188. 21-1381
beta-Na2Zn{SO4}2
Triklin
Dexp Dcal d(D) h k l
8.4900 8.4798 .0102 0 1 1
6.1800 6.1785 .0015 0 -1 1
5.1800 5.1795 .0005 -1 0 1
4.4300 4.4300 .0000 -1 -1 1
3.9200 3.9195 .0005 1 -2 1
3.8300 3.8360 -.0060 1 0 2
3.7500 3.7527 -.0027 1 2 2
3.3600 3.3588 .0012 2 1 0
3.1500 3.1512 -.0012 -2 0 1
2.9000 2.8997 .0003 2 -2 1
2.8600 2.8587 .0013 1 1 3
2.8400 2.8395 .0005 1 2 3
A= 7.120 DA= .001
B= 13.37187 DB= .00004
C= 9.069 DC= .001
GAMMA= 91.27 DGAMMA= .01
BETA = 84.63 DBETA = .01
ALPHA= 70.934 DALPHA= .001
V= 811.2
189. 21-1382
delta-Na2Zn{SO4}2
Triklin
Dexp Dcal d(D) h k l
6.0600 6.0599 .0001 -1 -1 2
4.4300 4.4302 -.0002 -1 1 1
4.3000 4.3002 -.0002 -1 -1 3
3.8300 3.8311 -.0011 0 -2 2
3.7600 3.7604 -.0004 -1 -2 3
3.3400 3.3341 .0059 2 0 1
3.1100 3.1084 .0016 -2 1 1
2.8900 2.8907 -.0007 -2 -3 3
2.8500 2.8491 .0009 -3 -2 3
2.8200 2.8221 -.0021 -3 -1 3
2.7600 2.7574 .0026 0 -3 1
2.7400 2.7413 -.0013 0 0 4
A= 8.992 DA= .005
B= 9.1992 DB= .0001
C= 12.912 DC= .004
GAMMA= 64.513 DGAMMA= .003
BETA =116.26 DBETA = .04
ALPHA=116.79 DALPHA= .02
V= 818.7
190. 21-1383
alfa-Na2Zn{SO4}2
Triklin
Dexp Dcal d(D) h k l
8.4100 8.4462 -.0362 0 0 1
7.4300 7.4361 -.0061 1 1 0
5.9800 5.9802 -.0002 2 0 0
4.7400 4.7471 -.0071 0 2 0
4.3400 4.3384 .0016 1 0 2
3.8600 3.8586 .0014 0 1 2
3.7000 3.7014 -.0014 -1 0 2
3.2200 3.2227 -.0027 -2 2 1
3.0600 3.0594 .0006 1 3 0
2.8200 2.8192 .0008 -1 3 1
2.7100 2.7096 .0004 -3 2 1
2.6200 2.6196 .0004 -4 0 1
2.5300 2.5300 -.0000 4 2 0
2.3900 2.3901 -.0001 5 1 1
a= 12.355 b= 9.494 c= 8.723 beta= 75.47
da= .006 db=.007 dc=.01 dbeta=.02
V= 990.8
191. 21-1384
Na2Zn{SO4}2*2H2O
Triklin
Dexp Dcal d(D) h k l
6.3200 6.3281 -.0081 1 -1 1
5.0000 5.0030 -.0030 -1 -2 1
4.7100 4.7015 .0085 1 1 1
4.5200 4.5253 -.0053 2 1 0
4.3000 4.3022 -.0021 -2 0 2
3.5000 3.5059 -.0059 3 0 0
3.3300 3.3301 -.0001 1 -3 1
3.1800 3.1802 -.0002 -1 -3 3
3.0700 3.0683 .0017 3 -1 1
2.8300 2.8296 .0004 -2 -2 4
2.6900 2.6892 .0008 2 3 0
2.6300 2.6294 .0006 4 0 0
A= 11.028 DA= .001
B= 10.840 DB= .001
C= 11.729 DC= .004
GAMMA= 84.842 DGAMMA= .006
BETA =107.27 DBETA = .01
ALPHA=116.67 DALPHA= .02
V=1194.3
192. 21-1396
SrZnP2O7
Triklin
Dexp Dcal d(D) h k l
6.9300 6.9293 .0007 1 0 0
6.4600 6.4566 .0034 1 1 0
6.3900 6.3807 .0093 0 1 1
4.4600 4.4531 .0069 -1 2 1
4.0700 4.0687 .0013 1 0 1
3.9000 3.8977 .0023 -1 0 2
3.7700 3.7689 .0011 -1 1 2
3.4500 3.4521 -.0021 0 1 2
3.3200 3.3236 -.0036 -2 0 2
3.2500 3.2475 .0025 0 -1 2
3.1500 3.1483 .0017 -2 2 1
3.0800 3.0783 .0017 0 4 0
A= 7.825 DA= .002
B= 12.468 DB= .004
C= 7.8188 DC= .0009
GAMMA= 83.94 DGAMMA= .01
BETA =116.47 DBETA = .01
ALPHA= 86.75 DALPHA= .03
V=674.8
193. 21-1468
C4H12N2O4Zn
Triklin
Dexp Dcal d(D) h k l
7.3500 7.3559 -.0059 0 0 2
6.3400 6.3308 .0092 1 0 1
