317. 29-1988
C10H24Br2N4Zn
Triklin
Dexp Dcal d(D) h k l
12.4000 12.4036 -.0036 1 0 0
6.0600 6.0607 -.0007 0 1 1
5.6000 5.5985 .0015 0 -1 1
5.1300 5.1300 .0000 1 1 1
4.8800 4.8794 .0006 2 1 0
4.6600 4.6601 -.0001 -2 0 1
4.4100 4.4101 -.0001 2 -1 1
4.1100 4.1102 -.0002 1 -2 1
3.5800 3.5798 .0002 -3 0 1
3.5400 3.5400 .0000 -2 3 0
3.1600 3.1602 -.0002 -3 -1 1
A= 12.8346 DA= .0003
B= 11.2745 DB= .0004
C= 6.9213 DC= .0006
GAMMA=104.846 DGAMMA= .005
BETA = 92.634 DBETA = .001
ALPHA= 84.484 DALPHA= .002
V= 963.4
318. 29-1989
C10H24Br2N4Zn
Triklin
Dexp Dcal d(D) h k l
12.3000 12.2819 .0181 0 1 1
9.5000 9.5002 -.0002 0 -1 1
7.0200 7.0232 -.0032 -1 1 0
5.9700 5.9680 .0020 -1 2 0
5.7100 5.7101 -.0001 -1 2 1
5.4800 5.4796 .0004 -1 -1 1
5.3000 5.2999 .0001 1 2 0
5.0900 5.0901 -.0001 1 0 2
4.8600 4.8601 -.0001 -1 3 0
4.4000 4.4001 -.0001 0 4 0
3.7900 3.7901 -.0001 -1 2 3
A= 7.328 DA= .001
B= 18.33686 DB= .00007
C= 13.8210 DC= .0004
GAMMA= 96.111 DGAMMA= .006
BETA = 87.777 DBETA = .003
ALPHA= 75.2166 DALPHA= .0002
V= 1781.1
319. 29-1990
C10H24Cl2N4Zn
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
12.5000 12.4796 .0204 1 0 1
6.2200 6.2398 -.0198 2 0 2
5.0500 5.0452 .0048 1 0 4
4.6200 4.6209 -.0009 3 0 2
4.2700 4.2727 -.0027 0 0 5
3.8400 3.8400 .0000 0 1 0
3.8400 3.8439 -.0039 4 0 0
3.7000 3.6980 .0020 3 0 4
a=15.376 b= 3.840000 c=21.364
da= .009 db= .000000 dc= .003
V=1261.4
320. 29-1991
C10H24Cl2N4Zn*H2O
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
12.5000 12.5162 -.0162 1 0 0
9.7000 9.7840 -.0840 0 1 1
7.3000 7.2457 .0543 1 0 2
5.9200 5.8600 .0600 0 2 0
5.5100 5.5204 -.0104 2 1 0
5.2900 5.2870 .0030 0 1 3
5.1200 5.1166 .0034 2 0 2
4.8700 4.8703 -.0003 1 1 3
4.4400 4.4430 -.0030 0 0 4
3.7300 3.7292 .0008 1 3 0
a=12.516 b=11.72 c=17.77
da= .008 db= .07 dc= .02
V=2607
321. 29-1992
C14H14O4S2Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
14.8000 14.7620 .0380 0 1 0
9.0600 9.0609 -.0009 1 1 0
7.3800 7.3810 -.0010 0 2 0
5.2800 5.2834 -.0034 -1 1 2
4.5100 4.5102 -.0002 2 1 2
4.2400 4.2414 -.0014 -1 3 1
3.5500 3.5493 .0007 3 0 2
3.4100 3.4115 -.0015 -2 0 3
