 0 1
4.2400 4.2403 -.0003 2 -1 1
3.9100 3.9113 -.0013 0 2 0
A= 9.9336 DA= .0001
B= 8.1064 DB= .0001
C= 10.7251 DC= .0001
GAMMA=104.8583 DGAMMA= .0001
BETA = 92.4570 DBETA = .0001
ALPHA= 92.5721 DALPHA= .0001
V=832.8
22. 22-1654
C3H8Br2CoN2S
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.2600 7.2610 -.0010 1 1 1
6.1100 6.1074 .0026 -1 1 1
3.9500 3.9473 .0027 3 0 0
3.8300 3.8299 .0001 3 1 1
3.7000 3.6987 .0013 1 3 1
3.5300 3.5317 -.0017 -2 0 2
3.4700 3.4699 .0001 1 1 3
3.3600 3.3620 -.0020 3 2 1
2.9900 2.9903 -.0003 -1 3 2
2.5000 2.4997 .0003 -2 2 3
a= 12.21 b=12.157 c=10.877 beta= 75.82
da=.04 db=.003 dc=.004 dbeta=.05
V= 1565.9
23. 22-1655
CH4Cl2CoO
Monoklin
Dexp Dcal d(D) h k l
8.4000 8.3989 .0011 1 1 0
7.2400 7.2378 .0022 0 1 1
5.5200 5.5186 .0014 -1 1 1
3.5000 3.4998 .0002 3 1 1
2.9400 2.9395 .0005 -1 4 1
2.8450 2.8442 .0008 3 2 2
2.0720 2.0720 .0000 2 2 4
1.9600 1.9603 -.0003 0 5 3
1.7920 1.7921 -.0001 6 0 0
1.7300 1.7298 .0002 -3 4 3
a= 11.063 b= 13.451 c=8.835 beta= 76.383
da=.001 db=.002 dc=.004 dbeta=.005
V= 1278
22-1657
C2H8Cl2O2
Triklin
Dexp Dcal d(D) h k l
7.7000 7.7048 -.0048 0 1 0
5.5800 5.5815 -.0015 -1 -1 1
4.6600 4.6593 .0007 0 -1 2
4.3900 4.3927 -.0027 -1 -2 1
3.5500 3.5514 -.0014 1 -1 2
3.2600 3.2591 .0009 -1 0 2
3.0600 3.0582 .0018 2 2 0
2.8800 2.8815 -.0015 -1 -2 3
2.8000 2.8001 -.0001 -1 2 0
2.6800 2.6805 -.0005 2 2 1
2.6200 2.6194 .0006 -1 -3 3
2.5400 2.5402 -.0002 2 1 2
A= 6.682 DA= .003
B= 9.342 DB= .001
C= 9.3823 DC= .0001
GAMMA= 67.63 DGAMMA= .02
BETA = 93.410 DBETA = .004
ALPHA=116.11 DALPHA= .01
V= 482.2
24. 22-1658
C3H8Cl2CoN2S
Triklin
Dexp Dcal d(D) h k l
7.5500 7.5276 .0224 1 0 0
7.0000 6.9924 .0076 -1 1 0
5.9700 6.0003 -.0303 0 0 1
5.3100 5.3066 .0034 0 -1 1
4.0100 4.0124 -.0024 1 1 1
3.8300 3.8286 .0014 -2 1 0
3.7600 3.7638 -.0038 2 0 0
3.6700 3.6773 -.0073 -1 3 0
3.4500 3.4520 -.0020 -1 -2 1
3.3000 3.3008 -.0008 -2 0 1
3.1000 3.0967 .0033 1 -3 1
3.0000 3.0002 -.0002 0 0 2
A= 7.7346 DA= .0001
B= 11.47 DB= .02
C= 6.0172 DC= .0009
GAMMA=102.6 DGAMMA= .1
BETA = 94.268 DBETA = .001
ALPHA= 89.54 DALPHA= .02
V= 519.5
25. 22-1659
C8H14BrCoN4O6*xH2O
Triklin
Dexp Dcal d(D) h k l
6.4200 6.3971 .0229 0 0 1
6.1100 6.1110 -.0010 1 -1 1
5.3400 5.3416 -.0016 1 0 1
4.4400 4.4458 -.0058 0 1 1
4.0900 4.0893 .0007 -1 2 0
4.0200 4.0203 -.0003 -1 0 1
3.7300 3.7288 .0012 -1 -1 1
3.5600 3.5608 -.0008 -1 1 1
3.4100 3.4099 .0001 0 -1 2
3.2000 3.1986 .0014 0 0 2
3.1400 3.1418 -.0018 0 -2 2
3.0400 3.0393 .0007 0 -3 1
