502. 43-0488
gamma-Zn2P2O7
Triklin
Dexp Dcal d(D) h k l
6.7000 6.6928 .0072 0 1 1
6.2100 6.2196 -.0096 0 -1 1
5.2100 5.2057 .0043 -1 -1 1
4.9800 4.9752 .0048 1 1 1
4.6400 4.6348 .0052 -2 0 1
4.4100 4.4177 -.0077 0 -1 2
4.2500 4.2395 .0105 -2 1 0
4.1300 4.1247 .0053 -1 -1 2
4.0600 4.0622 -.0022 2 0 1
3.9800 3.9792 .0008 -2 0 2
3.8800 3.8763 .0037 1 -1 2
3.8000 3.8014 -.0014 0 2 1
A= 9.6046 DA= .0008
B= 7.948 DB= .004
C= 11.527 DC= .006
GAMMA= 97.615 DGAMMA= .002
BETA =101.312 DBETA = .007
ALPHA= 84.16 DALPHA= .05
V=852.7
503. 43-0585
ZnH0.8La0.4{PO4}2*4H2O
Triklin
Dexp Dcal d(D) h k l
11.6000 11.5949 .0051 0 1 0
5.7500 5.7517 -.0017 0 -1 2
4.6100 4.6151 -.0051 1 0 2
4.5700 4.5676 .0024 -1 -2 1
4.4500 4.4526 -.0026 0 -2 2
4.1800 4.1851 -.0051 1 -1 2
3.9200 3.9212 -.0012 -1 -2 2
3.7800 3.7793 .0007 0 -3 1
3.5500 3.5519 -.0019 -1 -3 1
3.4900 3.4897 .0003 1 -2 2
3.4200 3.4194 .0006 0 -3 2
3.2400 3.2390 .0010 -1 -3 2
3.2000 3.1994 .0006 2 0 1
2.7900 2.7887 .0013 1 -1 4
2.6300 2.6300 .0000 2 -2 1
A= 6.69 DA= .01
B= 11.83 DB= .01
C= 12.715 DC= .001
GAMMA= 79.51 DGAMMA= .05
BETA = 89.52 DBETA = .09
ALPHA= 94.27 DALPHA= .08
V= 985.9
504. 43-0586
ZnCr0.85{PO4}2*xH2O
Triklin
Dexp Dcal d(D) h k l
8.8000 8.7921 .0079 1 1 0
4.6000 4.5991 .0009 -2 0 2
4.4600 4.4602 -.0002 -1 0 3
4.3300 4.3302 -.0002 -1 3 1
4.0000 4.0005 -.0005 0 3 2
3.9100 3.9114 -.0014 1 1 3
3.7800 3.7797 .0003 -2 0 3
3.6700 3.6686 .0014 1 3 2
3.4900 3.4895 .0005 1 4 0
2.6500 2.6496 .0004 3 1 3
2.6000 2.6004 -.0004 3 3 2
a= 11.06 b= 14.724 c= 13.933 beta= 97.59
da= .01 db=.002 dc=.003 dbeta=.05
V= 2248.6
505. 43-0587
ZnCr0.85{PO4}2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.3000 10.2802 .0198 0 1 0
5.1300 5.1254 .0046 2 1 2
4.5200 4.5173 .0027 -2 1 1
4.4500 4.4546 -.0046 3 0 1
4.2900 4.2898 .0002 2 1 3
3.8800 3.8792 .0008 2 2 2
3.8100 3.8092 .0008 1 0 4
3.7500 3.7499 .0001 2 0 4
3.5200 3.5228 -.0028 2 1 4
3.0600 3.0604 -.0004 1 2 4
3.0000 3.0002 -.0002 2 3 0
2.8000 2.7991 .0009 3 1 5
a= 13.42 b= 10.280 c= 15.32 beta= 67.69
da=.01 db=.001 dc=.04 dbeta=.09
V= 1955
506. 43-1441
Gaq6Mg22Zn52
Rombik
Groupa 32, 55
Dexp. Dcal. d(D) h k l
3.2110 3.2142 -.0032 0 0 3
2.9930 2.9952 -.0022 2 0 2
2.4040 2.4036 .0004 1 3 0
2.3430 2.3434 -.0004 3 1 1
2.2010 2.2005 .0005 1 1 4