5.9200 5.9256 -.0056 0 2 0
5.5200 5.5141 .0059 0 -2 2
5.4500 5.4480 .0020 1 1 1
5.2000 5.1922 .0078 1 0 2
5.0200 4.9915 .0285 0 2 1
4.9400 4.9433 -.0033 -1 1 1
4.7700 4.7691 .0009 -1 0 2
4.6500 4.6606 -.0106 -1 -2 1
4.2500 4.2526 -.0026 1 -2 2
4.1500 4.1471 .0029 0 -3 1
A= 6.7682 DA= .0001
B= 12.468 DB= .001
C= 15.490 DC= .001
GAMMA= 87.010 DGAMMA= .005
BETA = 86.266 DBETA = .006
ALPHA=107.598 DALPHA= .003
V=1240.5
194. 21-1470
Zn3B10O18*14H2O
Triklin
Dexp Dcal d(D) h k l
8.2000 8.1982 .0018 1 0 0
5.8000 5.8003 -.0003 0 1 0
5.4000 5.3999 .0001 0 1 1
5.0000 4.9884 .0116 0 -1 1
4.1100 4.1102 -.0002 -1 1 1
3.8300 3.8446 -.0146 0 0 3
3.2800 3.2802 -.0002 -2 -1 2
3.0200 3.0198 .0002 1 2 0
2.9000 2.9002 -.0002 0 2 0
2.8100 2.8060 .0040 -1 0 4
2.7100 2.7101 -.0001 2 1 3
2.5200 2.5200 .0000 -1 2 1
A= 8.579 DA= .001
B= 6.071 DB= .002
C= 11.620 DC= .004
GAMMA= 73.75 DGAMMA= .01
BETA = 94.108 DBETA = .02
ALPHA= 85.74 DALPHA= .01
V= 576.7
195. 21-1471
Zn2B6O11*7H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8000 5.8078 -.0078 1 1 1
4.3500 4.3520 -.0020 1 0 3
3.8600 3.8594 .0006 2 0 0
3.6200 3.6221 -.0021 2 1 1
3.3000 3.3002 -.0002 2 0 3
2.9800 2.9794 .0006 2 2 0
2.8800 2.8785 .0015 1 3 1
2.6000 2.6011 -.0011 -1 3 2
2.4800 2.4812 -.0012 3 1 0
2.3100 2.3104 -.0004 0 4 1
2.1700 2.1700 -.0000 1 4 2
2.0900 2.0904 -.0004 -1 0 6
a= 7.880 b= 9.3740 c= 14.07 beta= 78.4
da= .006 db=.0007 dc=.03 dbeta=.1
V= 1018
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8012 -.0012 1 0 0
4.3500 4.3401 .0099 0 1 1
3.8600 3.8612 -.0012 -1 -1 1
3.6200 3.6196 .0004 1 0 1
3.3000 3.3008 -.0008 1 -1 1
2.9800 2.9780 .0020 1 1 1
2.8800 2.8796 .0004 -1 -1 2
2.6000 2.6015 -.0015 -2 1 2
2.4800 2.4814 -.0014 2 1 0
2.3100 2.3099 .0001 -2 2 0
2.1700 2.1701 -.0001 0 2 2
2.0900 2.0892 .0008 0 0 3
A= 6.3648 DA= .0007
B= 6.291 DB= .004
C= 6.7932 DC= .0006
GAMMA= 99.107 DGAMMA= .007
BETA =112.62 DBETA = .07
ALPHA= 88.236 DALPHA= .004
V= 247.8
196. 21-1472
ZnB10O16*4.5H2O
Triklin
Dexp Dcal d(D) h k l
5.9000 5.8872 .0128 -1 1 1
5.2000 5.2042 -.0042 1 1 1
4.8000 4.7918 .0082 2 0 1
4.7000 4.6982 .0018 1 0 2
4.0400 4.0401 -.0001 -1 0 2
3.3200 3.3188 .0012 0 2 2
3.2300 3.2290 .0010 0 1 3
3.0000 3.0034 -.0034 3 0 2
2.6300 2.6301 -.0001 -2 1 3
2.5600 2.5586 .0014 3 0 3
2.4500 2.4499 .0001 1 0 4
2.3700 2.3695 .0005 1 -3 1
A= 10.453 DA= .002
B= 7.84408 DB= .00004
C= 9.9881 DC= .0005
GAMMA=105.120 DGAMMA= .009
BETA = 82.414 DBETA = .008
ALPHA= 79.283 DALPHA= .005
V=762.4
197. 21-1472
ZnB10O16*4.5H2O
Triklin
Dexp Dcal d(D) h k l
5.9000 5.8872 .0128 -1 1 1
5.2000 5.2042 -.0042 1 1 1
4.8000 4.7918 .0082 2 0 1
4.7000 4.6982 .0018 1 0 2
4.0400 4.0401 -.0001 -1 0 2
3.3200 3.3188 .0012 0 2 2
3.2300 3.2290 .0010 0 1 3
3.0000 3.0034 -.0034 3 0 2