3.1900 3.1902 -.0002 -3 0 2
2.7000 2.7000 .0000 -1 3 4
2.6100 2.6086 .0014 -3 2 3
a= 11.570 b= 14.762 c= 14.08 beta= 82.75
da= .02 db=.08 dc=.02 dbeta=.08
V= 2385.8
322. 29-1996
C14H10N4O2Zn
Monoklin
GRUPA 4,11
Dexp. Dcal. d(D) h k l
8.5500 8.6012 -.0512 -1 0 1
6.5900 6.6235 -.0335 1 0 2
5.0300 5.0594 -.0294 1 1 2
4.2700 4.2792 -.0092 2 1 2
3.9900 4.0034 -.0134 1 1 3
3.7400 3.7377 .0023 1 2 0
3.5100 3.5150 -.0050 0 0 4
3.1000 3.1028 -.0028 4 0 0
3.0300 3.0376 -.0076 4 0 2
2.6700 2.6741 -.0041 -4 0 2
2.3300 2.3282 .0018 2 0 6
2.1000 2.0990 .0010 6 0 1
a= 12.60 b= 7.84 c=14.27 beta= 80.11
da= .06 db=.01 dc=.02 dbet=.01
V=1357.4
Triklin
Dexp Dcal d(D) h k l
8.5500 8.5441 .0059 1 0 0
6.5900 6.5829 .0071 0 1 0
5.9900 6.0015 -.0115 -1 1 1
5.0300 5.0345 -.0045 1 0 1
4.2700 4.2721 -.0021 2 0 0
3.9900 3.9935 -.0035 -1 2 1
3.7400 3.7422 -.0022 0 -1 1
3.5100 3.5081 .0019 -1 1 2
3.1000 3.1010 -.0010 2 1 1
3.0300 3.0280 .0020 1 2 1
2.6700 2.6705 -.0005 1 2 2
2.3300 2.3301 -.0001 3 1 1
2.1000 2.0999 .0001 3 0 2
A= 9.193 DA= .001
B= 8.025 DB= .008
C= 7.223 DC= .005
GAMMA=111.66 DGAMMA= .02
BETA =100.913 DBETA = .002
ALPHA= 60.08 DALPHA= .03
V= 429.2
323. 29-1997
C14H36N8O2P2Se2Zn
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
10.8000 10.7860 .0140 0 1 0
7.6900 7.7188 -.0288 1 1 0
5.9500 5.9968 -.0468 0 0 2
5.5400 5.5254 .0146 2 0 0
5.3000 5.2707 .0293 1 0 2
4.5000 4.5501 -.0501 2 1 1
3.8000 3.8026 -.0026 2 1 2
3.5700 3.5499 .0201 1 1 3
3.4500 3.4439 .0061 0 3 1
3.2800 3.2879 -.0079 1 3 1
3.2100 3.2116 -.0016 0 2 3
3.0400 3.0418 -.0018 3 2 0
a=11.051 b=10.786 c=11.99
da= .007 db= .003 dc= .01
V=1430
Triklin
Dexp Dcal d(D) h k l
10.8000 10.8182 -.0182 1 0 0
7.6900 7.6864 .0036 1 0 1
5.9500 5.9549 -.0049 1 -2 1
5.5400 5.5475 -.0075 -2 1 0
5.3000 5.3066 -.0066 2 -1 1
4.5000 4.4999 .0001 0 0 2
3.8000 3.8003 -.0003 2 -2 2
3.5700 3.5698 .0002 1 -3 2
3.4500 3.4495 .0005 0 4 0
3.2800 3.2798 .0002 -3 3 0
3.2100 3.2092 .0008 3 -2 2
3.0400 3.0403 -.0003 2 2 2
A= 11.492 DA= .002
B= 14.4360 DB= .0001
C= 9.269 DC= .005
GAMMA=106.39 DGAMMA= .01
BETA = 77.06 DBETA = .02
