1.
Co
Triklin
Dexp Dcal d(D) h k l
6.8000 6.8148 -.0148 1 0 0
4.8800 4.8873 -.0073 1 1 1
4.3500 4.3448 .0052 -1 -1 1
4.1300 4.1286 .0014 -1 1 1
3.9000 3.9006 -.0006 0 0 2
3.6500 3.6509 -.0009 0 1 2
3.4200 3.4178 .0022 1 1 2
3.0500 3.0499 .0001 -1 1 2
2.8400 2.8404 -.0004 2 2 0
2.6800 2.6798 .0002 2 1 2
2.6000 2.6004 -.0004 0 0 3
2.4200 2.4200 -.0000 -2 2 0
A= 6.9299 DA= .0006
B= 8.238 DB= .001
C= 7.86451 DC= .00008
GAMMA= 80.295 DGAMMA= .001
BETA = 85.157 DBETA = .001
ALPHA= 83.848 DALPHA= .003
V=438.9
2. 1-0110
C4H6CoO4*4H2O
Triklin
Dexp Dcal d(D) h k l
6.9000 6.9027 -.0027 1 0 0
6.0000 5.9900 .0100 1 -1 0
4.7900 4.7937 -.0037 -1 0 1
4.4500 4.4464 .0036 0 -1 1
4.2200 4.2305 -.0105 0 1 2
4.0500 4.0636 -.0136 1 1 1
3.8200 3.8116 .0084 1 1 0
3.1800 3.1818 -.0018 0 -1 2
3.6000 3.5975 .0025 1 1 2
3.0500 3.0485 .0015 0 1 3
2.9000 2.8994 .0006 1 1 3
2.7100 2.7103 -.0003 2 0 3
A= 7.818 DA= .004
B= 6.802 DB= .001
C= 9.574 DC= .002
GAMMA=111.77 DGAMMA= .07
BETA = 77.59 DBETA = .03
ALPHA= 79.44 DALPHA= .02
V=442.2
2. 1-0120
Co3{AsO4}2*8H2O
Triklin
Dexp Dcal d(D) h k l
8.0000 8.0206 -.0206 1 1 0
6.7000 6.6986 .0014 -1 1 0
4.4800 4.4763 .0037 1 1 2
3.2400 3.2393 .0007 3 1 2
3.0100 3.0125 -.0025 -3 1 0
2.7300 2.7292 .0008 -1 3 2
2.5500 2.5488 .0012 2 4 0
2.4700 2.4698 .0002 -1 4 0
2.3400 2.3403 -.0003 -2 -2 2
2.2100 2.2088 .0012 1 2 4
2.1000 2.1002 -.0002 3 1 4
1.9700 1.9700 .0000 4 -2 2
A= 10.830 DA= .002
B= 11.702 DB= .007
C= 8.966 DC= .004
GAMMA= 73.14 DGAMMA= .05
BETA = 68.71 DBETA = .04
ALPHA= 68.05 DALPHA= .04
V= 966.0
3. 1-0121
Co3{PO4}2*8H2O
Triklin
Dexp Dcal d(D) h k l
8.0000 8.0046 -.0046 0 0 1
6.7000 6.6964 .0036 1 0 0
4.8700 4.8695 .0005 0 -2 1
4.5100 4.5080 .0020 1 1 1
4.0400 4.0417 -.0017 -1 2 0
3.8100 3.8093 .0007 -1 0 2
3.6000 3.6006 -.0006 0 -3 1
3.1900 3.1929 -.0029 2 2 0
2.9500 2.9504 -.0004 -2 -1 2
2.6900 2.6906 -.0006 -2 2 0
2.6000 2.5995 .0005 -2 -3 2
2.5000 2.5008 -.0008 -2 -4 1
A= 7.014 DA= .002
B= 12.061 DB= .001
C= 8.233 DC= .001
GAMMA= 77.65 DGAMMA= .01
BETA =103.162 DBETA = .002
ALPHA= 95.810 DALPHA= .007
V= 661.5
4. 1-0148
Na3Co{NO2}6
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
6.1000 6.1651 -.0651 1 1 0
5.0000 5.0007 -.0007 0 1 1
3.9100 3.9072 .0028 1 2 0
3.0800 3.0825 -.0025 2 2 0
2.5000 2.5004 -.0004 0 2 2
2.4100 2.4149 -.0049 3 2 0
2.1000 2.0993 .0007 3 0 2
1.9500 1.9473 .0027 3 3 1
1.8000 1.8024 -.0024 1 2 3
1.6700 1.6669 .0031 0 3 3
1.6700 1.6712 -.0012 5 0 1
1.5400 1.5413 -.0013 4 4 0
a= 8.689 b= 8.75 c= 6.0944
da= .007 db= .01 dc= .0005
V= 463
Triklin
Dexp Dcal d(D) h k l
6.1000 6.1255 -.0255 0 0 1
5.0000 5.0009 -.0009 1 0 1
3.9100 3.9103 -.0003 1 1 1
3.0800 3.0799 .0001 -1 -1 1
2.5000 2.5005 -.0005 2 0 2
2.4100 2.4109 -.0009 1 2 0
2.1000 2.1006 -.0006 3 0 2
1.9500 1.9501 -.0001 -2 2 3
1.8000 1.8000 -.0000 -3 3 2
1.6700 1.6698 .0002 -1 -1 3
1.5400 1.5400 .0000 -2 -2 2
1.5400 1.5400 .0000 -2 -2 2
A= 9.03738 DA= .00007
B= 6.0078 DB= .0002
C= 6.5273 DC= .0001
GAMMA=106.6421 DGAMMA= .0001
BETA = 95.6787 DBETA = .0002
ALPHA= 69.7960 DALPHA= .0002
V=318.7
5. 1-0180
Co{NH3}5*Cl3
Triklin
Dexp Dcal d(D) h k l
6.7000 6.7005 -.0005 1 0 0
6.1000 6.1054 -.0054 0 1 0
5.7000 5.6969 .0031 0 -1 1
5.2000 5.2044 -.0044 1 1 0
4.7500 4.7509 -.0009 -1 -1 1
4.0800 4.0755 .0045 0 0 2
3.9200 3.9254 -.0054 0 -1 2
3.5000 3.4966 .0034 -1 -1 2
3.2900 3.2871 .0029 1 -1 2
3.0800 3.0828 -.0028 1 2 0
2.9900 2.9820 .0080 1 1 2
2.8000 2.7955 .0045 -1 -2 2
A= 6.92107 DA= .00007
B= 6.53159 DB= .00004
C= 8.48177 DC= .00006
GAMMA= 76.4969 DGAMMA= .0002
BETA = 88.5139 DBETA = .0003
ALPHA=105.1714 DALPHA= .00031
V=358.1
6. 1-0193
CoCl2*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.6000 5.5882 .0118 2 0 0
4.8500 4.8605 -.0105 1 1 0
3.5200 3.5150 .0050 -1 1 2
3.1100 3.1067 .0033 -2 1 2
2.9400 2.9356 .0044 3 0 2
2.7300 2.7293 .0007 1 1 3
2.5600 2.5632 -.0032 -2 1 3
2.4000 2.4013 -.0013 4 0 2
2.2000 2.2002 -.0002 -2 2 2
2.0700 2.0701 -.0001 -5 0 2
2.0200 2.0192 .0008 -3 2 2
1.9800 1.9796 .0004 -2 2 3
a= 11.18 b= 5.3976 c= 10.013 beta= 92.15
da=.01 db=.0003 dc=.001 dbeta=.02
V= 604.0
Triklin
Dexp Dcal d(D) h k l
5.6000 5.6001 -.0001 1 0 0
4.8500 4.8566 -.0066 1 1 1
3.5200 3.5207 -.0007 -1 -1 1
3.1100 3.1125 -.0025 0 0 2
2.9400 2.9405 -.0005 1 -1 1
2.7300 2.7309 -.0009 1 2 2
2.5600 2.5597 .0003 -1 -2 1
2.4000 2.4012 -.0012 -1 1 2
2.2000 2.1979 .0021 -2 -2 1
2.0700 2.0694 .0006 2 3 0
2.0200 2.0193 .0007 1 0 3
1.9800 1.9811 -.0011 3 2 0
A= 6.283 DA= .005
B= 6.912 DB= .007
C= 6.593 DC= .003
GAMMA= 63.73 DGAMMA= .06
BETA = 76.60 DBETA = .04
ALPHA= 71.80 DALPHA= .03
V= 242.4
7. 1-0258
CoF2*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.8900 4.8868 .0032 2 1 0
4.1000 4.1040 -.0040 0 2 1
3.8000 3.7947 .0053 -3 0 1
3.5800 3.5793 .0007 2 2 0
3.1600 3.1593 .0007 0 0 3
2.9800 2.9820 -.0020 -2 0 3
2.7600 2.7595 .0005 4 1 0
2.5600 2.5611 -.0011 -4 1 2
2.4500 2.4517 -.0017 1 3 2
2.3200 2.3191 .0009 -1 1 4
2.2400 2.2404 -.0004 4 1 2
2.1600 2.1593 .0007 1 4 1
a= 11.735 b= 9.106 c= 9.602 beta= 99.23
da=.007 b=.006 dc=.001 dbeta=.03
V= 1012
Triklin
Dexp Dcal d(D) h k l
4.8900 4.9000 -.0100 1 0 0
4.1000 4.0970 .0030 1 1 1
3.8000 3.8028 -.0028 1 -1 1
3.5800 3.5821 -.0021 0 -1 1
3.1600 3.1677 -.0077 -1 2 0
2.9800 2.9855 -.0055 1 2 1
2.7600 2.7593 .0007 1 -2 1
2.5600 2.5598 .0002 2 1 1
2.4500 2.4500 -.0000 2 0 0
2.3200 2.3183 .0017 -1 3 0
2.2400 2.2398 .0002 0 2 2
2.1600 2.1592 .0008 2 2 1
A= 5.584 DA= .001
B= 7.460 DB= .002
C= 5.4741 DC= .0003
GAMMA= 93.34 DGAMMA= .06
BETA = 62.82 DBETA = .03
ALPHA= 79.25 DALPHA= .05
V=196.2
8. 1-0296
C2CoO4*2H2O
Triklin
Dexp Dcal d(D) h k l
4.7300 4.7282 .0018 1 0 0
3.9000 3.9021 -.0021 0 1 2
3.6000 3.6041 -.0041 0 -1 2
2.9500 2.9496 .0004 1 0 2
2.6500 2.6518 -.0018 1 2 0
2.5500 2.5474 .0026 0 -2 2
2.2300 2.2299 .0001 1 2 2
2.1600 2.1597 .0003 0 3 0
2.0800 2.0813 -.0013 -2 1 3
2.0200 2.0206 -.0006 0 3 2
1.8900 1.8892 .0008 1 0 4
1.7800 1.7799 .0001 1 3 2
A= 4.8820 DA= .0002
B= 6.50709 DB= .00001
C= 9.50673 DC= .00005
GAMMA= 92.2322 DGAMMA= .0001
BETA =104.401 DBETA = .001
ALPHA= 84.7859 DALPHA= .0002
V=291.2
9. 1-0317
Co{NO3}2*6H2O
Triklin
Dexp Dcal d(D) h k l
6.7000 6.7043 -.0043 0 1 1
5.8000 5.7965 .0035 1 0 0
5.5000 5.4973 .0027 0 -1 1
4.6000 4.5975 .0025 -1 2 0
3.8800 3.8815 -.0015 -1 0 1