2.6300 2.6301 -.0001 -2 1 3
2.5600 2.5586 .0014 3 0 3
2.4500 2.4499 .0001 1 0 4
2.3700 2.3695 .0005 1 -3 1
A= 10.453 DA= .002
B= 7.84408 DB= .00004
C= 9.9881 DC= .0005
GAMMA=105.120 DGAMMA= .009
BETA = 82.414 DBETA = .008
ALPHA= 79.283 DALPHA= .005
V=762.4
198. 21-1473
Zn2B6O11*3H2O
Triklin
Dexp Dcal d(D) h k l
4.2300 4.2234 .0066 -1 1 1
3.6700 3.6699 .0001 -1 -3 1
3.4800 3.4961 -.0161 1 2 2
3.1800 3.1813 -.0013 1 -1 3
2.9600 2.9605 -.0005 2 1 2
2.7800 2.7780 .0020 2 2 2
2.6500 2.6495 .0005 -2 -2 2
2.5300 2.5294 .0006 2 -2 2
2.3300 2.3308 -.0008 0 4 2
2.1100 2.1106 -.0006 3 3 1
1.9900 1.9901 -.0001 3 1 3
1.9400 1.9393 .0007 0 6 0
A= 6.7534 DA= .0004
B= 12.2133 DB= .0008
C= 10.5109 DC= .001
GAMMA= 76.73 DGAMMA= .02
BETA = 83.03 DBETA = .02
ALPHA= 99.78 DALPHA= .01
V=819.9
199. 21-1474
Zn6B10O21*3H2O
Triklin
Dexp Dcal d(D) h k l
4.6000 4.5992 .0008 -1 1 0
3.2100 3.2099 .0001 0 0 1
2.6300 2.6295 .0005 0 -2 1
2.0400 2.0396 .0004 -2 -2 1
1.8500 1.8497 .0003 -2 -3 1
1.7300 1.7288 .0012 -3 2 0
1.6100 1.6099 .0001 2 5 0
1.5200 1.5200 .0000 -1 0 2
1.4400 1.4398 .0002 3 -3 1
1.3700 1.3701 -.0001 -4 2 0
1.3100 1.3102 -.0002 2 -5 1
1.2600 1.2598 .0002 2 6 1
A= 6.289 DA= .001
B= 8.600 DB= .001
C= 3.2259 DC= .0002
GAMMA= 79.81 DGAMMA= .01
BETA = 85.32 DBETA = .01
ALPHA= 92.40 DALPHA= .01
V= 170.86
200. 21-1475
C20H30B4O22Zn
Triklin
Dexp Dcal d(D) h k l
7.5000 7.4990 .0010 -1 0 1
6.1000 6.1007 -.0007 0 1 1
5.3000 5.3026 -.0026 0 -1 1
3.9300 3.9277 .0023 2 1 1
3.5000 3.5023 -.0023 -1 -1 2
3.1800 3.1803 -.0003 1 2 1
3.0600 3.0595 .0005 3 1 1
2.8500 2.8504 -.0004 -2 0 3
2.7300 2.7299 .0001 3 -1 2
2.6000 2.6016 -.0016 4 -1 1
2.4900 2.4894 .0006 -4 0 2
2.3500 2.3503 -.0003 -1 3 1
2.1700 2.1700 -.0000 -4 0 3
A= 11.5144 DA= .0005
B= 7.09840 DB= .00008
C= 9.839 DC= .001
GAMMA= 97.49 DGAMMA= .01
BETA = 92.62 DBETA = .01
ALPHA= 81.283 DALPHA= .001
V= 787.8
201. 21-1481
ZnH2P2O7
Triklin
Dexp Dcal d(D) h k l
8.3700 8.3455 .0245 0 1 1
7.2100 7.1963 .0137 0 -1 1
6.3400 6.3414 -.0014 1 0 0
5.0000 5.0092 -.0092 1 2 1
4.8800 4.8795 .0005 -1 0 1
4.6600 4.6535 .0065 -1 -1 1
4.3800 4.3806 -.0006 -1 1 1
4.2100 4.2060 .0040 1 2 2
3.8500 3.8446 .0054 1 3 1
3.6000 3.5981 .0019 0 -2 2
3.4500 3.4499 .0001 1 1 3
3.2300 3.2321 -.0021 2 1 0
A= 6.746 DA= .001
B= 12.356 DB= .006
C= 10.698 DC= .003
GAMMA= 75.539 DGAMMA= .001
BETA = 73.802 DBETA = .005
ALPHA= 77.997 DALPHA= .001
V= 819.9
202. 21-1483
Zn3Mo2O9
Triklin
Dexp Dcal d(D) h k l
4.6000 4.5936 .0064 2 1 1
4.1900 4.1938 -.0038 2 -1 1
3.8800 3.8666 .0134 3 1 1
3.7200 3.7260 -.0060 -2 -1 1
3.5900 3.5863 .0037 4 0 0
3.4100 3.4069 .0031 2 4 0
3.2200 3.2188 .0012 -2 3 1
3.1700 3.1708 -.0008 -4 2 0
2.9760 2.9769 -.0009 -2 -3 1
2.7770 2.7773 -.0003 -1 -4 1
2.6880 2.6926 -.0046 -4 -1 1