ALPHA= 98.31 DALPHA= .01
V= 1432.4
324. 30-1015
K2ZnCl4
Triklin
Dexp Dcal d(D) h k l
6.1000 6.1005 -.0005 1 0 1
5.0800 5.0795 .0005 1 -1 1
4.4400 4.4400 .0000 -1 -2 1
3.9300 3.9301 -.0001 2 1 1
3.5700 3.5695 .0005 -1 -3 1
3.4000 3.3995 .0005 2 -1 1
3.1000 3.0982 .0018 1 -3 1
2.9800 2.9820 -.0020 -2 -3 1
2.8700 2.8689 .0011 0 -3 2
2.6700 2.6701 -.0001 2 3 2
2.5300 2.5297 .0003 0 1 3
2.4000 2.4007 -.0007 0 5 0
A= 8.448 DA= .004
B= 12.53 DB= .01
C= 7.9409 DC= .0008
GAMMA= 73.62 DGAMMA= .08
BETA = 81.39 DBETA = .04
ALPHA= 90.14 DALPHA= .09
V= 796.2
325. 30-1316
Sr{ZnCl4}*5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.0800 5.0780 .0020 2 1 0
3.7700 3.7695 .0005 3 0 1
3.6300 3.6302 -.0002 0 0 3
3.3600 3.3593 .0007 -2 2 1
3.2800 3.2796 .0004 1 0 3
3.0700 3.0706 -.0006 4 1 0
2.6440 2.6439 .0001 -2 1 4
2.5110 2.5108 .0002 -5 0 3
1.8730 1.8729 .0001 -3 0 6
1.7740 1.7741 -.0001 -4 1 6
1.5990 1.5990 -.0000 -5 4 1
a= 13.904 b= 7.820 c=11.3389 beta= 106.16
da= .003 db=.002 dc= .0007 dbeta=.01
V= 1184.16
326. 30-1469
Zn*Al**Si*O
Tetragon
Groupa 86
Dexp. Dcal. d(D) h k l
4.6100 4.6020 .0080 0 0 2
3.5100 3.5054 .0046 1 0 2
2.3300 2.3321 -.0021 2 0 2
2.3000 2.3010 -.0010 0 0 4
2.0300 2.0291 .0009 2 0 3
1.9000 1.8998 .0002 2 1 3
a= 5.410 c= 9.20
da= .006 dc= .02
V= 269.4
327. 30-1475
C2H4N2O4Zn
Triklin
Dexp Dcal d(D) h k l
5.5900 5.5900 -.0000 0 0 1
5.3800 5.3735 .0065 1 1 0
5.0200 5.0186 .0014 0 -2 1
4.9100 4.9077 .0023 1 2 0
4.3400 4.3403 -.0003 1 3 0
4.1700 4.1656 .0044 1 1 1
3.8800 3.8888 -.0088 0 -4 1
3.7900 3.7979 -.0079 1 4 0
3.2900 3.2891 .0009 -1 -3 1
3.0200 3.0204 -.0004 1 -5 1
2.8700 2.8725 -.0025 0 6 1
2.7500 2.7492 .0008 2 -1 0
A= 5.61911 DA= .00004
B= 20.69764 DB= .00001
C= 5.66261 DC= .00008
GAMMA= 89.986 DGAMMA= .001
BETA = 81.238 DBETA = .001
ALPHA= 92.7131 DALPHA= .0008
V=650.1
328. 30-1476
C2H8N4O4Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.0400 6.0336 .0064 1 1 1
5.3200 5.3147 .0053 -1 1 1
4.7500 4.7561 -.0061 -1 0 2
3.8000 3.8034 -.0034 2 0 3
3.3400 3.3414 -.0014 3 0 3
3.1100 3.1087 .0013 4 0 0
2.9600 2.9581 .0019 -1 2 2
2.8400 2.8418 -.0018 3 2 1