2.1610 2.1599 .0011 3 1 2
1.8430 1.8430 .0000 1 4 0
1.7960 1.7961 -.0001 3 3 0
a= 7.6444 b= 7.596 c= 9.643
da= .0008 db= .001 dc= .004
V= 559.9
507. 43-1442
Al25Mg37.5Zn37.5
Rombik
Groupa 32, 55
Dexp. Dcal. d(D) h k l
3.2640 3.2644 -.0004 0 0 1
2.4460 2.4441 .0019 0 2 1
2.3830 2.3846 -.0016 1 2 1
2.2400 2.2396 .0004 2 3 0
1.8730 1.8728 .0002 5 2 0
1.8230 1.8230 .0000 4 3 0
a=10.871 b= 7.374 c= 3.264
da= .001 db= .011 dc= .001
V= 261.7
508. 43-1801
C28H16B2O12Zn*10H2O
Triklin
Dexp Dcal d(D) h k l
13.9910 13.9783 .0127 1 0 0
7.4010 7.4146 -.0136 -1 1 1
7.0300 7.0141 .0159 -1 -1 1
6.0580 6.0569 .0011 -2 0 1
5.8080 5.8007 .0073 2 -1 1
5.6340 5.6378 -.0038 1 -2 1
5.1840 5.1905 -.0065 -1 0 2
4.7570 4.7555 .0015 -3 1 0
4.4930 4.4921 .0009 1 2 1
4.1580 4.1583 -.0003 2 2 0
3.9350 3.9340 .0010 -1 2 2
3.7420 3.7448 -.0028 2 2 1
A= 14.4135 DA= .0009
B= 12.809 DB= .002
C= 10.9893 DC= .0009
GAMMA=103.68 DGAMMA= .02
BETA = 92.001 DBETA = .004
ALPHA= 96.027 DALPHA= .009
V=1957.3
509. 43-1835
C8H6N4O4S2Zn*2H2O
Rombik
Groupa 19
Dexp. Dcal. d(D) h k l
8.8100 8.8056 .0044 0 1 1
7.3300 7.2983 .0317 0 2 0
5.5200 5.5204 -.0004 0 0 2
4.2300 4.2401 -.0101 1 1 1
4.0400 4.0324 .0076 1 2 0
3.6900 3.6803 .0097 0 0 3
3.4300 3.4306 -.0006 1 3 0
2.7100 2.7122 -.0022 0 1 4
2.5000 2.4995 .0005 1 5 0
2.4300 2.4328 -.0028 0 6 0
2.0500 2.0490 .0010 0 7 1
a= 4.838 b=14.5965 c=11.04
da= .005 db= .0006 dc= .01
V= 779.6
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.8100 8.8061 .0039 1 1 0
7.3300 7.3228 .0072 1 1 1
5.5200 5.5208 -.0008 0 2 1
4.2300 4.2305 -.0005 2 2 1
4.0400 4.0389 .0011 3 0 1
3.6900 3.6901 -.0001 1 1 3
3.4300 3.4308 -.0008 3 1 2
2.7100 2.7101 -.0001 3 3 2
2.5000 2.5002 -.0002 0 5 0
2.4300 2.4295 .0005 1 4 3
2.0500 2.0501 -.0001 0 3 5
a= 12.478 b= 12.501 c= 11.841 beta= 83.87
da= .009 db=.004 dc=.006 dbeta=.09
V= 1836.5
510. 43-1885
C10H24N2O4S4Se2Zn
Triklin
Dexp Dcal d(D) h k l
7.1900 7.1867 .0033 1 0 0
6.6100 6.6119 -.0019 -1 1 0
5.7900 5.8051 -.0151 0 1 1
5.5000 5.5155 -.0155 -1 1 1
4.9600 4.9610 -.0010 -1 2 0
4.0000 4.0060 -.0060 -1 -2 1
3.5800 3.5933 -.0133 2 0 0
3.4400 3.4409 -.0009 -1 3 1
3.3000 3.3000 .0000 0 -1 2
3.1000 3.0998 .0002 1 -3 1
2.9500 2.9480 .0020 -2 -2 1
2.6400 2.6391 .0009 1 1 2
A= 7.63655 DA= .00003
B= 11.993 DB= .002