2.6270 2.6334 -.0064 -5 2 0
A= 14.5799 DA= .0006
B= 15.25 DB= .02
C= 5.343 DC= .003
GAMMA= 85.44 DGAMMA= .06
BETA = 80.19 DBETA = .01
ALPHA= 80.98 DALPHA= .08
V=1152.3
203. 21-1483
Zn3Mo2O9
Triklin
Dexp Dcal d(D) h k l
4.6000 4.6002 -.0002 2 1 0
4.1900 4.1873 .0027 0 3 0
3.8800 3.8772 .0028 3 0 0
3.7200 3.7149 .0051 -3 3 0
3.5900 3.5893 .0007 2 2 0
3.4100 3.4191 -.0091 -2 4 0
3.2200 3.2190 .0010 1 0 1
3.1700 3.1656 .0044 -3 4 0
2.9760 2.9756 .0004 0 -2 1
2.7770 2.7822 -.0052 -2 -1 1
2.6880 2.6879 .0001 2 1 1
2.6270 2.6248 .0022 0 -3 1
A= 12.807 DA= .007
B= 13.814 DB= .006
C= 3.4057 DC= .0001
GAMMA=114.582 DGAMMA= .002
BETA = 93.50 DBETA = .01
ALPHA= 87.97 DALPHA= .04
V=547.1
204. 21-1486
ZnO
Triklin
Dexp Dcal d(D) h k l
3.3900 3.3880 .0020 0 1 1
3.1100 3.1054 .0046 0 -1 1
2.8900 2.8934 -.0034 1 1 1
2.6600 2.6618 -.0018 1 1 2
2.4600 2.4630 -.0030 -1 -1 1
2.3000 2.3008 -.0008 0 1 3
2.1500 2.1500 .0000 -1 1 1
2.0300 2.0312 -.0012 1 -1 2
1.9100 1.9129 -.0029 1 1 4
1.6800 1.6811 -.0011 0 -2 1
1.5700 1.5697 .0003 0 2 3
1.4800 1.4799 .0001 -1 1 4
A= 3.7085 DA= .0001
B= 3.6573 DB= .0001
C= 8.5322 DC= .0005
GAMMA= 75.944 DGAMMA= .006
BETA = 76.073 DBETA = .008
ALPHA= 80.131 DALPHA= .005
V=108.15
205. 21-1978
C18H24Cl2NPZn
Triklin
Dexp Dcal d(D) h k l
12.5000 12.4954 .0046 1 -1 0
9.9100 9.8786 .0314 1 1 0
7.7900 7.8099 -.0199 0 0 1
6.3900 6.3848 .0052 0 2 0
5.8900 5.8939 -.0039 2 0 1
5.7700 5.7602 .0098 1 -2 1
5.3200 5.3381 -.0181 4 0 0
5.1800 5.1896 -.0096 -3 -1 1
4.5300 4.5216 .0084 4 1 0
4.3300 4.3271 .0029 1 -3 1
4.2500 4.2565 -.0065 0 3 0
4.1900 4.1908 -.0008 4 -2 1
A= 22.206 DA= .006
B= 13.646 DB= .002
C= 8.148 DC= .009
GAMMA=103.43 DGAMMA= .02
BETA = 94.91 DBETA = .08
ALPHA=104.17 DALPHA= .04
V=2303
206. 21-1979
C30H33Cl2NP2Zn
Triklin
Dexp Dcal d(D) h k l
10.3000 10.2818 .0182 0 1 1
8.8800 8.8636 .0164 -1 1 1
8.5500 8.5482 .0018 0 -1 1
7.5100 7.4999 .0101 1 0 1
6.2900 6.2780 .0120 -1 2 1
5.5000 5.4976 .0024 2 0 0
5.1900 5.1813 .0087 -1 -1 2
5.0900 5.0898 .0002 1 2 1
4.8900 4.8931 -.0031 2 1 0
4.5100 4.5127 -.0027 0 3 0
4.4300 4.4318 -.0018 -2 2 2
4.2900 4.2969 -.0069 0 1 3
A= 11.4914 DA= .0001
B= 13.97684 DB= .00008
C= 13.4948 DC= .0001
GAMMA= 99.8718 DGAMMA= .0009
BETA =105.4739 DBETA = .0004
ALPHA= 77.3358 DALPHA= .0004
V=2023.5
207. 21-1980
C16H14S4Zn
Triklin
Dexp Dcal d(D) h k l
9.4600 9.4539 .0061 -1 0 1
6.0800 6.0895 -.0095 -1 1 1
5.7700 5.7697 .0003 1 -1 1
5.3400 5.3351 .0049 -2 0 1
4.9700 4.9692 .0008 -1 0 3
4.4200 4.4182 .0018 2 -1 1
4.2600 4.2584 .0016 -2 1 2
3.9000 3.9022 -.0022 2 -1 2
3.7300 3.7304 -.0004 1 1 3
3.5000 3.4995 .0005 -3 1 1
3.1900 3.1901 -.0001 -2 2 0
3.1500 3.1513 -.0013 -3 0 3
3.0000 2.9998 .0002 3 1 0
2.8850 2.8848 .0002 2 -2 2
2.6550 2.6550 .0000 4 0 1