2.7800 2.7806 -.0006 -3 1 2
2.6700 2.6683 .0017 4 1 3
2.4600 2.4609 -.0009 4 2 1
2.1000 2.0999 .0001 2 3 3
2.0600 2.0599 .0001 -4 1 3
a= 12.98 b= 7.555 c= 12.088 beta= 73.39
da= .02 db=.006 dc=.002 dbeta=.01
V= 1135.7
329. 3-1477
C2H4O4Zn*H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
6.5800 6.5899 -.0099 0 1 0
5.2600 5.2636 -.0036 -2 1 1
4.5600 4.5616 -.0016 -3 1 1
3.6900 3.6893 .0007 -5 0 2
3.5500 3.5504 -.0004 3 1 2
3.0900 3.0894 .0006 -4 0 4
2.9800 2.9795 .0005 4 0 3
2.7500 2.7502 -.0002 -7 0 2
2.6500 2.6502 -.0002 -2 2 3
2.4700 2.4672 .0028 2 0 5
2.3200 2.3206 -.0006 -6 2 1
2.2100 2.2100 .0000 4 2 3
a= 19.62 b= 6.590 c= 13.83 beta= 102.33
da= .02 db=.002 dc=.01 dbeta=.09
V= 1747
Triklin
Dexp Dcal d(D) h k l
6.5800 6.5893 -.0093 0 0 1
5.2600 5.2601 -.0001 -1 1 0
4.5600 4.5633 -.0033 0 -2 1
3.6900 3.6922 -.0022 -1 3 1
3.5500 3.5505 -.0005 -1 -3 1
3.0900 3.0883 .0017 -2 1 1
2.9800 2.9772 .0028 0 -4 1
2.7500 2.7505 -.0005 2 2 0
2.6500 2.6496 .0004 -2 -3 1
2.4700 2.4699 .0001 1 0 2
2.3200 2.3206 -.0006 2 4 0
2.2100 2.2102 -.0002 -1 6 1
A= 6.3524 DA= .0002
B= 14.280 DB= .006
C= 7.240 DC= .002
GAMMA= 89.01 DGAMMA= .01
BETA =113.58 DBETA = .05
ALPHA= 84.16 DALPHA= .04
V= 597.6
330. 30-1484
Zn3Mo2O9
Triklin
Dexp Dcal d(D) h k l
7.4700 7.4571 .0129 1 0 0
6.9100 6.9136 -.0036 0 1 0
4.9700 4.9616 .0084 0 1 1
4.1900 4.1985 -.0085 1 1 0
3.8900 3.8920 -.0020 -1 2 0
3.7300 3.7286 .0014 2 0 0
3.6100 3.6132 -.0032 1 1 1
3.5800 3.5769 .0031 0 0 2
3.4600 3.4568 .0032 0 2 0
3.4200 3.4219 -.0019 1 -2 1
3.3000 3.3004 -.0004 2 0 1
3.2200 3.2195 .0005 1 0 2
A= 8.396 DA= .007
B= 7.784 DB= .004
C= 7.154 DC= .003
GAMMA=117.36 DGAMMA= .02
BETA = 90.18 DBETA = .05
ALPHA= 90.1308 DALPHA= .0007
V= 415.3
331. 30-1491
Zn3{PO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
7.9200 7.9255 -.0055 0 1 0
5.2500 5.2451 .0049 -1 -1 1
4.8100 4.8070 .0030 0 -1 2
4.4900 4.4877 .0023 1 1 1
4.2600 4.2605 -.0005 1 -1 1
3.9200 3.9199 .0001 1 0 2
3.6400 3.6381 .0019 -1 -2 1
3.5100 3.5093 .0007 1 1 2
3.2000 3.1996 .0004 2 0 0
3.0200 3.0181 .0019 -1 2 1
2.9380 2.9367 .0013 -2 0 2