C= 7.1433 DC= .0006
GAMMA= 98.614 DGAMMA= .008
BETA =107.757 DBETA = .003
ALPHA= 89.3854 DALPHA= .0006
V=615.6
511. 43-1896
C10H24N2O4S4Se2Zn
Triklin
Dexp Dcal d(D) h k l
7.1900 7.1911 -.0011 1 0 0
6.6100 6.6052 .0048 0 1 1
5.7900 5.7790 .0110 0 -1 1
4.9600 4.9543 .0057 1 -1 1
4.0000 3.9970 .0030 0 2 0
3.5800 3.5753 .0047 -1 1 2
3.4400 3.4444 -.0044 -1 2 1
3.1000 3.0995 .0005 -2 1 1
2.9500 2.9509 -.0009 2 1 2
2.6400 2.6409 -.0009 -2 1 2
2.5300 2.5303 -.0003 -1 -2 2
A= 7.331 DA= .001
B= 8.0895 DB= .0002
C= 9.863 DC= .003
GAMMA= 94.175 DGAMMA= .007
BETA = 80.20 DBETA = .02
ALPHA= 83.089 DALPHA= .002
V= 569.6
512. 43-1896
C10H24N2O4S4Se2Zn
Rombik
Groupa 31,59
Dexp. Dcal. d(D) h k l
7.1900 7.1799 .0101 0 1 1
6.6100 6.6531 -.0431 1 1 0
5.7900 5.7695 .0205 0 0 2
4.9600 4.9540 .0060 1 0 2
4.0000 4.0091 -.0091 2 1 1
3.5800 3.5738 .0062 1 0 3
3.4400 3.4351 .0049 2 1 2
3.1000 3.1031 -.0031 3 0 1
2.9500 2.9553 -.0053 0 3 1
2.6400 2.6362 .0038 3 2 0
2.3400 2.3366 .0034 4 1 0
2.1500 2.1491 .0009 3 0 4
a= 9.665 b= 9.172 c=11.54
da= .004 db= .002 dc= .01
v=1022.9
513. 43-1897
C6H16N6Se2Zn
Triklin
Dexp Dcal d(D) h k l
7.3800 7.3799 .0001 0 1 1
6.5600 6.5611 -.0011 1 1 0
5.5400 5.5392 .0008 0 -1 1
4.6200 4.6226 -.0026 -1 1 1
4.3500 4.3520 -.0020 -1 0 2
3.8300 3.8273 .0027 2 0 0
3.5800 3.5762 .0038 -2 0 1
3.4100 3.4105 -.0005 2 2 1
3.2800 3.2806 -.0006 2 2 0
2.8000 2.8024 -.0024 -1 -2 2
2.6900 2.6886 .0014 3 1 0
2.5600 2.5602 -.0002 2 -1 2
A= 8.139 DA= .002
B= 8.5643 DB= .0007
C= 11.385 DC= .005
GAMMA= 70.20 DGAMMA= .02
BETA = 82.374 DBETA = .02
ALPHA= 71.32 DALPHA= .01
V= 707.0
514. 43-1898
C28H48Na2N4O12Se4Zn
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
5.3700 5.3752 -.0052 0 0 2
4.8000 4.8083 -.0083 0 1 2
4.3700 4.3841 -.0141 1 0 0
4.0600 4.0599 .0001 1 1 0
3.9500 3.9442 .0058 1 1 1
3.4300 3.4260 .0040 1 1 2
3.0800 3.0808 -.0008 -1 1 2
2.9800 2.9822 -.0022 0 2 3
2.6400 2.6398 .0002 -1 3 1
2.3600 2.3597 .0003 -1 2 3
2.2000 2.1996 .0004 2 0 1
1.9500 1.9504 -.0004 -2 0 2
a= 4.4154 b= 10.757 c= 10.827 beta= 83.17
da= .0005 db=.009 dc= .005 dbet=.06
V=510.3
Triklin
Dexp Dcal d(D) h k l
5.3700 5.3741 -.0041 1 0 0
4.8000 4.7950 .0050 1 1 0
4.3700 4.3609 .0091 1 0 1
4.0600 4.0515 .0085 -1 -1 1
3.9500 3.9592 -.0092 0 2 0
3.6800 3.6801 -.0001 0 0 2