A= 11.199 DA= .003
B= 7.0021 DB= .0006
C= 16.024 DC= .001
GAMMA=100.92 DGAMMA= .02
BETA = 95.85 DBETA = .03
ALPHA= 87.550 DALPHA= .001
V= 1227
208. 21-1982
C16H14S6Zn
Triklin
Dexp Dcal d(D) h k l
9.9100 9.9178 -.0078 1 0 0
9.8600 9.8549 .0051 -1 1 0
8.4600 8.4578 .0022 0 0 1
5.7600 5.7645 -.0045 -1 2 0
4.7800 4.7810 -.0010 1 1 1
4.6100 4.6099 .0001 -2 0 1
4.4200 4.4209 -.0009 -1 1 2
4.2300 4.2289 .0011 0 0 2
3.8100 3.8095 .0005 1 2 0
3.4200 3.4201 -.0001 -1 -1 2
3.2600 3.2600 -.0000 -3 0 1
2.8860 2.8859 .0001 -3 4 1
A= 11.79 DA= .01
B= 11.99 DB= .01
C= 8.907 DC= .001
GAMMA=121.60 DGAMMA= .07
BETA =105.90 DBETA = .02
ALPHA= 74.12 DALPHA= .01
V= 1018.8
208. 21-1983
C16H14S5Zn
Triklin
Dexp Dcal d(D) h k l
9.4600 9.4794 -.0194 0 0 1
8.4600 8.4620 -.0020 1 0 0
6.3400 6.3436 -.0036 0 -2 1
5.7800 5.7765 .0035 0 2 1
5.6100 5.6176 -.0076 1 2 0
4.6600 4.6613 -.0013 0 -1 2
4.4200 4.4218 -.0018 0 1 2
3.9300 3.9314 -.0014 2 -1 1
3.8000 3.7998 .0002 -2 2 0
3.6900 3.6894 .0006 0 -3 2
3.5000 3.5000 -.0000 1 -3 2
3.4300 3.4284 .0016 2 2 1
A= 8.497 DA= .003
B= 15.770 DB= .002
C= 9.552 DC= .001
GAMMA= 93.17 DGAMMA= .04
BETA = 85.535 DBETA = .008
ALPHA= 95.69 DALPHA= .01
V= 1268.3
210. 21-1984
C12H12N2S2Zn
Triklin
Dexp Dcal d(D) h k l
4.5900 4.5858 .0042 0 1 1
4.2700 4.2592 .0108 -1 1 0
3.5700 3.5683 .0017 0 -1 1
3.2800 3.2825 -.0025 1 1 1
3.0000 2.9995 .0005 -1 0 1
2.7100 2.7101 -.0001 -1 2 1
2.5500 2.5474 .0026 0 1 2
2.4100 2.4083 .0017 1 2 0
2.3100 2.3133 -.0033 -2 1 0
2.2000 2.1986 .0014 1 -1 2
2.1500 2.1513 -.0013 0 -1 2
2.0900 2.0906 -.0006 -1 1 2
A= 4.72199 DA= .00004
B= 7.06723 DB= .00002
C= 5.21601 DC= .00004
GAMMA=101.7659 DGAMMA= .0002
BETA = 79.5896 DBETA = .0002
ALPHA= 77.8588 DALPHA= .0004
V=162.1
211. 21-1396
SrZnP2O7
Triklin
Dexp Dcal d(D) h k l
6.9300 6.9385 -.0085 0 1 1
6.4600 6.4523 .0077 -1 0 1
6.3900 6.3900 -.0000 0 -1 1
4.4600 4.4508 .0092 2 -1 1
4.0700 4.0726 -.0026 0 1 2
3.9000 3.8994 .0006 -1 1 2
3.7700 3.7663 .0037 1 -1 2
3.4500 3.4491 .0009 -1 -1 2
3.3200 3.3211 -.0011 2 0 2
3.2500 3.2488 .0012 -2 3 1
3.1500 3.1491 .0009 -3 2 1
3.0800 3.0806 -.0006 1 3 0
A= 10.711 DA= .006
B= 11.1689 DB= .0006
C= 8.545 DC= .004
GAMMA=107.11 DGAMMA= .01
BETA = 89.73 DBETA = .03
ALPHA= 85.472 DALPHA= .004
V= 973.6
212. 21-1468
C4H12N2O4Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
7.3500 7.3260 .0240 1 0 1
7.3500 7.4043 -.0543 -1 1 1
6.3400 6.3056 .0344 2 0 0
5.9200 5.9068 .0132 -1 0 2
5.5200 5.5383 -.0183 -2 1 1
5.4500 5.4424 .0076 2 1 0
5.0200 5.0009 .0191 0 1 2
4.9400 4.9552 -.0152 1 2 0
4.7700 4.7635 .0065 -1 2 1
4.6500 4.6292 .0208 1 0 2
4.2500 4.2534 -.0034 1 1 2
4.1500 4.1369 .0131 -2 2 1
a= 13.31 b= 10.78 c= 11.92 beta= 108.69
da=.02 db=.04 dc=.01 dbeta=.09
V= 1620.