2.8550 2.8536 .0014 -1 -2 3
A= 6.5416 DA= .0004
B= 8.098 DB= .001
C= 11.1968 DC= .0008
GAMMA= 80.66 DGAMMA= .01
BETA = 98.751 DBETA = .004
ALPHA= 98.55 DALPHA= .02
V=573.8
332. 30-1493
beta-ZnTi}O4
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
5.9600 5.9718 -.0119 0 1 1
4.8700 4.8752 -.0052 1 1 1
3.4800 3.4862 -.0062 2 1 0
3.0000 3.0023 -.0023 1 1 3
2.9850 2.9859 -.0009 0 2 2
2.5500 2.5520 -.0020 1 0 4
2.5300 2.5250 .0050 -3 0 1
2.4400 2.4405 -.0005 3 0 2
2.3400 2.3401 -.0001 -2 2 2
2.2500 2.2500 .0000 -1 3 1
2.1200 2.1200 .0000 -2 0 4
a= 7.97 b= 7.258 c= 10.538 beta= 85.71
da= .01 db= .003 dc=.002 dbet=.01
V=606.6
333. 30-1999
C36H24Cl4N6O3Zn2*2H2O
Triklin
Dexp Dcal d(D) h k l
9.9300 9.9291 .0009 0 1 0
8.6600 8.6667 -.0067 1 0 1
6.5100 6.5006 .0094 0 -1 2
5.8600 5.8532 .0068 2 -1 1
5.7900 5.7939 -.0039 1 0 2
5.6400 5.6401 -.0001 1 -2 2
5.2100 5.2127 -.0027 1 1 1
4.3500 4.3525 -.0025 -2 1 1
4.2700 4.2748 -.0048 2 -2 3
4.1900 4.1848 .0052 2 -1 3
4.0200 4.0220 -.0020 0 -2 3
3.9300 3.9300 -.0000 1 2 0
A= 11.716 DA= .007
B= 12.186 DB= .001
C= 14.481 DC= .008
GAMMA=118.334 DGAMMA= .006
BETA = 68.40 DBETA = .04
ALPHA=118.985 DALPHA= .009
V= 1566.2
334. 30-2000
C36H28I6N4Zn
Triklin
Dexp Dcal d(D) h k l
7.6600 7.6426 .0174 0 1 1
6.6700 6.6860 -.0160 1 1 0
6.4100 6.4090 .0010 0 -1 1
5.3200 5.3150 .0050 0 2 0
5.1900 5.1900 .0000 1 -1 1
4.1300 4.1274 .0026 1 2 2
3.8200 3.8213 -.0013 0 2 2
3.7000 3.6978 .0022 -1 -2 1
3.5200 3.5203 -.0003 0 3 1
3.4400 3.4413 -.0013 1 3 0
3.3500 3.3498 .0002 -2 1 0
3.2200 3.2203 -.0003 1 0 3
3.1400 3.1400 .0000 1 2 3
2.8100 2.8101 -.0001 0 -1 3
A= 8.16 DA= .01
B= 11.146 DB= .004
C= 10.016 DC= .003
GAMMA= 75.66 DGAMMA= .06
BETA = 68.50 DBETA = .02
ALPHA= 75.55 DALPHA= .03
V= 808.4
335. 31-0079
{NH4}2Zn10{TeMo6O24}4{OH}3*46H2O
Triklin
Dexp Dcal d(D) h k l
8.0600 8.0495 .0105 1 0 0
6.2300 6.2312 -.0012 1 1 0
5.6900 5.6984 -.0084 0 1 1
4.9400 4.9414 -.0014 -1 1 1
4.6500 4.6522 -.0022 1 0 1
3.8700 3.8708 -.0008 1 2 0
3.3800 3.3812 -.0012 1 2 1
3.2100 3.2082 .0018 -1 -1 2
3.1200 3.1191 .0009 2 0 1
3.0500 3.0527 -.0027 0 -1 2