3.7000 3.6992 .0008 -1 2 1
3.5000 3.5000 -.0000 1 1 2
3.2900 3.2889 .0011 1 -1 2
3.1600 3.1590 .0010 0 -1 2
3.0500 3.0496 .0004 2 0 1
2.9300 2.9298 .0002 -1 -2 1
2.8200 2.8202 -.0002 -2 2 0
A= 6.175 DA= .001
B= 12.269 DB= .009
C= 7.4885 DC= .0009
GAMMA= 97.118 DGAMMA= .009
BETA = 72.852 DBETA = .003
ALPHA= 79.862 DALPHA= .00239
V= 524.2
10. 1-0373
Co3{PO4}2
Triklin
Dexp Dcal d(D) h k l
4.3300 4.3309 -.0009 -1 1 1
4.0900 4.0976 -.0076 2 0 1
3.8500 3.8517 -.0017 -1 -1 1
3.4400 3.4405 -.0005 -2 1 1
3.2100 3.2178 -.0078 2 0 2
3.0000 2.9980 .0020 0 0 3
2.9000 2.9001 -.0001 -2 1 2
2.7800 2.7782 .0018 -3 1 0
2.6000 2.6012 -.0012 -1 2 0
2.5100 2.5132 -.0032 2 0 3
2.4200 2.4210 -.0010 -3 -1 1
2.3000 2.3000 .0000 4 0 0
A= 9.2504 DA= .0005
B= 5.29953 DB= .00008
C= 9.01 DC= .01
GAMMA= 96.00 DGAMMA= .01
BETA = 90.32 DBETA = .09
ALPHA= 86.28 DALPHA= .01
V=438.9
11. 1-0468
Co{C2H3O2}2*4H2O
Rombik
Groupa 33,49,62
Dexp. Dcal. d(D) h k l
6.8000 6.8208 -.0208 1 1 0
4.8800 4.8903 -.0103 2 1 0
4.3500 4.3389 .0111 1 1 1
4.1300 4.1269 .0031 2 0 1
3.9000 3.9026 -.0026 1 2 0
3.6500 3.6350 .0150 3 1 0
3.4200 3.4104 .0096 2 2 0
3.0500 3.0527 -.0027 3 1 1
2.8400 2.8502 -.0102 4 1 0
2.6800 2.6797 .0003 1 3 0
2.6000 2.5995 .0005 1 1 2
2.4200 2.4191 .0009 1 3 1
a=12.15 b= 8.2419 c= 5.623
da= .01 db= .0007 dc= .003
V= 563
Triklin
Dexp Dcal d(D) h k l
6.8000 6.8148 -.0148 1 0 0
4.8800 4.8873 -.0073 1 1 1
4.3500 4.3448 .0052 -1 -1 1
4.1300 4.1286 .0014 -1 1 1
3.9000 3.9006 -.0006 0 0 2
3.6500 3.6509 -.0009 0 1 2
3.4200 3.4178 .0022 1 1 2
3.0500 3.0499 .0001 -1 1 2
2.8400 2.8404 -.0004 2 2 0
2.6800 2.6798 .0002 2 1 2
2.6000 2.6004 -.0004 0 0 3
2.4200 2.4200 -.0000 -2 2 0
A= 6.9299 DA= .0006
B= 8.238 DB= .001
C= 7.86451 DC= .00008
GAMMA= 80.295 DGAMMA= .001
BETA = 85.157 DBETA = .001
ALPHA= 83.848 DALPHA= .003
V=438.9
12. 1-0474
Co{NH3}6I3
Triklin
Dexp Dcal d(D) h k l
3.8600 3.8679 -.0079 0 1 0
3.1400 3.1395 .0005 0 -1 2
2.7100 2.7079 .0021 1 -1 1
2.5100 2.5080 .0020 -1 0 1
2.2200 2.2188 .0012 1 -1 3
1.9200 1.9202 -.0002 1 -2 1
1.7200 1.7196 .0004 -1 1 3
1.5700 1.5697 .0003 0 -2 4
1.4600 1.4598 .0002 0 1 5
1.3600 1.3597 .0003 2 0 2
1.2800 1.2798 .0002 -1 -1 5
1.2200 1.2200 .0000 1 -1 7
A= 2.9246 DA= .0003
B= 4.151 DB= .001
C= 8.769 DC= .0004
GAMMA=108.90 DGAMMA= .01
BETA = 78.463 DBETA = .002
ALPHA=103.07 DALPHA= .01
V= 97.2
13. 1-0522
Co{NH3}6Cl3
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8050 -.0050 1 0 0
5.3000 5.2991 .0009 0 1 1
4.9800 4.9600 .0200 1 -1 1
3.6000 3.5980 .0020 1 1 1
3.4700 3.4691 .0009 1 0 3
3.1500 3.1548 -.0048 2 -1 1
3.0200 3.0207 -.0007 1 -2 1
2.9300 2.9319 -.0019 0 2 0
2.6300 2.6284 .0016 -2 0 1
2.4800 2.4800 -.0000 2 -2 2
2.3600 2.3627 -.0027 0 -1 4
2.3000 2.3006 -.0006 2 1 0
A= 6.416 DA= .001
B= 6.262 DB= .001
C= 11.058 DC= .005
GAMMA=110.164 DGAMMA= .004
BETA = 75.015 DBETA = .004
ALPHA= 91.414 DALPHA= .009
V= 401.9
14. 1-0619
CoSO4*H2O
Triklin
Dexp Dcal d(D) h k l
4.8200 4.8260 -.0060 -1 1 1
3.8000 3.7991 .0009 1 1 0
3.4000 3.4009 -.0009 -1 2 0
3.3000 3.2994 .0006 0 2 0
3.0800 3.0799 .0001 -2 0 1
2.5700 2.5715 -.0015 -1 -2 1
2.5100 2.5098 .0002 -2 -1 1
2.4000 2.3990 .0010 2 1 0
2.3500 2.3497 .0003 0 -1 3
2.2000 2.1996 .0004 0 3 0
2.1000 2.1005 -.0005 2 1 1
2.0500 2.0500 .0000 0 3 1
A= 6.5290 DA= .0003
B= 6.9999 DB= .0007
C= 7.663 DC= .001
GAMMA=108.69 DGAMMA= .01
BETA =107.69 DBETA = .01
ALPHA= 89.52527 DALPHA= .00003
V=314.4
15. 1-1126
CoMn2O4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.8500 4.8513 -.0013 -1 1 1
4.3800 4.3789 .0011 -2 0 1
3.9000 3.8960 .0040 -1 0 2
2.9900 2.9921 -.0021 3 0 0
2.7100 2.7095 .0005 -3 0 2
2.4800 2.4812 -.0012 2 2 1
2.3100 2.3124 -.0024 1 0 3
2.0400 2.0395 .0005 -2 2 3
1.7500 1.7499 .0001 -1 3 3
1.6900 1.6901 -.0001 3 1 3
1.6000 1.5989 .0011 -1 4 2
1.5700 1.5698 .0002 4 2 2
a= 9.27 b= 7.01318 c=7.923 beta= 104.4
da=.02 db=.00006 dc= .008 dbeta=.01
V= 498.7
Triklin
Dexp Dcal d(D) h k l
4.8500 4.8522 -.0022 -1 0 1
4.3800 4.3812 -.0012 0 1 1
3.9000 3.8954 .0046 0 -1 1
2.9900 2.9924 -.0024 0 2 0
2.7100 2.7117 -.0017 -2 2 1
2.4800 2.4801 -.0001 2 1 0
2.3100 2.3094 .0006 -2 2 2
2.0400 2.0404 -.0004 -3 2 0
1.7500 1.7501 -.0001 1 3 0
1.6900 1.6904 -.0004 0 2 3
1.6000 1.5997 .0003 -2 4 1
1.5700 1.5700 .0000 4 0 0
A= 6.9349 DA= .0001
B= 6.4458 DB= .0004
C= 5.9922 DC= .0001
GAMMA=110.80 DGAMMA= .01
BETA =107.61 DBETA = .02
ALPHA= 77.78 DALPHA= .01
V= 237.1
16. 1-1137
Co2SnO4
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
3.4000 3.3914 .0086 3 0 1
2.6700 2.6707 -.0007 4 0 1
2.4500 2.4530 -.0030 0 0 3
2.0200 2.0201 -.0001 2 1 0
1.7700 1.7708 -.0008 2 1 2
1.5600 1.5594 .0006 2 1 3
1.4300 1.4307 -.0007 6 1 0
1.2300 1.2297 .0003 7 1 2
1.0800 1.0793 .0007 0 2 0
1.0600 1.0607 -.0007 2 2 0
.8500 .8500 .0000 12 1 2
a=11.464 b= 2.1586 c= 7.3589
da= .001 db= .0003 dc= .0009
V= 182.11
17. 1-1145
CoB2O4
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
2.8800 2.8800 .0000 3 0 1
2.5300 2.5359 -.0059 1 1 1
2.4400 2.4352 .0048 4 0 0
2.0800 2.0787 .0013 0 0 3
2.0300 2.0329 -.0029 1 0 3
1.8600 1.8595 .0005 5 0 1
1.7500 1.7507 -.0007 3 0 3
1.6500 1.6522 -.0022 5 0 2
1.6000 1.5998 .0002 4 1 2
1.5600 1.5590 .0010 0 0 4
1.4300 1.4322 -.0022 1 2 0
1.3700 1.3727 -.0027 0 1 4
a= 9.741 b= 2.896 c= 6.236
da= .002 db= .004 dc= .003
V= 175.9
18. 1-1254
Co
Rombik
Groupa 50
Dexp. Dcal. d(D) h k l
2.1600 2.1597 .0003 0 2 3
2.0400 2.0397 .0003 2 0 2
1.9200 1.9231 -.0031 1 3 0
1.7700 1.7676 .0024 0 0 5
1.4800 1.4797 .0003 1 4 1
1.2500 1.2500 -.0000 3 2 3
1.1500 1.1497 .0003 4 0 0
1.0700 1.0700 .0000 3 4 2
1.0500 1.0501 -.0001 4 2 2
1.0200 1.0199 .0001 4 0 4
.9500 .9502 -.0002 2 2 8
.8500 .8501 -.0001 4 0 7
a= 4.59873 b= 6.351 c= 8.838
da= .00001 db= .001 dc= .003
V= 258.1
Triklin
Dexp Dcal d(D) h k l
2.1600 2.1598 .0002 -2 0 1
2.0400 2.0401 -.0001 1 1 0
1.9200 1.9199 .0001 0 1 1
1.7700 1.7698 .0002 2 1 0
1.4800 1.4797 .0003 3 1 0
1.2500 1.2500 .0000 -3 0 2
1.1500 1.1504 -.0004 4 0 2
1.0700 1.0696 .0004 4 1 2
1.0500 1.0500 .0000 5 1 0
1.0200 1.0200 -.0000 2 2 0
.9500 .9498 .0002 -4 -1 2
.8500 .8499 .0001 1 -2 2
A= 5.8713 DA= .0007
B= 2.15324 DB= .00002
C= 3.4714 DC= .0002
GAMMA= 86.395 DGAMMA= .009
BETA = 85.92 DBETA = .01
ALPHA= 82.797 DALPHA= .003
V= 43.36
19. 1-1255
Co
Geks.