3.4300 3.4235 .0065 0 2 1
3.0800 3.0819 -.0019 1 2 1
2.9800 2.9804 -.0004 -1 2 0
2.6400 2.6394 .0006 0 3 0
2.3600 2.3604 -.0004 1 3 1
2.2000 2.2004 -.0004 -1 -1 3
2.0200 2.0203 -.0003 2 -2 1
1.9500 1.9498 .0002 1 -3 2
A= 5.4362 DA= .0006
B= 8.01740 DB= .00002
C= 7.3676 DC= .0006
GAMMA= 81.36 DGAMMA= .01
BETA = 89.824 DBETA = .003
ALPHA= 92.51 DALPHA= .01
V=317.2
515. 43-1899
C26H16N6Se2Zn
Triklin
Dexp Dcal d(D) h k l
7.3000 7.3061 -.0061 0 1 1
5.8900 5.8985 -.0085 0 -1 1
5.0700 5.0658 .0042 -1 1 0
4.6800 4.6757 .0043 1 1 0
4.3500 4.3475 .0025 -1 2 1
3.8500 3.8482 .0018 1 1 1
3.4400 3.4407 -.0007 -1 2 2
3.2900 3.2911 -.0011 1 -2 1
2.9500 2.9492 .0008 0 -2 2
2.6400 2.6400 .0000 0 -4 1
2.2900 2.2902 -.0002 -2 -2 1
2.1800 2.1800 .0000 0 -2 3
2.0000 2.0001 -.0001 2 0 2
1.9300 1.9300 .0000 1 -2 3
1.8400 1.8400 -.0000 1 6 0
A= 5.4709 DA= .0006
B= 12.7893 DB= .0006
C= 8.0859 DC= .0003
GAMMA= 99.426 DGAMMA= .002
BETA =103.30 DBETA = .01
ALPHA= 74.758 DALPHA= .001
V= 528.0
516. 43-1900
C22H16N6Se2Zn
Rombik
Groupa 31, 59
Dexp. Dcal. d(D) h k l
7.2500 7.3043 -.0543 2 0 0
6.3200 6.2802 .0398 2 1 0
6.1000 6.1496 -.0496 0 2 0
4.8600 4.8695 -.0095 3 0 0
4.3000 4.3048 -.0048 0 1 1
3.9500 3.9472 .0028 1 3 0
3.0600 3.0593 .0007 0 3 1
2.8600 2.8592 .0008 4 0 1
2.6000 2.5999 .0001 3 4 0
a=14.608530 b=12.299130 c= 4.595507
da= .016321 db= .003068 dc= .000950
V= 825.7
517. 44-0738
NH4Zn5{OH}9{NO3}2*3H2O
Triklin
Dexp Dcal d(D) h k l
10.1600 10.1818 -.0218 0 0 1
5.9300 5.9234 .0066 1 1 0
5.0900 5.0909 -.0009 0 0 2
4.9100 4.9124 -.0024 0 -2 1
4.5800 4.5867 -.0067 1 1 2
4.0400 4.0414 -.0014 2 0 2
4.0000 4.0041 -.0041 0 2 2
3.8000 3.7972 .0028 2 1 1
3.6600 3.6601 -.0001 -2 1 1
3.5600 3.5552 .0048 -1 2 2
3.4700 3.4724 -.0024 -2 0 1
3.4100 3.4102 -.0002 1 1 3
A= 9.631 DA= .001
B= 12.53519 DB= .00002
C= 10.938 DC= .001
GAMMA=110.309 DGAMMA= .002
BETA = 69.042 DBETA = .008
ALPHA= 93.1250 DALPHA= .0004
V=1153.5
518. 44-0740
NH4Zn3{OH}6NO3
Triklin
Dexp Dcal d(D) h k l
10.3200 10.3275 -.0075 0 1 1
5.1500 5.1570 -.0070 1 0 2
4.6100 4.6066 .0034 1 -1 2
4.0500 4.0484 .0016 0 -3 1
4.0000 4.0031 -.0031 0 -2 2
3.8400 3.8400 -.0000 1 3 2
3.6900 3.6881 .0019 0 4 1
3.5700 3.5720 -.0020 0 4 0
3.4800 3.4744 .0056 -1 3 2
3.4400 3.4425 -.0025 0 3 3