2.8500 2.8492 .0008 0 2 2
2.8000 2.7994 .0006 1 -2 1
A= 8.4795 DA= .0002
B= 8.226 DB= .005
C= 7.336 DC= .009
GAMMA= 82.61 DGAMMA= .01
BETA =105.82 DBETA = .01
ALPHA= 84.26 DALPHA= .08
V= 483.3
336. 31-1135
K2Zn{IO3}4*2H2O
Triklin
Dexp Dcal d(D) h k l
6.2200 6.2256 -.0056 0 0 1
5.4300 5.4211 .0089 1 0 0
4.1200 4.1205 -.0005 0 -2 1
3.8200 3.8195 .0005 -1 -1 1
3.4400 3.4398 .0002 1 -2 1
3.2800 3.2753 .0047 0 -1 2
3.1400 3.1414 -.0014 -1 -2 1
2.8000 2.7959 .0041 1 0 2
2.7400 2.7428 -.0028 1 -2 2
2.5600 2.5598 .0002 2 0 1
2.4800 2.4781 .0019 -1 -3 1
2.2300 2.2301 -.0001 2 2 0
A= 5.452 DA= .001
B= 8.818 DB= .001
C= 6.593 DC= .005
GAMMA= 94.09 DGAMMA= .01
BETA = 84.44 DBETA = .02
ALPHA=108.71 DALPHA= .04
V= 298.5
337. 31-1464
{Zn{NH3}4}{BH4}2
Triklin
Dexp Dcal d(D) h k l
5.2000 5.1944 .0056 1 0 0
4.0300 4.0350 -.0050 -1 1 0
3.5900 3.5824 .0076 0 0 1
3.2200 3.2191 .0009 0 -1 1
2.9400 2.9441 -.0041 0 2 0
2.6600 2.6599 .0001 -1 0 1
2.4900 2.4891 .0009 1 2 0
2.3400 2.3372 .0028 2 -1 1
2.0700 2.0695 .0005 1 2 1
1.9300 1.9307 -.0007 -1 2 1
1.7200 1.7212 -.0012 3 -1 1
1.6200 1.6203 -.0003 -2 3 0
A= 5.384 DA= .002
B= 5.952 DB= .004
C= 3.727 DC= .002
GAMMA= 95.67 DGAMMA= .09
BETA = 75.25 DBETA = .03
ALPHA= 97.44 DALPHA= .05
V= 114.2
338. 31-1465
Zn{NH3}2CS3
Triklin
Dexp Dcal d(D) h k l
5.9800 5.9803 -.0003 -1 1 0
5.6700 5.6683 .0017 -1 1 1
4.9800 4.9803 -.0003 -1 -1 1
4.5500 4.5514 -.0014 1 0 1
3.6000 3.6000 .0000 -2 1 1
3.2100 3.2123 -.0023 1 -2 1
3.1500 3.1498 .0002 0 -1 2
2.6960 2.6957 .0003 0 -2 2
2.2790 2.2790 .0000 -1 -1 3
2.1590 2.1589 .0001 1 1 3
2.1200 2.1200 -.0000 -1 4 3
2.0650 2.0650 -.0000 1 3 3
1.9087 1.9088 -.0001 -2 -4 2
1.8937 1.8939 -.0002 -3 4 2
A= 7.718 DA= .004
B= 11.656 DB= .002
C= 7.591 DC= .001
GAMMA= 89.29 DGAMMA= .03
BETA =104.93 DBETA = .02
ALPHA= 75.581 DALPHA= .003
V= 636.9
339. 31-1474
ZnSO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.6500 4.6626 -.0126 -1 0 2
4.3000 4.2995 .0005 2 1 1
4.0400 4.0473 -.0073 -2 0 2
3.9320 3.9338 -.0018 0 2 0
3.6960 3.6983 -.0023 2 0 2
3.6390 3.6400 -.0010 0 2 1
3.0080 3.0091 -.0011 -1 2 2
2.9200 2.9205 -.0005 -4 1 1