213. 21-1470
Zn3B10O18*14H2O
Triklin
Dexp Dcal d(D) h k l
8.2000 8.1987 .0013 0 -1 1
5.8000 5.7724 .0276 1 0 1
5.4000 5.3999 .0001 0 -1 3
5.0000 4.9952 .0048 1 1 0
4.1100 4.1108 -.0008 1 1 2
3.8300 3.8295 .0005 0 2 1
3.2800 3.2798 .0002 -1 -2 3
3.0200 3.0203 -.0003 0 1 5
2.9000 2.8992 .0008 -2 0 2
2.8100 2.8101 -.0001 0 -3 1
2.7100 2.7091 .0009 2 0 3
2.5200 2.5199 .0001 1 -3 1
A= 6.12533 DA= .00009
B= 8.4557 DB= .0006
C= 18.167 DC= .002
GAMMA= 87.922 DGAMMA= .004
BETA = 90.877 DBETA = .008
ALPHA=102.85 DALPHA= .01
V=917.3
214. 21-1471
Zn2B6O11*7H2O
Triklin
Dexp Dcal d(D) h k l
5.8000 5.8012 -.0012 1 0 0
4.3500 4.3401 .0099 0 1 1
3.8600 3.8612 -.0012 -1 -1 1
3.6200 3.6196 .0004 1 0 1
3.3000 3.3008 -.0008 1 -1 1
2.9800 2.9780 .0020 1 1 1
2.8800 2.8796 .0004 -1 -1 2
2.6000 2.6015 -.0015 -2 1 2
2.4800 2.4814 -.0014 2 1 0
2.3100 2.3099 .0001 -2 2 0
2.1700 2.1701 -.0001 0 2 2
2.0900 2.0892 .0008 0 0 3
A= 6.3648 DA= .0007
B= 6.291 DB= .003
C= 6.7933 DC= .0006
GAMMA= 99.107 DGAMMA= .007
BETA =112.62 DBETA = .07
ALPHA= 88.236 DALPHA= .004
V= 247.8
215. 21-1472
ZnB10O16*4.5H2O
Triklin
Dexp Dcal d(D) h k l
5.9000 5.9032 -.0032 1 1 1
5.2000 5.1989 .0011 2 1 0
4.8000 4.8031 -.0031 -1 -1 1
4.7000 4.6885 .0115 2 0 0
4.0400 4.0388 .0012 2 2 1
3.3200 3.3213 -.0013 0 1 2
3.2300 3.2273 .0027 2 3 1
3.0000 3.0001 -.0001 2 1 2
2.6300 2.6300 .0000 -2 -1 2
2.5600 2.5598 .0002 4 1 0
2.4500 2.4493 .0007 3 3 2
2.3700 2.3705 -.0005 2 -1 2
A= 10.53 DA= .01
B= 10.27 DB= .01
C= 6.813 DC= .002
GAMMA= 62.99 DGAMMA= .08
BETA = 82.52 DBETA = .06
ALPHA= 77.02 DALPHA= .04
V= 639.6
216. 21-1473
Zn2B6O11*3H2O
Triklin
Dexp Dcal d(D) h k l
4.2300 4.2310 -.0010 2 0 1
3.6700 3.6693 .0007 2 -2 1
3.4800 3.4850 -.0050 -2 0 1
3.1800 3.1804 -.0004 2 0 2
2.9600 2.9595 .0005 -2 -2 1
2.7800 2.7790 .0010 2 2 1
2.6500 2.6487 .0013 -2 2 1
2.5300 2.5305 -.0005 2 -1 3
2.3300 2.3308 -.0008 0 4 0
2.1100 2.1099 .0001 2 -4 3
1.9900 1.9878 .0022 2 -2 4
1.9400 1.9399 .0001 -2 -4 2
A= 9.247 DA= .004
B= 10.106 DB= .001
C= 8.0878 DC= .0008
GAMMA= 99.235 DGAMMA= .003
BETA = 75.07 DBETA = .01
ALPHA=112.37 DALPHA= .01
V=673.3
217. 21-1474
Zn6B10O21*3H2O
Triklin
Dexp Dcal d(D) h k l
4.6000 4.6008 -.0008 1 0 0
3.2100 3.2099 .0001 1 1 0
2.6300 2.6278 .0022 -1 -1 1
2.0400 2.0414 -.0014 1 1 1
1.8500 1.8500 -.0000 0 -2 1
1.7300 1.7296 .0004 -2 0 1
1.6100 1.6100 .0000 1 -2 1
1.5200 1.5196 .0004 0 -2 2
1.4400 1.4402 -.0002 2 -1 2
1.3700 1.3693 .0007 1 2 1
1.3100 1.3104 -.0004 0 2 1
1.2600 1.2602 -.0002 2 1 2
A= 4.8102 DA= .0004
B= 3.83688 DB= .0004
C= 3.54922 DC= .0003
GAMMA= 76.776 DGAMMA= .003
BETA = 85.22 DBETA = .02
ALPHA=111.77 DALPHA= .01