3.1000 3.1001 -.0001 -1 2 3
2.9700 2.9633 .0067 0 1 4
A= 7.392 DA= .001
B= 14.7797 DB= .0001
C= 12.231 DC= .002
GAMMA= 91.06 DGAMMA= .07
BETA = 76.09 DBETA = .04
ALPHA= 75.93 DALPHA= .02
V=1253.4
519. 44-0759
{NH4}2Zn{SO4}2*6H2O
Triklin
Dexp Dcal d(D) h k l
7.3000 7.3016 -.0016 0 1 1
6.6300 6.6252 .0048 1 1 0
5.9600 5.9628 -.0028 0 -1 1
5.5700 5.5729 -.0029 1 -1 1
4.9300 4.9253 .0047 1 2 0
4.7900 4.7964 -.0064 -1 0 1
4.3800 4.3728 .0072 1 -2 1
4.2700 4.2825 -.0125 0 3 1
3.6500 3.6508 -.0008 0 2 2
3.5300 3.5303 -.0003 1 -1 2
3.4600 3.4569 .0031 1 -3 1
A= 8.3891 DA= .0003
B= 13.6929 DB= .0001
C= 8.0583 DC= .0003
GAMMA= 90.637 DGAMMA= .002
BETA = 73.076 DBETA = .001
ALPHA= 77.274 DALPHA= .001
V=861.3
520. 44-0760
{NH42ZnH4{P2O7}2*2H2O
Triklin
Dexp Dcal d(D) h k l
8.6300 8.6391 -.0091 -1 0 1
4.4800 4.4856 -.0056 0 2 1
4.3100 4.3062 .0038 0 -2 1
4.1500 4.1421 .0079 -2 2 1
3.3300 3.3321 -.0021 -2 0 3
3.2100 3.2119 -.0019 0 0 3
3.0800 3.0794 .0006 -2 2 3
3.0400 3.0337 .0063 -2 3 0
2.9600 2.9623 -.0023 -3 2 0
2.9100 2.9093 .0007 1 3 0
2.6800 2.6801 -.0001 -1 -2 3
2.5300 2.5304 -.0004 -1 4 0
A= 10.6048 DA= .0008
B= 10.2526 DB= .0006
C= 10.6089 DC= .0009
GAMMA=105.40 DGAMMA= .01
BETA =114.586 DBETA = .007
ALPHA= 81.118 DALPHA= .007
V=1010.2
521. 44-0769
Zn2P2O7*2H2O
Triklin
Dexp Dcal d(D) h k l
9.7500 9.7439 .0061 0 0 1
7.5200 7.5180 .0020 1 0 0
6.3800 6.3776 .0024 0 -2 1
5.1800 5.1804 -.0004 -1 2 0
4.7900 4.7897 .0003 1 2 1
3.7400 3.7396 .0004 0 -4 1
3.5000 3.4984 .0016 -2 -1 1
3.4200 3.4184 .0016 -1 -3 2
3.2400 3.2388 .0012 0 -1 3
3.1000 3.0996 .0004 0 -2 3
2.9600 2.9598 .0002 -2 0 2
2.8900 2.8919 -.0019 -1 -2 3
A= 7.550 DA= .001
B= 15.7314 DB= .0008
C= 9.784 DC= .003
GAMMA= 84.766 DGAMMA= .001
BETA = 89.83 DBETA = .01
ALPHA= 95.16 DALPHA= .01
V= 1152.5
522. 44-0816
C2H8N4O2*Zn{NO3}2*4H2O
Triklin
Dexp Dcal d(D) h k l
9.7700 9.7320 .0380 1 0 0
6.6700 6.6789 -.0089 0 1 0
5.8500 5.8421 .0079 1 0 2
5.2000 5.2009 -.0009 -1 1 0
4.8000 4.7911 .0089 0 -1 2
4.7100 4.7094 .0006 0 1 2
4.5400 4.5415 -.0015 1 1 2
4.2000 4.2010 -.0010 2 1 0
3.9900 3.9902 -.0002 -1 1 2
3.7000 3.7012 -.0012 2 1 2
3.2900 3.2926 -.0026 1 2 0
3.2500 3.2550 -.0050 0 -2 1
A= 9.86729 DA= .00002
B= 6.73594 DB= .00006
C= 13.5860 DC= .0002
GAMMA= 82.610 DGAMMA= .001