2.9700 2.9698 .0002 1 -3 2
A= 7.287 DA= .006
B= 9.9530 DB= .0005
C= 7.453 DC= .001
GAMMA=112.884 DGAMMA= .008
BETA = 66.27 DBETA = .02
ALPHA=116.722 DALPHA= .002
V=426.7
26. 22-1660
C8H14ClCoN4O6*H2O
Triklin
Dexp Dcal d(D) h k l
10.0000 9.9808 .0192 1 0 0
8.7500 8.7064 .0436 0 1 0
8.2600 8.2992 -.0392 0 0 1
5.9700 5.9662 .0038 -1 -1 1
5.8100 5.8106 -.0006 0 1 1
5.1600 5.1579 .0021 -1 1 1
4.7900 4.7897 .0003 1 -1 1
4.7200 4.7216 -.0016 -2 0 1
4.3500 4.3532 -.0032 0 2 0
4.1500 4.1496 .0004 0 0 2
3.9700 3.9692 .0008 0 -2 1
3.8500 3.8504 -.0004 0 -1 2
3.6500 3.6495 .0005 0 1 2
A= 10.296 DA= .002
B= 8.815 DB= .006
C= 8.5162 DC= .0004
GAMMA= 81.92 DGAMMA= .02
BETA =102.36 DBETA = .01
ALPHA= 95.56 DALPHA= .01
V= 745.7
27. 22-1661
C16H28CoN4)10S*xH2O
Triklin
Dexp Dcal d(D) h k l
9.5400 9.4744 .0656 1 0 0
8.6900 8.7789 -.0889 0 1 0
7.9700 7.9429 .0271 0 0 1
6.9500 6.9939 -.0439 -1 1 0
6.4500 6.4387 .0113 0 -1 1
5.9700 5.9543 .0157 -1 0 1
5.7400 5.7378 .0022 1 -1 1
5.4700 5.4612 .0088 0 1 1
4.9800 4.9907 -.0107 -1 -1 1
4.8600 4.8672 -.0072 -1 1 1
4.6000 4.6064 -.0064 1 1 1
4.4000 4.3895 .0105 0 2 0
A= 9.6122 DA= .0001
B= 9.01944 DB= .00001
C= 8.07327 DC= .00005
GAMMA= 99.3632 DGAMMA= .0004
BETA = 85.84393 DBETA = .00004
ALPHA= 99.98145 DALPHA= .00002
V=679.5
28. 22-1662
C20H16Cl3CoN4O4
Triklin
Dexp Dcal d(D) h k l
9.7100 9.7268 -.0168 1 0 0
9.1100 9.0956 .0144 1 1 0
7.2500 7.2489 .0011 0 0 1
5.8300 5.8310 -.0010 0 1 1
5.4700 5.4702 -.0002 1 1 1
5.1800 5.1815 -.0015 1 2 0
4.2500 4.2479 .0021 -1 -2 1
3.9900 3.9911 -.0011 -2 -2 1
3.5700 3.5701 -.0001 -1 2 0
3.1200 3.1201 -.0001 -2 -3 1
2.6600 2.6599 .0001 -1 2 2
A= 11.04 DA= .04
B= 10.36 DB= .03
C= 7.3135 DC= .0005
GAMMA= 62.7 DGAMMA= .2
BETA = 97.12 DBETA = .01
ALPHA= 90.84 DALPHA= .01
V= 737.3
29. 22-1668
C48H33Cl8Co3N8*Hcl
Triklin
Dexp Dcal d(D) h k l
15.2000 15.2174 -.0174 1 0 0
10.5000 10.5007 -.0007 0 1 0
9.7800 9.7486 .0314 0 1 1
8.7300 8.7325 -.0025 -1 0 1
8.2300 8.2440 -.0140 1 0 1
7.7500 7.7335 .0165 -1 1 0
6.1100 6.1078 .0022 0 -1 1
5.2800 5.2842 -.0042 -2 -1 1
4.9200 4.9181 .0019 1 2 2
4.6000 4.5999 .0001 -1 2 0
4.3900 4.3893 .0007 -2 1 2
4.1300 4.1312 -.0012 -2 2 1
4.0200 4.0190 .0010 1 3 1
3.8600 3.8613 -.0013 1 3 2
3.5500 3.5496 .0004 -4 -1 1
A= 15.818 DA= .004
B= 12.108 DB= .006
C= 11.368 DC= .007
GAMMA= 74.56 DGAMMA= .01
BETA = 86.43 DBETA = .01
ALPHA= 64.13 DALPHA= .02
V= 1884.6
30. 22-1669
C24H16Cl3CoN4*4H2O
Triklin
Dexp Dcal d(D) h k l
10.1000 10.1006 -.0006 1 0 0