2.8980 2.8997 -.0017 3 2 0
2.8300 2.8279 .0021 -3 2 1
2.7980 2.7972 .0008 -2 1 3
2.6880 2.6917 -.0037 2 2 2
A= 12.943 DA= .004
B= 7.8676 DB= .0005
C= 9.688 DC= .001
BETA = 95.384 DBETA = .02
V =982.1
340. 31-1475
ZnSO3*0.5H2O
Triklin
Dexp Dcal d(D) h k l
6.1900 6.1926 -.0026 0 1 1
6.0300 6.0306 -.0006 0 -1 1
5.8900 5.8965 -.0065 -1 1 0
5.3300 5.3370 -.0070 1 -1 1
4.2300 4.2292 .0008 0 -1 3
4.1000 4.0995 .0005 1 1 1
3.7470 3.7483 -.0013 1 1 2
3.7000 3.7006 -.0006 2 0 0
3.5560 3.5527 .0033 2 -1 1
3.5310 3.5303 .0007 0 -1 4
3.4210 3.4243 -.0033 -2 1 3
3.3080 3.3096 -.0016 -1 0 5
A= 7.899 DA= .006
B= 6.907 DB= .001
C= 17.469 DC= .004
GAMMA=108.76 DGAMMA= .07
BETA = 99.503 DBETA = .008
ALPHA= 84.823 DALPHA= .007
V= 889.4
341. 31-1550
C12H46B4BaO3Zn
Triklin
Dexp Dcal d(D) h k l
4.1200 4.1203 -.0003 0 1 0
3.0400 3.0399 .0001 -1 -1 1
2.5300 2.5309 -.0009 0 -1 2
2.1700 2.1695 .0005 -2 0 1
1.8000 1.8000 -.0000 -2 0 2
1.6600 1.6611 -.0011 2 2 0
1.4800 1.4799 .0001 -2 -1 3
1.3900 1.3900 -.0000 3 -1 1
1.2800 1.2799 .0001 1 3 1
1.2300 1.2301 -.0001 2 -2 3
1.1800 1.1800 .0000 4 0 0
1.1500 1.1498 .0002 -2 -2 4
A= 4.7596 DA= .0005
B= 4.21605 DB= .00001
C= 5.706 DC= .001
GAMMA= 82.611 DGAMMA= .006
BETA = 90.790 DBETA = .005
ALPHA= 99.802 DALPHA= .004
V= 111.9
342. 31-1989
C26H20N6O4Zn
Triklin
Dexp Dcal d(D) h k l
9.7000 9.7009 -.0009 1 0 0
8.8000 8.7996 .0004 0 1 0
7.1000 7.0992 .0008 0 1 1
5.6600 5.6614 -.0014 -1 -1 1
5.2500 5.2501 -.0001 1 1 2
4.8900 4.8901 -.0001 -1 1 1
4.6900 4.6899 .0001 0 -1 2
4.4000 4.3998 .0002 0 2 0
4.1600 4.1602 -.0002 0 2 1
4.0100 4.0098 .0002 -2 -1 1
A= 10.5708 DA= .0001
B= 9.188 DB= .001
C= 11.971 DC= .002
GAMMA= 73.44 DGAMMA= .01
BETA = 71.933 DBETA = .005
ALPHA= 82.81 DALPHA= .01
V= 1058.56
343. 31-1990
C16H14N4O4Zn
Triklin
Dexp Dcal d(D) h k l
9.9000 9.9025 -.0025 1 0 0
8.6000 8.6158 -.0158 0 1 0
7.3000 7.2996 .0004 0 -1 1
5.8700 5.8678 .0022 1 -1 1
5.4000 5.3996 .0004 0 -1 2
5.1600 5.1601 -.0001 -1 0 2
4.9300 4.9309 -.0009 1 -1 2
4.7000 4.7002 -.0002 2 1 1
4.1400 4.1397 .0003 1 2 1
3.9700 3.9699 .0001 1 -1 3
A= 10.325 DA= .003