Groupa 184,192
Dexp. Dcal. d(D) h k l
2.0400 2.0398 .0002 2 2 0
1.7700 1.7697 .0003 2 2 2
1.2500 1.2503 -.0003 4 2 2
1.0700 1.0697 .0003 3 2 5
1.0200 1.0199 .0001 4 4 0
.8900 .8902 -.0002 6 3 0
.8100 .8102 -.0002 3 1 8
.7900 .7901 -.0001 7 3 1
.7200 .7201 -.0001 4 4 7
.6800 .6799 .0001 6 6 0
a= 8.159 c= 7.118
da=.001 dc=.002
V= 410.36
Triklin
Dexp Dcal d(D) h k l
2.0400 2.0400 .0000 1 1 0
1.7700 1.7700 .0000 -1 0 1
1.2500 1.2500 .0000 -1 -2 1
1.0700 1.0700 .0000 -2 2 0
1.0200 1.0200 .0000 2 2 0
.8900 .8900 .0000 1 0 2
.8100 .8100 .0000 2 3 1
.7900 .7900 .0000 -3 1 0
.7200 .7200 .0000 -1 6 1
.6800 .6800 .0000 3 3 0
A= 2.45414 DA= .00001
B= 4.42338 DB= .00001
C= 2.18688 DC= .00001
GAMMA= 95.8211 DGAMMA= .0002
BETA =103.2116 DBETA = .0002
ALPHA= 78.0056 DALPHA= .0003
V= 22.57
20. 2-0214
CoO{OH}
monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.0200 5.0244 -.0044 -1 0 1
4.5500 4.5498 .0002 1 1 0
2.6100 2.6098 .0002 -3 0 1
2.4800 2.4793 .0007 3 0 1
2.3600 2.3597 .0003 2 0 2
2.0300 2.0302 -.0002 -4 0 1
1.8400 1.8398 .0002 -2 2 2
1.6000 1.5998 .0002 0 2 3
1.5300 1.5300 .0000 5 1 1
1.4500 1.4499 .0001 1 0 4
1.3800 1.3801 -.0001 5 1 2
1.2300 1.2303 -.0003 0 4 2
a= 8.4515 b= 5.4039 c= 5.9689 beta= 93.798
da=.0009 db= .0004 dc=.0005 dbeta=.003
V= 272.0
21. 2-0925
alfa-Co{OH}2
Triklin
Dexp Dcal d(D) h k l
4.6600 4.6595 .0005 0 1 0
4.0000 4.0000 .0000 1 0 1
2.7400 2.7392 .0008 0 -1 2
2.6800 2.6809 -.0009 0 0 2
2.3700 2.3703 -.0003 1 0 2
2.0000 2.0000 .0000 2 0 2
1.7800 1.7797 .0003 3 -1 2
1.5800 1.5800 -.0000 3 2 0
1.5300 1.5300 .0000 0 2 2
1.5000 1.5000 .0000 -4 0 3
1.3500 1.3500 .0000 1 -1 4
1.3100 1.3099 .0001 2 2 2
A= 8.064 DA= .002
B= 4.9735 DB= .0002
C= 5.76180 DC= .00005
GAMMA= 97.96 DGAMMA= .01
BETA =100.36 DBETA = .01
ALPHA=106.928 DALPHA= .006
V= 212.96
22. 2-0962
{Co,Ni}As2
Triklin
Dexp Dcal d(D) h k l
6.0000 6.0001 -.0001 1 0 0
4.2000 4.1912 .0088 0 1 1
3.4000 3.3992 .0008 0 -1 1
2.9000 2.8992 .0008 1 1 2
2.6200 2.6200 -.0000 2 1 1
2.2200 2.2223 -.0023 1 2 1
2.0700 2.0698 .0002 -3 0 1
1.9500 1.9510 -.0010 0 0 4
1.8700 1.8703 -.0003 -2 0 4
1.7700 1.7696 .0004 -1 2 3
1.6900 1.6901 -.0001 2 -1 2
1.6300 1.6303 -.0003 -3 1 3
A= 6.3874 DA= .0002
B= 4.512 DB= .001
C= 8.220 DC= .001
GAMMA= 76.44 DGAMMA= .01
BETA =101.67 DBETA = .01
ALPHA= 79.26 DALPHA= .01
V=218.6
23. 2-1119
Co8O6Cl4*7H2O
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
5.6000 5.6098 -.0098 1 0 1
2.7700 2.7687 .0013 -1 1 2
2.6900 2.6889 .0011 -1 0 3
2.2900 2.2897 .0003 3 0 0
2.1000 2.0990 .0010 -1 0 4
1.9500 1.9486 .0014 -2 1 3
1.8300 1.8305 -.0005 -1 2 2
1.7100 1.7100 .0000 3 1 3
1.5400 1.5400 .0000 3 2 1
1.4600 1.4600 .0000 -2 1 5
a= 6.87995 b=4.2260 c= 8.99244 beta= 86.7719
da=.00002 db=.0001 dc=.00003 dbet=.0002
V=261.1
24. 2-1198
Co4W2C
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
3.9400 3.9416 -.0016 0 1 2
2.7600 2.7591 .0009 0 0 4
2.5200 2.5177 .0023 1 0 0
2.2500 2.2502 -.0002 1 1 1
2.1200 2.1218 -.0018 1 1 2
1.9500 1.9493 .0007 1 1 3
1.5400 1.5400 .0000 0 2 6
1.4300 1.4299 .0001 1 2 5
1.3400 1.3399 .0001 0 1 8
1.3000 1.3002 -.0002 1 1 7
a= 2.5177 b= 5.632 c=11.036
da= .0007 db= .005 dc= .005
V= 156.5
25. 2-1201
{Co,Mg}O
Geksagon
Groupa 185,188,193
Dexp. Dcal. d(D) h k l
2.4400 2.4404 -.0004 1 1 0
2.1100 2.1099 .0001 1 1 1
1.4900 1.4894 .0006 2 0 2
1.2700 1.2714 -.0014 2 1 2
1.2200 1.2202 -.0002 2 2 0
1.0500 1.0497 .0003 0 0 4
.9700 .9697 .0003 3 2 0
.9400 .9401 -.0001 2 0 4
a= 4.881 c= 4.1988
da=.003 dc= .0004
V= 86.6
26. 2-1393
Co2TiO4
Rombik
Groupa 36,40,63
Dexp. Dcal. d(D) h k l
2.9900 2.9904 -.0004 0 0 2
2.5500 2.5451 .0049 1 1 1
2.4300 2.4336 -.0036 1 2 0
2.1000 2.1023 -.0023 0 4 0
1.7200 1.7198 .0002 0 4 2
1.6270 1.6264 .0006 1 1 3
1.4920 1.4921 -.0001 2 0 0
1.4270 1.4269 .0001 1 3 3
1.3350 1.3352 -.0002 2 0 2
1.2870 1.2863 .0007 2 3 1
1.2730 1.2725 .0005 2 2 2
1.2170 1.2168 .0002 2 4 0
a= 2.9843 b= 8.409 c= 5.981
da= .0006 db= .002 dc= .001
V= 150.1
27. 3-0105
CoSO4*4H2O
Triklin
Dexp Dcal d(D) h k l
6.7500 6.7378 .0122 0 1 1
5.5000 5.4975 .0025 -1 1 1
4.7500 4.7478 .0022 0 -1 1
4.4000 4.3895 .0105 1 -1 1
3.9000 3.9003 -.0003 -1 -1 1
3.6000 3.5993 .0007 -1 1 2
3.3700 3.3689 .0011 0 2 2
3.2000 3.2001 -.0001 -2 2 1
2.9500 2.9512 -.0012 1 -1 2
2.7000 2.6996 .0004 1 -3 0
2.5400 2.5403 -.0003 0 2 3
2.3800 2.3803 -.0003 -2 3 2
A= 8.4449 DA= .0001
B= 8.68993 DB= .00004
C= 7.9539 DC= .0001
GAMMA= 99.4703 DGAMMA= .0008
BETA = 90.2247 DBETA = .0005
ALPHA= 70.5304 DALPHA= .0002
V=542.1
28. 3-0731
Co3S4
Triklin
Dexp Dcal d(D) h k l
3.3500 3.3507 -.0007 1 0 0
2.8200 2.8206 -.0006 -1 1 1
2.3800 2.3807 -.0007 -1 -1 1
1.9100 1.9098 .0002 0 0 2
1.8200 1.8202 -.0002 1 -2 1
1.6800 1.6800 -.0000 1 1 1
1.4400 1.4398 .0002 -2 -1 2
1.3700 1.3701 -.0001 2 -2 1
1.2300 1.2300 .0000 0 3 1
1.1700 1.1699 .0001 -3 2 0
1.0900 1.0900 -.0000 -3 0 3
1.0600 1.0600 .0000 0 -4 1
A= 3.85330 DA= .00006
B= 4.45991 DB= .00003
C= 4.19640 DC= .00005
GAMMA=107.554 DGAMMA= .002
BETA =111.804 DBETA = .005
ALPHA= 93.623 DALPHA= .005
V= 62.6
29. 4-0226
{NH4}3H6{Co{NoO4}6}*7H2O
Triklin
Dexp Dcal d(D) h k l
5.8600 5.8605 -.0005 1 0 0
5.2100 5.2135 -.0035 0 1 0
3.7200 3.7197 .0003 0 -1 2
3.4200 3.4195 .0005 1 1 1