V= 58.2
218. 21-1481
ZnH2P2O7
Triklin
Dexp Dcal d(D) h k l
8.3700 8.3455 .0245 0 1 1
7.2100 7.1963 .0137 0 -1 1
6.3400 6.3414 -.0014 1 0 0
5.0000 5.0092 -.0092 1 2 1
4.8800 4.8795 .0005 -1 0 1
4.6600 4.6535 .0065 -1 -1 1
4.3800 4.3806 -.0006 -1 1 1
4.2100 4.2060 .0040 1 2 2
3.8500 3.8446 .0054 1 3 1
3.6000 3.5981 .0019 0 -2 2
3.4500 3.4499 .0001 1 1 3
3.2300 3.2321 -.0021 2 1 0
A= 6.746 DA= .001
B= 12.356 DB= .006
C= 10.698 DC= .003
GAMMA= 75.539 DGAMMA= .001
BETA = 73.802 DBETA = .005
ALPHA= 77.997 DALPHA= .001
V= 819.9
219. 21-1483
Zn3Mo2O9
Triklin
Dexp Dcal d(D) h k l
4.6000 4.6078 -.0078 1 1 1
4.1900 4.1898 .0002 1 0 2
3.8800 3.8752 .0048 2 0 0
3.7200 3.7253 -.0053 -1 0 2
3.5900 3.5896 .0004 1 -1 1
3.4100 3.4079 .0021 -2 0 1
3.2200 3.2210 -.0010 -2 -1 1
3.1700 3.1724 -.0024 2 0 2
2.9760 2.9745 .0015 1 0 3
2.7770 2.7783 -.0013 -2 0 2
2.6880 2.6882 -.0002 1 2 0
2.6880 2.6882 -.0002 1 2 0
A= 8.1704 DA= .0004
B= 5.396 DB= .001
C= 9.2452 DC= .0008
GAMMA= 73.18 DGAMMA= .01
BETA = 81.55 DBETA = .01
ALPHA= 86.16 DALPHA= .01
V=385.6
220. 21-1485
Zn{NO3}2*8H2O
Triklin
Dexp Dcal d(D) h k l
7.5200 7.5174 .0026 -1 0 1
6.2000 6.1924 .0076 -1 1 0
6.0600 6.0749 -.0149 1 0 1
5.9300 5.9343 -.0043 0 -1 1
5.7700 5.7818 -.0118 2 0 0
5.4300 5.4273 .0027 1 1 0
5.3500 5.3369 .0131 -1 -1 1
4.1900 4.1967 -.0067 -2 -1 1
4.1100 4.1116 -.0016 -2 1 1
4.0800 4.0716 .0084 2 1 0
3.9500 3.9500 .0000 0 -1 2
3.8600 3.8545 .0055 3 0 0
A= 11.92 DA= .01
B= 6.911 DB= .005
C= 8.611 DC= .001
GAMMA= 95.88 DGAMMA= .02
BETA =101.1495 DBETA = .0006
ALPHA=102.79 DALPHA= .03
V=670.2
221. 21-1978
C18H24Cl2NPZn
Triklin
Dexp Dcal d(D) h k l
12.5000 12.5534 -.0534 1 0 0
9.9100 9.9426 -.0326 0 1 0
7.7900 7.8196 -.0296 1 1 1
6.3900 6.3664 .0235 1 -1 2
5.8900 5.8875 .0025 1 1 2
5.7700 5.7789 -.0089 2 1 0
5.3200 5.3191 .0009 -1 0 2
5.1800 5.1892 -.0092 2 -1 2
4.5300 4.5310 -.0010 3 0 2
4.3300 4.3395 -.0095 -1 1 2
4.2500 4.2576 -.0076 2 2 1
4.1900 4.1845 .0055 3 0 0
A= 13.91 DA= .01
B= 10.159 DB= .001
C= 15.81 DC= .01
GAMMA= 83.5 DGAMMA= .1
BETA = 66.4 DBETA = .1
ALPHA= 96.4 DALPHA= .1
V=2005
222. 21-1980
C16H14S4Zn
Triklin
Dexp Dcal d(D) h k l
9.4600 9.4658 -.0058 0 1 1
6.0800 6.0729 .0071 0 -1 1
5.7700 5.7716 -.0016 1 1 1
5.3400 5.3334 .0066 1 0 1
4.9700 4.9747 -.0047 -1 -1 1
4.4200 4.4167 .0033 1 1 2
4.2600 4.2602 -.0002 -1 1 2
3.9000 3.9011 -.0011 0 1 3
3.7300 3.7300 .0000 -1 -2 1
3.5000 3.4986 .0014 1 3 1
3.1900 3.1921 -.0021 1 -1 2
3.1500 3.1494 .0006 -2 -1 1
A= 6.711 DA= .002
B= 11.11 DB= .01
C= 11.727 DC= .007
GAMMA= 77.26 DGAMMA= .04
BETA = 89.76 DBETA = .02
ALPHA= 65.88 DALPHA= .01
V= 774.5
223. 21-1982