8.3000 8.2841 .0159 -1 1 0
7.6000 7.6164 -.0164 1 1 1
7.4000 7.3855 .0145 1 1 0
6.7400 6.7367 .0033 -1 1 1
6.1300 6.1310 -.0010 0 2 0
5.8700 5.8524 .0176 1 1 2
5.1800 5.1865 -.0065 2 0 1
4.9900 4.9896 .0004 1 2 0
4.8500 4.8478 .0022 -1 1 2
4.7400 4.7422 -.0022 -1 0 2
4.4900 4.4892 .0008 2 1 0
A= 10.4969 DA= .0003
B= 12.694 DB= .001
C= 13.208 DC= .001
GAMMA= 92.997 DGAMMA= .006
BETA = 75.666 DBETA = .005
ALPHA= 76.560 DALPHA= .001
V=1646
31. 22-1670
C12H8Cl3CoN2O4*3H2O
Triklin
Dexp Dcal d(D) h k l
9.8000 9.8395 -.0395 1 0 0
8.5000 8.4946 .0054 0 1 1
7.3800 7.3663 .0137 0 -1 1
6.3900 6.3896 .0004 -1 -1 1
5.5900 5.5826 .0074 1 2 1
5.1000 5.1034 -.0034 2 1 0
4.7900 4.7904 -.0004 1 1 2
4.5400 4.5387 .0013 0 -1 2
4.4200 4.4187 .0013 -2 -1 1
4.1700 4.1719 -.0019 1 3 0
3.6600 3.6599 .0001 2 2 2
3.4800 3.4797 .0003 -2 -1 2
3.2800 3.2798 .0002 3 0 0
2.4900 2.4901 -.0001 -1 0 4
A= 10.314 DA= .004
B= 12.77 DB= .01
C= 10.523 DC= .003
GAMMA= 72.65 DGAMMA= .03
BETA = 85.54 DBETA = .03
ALPHA= 80.83 DALPHA= .04
V= 1305.7
32. 22-1671
C48H32Cl8Co3N8*1.5H2O
Triklin
Dexp Dcal d(D) h k l
12.3000 12.3216 -.0216 1 0 0
8.0800 8.0632 .0168 -1 1 0
7.6100 7.6101 -.0001 0 0 1
6.6400 6.6332 .0068 1 -1 1
5.7300 5.7412 -.0112 -1 -1 1
5.5700 5.5670 .0030 1 1 1
5.1500 5.1484 .0016 1 2 0
4.3100 4.3071 .0029 -2 -1 1
4.2200 4.2204 -.0004 2 2 0
4.0600 4.0609 -.0009 0 2 1
3.9800 3.9805 -.0005 3 0 1
3.8500 3.8496 .0004 -2 1 1
3.6600 3.6598 .0002 3 1 1
A= 12.603 DA= .005
B= 11.40 DB= .01
C= 7.989 DC= .004
GAMMA= 90.14 DGAMMA= .06
BETA = 78.171 DBETA = .007
ALPHA=103.03 DALPHA= .06
V= 1093.4
33. 22-1672
C4h4CoO4
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
9.5000 9.5691 -.0691 0 0 1
8.7500 8.7648 -.0148 2 0 0
4.6100 4.6157 -.0057 1 0 2
4.3700 4.3824 -.0124 4 0 0
3.5100 3.5059 .0041 5 0 0
2.8000 2.7997 .0003 3 0 3
2.6500 2.6501 -.0001 0 1 0
2.5540 2.5539 .0001 0 1 1
2.3080 2.3079 .0001 2 0 4
a=17.53 b= 2.65006 c= 9.569
da= .02 db= .00006 dc= .001
V= 444.5
34. 22-1673
C4H4CoO4*4H2O
Triklin
Dexp Dcal d(D) h k l
7.3400 7.3372 .0028 -1 0 1
6.8500 6.8269 .0231 1 1 0
5.4200 5.4117 .0083 0 0 2
5.3300 5.3309 -.0009 0 -2 1
5.2000 5.1935 .0065 -1 -2 1
4.5600 4.5596 .0004 -1 -2 2
4.1700 4.1667 .0033 -1 1 2
4.1000 4.1021 -.0021 -1 2 0
3.7800 3.7821 -.0021 1 -1 2
3.7000 3.7001 -.0001 -1 0 3
3.6700 3.6697 .0003 0 -3 1
3.5500 3.5521 -.0021 -1 -3 2
A= 8.282 DA= .004
B= 11.440 DB= .007
C= 11.8027 DC= .0002
GAMMA= 75.53 DGAMMA= .01
BETA =109.80 DBETA = .04
ALPHA=106.79 DALPHA= .05
V=993.1