3.0700 3.0691 .0009 1 -1 3
2.8600 2.8598 .0002 0 1 3
2.6600 2.6607 -.0007 -2 0 1
2.6000 2.5998 .0002 0 0 4
2.2700 2.2700 -.0000 -2 2 0
1.8500 1.8500 .0000 3 -2 2
1.7800 1.7799 .0001 -2 -1 3
1.7400 1.7401 -.0001 1 -1 6
1.5300 1.5300 -.0000 -1 -3 1
A= 6.28071 DA= .00005
B= 5.4294 DB= .0004
C= 10.7460 DC= .001
GAMMA=106.179 DGAMMA= .002
BETA = 75.446 DBETA = .007
ALPHA= 95.111 DALPHA= .007
V= 340.6
30. 4-0647
{NH4}3H5{Co{OH}{MoO4}5}*3H2O
Triklin
Dexp Dcal d(D) h k l
8.4100 8.4181 -.0081 0 1 0
6.9600 6.9607 -.0007 1 0 0
3.9300 3.9281 .0019 0 -1 2
3.7600 3.7564 .0036 -1 -1 2
3.5800 3.5829 -.0029 1 0 2
3.4500 3.4504 -.0004 1 1 2
3.3200 3.3184 .0016 -1 2 0
3.0100 3.0097 .0003 -2 1 0
2.4500 2.4491 .0009 -1 -2 3
2.3200 2.3202 -.0002 3 0 0
2.0900 2.0900 .0000 1 -3 2
2.0300 2.0298 .0002 2 2 3
A= 7.1565 DA= .0006
B= 8.594 DB= .002
C= 9.051 DC= .001
GAMMA= 78.469 DGAMMA= .003
BETA = 96.82 DBETA = .01
ALPHA= 90.15 DALPHA= .02
V= 541.4
31. 4-0848
Co2Si
Geksagon
Groupa 184,192
Dexp. Dcal. d(D) h k l
2.0500 2.0490 .0010 3 0 0
2.0000 2.0012 -.0012 2 1 1
1.9700 1.9697 .0003 0 0 2
a= 7.098 c= 3.94
da=.004 dc= .01
V= 171.9
32. 5-0029
C63H88CoN14O13P
Triklin
Dexp Dcal d(D) h k l
16.1000 16.1216 -.0216 1 0 0
13.0000 12.9895 .0105 0 1 0
12.2000 12.1803 .0197 1 0 1
11.4000 11.4163 -.0163 1 -1 1
9.7000 9.7143 -.0143 -1 0 1
8.8700 8.8750 -.0050 1 1 0
7.5700 7.5869 -.0169 -1 -1 1
7.1900 7.2027 -.0127 1 0 2
6.7500 6.7867 -.0367 -1 2 0
6.4200 6.4243 -.0043 2 -2 1
5.8300 5.8364 -.0064 0 1 2
5.2700 5.2929 -.0229 3 -2 1
4.9500 4.9505 -.0005 -3 2 0
A= 17.770 DA= .004
B= 14.224 DB= .001
C= 15.406 DC= .001
GAMMA=111.437 DGAMMA= .005
BETA = 72.36 DBETA = .02
ALPHA=106.43 DALPHA= .03
V=3388
33. 5-0706
sigma-CrCo
Triklin
Dexp Dcal d(D) h k l
4.0100 4.0068 .0032 1 2 0
3.6200 3.6191 .0009 1 0 1
2.6200 2.6206 -.0006 -1 -2 2
2.3600 2.3589 .0011 1 0 2
2.2600 2.2619 -.0019 -2 -2 2
2.2000 2.1991 .0009 2 2 1
2.1500 2.1510 -.0010 -1 4 0
2.1280 2.1265 .0015 -1 3 2
2.0660 2.0652 .0008 -2 2 2
2.0140 2.0141 -.0001 -2 3 0
1.9620 1.9610 .0010 -1 -4 2
1.9260 1.9265 -.0005 -3 -2 1
A= 5.978 DA= .001
B= 9.942 DB= .001
C= 6.116 DC= .001
GAMMA= 81.73 DGAMMA= .01
BETA =106.12 DBETA = .01
ALPHA= 92.137 DALPHA= .001
V=345.6
34. 6-0491
LaCoO3
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
3.8200 3.8238 -.0038 1 0 1
2.7210 2.7194 .0016 0 2 0
2.6810 2.6868 -.0058 2 0 1
2.2130 2.2161 -.0031 1 2 1
2.1780 2.1801 -.0021 3 0 0
1.9110 1.9112 -.0002 2 2 1
1.7190 1.7184 .0006 1 2 2
1.7010 1.7009 .0001 3 2 0
1.5680 1.5640 .0040 2 2 2
1.5680 1.5658 .0022 4 1 0
1.5450 1.5447 .0003 4 0 1
1.3600 1.3597 .0003 0 4 0
a= 6.5402 b= 5.4387 c= 4.713
da= .0007 db= .0001 dc= .002
V= 167.6
Triklin
Dexp Dcal d(D) h k l
3.8200 3.8213 -.0013 -1 0 1
2.7210 2.7200 .0010 -1 -1 1
2.6810 2.6814 -.0004 -1 0 2
2.2130 2.2127 .0003 0 -1 2
2.1780 2.1798 -.0018 -1 1 2
1.9110 1.9113 -.0003 0 2 0
1.7190 1.7182 .0008 -1 -2 1
1.7010 1.7007 .0003 -1 2 1
1.5680 1.5673 .0007 1 -2 1
1.5450 1.5454 -.0004 -1 2 2
1.3600 1.3591 .0009 1 -2 2
1.3430 1.3427 .0003 -2 2 2
A= 4.1145 DA= .0008
B= 3.823 DB= .001
C= 5.729 DC= .001
GAMMA= 89.495 DGAMMA= .009
BETA =110.10 DBETA = .06
ALPHA= 90.84 DALPHA= .03
V= 84.6
35. 6-0595
Co2P
Triklin
Dexp Dcal d(D) h k l
2.8500 2.8551 -.0051 1 1 0
2.7310 2.7295 .0015 -1 -1 1
2.2250 2.2246 .0004 -1 -1 3
2.1620 2.1622 -.0002 0 -1 4
2.1010 2.0999 .0011 2 1 0
2.0590 2.0593 -.0003 1 -1 4
1.8780 1.8784 -.0004 0 -1 5
1.8370 1.8369 .0001 -1 1 5
1.8220 1.8223 -.0003 3 0 1
1.7720 1.7721 -.0001 3 0 2
1.7570 1.7565 .0005 2 -1 4
1.7420 1.7419 .0001 -1 -1 5
A= 5.5013 DA= .0007
B= 3.4378 DB= .0007
C= 11.610 DC= .001
GAMMA= 92.31 DGAMMA= .01
BETA = 87.05 DBETA = .02
ALPHA= 87.38 DALPHA= .01
V=219.0
36. 7-0049
Cr-Co-Mo
Triklin
Dexp Dcal d(D) h k l
2.5290 2.5295 -.0005 -3 1 0
2.4730 2.4723 .0007 1 -1 1
2.3370 2.3372 -.0002 2 1 1
2.2910 2.2904 .0006 1 -2 1
2.2380 2.2385 -.0005 4 2 0
2.1710 2.1718 -.0008 -2 -1 1
2.1590 2.1591 -.0001 1 3 1
2.1060 2.1066 -.0006 4 0 0
2.0520 2.0523 -.0003 4 4 0
2.0050 2.0047 .0003 -1 5 0
1.9870 1.9869 .0001 -1 -4 1
1.9660 1.9659 .0001 0 -4 1
A= 8.994 DA= .001
B= 11.930 DB= .004
C= 2.61688 DC= .00009
GAMMA= 70.350 DGAMMA= .007
BETA = 85.03 DBETA = .02
ALPHA= 91.49 DALPHA= .02
V=263.0
37. 7-0056
Cr-Co-Mo
Triklin
Dexp Dcal d(D) h k l
2.5110 2.5094 .0016 1 2 0
2.3860 2.3859 .0001 3 1 1
2.3670 2.3681 -.0011 -1 -2 1
2.3040 2.3054 -.0014 0 -2 2
2.2530 2.2527 .0003 1 1 3
2.1850 2.1844 .0006 3 -1 3
2.1700 2.1700 -.0000 2 2 0
2.1170 2.1170 .0000 -1 0 3
2.0660 2.0642 .0018 -1 -2 2
2.0180 2.0189 -.0009 -2 -2 1
2.0020 2.0022 -.0002 3 -2 1
1.9800 1.9805 -.0005 2 0 4
A= 8.3311 DA= .0002
B= 5.4192 DB= .0001
C= 8.05036 DC= .00002
GAMMA= 94.632 DGAMMA= .001
BETA = 67.2353 DBETA = .0002
ALPHA= 98.249 DALPHA= .001
V=331.2
38. 9-0267
delta-Co1.3Ni4.1Mo4.6
Triklin
Dexp Dcal d(D) h k l
2.6790 2.6783 .0007 0 4 0
2.6600 2.6633 -.0033 -3 2 0
2.4280 2.4277 .0003 0 0 2
2.3840 2.3835 .0005 0 1 2
2.2040 2.2040 -.0000 -1 2 2
2.1920 2.1911 .0009 -1 5 0
2.1560 2.1564 -.0004 -2 -3 1
2.1420 2.1426 -.0006 0 5 0
2.1130 2.1135 -.0005 1 2 2
2.0840 2.0842 -.0002 -4 1 0
2.0560 2.0556 .0004 -4 2 0
2.0370 2.0370 -.0000 0 3 2
A= 8.3396 DA= .0007
B= 10.9738 DB= .0006
C= 4.8576 DC= .0006