BETA = 84.1064 DBETA = .0007
ALPHA= 90.2204 DALPHA= .0007
V=889.3
523. 44-1524
C4H5FN2O4Zn*H2O
Rombik
Groupa 33, 49, 62
Dexp. Dcal. d(D) h k l
5.8166 5.8072 .0094 0 1 1
4.8702 4.8932 -.0230 0 2 0
3.6079 3.6074 .0005 0 0 2
3.3704 3.3744 -.0040 2 1 1
3.0345 3.0357 -.0012 1 3 0
2.6614 2.6601 .0013 3 1 0
2.5659 2.5638 .0021 2 3 0
2.0727 2.0731 -.0004 4 0 0
1.4862 1.4862 -.0000 0 6 2
1.4606 1.4606 .0000 3 5 2
a= 8.292 b= 9.7864 c= 7.215
da= .002 db= .000519 dc= .004
V= 585.5
524. 44-1525
C6H6Cl2N2O2Zn*2H2O
Triklin
Dexp Dcal d(D) h k l
11.9240 11.9214 .0026 1 1 0
9.2824 9.2701 .0123 0 1 1
8.3640 8.3763 -.0123 0 -1 1
7.5958 7.6033 -.0075 1 2 0
7.0172 7.0251 -.0079 0 2 0
6.4451 6.4438 .0013 1 2 1
6.1888 6.1697 .0191 -1 -2 1
6.0160 6.0167 -.0007 2 0 0
5.8855 5.8761 .0094 -2 -1 1
5.4362 5.4260 .0102 0 1 2
4.6555 4.6582 -.0027 -2 1 1
3.9738 3.9738 .0000 3 3 0
A= 13.270 DA= .001
B= 15.49471 DB= .00008
C= 11.3516 DC= .0006
GAMMA= 65.743 DGAMMA= .001
BETA = 93.812 DBETA = .002
ALPHA= 86.171 DALPHA= .003
V=2111.8
525. 44-1526
Cl2H10N4O4Zn*2H2O
Triklin
Dexp Dcal d(D) h k l
6.7862 6.7831 .0031 -1 1 0
6.5201 6.5198 .0003 1 1 0
5.9481 5.9474 .0007 -1 -1 1
4.8002 4.8059 -.0057 0 1 1
3.9885 3.9889 -.0004 -3 -1 1
3.8366 3.8361 .0005 0 -2 1
3.6158 3.6145 .0013 0 2 0
3.4646 3.4647 -.0001 4 -1 2
3.3836 3.3833 .0003 5 0 0
3.2911 3.2919 -.0008 5 -1 1
3.2291 3.2278 .0013 -1 -2 2
3.0567 3.0565 .0002 4 -2 1
A= 17.325 DA= .002
B= 7.7562 DB= .0005
C= 9.4583 DC= .001
GAMMA= 97.19 DGAMMA= .04
BETA = 77.9308 DBETA = .0003
ALPHA=111.03 DALPHA= .01
V=1159.0
526. 44-1571
C24H26Clo2N6O4Zn
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
9.8089 9.8195 -.0106 -2 0 1
7.8172 7.8298 -.0126 -2 0 2
4.9774 4.9750 .0024 -1 0 4
4.3799 4.3794 .0005 -3 0 4
4.0719 4.0714 .0005 5 0 0
3.8462 3.8442 .0020 5 0 1
3.4421 3.4424 -.0003 2 0 5
2.8061 2.8061 .0000 3 1 4
a= 20.728 b= 4.37900 c= 19.9276 beta= 100.858
da= .003 db=.00001 dc=.0006 dbet=.004
V=1777.1
527. 44-1572
C24H24N6O4Zn
Triklin
Dexp Dcal d(D) h k l
12.6220 12.6401 -.0181 -1 1 0
12.0870 12.0739 .0131 1 1 0
10.1580 10.1542 .0038 0 0 1
7.1561 7.1691 -.0130 1 -1 1
6.2959 6.2923 .0036 0 -2 1
5.6041 5.6026 .0015 -1 3 0
4.7915 4.7907 .0008 -1 -1 2
4.3380 4.3369 .0011 -4 0 1
4.2146 4.2134 .0012 -3 3 0
4.0083 4.0139 -.0056 -2 -2 2