B= 8.725 DB= .001
C= 14.411 DC= .002
GAMMA= 80.95 DGAMMA= .01
BETA = 75.956 DBETA = .01
ALPHA= 87.22 DALPHA= .01
V=1243.8
344. 31-1991
C12H8N2O4Zn
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
7.3000 7.2917 .0083 -1 0 1
6.2000 6.1893 .0107 0 1 1
5.1500 5.1286 .0214 0 0 2
4.8400 4.8287 .0113 1 1 1
4.2900 4.2955 -.0055 -2 0 1
3.8100 3.8132 -.0032 2 1 0
3.6300 3.6296 .0004 0 2 1
3.4100 3.4148 -.0048 2 1 1
3.1000 3.1014 -.0014 -1 1 3
2.8800 2.8796 .0004 -2 2 1
2.8100 2.8127 -.0027 1 1 3
2.7500 2.7496 .0004 -3 1 1
a= 8.882 b= 7.761 c=10.405 beta= 99.66
da=.008 db=.006 dc= .002 dbet=.01
V=707.6
Triklin
Dexp Dcal d(D) h k l
7.3000 7.2796 .0204 0 1 1
6.2000 6.2000 -.0000 1 0 1
5.1500 5.1475 .0025 0 -1 1
4.8400 4.8403 -.0003 -1 1 1
4.2900 4.2857 .0043 1 2 1
3.8100 3.8099 .0001 2 0 1
3.6300 3.6286 .0014 -2 1 0
3.4100 3.4125 -.0025 2 -1 1
3.1000 3.1000 -.0000 2 0 2
2.8800 2.8779 .0022 -2 2 1
2.8100 2.8125 -.0025 -2 -1 1
2.7500 2.7499 .0001 1 1 3
A= 7.889 DA= .001
B= 10.1640 DB= .0002
C= 8.322 DC= .005
GAMMA= 88.68 DGAMMA= .08
BETA = 76.24 DBETA = .06
ALPHA= 70.27 DALPHA= .02
V= 608.8
345. 31-1992
C12H8N2O4Zn*4H2O
Triklin
Dexp Dcal d(D) h k l
7.5000 7.5051 -.0051 0 1 1
6.6000 6.5887 .0113 0 -1 1
6.0000 6.0032 -.0032 1 1 1
5.3000 5.3069 -.0069 -1 0 1
5.1000 5.0983 .0017 1 2 0
4.2300 4.2293 .0007 0 1 2
3.9600 3.9642 -.0042 -1 2 1
3.8800 3.8787 .0013 0 -1 2
3.8000 3.7974 .0026 1 3 0
3.5700 3.5740 -.0040 1 -1 2
3.4400 3.4445 -.0045 2 2 1
3.3400 3.3394 .0006 -1 -1 2
A= 7.743 DA= .004
B= 12.417 DB= .002
C= 8.779 DC= .004
GAMMA= 80.48 DGAMMA= .02
BETA = 80.48 DBETA = .02
ALPHA= 80.74 DALPHA= .01
V= 813.1
346. 31-1993
C12H8N2O6Zn*5H2O
Rombik
Groupa 27
Dexp. Dcal. d(D) h k l
18.4000 18.2468 .1532 1 0 0
9.7100 9.5220 .1880 0 2 0
6.5600 6.5876 -.0276 2 2 0
6.1000 6.0823 .0177 3 0 0
5.8200 5.7939 .0261 3 1 0
4.7400 4.7610 -.0210 0 4 0
4.6200 4.6068 .0132 1 4 0
4.1100 4.1140 -.0040 4 2 0
3.5200 3.5148 .0052 2 5 0
3.2900 3.2938 -.0038 4 4 0
3.2300 3.2281 .0019 3 5 0
3.1200 3.1200 .0000 4 2 1
2.6900 2.6908 -.0008 1 7 0
a=18.25 b=19.044 c= 4.79
da= .02 db= .001 dc= .02
v=1663