GAMMA=102.398 DGAMMA= .009
BETA = 89.912 DBETA = .004
ALPHA= 88.30 DALPHA= .01
V=434.1
39. 10-0757
C6H25CoN6O7P2
Triklin
Dexp Dcal d(D) h k l
10.0000 9.9896 .0104 0 1 1
8.3000 8.3018 -.0018 1 1 0
7.6000 7.5919 .0081 0 -1 1
6.7000 6.6892 .0108 -1 0 1
6.0400 6.0410 -.0010 -1 1 0
5.4100 5.4142 -.0042 1 2 2
4.8100 4.8008 .0092 -1 0 2
4.3600 4.3610 -.0010 2 0 1
4.0000 3.9980 .0020 0 2 3
3.7400 3.7399 .0001 2 1 3
3.4600 3.4603 -.0003 -1 -3 1
3.1200 3.1207 -.0007 -2 1 2
2.9400 2.9400 .0000 2 4 3
A= 9.5805 DA= .0007
B= 12.817 DB= .003
C= 14.050 DC= .005
GAMMA= 67.23 DGAMMA= .02
BETA = 73.21 DBETA = .01
ALPHA= 69.51 DALPHA= .03
V= 1466.3
40. 10-0762
C6H26CoN6O10P3*2H2O
Triklin
Dexp Dcal d(D) h k l
12.0000 11.9581 .0419 1 0 0
9.4000 9.4229 -.0229 0 1 0
8.6000 8.6094 -.0094 0 0 1
7.8000 7.8019 -.0019 1 0 1
6.5100 6.5092 .0008 1 1 0
5.9200 5.9190 .0010 -2 1 0
5.3200 5.3141 .0059 0 1 1
4.7100 4.7114 -.0014 0 2 0
3.9400 3.9416 -.0016 -1 -1 2
3.8000 3.8050 -.0050 -1 0 2
3.6700 3.6704 -.0004 1 -3 2
3.5400 3.5387 .0013 0 2 1
A= 13.6454 DA= .0008
B= 11.661 DB= .002
C= 10.389 DC= .005
GAMMA=116.36 DGAMMA= .01
BETA = 66.788 DBETA = .005
ALPHA=122.080 DALPHA= .009
V= 1227.6
41. 10-0763
C6H25CoN6O7P2*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.3000 9.3413 -.0413 1 1 0
8.4000 8.3631 .0369 0 1 1
7.2000 7.2062 -.0062 1 0 1
6.5900 6.5972 -.0072 2 0 0
6.0600 6.0400 .0200 -2 1 1
5.7800 5.7536 .0264 -1 0 2
4.9900 4.9973 -.0073 0 1 2
4.7500 4.7373 .0127 -2 2 1
4.3400 4.3408 -.0008 -1 2 2
4.0100 4.0112 -.0012 -3 1 2
3.7000 3.6977 .0023 -2 3 1
3.6000 3.5983 .0017 0 0 3
a= 14.09 b= 13.223 c=11.53 beta=110.6
da=.01 db=.008 dc=.03 dbeta=.3
V= 2012
Triklin
Dexp Dcal d(D) h k l
9.3000 9.2884 .0116 0 1 1
8.4000 8.3776 .0224 0 -1 1
7.2000 7.1990 .0010 1 1 0
6.5900 6.5937 -.0037 -1 0 1
6.0600 6.0600 .0000 0 1 2
5.7800 5.7770 .0030 -1 1 1
4.9900 4.9964 -.0064 1 2 0
4.7500 4.7536 -.0036 -1 0 2
4.3400 4.3377 .0023 -1 -1 2
4.0100 4.0111 -.0011 0 -1 3
3.7000 3.7011 -.0011 -2 -1 1
3.6000 3.5995 .0005 2 2 0
A= 9.066 DA= .007
B= 11.836 DB= .006
C= 13.831 DC= .009
GAMMA= 85.33 DGAMMA= .07
BETA = 75.14 DBETA = .05
ALPHA= 83.07 DALPHA= .05
V= 1422.1
42. 11-0051
{Co{NH3}5{N3}}{N3}2
Triklin
Dexp Dcal d(D) h k l
6.3900 6.3905 -.0005 1 0 0
5.5200 5.5221 -.0021 -1 1 0
5.2600 5.2564 .0036 -1 0 1
5.0400 5.0387 .0013 1 1 0
4.0400 4.0433 -.0033 0 -1 2
3.6200 3.6209 -.0009 -1 -1 2
3.2500 3.2438 .0062 1 -1 2
3.1800 3.1841 -.0041 -1 2 1
3.1000 3.1019 -.0019 1 -2 2
3.0100 3.0123 -.0023 -2 -1 1
2.9000 2.8985 .0015 -1 3 0
2.7600 2.7610 -.0010 -2 2 0
A= 6.4703 DA= .0002
B= 10.094 DB= .003
C= 8.149 DC= .003
GAMMA= 92.46 DGAMMA= .01
BETA = 97.066 DBETA = .001
ALPHA=112.48 DALPHA= .03
V= 485.7
43. 11-0052
{Co{NH3}6}{N3}3
Triklin
Dexp Dcal d(D) h k l
6.2400 6.2592 -.0192 0 1 1
6.0200 6.0023 .0177 -1 0 1
5.8300 5.8238 .0062 0 -1 1
5.3800 5.3786 .0014 1 1 0
5.2200 5.2184 .0016 1 0 1
3.9100 3.9082 .0018 -1 2 0
3.7300 3.7269 .0031 -1 1 2
3.6700 3.6800 -.0100 0 -1 2
3.5800 3.5857 -.0057 1 2 0
3.4700 3.4741 -.0041 -2 1 1
3.3000 3.2972 .0028 2 1 0
3.1800 3.1762 .0038 -2 -1 1
A= 7.550 DA= .002
B= 8.7215 DB= .0008
C= 8.530 DC= .004
GAMMA= 96.34 DGAMMA= .08
BETA = 98.538 DBETA = .009
ALPHA= 85.01 DALPHA= .01
V=550.5
44. 11-0053
{Co{NH3}3{N3}3}
Triklin
Dexp Dcal d(D) h k l
7.3200 7.2912 .0288 1 0 0
6.3500 6.3793 -.0293 0 1 1
5.6000 5.5850 .0150 0 -1 1
5.0100 5.0228 -.0128 0 2 0
4.6100 4.6011 .0089 -1 0 1
4.2100 4.2137 -.0037 -1 1 1
3.9100 3.9064 .0036 0 -2 1
3.7200 3.7164 .0036 1 0 2
3.3500 3.3486 .0014 0 3 0
3.1900 3.1897 .0003 0 2 2
3.0800 3.0805 -.0005 2 1 2
2.9800 2.9818 -.0018 -1 0 2
A= 7.66 DA= .01
B= 10.26 DB= .01
C= 7.773 DC= .007
GAMMA= 81.31 DGAMMA= .09
BETA = 73.24 DBETA = .07
ALPHA= 79.94 DALPHA= .05
V= 572.6
45. 11-0054
Na3{Co{NH3}6*{N3}6}
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.5600 7.5782 -.0182 1 -1 0
6.0000 5.9795 .0205 0 0 1
5.6400 5.6395 .0005 0 2 0
4.8900 4.8851 .0049 1 0 1
4.4700 4.4795 -.0095 1 -1 1
4.1000 4.0981 .0019 0 -2 1
3.7900 3.7902 -.0002 2 2 0
3.6900 3.6888 .0012 1 -2 1
3.1800 3.1796 .0004 0 -3 1
3.1500 3.1509 -.0009 -3 0 1
2.9900 2.9898 .0002 0 0 2
2.8200 2.8197 .0003 0 4 0
A= 10.3280 DA= .0003
B= 11.279 DB= .002
C= 6.0342 DC= .0006
BETA = 97.72 DBETA = .02
V=696.8
Triklin
Dexp Dcal d(D) h k l
7.5600 7.5603 -.0003 1 0 0
6.0000 6.0020 -.0020 0 1 1
5.6400 5.6426 -.0026 -1 0 1
4.8900 4.8801 .0099 1 1 1
4.4700 4.4690 .0010 1 0 1
4.1000 4.1049 -.0049 0 -1 1
3.7900 3.7802 .0098 2 0 0
3.6900 3.6876 .0024 1 2 0
3.1800 3.1819 -.0019 1 -1 1
3.1500 3.1492 .0008 2 2 0
2.9900 2.9896 .0004 2 0 1
2.9000 2.8984 .0016 -1 -2 1
A= 8.0849 DA= .0009
B= 7.8362 DB= .0008
C= 7.0965 DC= .0004
GAMMA= 73.99 DGAMMA= .01
BETA = 97.200 DBETA = .008
ALPHA= 71.82 DALPHA= .01
V=399.4
46. 11-0167
{Co{NH3}4{N3}3}
Triklin
Dexp Dcal d(D) h k l
6.9000 6.9016 -.0016 1 1 0
6.5300 6.5452 -.0152 0 1 1
6.2000 6.1893 .0107 0 -1 1
5.7200 5.7155 .0045 -1 0 1
5.5200 5.5272 -.0072 1 0 2
5.1500 5.1454 .0046 -1 -1 1
4.7300 4.7209 .0091 1 -1 1
4.5800 4.5773 .0027 2 1 1
4.0500 4.0535 -.0035 2 0 0
3.8700 3.8724 -.0024 0 2 0
3.7300 3.7273 .0027 0 2 1
3.5900 3.5921 -.0021 0 -2 1
A= 9.30789 DA= .00001
B= 8.40323 DB= .00009
C= 12.0451 DC= .0003