3.8366 3.8365 .0001 2 4 0
3.6150 3.6149 .0001 3 -3 1
A= 17.857 DA= .002
B= 17.6215 DB= .0005
C= 10.4425 DC= .0003
GAMMA= 93.995 DGAMMA= .008
BETA =101.99 DBETA = .01
ALPHA= 83.065 DALPHA= .003
V=3187.6
528. 44-1612
C22H18N6O4Zn
Trikln
Dexp Dcal d(D) h k l
8.3128 8.3059 .0069 0 1 1
7.0890 7.0950 -.0060 1 0 0
6.1165 6.1121 .0044 0 -1 1
5.8718 5.8741 -.0023 -1 1 0
5.1195 5.1148 .0047 1 0 2
4.7624 4.7609 .0015 1 1 2
4.1470 4.1472 -.0002 0 1 3
3.6063 3.6073 -.0010 2 0 1
3.3746 3.3736 .0010 -1 -1 2
3.2074 3.2079 -.0005 -1 0 3
2.9625 2.9628 -.0003 0 3 2
2.6869 2.6867 .0002 -2 2 2
2.0922 2.0922 .0000 0 1 6
1.5829 1.5829 -.0000 0 -1 7
A= 7.270 DA= .002
B= 9.047 DB= .001
C= 12.7866 DC= .0005
GAMMA= 94.54 DGAMMA= .02
BETA = 80.179 DBETA = .009
ALPHA= 72.84 DALPHA= .003
V= 784.2
529. 44-1746
C22H16N6O4Zn
Triklin
Dexp Dcal d(D) h k l
13.0800 13.0658 .0142 0 0 1
10.8790 10.8678 .0112 0 1 0
9.3567 9.3295 .0272 2 0 0
7.7186 7.7212 -.0026 2 1 0
6.0727 6.0716 .0011 1 -1 1
5.5920 5.5938 -.0018 -1 2 1
5.4349 5.4339 .0010 0 -2 0
4.6378 4.6450 -.0072 2 0 2
4.5545 4.5616 -.0071 4 1 0
4.3137 4.3155 -.0018 0 2 3
4.1385 4.1373 .0012 -3 -2 1
3.8803 3.8801 .0002 3 0 2
A= 19.91 DA= .01
B= 11.803 DB= .002
C= 14.93998 DC= .00004
GAMMA= 88.30 DGAMMA= .01
BETA =108.31 DBETA = .02
ALPHA= 68.9057 DALPHA= .0004
V3073.2
530. 44-1751
C10H8N4O6Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.1250 10.0715 .0535 1 0 0
6.9850 7.0009 -.0159 1 1 0
6.7120 6.7082 .0038 0 0 1
5.6420 5.6510 -.0090 -1 0 1
5.5260 5.5244 .0016 0 1 1
4.8640 4.8692 -.0052 0 2 0
4.0790 4.0783 .0007 -2 0 1
3.9780 3.9781 -.0001 2 0 1
3.3570 3.3572 -.0002 3 0 0
3.1570 3.1579 -.0009 1 0 2
2.7520 2.7588 -.0068 2 0 2
2.6500 2.6495 .0005 1 2 2
2.5400 2.5398 .0002 -2 3 1
a= 10.075 b= 9.74 c= 6.71 beta= 91.5
da= .008 db=.01 dc=.02 dbeta=.2
V= 658
Triklin
Dexp Dcal d(D) h k l
10.1250 10.1106 .0144 1 0 0
6.9850 6.9809 .0041 -1 1 0
6.7120 6.7137 -.0017 -1 0 1
5.6420 5.6434 -.0014 1 -1 1
5.5260 5.5255 .0005 -1 -1 1
4.8640 4.8606 .0034 -2 1 0
4.0790 4.0801 -.0011 2 -1 1
3.9780 3.9803 -.0023 -2 1 1
3.3570 3.3568 .0002 -2 0 2
3.1570 3.1574 -.0004 -1 -2 2
2.7520 2.7520 .0000 1 -3 1
2.6500 2.6500 .0000 2 2 0
2.5400 2.5399 .0001 0 -2 3
A= 10.666 DA= .004
B= 8.26881 DB= .00005
C= 7.9803 DC= .0007
GAMMA=101.771 DGAMMA= .009