GAMMA= 67.4147 DGAMMA= .0007
BETA = 67.955 DBETA = .001
ALPHA= 78.749 DALPHA= .001
V=805.4
47. 11-0168
{Co{NH3}4{N3}2}{N3}
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.6700 7.6823 -.0123 1 0 1
6.4300 6.3985 .0315 1 1 0
5.7900 5.7795 .0105 -2 0 1
5.5500 5.5142 .0358 0 0 2
4.4400 4.4374 .0026 0 1 2
4.2100 4.2026 .0074 2 1 1
4.0200 4.0257 -.0057 1 1 2
3.6700 3.6762 -.0062 0 0 3
3.5700 3.5702 -.0002 -3 0 2
3.2200 3.2215 -.0015 -3 1 2
2.8600 2.8591 .0009 4 1 0
2.7800 2.7811 -.0011 -1 0 4
a=12.519 b=7.475 c= 11.154 beta= 98.61
da=.004 db= .007 dc= 2.695 dbeta=.03
V= 1032
Triklin
Dexp Dcal d(D) h k l
7.6700 7.6752 -.0052 1 0 0
6.4300 6.4328 -.0028 0 -1 1
5.7900 5.7918 -.0018 1 0 1
5.5500 5.5594 -.0094 0 0 2
4.4400 4.4401 -.0001 -1 1 0
4.2100 4.2162 -.0062 1 -1 1
4.0200 4.0212 -.0012 -2 -1 1
3.6700 3.6695 .0005 0 -1 3
3.5700 3.5691 .0009 -1 -2 1
2.8600 2.8596 .0004 2 -1 1
2.8600 2.8596 .0004 2 -1 1
2.7800 2.7797 .0003 0 0 4
A= 8.311 DA= .003
B= 7.193 DB= .004
C= 12.058 DC= .007
GAMMA= 70.58 DGAMMA= .01
BETA =106.97 DBETA = .02
ALPHA=109.68 DALPHA= .07
V=626.1
48. 11-0422
Ca2Co{AsO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
6.4000 6.3978 .0022 0 0 1
5.6600 5.6680 -.0080 -1 -1 1
5.1200 5.1241 -.0041 0 -2 1
4.6800 4.6861 -.0061 -1 1 1
3.9800 3.9843 -.0043 0 -3 1
3.5900 3.5900 .0000 1 1 1
3.3800 3.3788 .0012 -1 0 2
3.2200 3.2202 -.0002 0 4 0
3.0800 3.0775 .0025 2 1 0
2.7500 2.7492 .0008 1 3 1
2.6100 2.6086 .0014 -1 -5 1
2.5200 2.5193 .0007 -1 4 1
A= 6.758 DA= .001
B= 13.389 DB= .003
C= 7.100 DC= .001
GAMMA= 80.13 DGAMMA= .01
BETA =112.6709 DBETA = .0009
ALPHA=105.19 DALPHA= .01
V= 570.3
49. 12-0113
Co{NH3}3{NO2}3
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
6.4200 6.3988 .0212 1 2 0
6.0300 6.0332 -.0032 2 0 0
5.8000 5.8058 -.0058 0 0 1
5.5800 5.6023 -.0223 2 1 0
5.2200 5.2317 -.0117 1 0 1
5.0100 5.0316 -.0216 0 3 0
4.6000 4.6018 -.0018 0 2 1
4.0400 4.0315 .0085 2 1 1
2.9300 2.9287 .0013 1 5 0
a=12.07 b=15.09 c= 5.8058
da= .01 db= .03 dc= .0003
V=1057
50. 12-0572
Co{NO3}2*6H2O
Triklin
Dexp Dcal d(D) h k l
6.6500 6.6485 .0015 0 1 1
6.0200 6.0238 -.0038 -1 -1 1
5.8500 5.8416 .0084 0 -1 1
5.6750 5.6751 -.0001 1 1 1
5.5750 5.5713 .0037 -1 1 1
5.4400 5.4456 -.0056 -1 1 0
4.6350 4.6332 .0018 -1 -1 2
4.6200 4.6187 .0013 1 0 2
3.8600 3.8608 -.0008 -2 1 2
3.7100 3.7073 .0027 -3 0 1
3.5100 3.5116 -.0016 3 0 0
3.4180 3.4188 -.0008 -2 -1 3
A= 11.3145 DA= .0001
B= 7.4481 DB= .0002
C= 12.737 DC= .001
GAMMA= 79.57 DGAMMA= .01
BETA =107.511 DBETA = .009
ALPHA= 85.303 DALPHA= .001
V=996
51. 13-0636
C12H42Co4N18O24
Triklin
13.8000 13.7729 .0271 1 0 0
12.8000 12.7975 .0025 0 1 0
10.6700 10.6915 -.0215 0 1 1
9.7000 9.6871 .0129 1 0 1
8.7800 8.7670 .0130 -1 1 0
7.6200 7.6332 -.0132 0 -1 1
6.3400 6.3237 .0163 2 0 1
5.7000 5.6919 .0081 -2 0 1
5.2700 5.2682 .0018 -2 1 1
4.5900 4.5910 -.0010 3 0 0
4.4800 4.4766 .0034 3 0 1
4.2900 4.2896 .0004 -2 0 2
A= 14.150 DA= .007
B= 13.800 DB= .002
C= 12.990 DC= .007
GAMMA= 78.73 DGAMMA= .02
BETA = 79.62 DBETA = .04
ALPHA= 69.58 DALPHA= .05631
V= 2313.8
52. 13-0735
C10H14CoO4
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
11.8000 11.6914 .1086 0 1 0
10.4000 10.3131 .0869 0 0 1
8.5100 8.5029 .0071 1 0 1
7.4700 7.5127 -.0427 2 0 0
6.8300 6.8766 -.0466 1 1 1
6.3500 6.3203 .0297 2 1 0
5.8600 5.8457 .0143 0 2 0
5.4000 5.3889 .0111 2 1 1
5.1000 5.0855 .0145 0 2 1
4.8100 4.8171 -.0071 1 2 1
3.5400 3.5427 -.0027 1 3 1
3.1600 3.1602 -.0002 4 2 0
a=15.025 b=11.69 c=10.313
da= .003 db= .01 dc= .005
V=1811
53. 13-0803
C32H36CoN4
Triklin
Dexp Dcal d(D) h k l
12.7000 12.6962 .0038 1 0 0
11.5000 11.4993 .0007 0 1 0
10.2000 10.2167 -.0167 0 -1 1
9.3400 9.3335 .0065 1 1 0
8.3100 8.3145 -.0045 1 0 1
7.0900 7.0985 -.0085 -1 1 1
6.6900 6.6869 .0031 -2 0 1
5.8100 5.8129 -.0029 0 -2 1
5.1100 5.1084 .0016 0 -2 2
4.5900 4.5887 .0013 -1 2 1
4.4800 4.4806 -.0006 -3 0 1
4.0600 4.0654 -.0054 -1 -3 1
A= 13.9427 DA= .0002
B= 12.228 DB= .002
C= 16.223 DC= .003
GAMMA= 74.80 DGAMMA= .01
BETA =112.56 DBETA = .07
ALPHA=107.50 DALPHA= .02
V=2395
54. 14-0086
CoMoO6*0.9H2O
Triklin
Dexp Dcal d(D) h k l
4.3100 4.3085 .0015 0 1 1
4.1900 4.1828 .0072 1 1 0
4.0300 4.0381 -.0081 0 -1 1
3.4200 3.4183 .0017 0 0 2
3.3200 3.3208 -.0008 1 -1 1
3.3200 3.3208 -.0008 1 -1 1
3.0600 3.0601 -.0001 -2 -1 1
2.9800 2.9770 .0030 2 1 0
2.8600 2.8629 -.0029 2 0 1
2.7300 2.7307 -.0007 1 0 2
2.5100 2.5098 .0002 0 2 1
2.4300 2.4300 .0000 1 2 0
A= 8.346 DA= .002
B= 5.299 DB= .002
C= 7.5163 DC= .0005
GAMMA= 96.22 DGAMMA= .01
BETA =114.278 DBETA = .005
ALPHA= 83.971 DALPHA= .009
V=300.5
55. 14-0087
Co1.2MoO4.2*1.3H2O
Triklin
Dexp Dcal d(D) h k l
9.2300 9.2582 -.0282 0 1 1
7.3300 7.3251 .0049 1 0 0
6.8600 6.8532 .0068 0 -1 1
5.1700 5.1649 .0051 1 -1 1
4.8000 4.7911 .0089 1 0 2
4.2700 4.2712 -.0012 -1 1 2
4.0000 4.0017 -.0017 1 -1 2
3.8000 3.8026 -.0026 0 0 3
3.6400 3.6403 -.0003 0 2 3
3.3700 3.3702 -.0002 -2 0 1
3.2900 3.2899 .0001 0 -1 3
3.1600 3.1603 -.0003 2 2 1
A= 7.391 DA= .004
B= 11.169 DB= .004
C= 12.036 DC= .002
GAMMA= 86.77 DGAMMA= .06
BETA = 82.39 DBETA = .05
ALPHA= 72.72 DALPHA= .01
V= 940.3
56. 14-0309
CoSO4
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7900 4.7835 .0065 -2 1 1
4.3300 4.3299 .0001 -4 0 1
4.1500 4.1488 .0012 3 1 2
3.9300 3.9265 .0035 5 0 2
3.6000 3.5999 .0001 -5 0 1
3.5200 3.5199 .0001 -4 0 2
3.3600 3.3636 -.0036 5 1 2
2.6400 2.6390 .0010 5 1 4
2.6000 2.5973 .0027 -3 0 4
2.5100 2.5117 -.0017 0 0 5
2.4500 2.4493 .0007 5 0 5
2.3400 2.3388 .0012 6 0 5
a= 21.113 b= 6.520 c= 13.0310 beta= 74.518
da=.001 db= .001 dc=.0001 dbeta=.0004
V= 1729
Triklin
Dexp Dcal d(D) h k l
4.7900 4.7898 .0002 1 0 0
4.3300 4.3312 -.0012 -1 1 1
4.1500 4.1511 -.0011 -1 -1 1
3.9300 3.9313 -.0013 0 -2 1
3.6000 3.5969 .0031 -1 2 0
3.5200 3.5201 -.0001 -1 -2 1
3.3600 3.3595 .0005 1 1 1
2.6400 2.6392 .0008 -1 3 2
2.6000 2.6015 -.0015 -1 4 1
2.5100 2.5102 -.0002 -2 0 1
2.4500 2.4496 .0004 -1 -4 1
2.3400 2.3395 .0005 1 1 2
A= 5.0402 DA= .0004
B= 12.446 DB= .009
C= 6.613 DC= .001
GAMMA= 88.121 DGAMMA= .007
BETA =107.31 DBETA = .02
ALPHA= 78.86 DALPHA= .02
V= 386.8
57. 14-0587
CoMoO4
Triklin
Dexp Dcal d(D) h k l
6.3300 6.3424 -.0124 1 0 0
5.5800 5.5803 -.0003 1 1 0
4.7500 4.7405 .0095 1 1 1
4.4600 4.4555 .0045 0 1 1
4.1300 4.1374 -.0074 -1 0 1
3.7700 3.7646 .0054 -1 1 0
3.5400 3.5523 -.0123 1 -1 1
3.3800 3.3812 -.0012 2 1 0
3.1500 3.1469 .0031 1 1 2
3.0600 3.0634 -.0034 1 2 1
2.7700 2.7662 .0038 -2 -1 1
2.4900 2.4881 .0019 2 -1 1
A= 7.065 DA= .001
B= 6.640 DB= .001
C= 6.961 DC= .001
GAMMA= 67.85 DGAMMA= .03
BETA = 75.54 DBETA = .04
ALPHA= 86.57 DALPHA= .06
V=292.7
58. 14-0718
C4H6CoO4*4H2O
Triklin
Dexp Dcal d(D) h k l
6.9000 6.9081 -.0081 0 1 1
6.0000 6.0071 -.0071 0 -1 1
4.7900 4.7864 .0036 0 2 0
4.4500 4.4582 -.0082 0 2 1
4.2200 4.2086 .0114 -1 1 0
4.0500 4.0553 -.0053 -1 0 1
3.8200 3.8103 .0097 -1 -1 1
3.6000 3.6064 -.0064 1 0 2
3.1800 3.1818 -.0018 -1 -2 1
3.0500 3.0495 .0005 1 -2 1
2.9000 2.9004 -.0004 1 3 0
2.7100 2.7100 .0000 1 3 2
A= 5.2064 DA= .0004
B= 9.8264 DB= .0004
C= 8.898 DC= .001
GAMMA= 79.687 DGAMMA= .005
BETA = 78.432 DBETA = .007
ALPHA= 80.190 DALPHA= .006
V=434.5
59. 14-0741
C2CoO4*2H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7300 4.7282 .0018 2 1 0
3.9000 3.9014 -.0014 -2 2 1
3.6000 3.6000 .0000 0 3 1
2.9500 2.9500 -.0000 -3 2 2
2.6500 2.6502 -.0002 3 0 2
2.5500 2.5499 .0001 0 4 2
2.2300 2.2303 -.0003 0 5 1
2.1600 2.1601 -.0001 -5 0 1
2.0800 2.0798 .0002 5 0 0
2.0200 2.0201 -.0001 -2 3 5
1.8900 1.8900 .0000 2 5 2
1.7800 1.7800 -.0000 1 1 6
a= 10.875 b= 11.3652 c= 12.089 beta=107.01
da=.002 db=.0007 dc=.001 dbeta=.02
V= 1429
Triklin
Dexp Dcal d(D) h k l
4.7300 4.7253 .0047 1 0 0
3.9000 3.9003 -.0003 1 1 1
3.6000 3.6030 -.0030 1 -1 1
2.9500 2.9494 .0006 -1 0 1
2.6500 2.6491 .0009 1 2 0
2.5500 2.5450 .0050 1 -2 1
2.2300 2.2308 -.0008 -2 1 0
2.1600 2.1588 .0012 0 2 2
2.0800 2.0785 .0015 0 3 1
2.0200 2.0175 .0025 1 3 1
1.8900 1.8913 -.0013 1 -3 1
1.7800 1.7796 .0004 -2 -1 1
A= 5.20368 DA= .00221
B= 6.51386 DB= .00210
C= 5.80615 DC= .00489
GAMMA= 88.01422 DGAMMA= .03906
BETA = 65.26112 DBETA = .03823
ALPHA= 83.25681 DALPHA= .05999
V=177.7
60. 14-0776
C3H21CoMo6O24*6H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.1500 5.1612 -.0112 2 0 1
3.6700 3.6690 .0010 -2 1 1
3.3100 3.3128 -.0028 0 1 2
3.1300 3.1294 .0006 -3 1 1
3.0100 3.0099 .0001 -2 1 2
2.7200 2.7200 -.0000 -4 0 2
2.5800 2.5806 -.0006 4 0 2
2.4400 2.4417 -.0017 1 2 0
2.2400 2.2387 .0013 2 2 1
2.1600 2.1611 -.0011 -6 0 1
2.0300 2.0286 .0014 0 1 4
1.9700 1.9699 .0001 4 1 3
1.7700 1.7699 .0001 -3 2 3
1.6500 1.6499 .0001 1 1 5
1.5500 1.5500 .0000 3 3 0
a= 13.205 b= 4.9693 c=8.902 beta= 93.14
da=.001 db=.0001 dc=.004 dbeta=.01
V= 583.3
61. 14-0839
C12H30As2Cl2Co
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
5.5000 5.4911 .0089 0 0 1
4.2700 4.2545 .0155 1 1 0
2.8500 2.8439 .0061 3 0 1
2.7100 2.7149 -.0049 3 1 0
2.6500 2.6471 .0029 1 0 2
2.3700 2.3712 -.0012 0 1 2
2.2900 2.2892 .0008 1 2 0
2.1400 2.1414 -.0014 2 1 2
a= 9.97 b= 4.704 c= 5.491
da= .02 db= .003 dc= .001
V=257.6
62. 14-0842
C6H15AsCl2Co
Triklin
Dexp Dcal d(D) h k l
7.2000 7.2079 -.0079 0 1 1
6.4200 6.4246 -.0046 1 0 0
5.9900 6.0012 -.0112 0 -1 1
4.2900 4.2963 -.0063 0 2 0
4.1900 4.1867 .0033 1 2 0
3.9300 3.9290 .0010 -1 1 2
3.8300 3.8340 -.0040 -1 -2 1
3.6900 3.6904 -.0004 1 1 2
3.3400 3.3396 .0004 0 0 3
3.1800 3.1792 .0008 -1 -2 2
2.9900 2.9900 .0000 -2 -2 1
2.8200 2.8201 -.0001 1 -2 1
A= 6.861 DA= .001
B= 9.058 DB= .004
C= 10.400 DC= .002
GAMMA= 74.78 DGAMMA= .01
BETA =101.512 DBETA = .009
ALPHA= 83.06 DALPHA= .01
V= 600.8
63. 14-0843
C6H15AsBr2Co
Triklin
Dexp Dcal d(D) h k l
6.4200 6.4209 -.0009 1 0 0
6.0300 6.0372 -.0072 -1 1 1
5.3400 5.3401 -.0001 -1 -1 1
4.9800 4.9705 .0095 0 1 2
4.7600 4.7561 .0039 1 0 1
4.3100 4.3106 -.0006 1 -1 1
4.2100 4.2073 .0027 -1 -2 1
4.0400 4.0471 -.0071 -1 -1 2
3.8700 3.8702 -.0002 -1 3 1
3.7200 3.7185 .0015 0 3 2
3.6500 3.6475 .0025 1 -2 1
3.5900 3.5889 .0011 -1 3 2
A= 6.7391 DA= .0005
B= 13.4871 DB= .0001
C= 10.531 DC= .001
GAMMA= 94.475 DGAMMA= .007
BETA =107.683 DBETA = .005
ALPHA= 75.424 DALPHA= .005
V=882.8
64. 14-0844
C8Co3O9
Triklin
Dexp Dcal d(D) h k l
11.6000 11.6036 -.0036 1 0 0
8.6300 8.6210 .0090 0 1 0
6.3100 6.3124 -.0024 0 0 1
5.0000 5.0094 -.0094 0 -1 1
4.8700 4.8693 .0007 -2 1 0
3.7400 3.7394 .0006 -2 -1 1
3.6200 3.6199 .0001 0 2 1
3.2700 3.2723 -.0023 -3 0 1