BETA = 98.89 DBETA = .01
ALPHA=111.204 DALPHA= .009
V= 622.0
531. 44-1840
C10H11N3O3*ZnCl2
Triklin
Dexp Dcal d(D) h k l
10.2540 10.2579 -.0039 1 0 0
7.7419 7.7415 .0004 1 1 1
6.2157 6.2180 -.0023 1 2 0
6.0974 6.0943 .0031 1 -1 2
5.9124 5.9165 -.0041 0 2 0
5.6037 5.5983 .0054 2 1 1
5.2884 5.3056 -.0172 0 -2 2
5.0645 5.0614 .0031 1 -2 1
4.7236 4.7282 -.0046 2 -1 1
4.5787 4.5790 -.0003 0 2 1
4.3046 4.3028 .0018 -1 0 2
4.2446 4.2459 -.0013 1 3 0
A= 11.6821 DA= .0009
B= 13.2808 DB= .0008
C= 13.266 DC= .005
GAMMA= 75.901 DGAMMA= .004
BETA = 70.97 DBETA = .02
ALPHA=106.43 DALPHA= .01
V=1734.1
532. 44-1976
C4H6N2S4Zn
Monoklin
Dexp Dcal d(D) h k l
8.3800 8.3856 -.0056 1 1 0
6.9100 6.9223 -.0123 1 1 1
5.7300 5.7414 -.0114 2 1 1
5.0900 5.0908 -.0008 -2 0 1
4.8200 4.8247 -.0047 1 2 0
4.4900 4.4898 .0002 1 2 1
4.1200 4.1143 .0057 2 2 1
3.6700 3.6696 .0004 4 0 0
3.6300 3.6314 -.0014 -3 1 1
3.4600 3.4611 -.0011 2 2 2
3.0200 3.0216 -.0016 0 1 3
2.8700 2.8707 -.0007 4 2 2
a= 15.441 b= 10.217 c= 9.982 beta= 71.907
da= .002 db=.003 dc=.006 dbeta=.01
V= 1497.0
Triklin
Dexp Dcal d(D) h k l
8.3800 8.3754 .0046 0 1 1
6.9100 6.9173 -.0073 0 -1 1
5.7300 5.7376 -.0076 1 1 0
5.0900 5.0894 .0006 -1 -1 1
4.8200 4.8212 -.0012 -1 0 2
4.4900 4.4940 -.0040 -1 1 1
4.1200 4.1203 -.0003 1 2 1
3.6700 3.6698 .0002 -1 -2 1
3.6300 3.6286 .0014 -1 1 3
3.4600 3.4586 .0014 0 -2 2
3.0200 3.0203 -.0003 0 -2 3
2.8700 2.8696 .0004 -2 0 2
A= 6.489 DA= .002
B= 9.0714 DB= .0008
C= 16.597 DC= .003
GAMMA= 75.303 DGAMMA= .006
BETA = 83.609 DBETA = .004
ALPHA= 75.686 DALPHA= .007
V= 914.4
533. 44-1977
C8H12MnN4S8Zn
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
7.9300 7.9447 -.0147 0 0 2
6.9000 6.9031 -.0031 1 0 2
4.4800 4.4818 -.0018 2 2 2
4.1300 4.1299 .0001 1 4 0
4.0200 4.0122 .0078 3 0 2
3.1900 3.1925 -.0025 4 0 2
3.0200 3.0199 .0001 3 0 4
a=13.94 b=17.2952 c=15.889
da= .01 db= .0008 dc= .008
V=3832
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
7.9300 7.9289 .0011 1 0 1
6.9000 6.8989 .0011 0 1 1
6.4800 6.4816 -.0016 -1 1 1
4.4800 4.4813 -.0013 0 0 3
4.1300 4.1296 .0004 -3 0 2
4.0200 4.0190 .0010 0 2 0
3.1900 3.1910 -.0010 1 2 2
3.0200 3.0200 .0000 -4 0 3
a= 12.981 b= 8.0380 c= 14.1601 beta= 108.296
da= .001 db=.0001 dc= .0005 dbet= .003
V=1402.3