3.0600 3.0593 .0007 1 0 2
2.8590 2.8583 .0007 1 -1 2
2.8440 2.8441 -.0001 3 2 0
2.2520 2.2521 -.0001 4 2 1
A= 11.609 DA= .001
B= 8.629 DB= .001
C= 6.3173 DC= .0007
GAMMA= 91.387 DGAMMA= .005
BETA = 89.04 DBETA = .01
ALPHA= 88.00 DALPHA= .04
V=631.6
65. 14-0893
C30H27CoO6
Triklin
Dexp Dcal d(D) h k l
11.1000 11.2532 -.1532 1 0 0
9.3600 9.3987 -.0387 0 1 0
8.2800 8.2817 -.0017 0 0 1
7.0700 7.0708 -.0008 -1 0 1
5.9900 5.9876 .0024 0 -1 1
5.6300 5.6266 .0034 2 0 0
5.0700 5.0711 -.0011 1 -1 1
4.7000 4.6993 .0007 0 2 0
4.1100 4.1098 .0002 2 1 1
3.5500 3.5499 .0001 -2 2 0
A= 11.332 DA= .009
B= 9.43 DB= .01
C= 8.360 DC= .008
GAMMA= 88.62 DGAMMA= .09
BETA = 96.51 DBETA = .08
ALPHA= 85.75 DALPHA= .09
V= 884.7
66. 14-0968
C30H27CoO6
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
9.7200 9.8283 -.1083 0 1 0
8.3400 8.3422 -.0022 0 0 1
7.7000 7.7355 -.0355 1 0 1
7.1300 7.1208 .0092 2 1 0
6.3900 6.3600 .0300 0 1 1
5.6400 5.6403 -.0003 3 1 0
4.7800 4.7808 -.0008 1 2 0
4.1700 4.1711 -.0011 0 0 2
3.8400 3.8396 .0004 0 1 2
a=20.662 b= 9.8283 c= 8.342
da= .001 db= .0008 dc= .002
V=1694.1
67. 15-0387
Co3Si4O10{OH}2
Geksag
Groupa 143
Dexp. Dcal. d(D) h k l
9.5200 9.0658 .4542 0 0 1
4.7200 4.6950 .0250 1 0 1
4.5800 4.5329 .0471 0 0 2
3.1500 3.1687 -.0187 1 1 0
2.6400 2.6472 -.0072 1 0 3
2.2620 2.2665 -.0045 0 0 4
1.5750 1.5737 .0013 1 1 5
1.5290 1.5302 -.0012 2 1 4
a= 6.34 c= 9.07
da=.04 dc=.05
v= 315
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.5200 9.5210 -.0010 0 0 2
4.7200 4.7202 -.0002 2 1 0
4.5800 4.5800 .0000 0 2 0
3.1500 3.1500 -.0000 -3 1 2
2.6400 2.6400 .0000 2 2 5
2.2620 2.2620 .0000 -4 2 2
1.5750 1.5750 .0000 -6 2 4
1.5290 1.5290 .0000 7 1 3
a= 11.0382 b= 9.160 c=19.081 beta= 86.32
da=.0002 db=.001 dc=.009 dbeta=.01
V= 1925
68. 15-0585
{Co{NH3}5I}I2
Rombik
Groupa 29,57
Dexp. Dcal. d(D) h k l
5.3500 5.3438 .0062 0 1 0
3.8300 3.8276 .0024 1 1 0
2.7200 2.7232 -.0032 0 0 2
2.2200 2.2189 .0011 1 1 2
1.9300 1.9324 -.0024 2 0 2
1.7300 1.7299 .0001 3 1 0
1.4500 1.4483 .0017 1 2 3
1.3000 1.2980 .0020 1 4 0
1.2200 1.2200 .0000 4 2 0
1.1700 1.1717 -.0017 1 4 2
1.0700 1.0699 .0001 3 1 4
a= 5.485 b= 5.34 c= 5.446
da= .004 db= .02 dc= .001
V= 159.6
69. 15-0586
K3{Co{CN}6}
Triklin
Dexp Dcal d(D) h k l
6.6300 6.6265 .0035 -1 0 1
5.8600 5.8618 -.0018 0 1 1
5.1500 5.1483 .0017 0 -1 1
4.0800 4.0813 -.0013 -1 -1 1
3.6900 3.6889 .0011 1 1 1
3.3300 3.3298 .0002 1 -2 1
3.0400 3.0376 .0024 2 0 1
2.9200 2.9193 .0007 -2 -1 1
2.6100 2.6097 .0003 0 0 3
2.1700 2.1702 -.0002 -2 -1 3
2.0700 2.0700 -.0000 1 3 1
1.8600 1.8603 -.0003 3 0 2
1.8400 1.8400 .0000 0 -1 4
A= 9.458 DA= .002
B= 9.119 DB= .001
C= 8.7809 DC= .0007
GAMMA=122.27 DGAMMA= .01
BETA =115.963 DBETA = .009
ALPHA= 70.630 DALPHA= .002
V=571.4
70. 15-0933
C9H30Cl6CoMnN6
Groupa 16
Dexp. Dcal. d(D) h k l
9.2800 9.2374 .0426 0 0 1
5.4200 5.4051 .0149 1 0 0
4.6400 4.6187 .0213 0 0 2
4.2700 4.2826 -.0126 0 1 2
3.8100 3.8121 -.0021 0 3 0
3.5300 3.5238 .0062 0 3 1
3.3600 3.3567 .0033 1 1 2
2.9500 2.9519 -.0019 1 3 1
2.7100 2.7110 -.0010 0 2 3
2.3100 2.3093 .0007 0 0 4
2.0300 2.0311 -.0011 2 0 3
1.0200 1.0200 .0000 5 0 3
a= 5.405076 b=11.436160 c= 9.237352
da= .004436 db= .009291 dc= .005580
V= 571
71. 15-0934
C9H30Cl6CoCrN6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.1400 9.2211 -.0811 1 0 0
5.3300 5.3636 -.0336 1 1 0
4.7000 4.7143 -.0143 0 1 1
4.2200 4.2247 -.0047 -2 0 1
3.7800 3.7785 .0015 2 1 0
3.4900 3.4911 -.0011 2 0 1
3.2900 3.2969 -.0069 0 2 0
2.9000 2.8958 .0042 -1 2 1
2.6800 2.6818 -.0018 2 2 0
2.4900 2.4918 -.0018 2 0 2
2.3700 2.3716 -.0016 -3 1 2
2.2900 2.2929 -.0029 -1 0 3
a= 9.416 b= 6.594 c= 6.885 beta= 101.66
da= .005 db=.008 dc= .003 dbeta=.01
V= 418.6
72. 15-0935
C9H30Cl6CoFeN6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.2400 9.2388 .0012 1 0 1
5.3600 5.3623 -.0023 2 1 1
4.6300 4.6291 .0009 0 1 2
4.2300 4.2291 .0009 3 0 1
3.8000 3.8053 -.0053 0 3 0
3.5200 3.5185 .0015 1 3 1
3.3300 3.3285 .0015 -1 3 1
2.9300 2.9317 -.0017 -1 1 3
2.6900 2.6901 -.0001 4 0 3
2.5100 2.5115 -.0015 -3 2 2
2.4000 2.3992 .0008 -2 2 3
2.3100 2.3097 .0003 4 0 4
a=12.77 b= 11.416 c=10.594 beta=72.94
da=.02 db=.008 dc= .001 dbeta=.05
V= 1476.4
Triklin
Dexp Dcal d(D) h k l
9.2400 9.2401 -.0001 0 0 1
5.3600 5.3609 -.0009 -1 0 1
4.6300 4.6303 -.0003 0 -2 1
4.2300 4.2308 -.0008 0 -1 2
3.8000 3.7995 .0005 -1 -2 1
3.5200 3.5214 -.0014 0 2 2
3.3300 3.3309 -.0009 -2 0 1
2.9300 2.9311 -.0011 2 2 2
2.6900 2.6899 .0001 0 4 0
2.5100 2.5098 .0002 2 3 2
2.4000 2.4002 -.0002 -2 -2 2
2.3100 2.3100 -.0000 0 0 4
A= 8.141 DA= .002
B= 10.761 DB= .001
C= 9.552 DC= .002
GAMMA= 89.29 DGAMMA= .04
BETA = 75.333 DBETA = .008
ALPHA= 89.30 DALPHA= .02
V= 809.4
73. 15-0936
C9H30Cl6CoInN6
Triklin
Dexp Dcal d(D) h k l
9.4000 9.3999 .0001 1 0 0
7.2200 7.2260 -.0060 0 1 0
5.4600 5.4591 .0009 0 -1 1
4.7300 4.7398 -.0098 -2 1 0
4.3400 4.3452 -.0052 0 0 2
3.8800 3.8774 .0026 1 0 2
3.5800 3.5797 .0003 1 -1 2
3.3800 3.3802 -.0002 0 2 1
3.0300 3.0303 -.0003 3 -1 1
2.7200 2.7201 -.0001 -2 -1 2
2.5500 2.5498 .0002 1 -3 0
2.4400 2.4396 .0004 -4 1 1
A= 10.007 DA= .003
B= 7.690 DB= .001
C= 8.713 DC= .006
GAMMA=109.91 DGAMMA= .04
BETA = 93.54 DBETA = .03
ALPHA= 86.84 DALPHA= .02
V= 628.8