C16H14S6Zn
Triklin
Dexp Dcal d(D) h k l
9.9100 9.9122 -.0022 -1 0 1
9.8600 9.8501 .0099 0 1 0
8.4600 8.4597 .0003 1 0 1
5.7600 5.7605 -.0005 2 1 0
4.7800 4.7810 -.0010 -2 1 1
4.6100 4.6108 -.0008 -1 0 3
4.4200 4.4199 .0001 -1 -2 1
4.2300 4.2299 .0001 2 0 2
3.8100 3.8102 -.0002 -2 1 3
3.4200 3.4201 -.0001 -2 2 0
3.2600 3.2598 .0002 -2 0 4
2.8860 2.8860 .0000 -3 2 1
A= 12.3795 DA= .0007
B= 10.468 DB= .001
C= 14.659 DC= .001
GAMMA= 78.077 DGAMMA= .005
BETA = 95.75 DBETA = .01
ALPHA= 75.76 DALPHA= .01
V= 1778.5
224. 21-1983
C16H14S5Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
9.4600 9.4180 .0420 1 1 0
8.4600 8.3691 .0909 1 1 1
6.3400 6.3194 .0206 1 2 0
5.7800 5.7889 -.0089 -1 0 2
5.6100 5.6114 -.0014 -1 2 1
4.6600 4.6544 .0056 0 3 1
4.4200 4.4285 -.0085 1 3 1
3.9300 3.9297 .0003 3 1 0
3.8000 3.8018 -.0018 2 3 1
3.6900 3.6905 -.0005 0 4 0
3.5000 3.5001 -.0001 -2 0 3
3.4300 3.4291 .0009 0 3 3
a= 12.396 b= 14.762 c= 14.54 beta= 80.6
da= .009 db= .006 dc=.05 dbeta=.1
V= 2625
Triklin
Dexp Dcal d(D) h k l
9.4600 9.4946 -.0346 1 0 0
8.4600 8.4623 -.0023 0 1 0
6.3400 6.3208 .0192 -1 0 1
5.7800 5.8007 -.0207 1 1 0
5.6100 5.6144 -.0044 1 0 1
4.6600 4.6536 .0064 0 -2 1
4.4200 4.4154 .0046 1 -2 1
3.9300 3.9293 .0007 -2 -1 1
3.8000 3.7998 .0002 1 -1 2
3.6900 3.6877 .0023 -1 0 2
3.5000 3.5011 -.0011 -2 2 0
3.4300 3.4343 -.0043 -1 -2 2
A= 9.675 DA= .007
B= 9.501 DB= .006
C= 8.451 DC= .006
GAMMA= 98.680 DGAMMA= .006
BETA = 92.57 DBETA = .02
ALPHA=114.95 DALPHA= .09
V= 691.2
225. 21-1984
C12H12N2S2Zn
Triklin
Dexp Dcal d(D) h k l
4.5900 4.5900 -.0000 -1 0 1
4.2700 4.2698 .0002 -1 1 0
3.5700 3.5697 .0003 1 -1 2
3.2800 3.2802 -.0002 -1 1 1
3.0000 3.0000 -.0000 -2 0 1
2.7100 2.7099 .0001 0 -2 2
2.5500 2.5530 -.0030 -1 -2 2
2.5000 2.4989 .0011 2 -1 3
2.4100 2.4096 .0004 -2 -1 2
2.3100 2.3106 -.0006 -1 2 1
2.2000 2.2010 -.0010 1 -2 3
2.1500 2.1496 .0004 2 0 4
A= 9.123 DA= .006
B= 6.8293 DB= .0006
C= 8.6206 DC= .0002
GAMMA= 72.028 DGAMMA= .004
BETA = 65.985 DBETA = .009
ALPHA= 91.492 DALPHA= .009
V= 459.5
226. 21-1985
beta-C32H16N8Zn
Triklin
Dexp Dcal d(D) h k l
12.6000 12.6007 -.0007 1 0 0
9.5000 9.4945 .0055 -1 -1 1
8.3400 8.3732 -.0332 -1 0 1
7.0300 7.0079 .0221 1 0 1
6.3700 6.3640 .0060 -1 -2 1
5.8100 5.8082 .0018 1 2 0
4.8600 4.8618 -.0018 2 0 1
4.7400 4.7473 -.0073 -2 -2 2
4.5300 4.5364 -.0064 -3 -2 1
4.4000 4.3954 .0046 0 -2 2
4.2100 4.2087 .0013 1 0 2
4.1000 4.0946 .0054 3 2 0
A= 14.313 DA= .006
B= 12.949 DB= .005
C= 10.762 DC= .008
GAMMA= 63.57 DGAMMA= .04
BETA =109.9532 DBETA = .0002
ALPHA=115.77 DALPHA= .03
V=1582.0
227. 21-1986
C32H16N8Zn
Triklin
Dexp Dcal d(D) h k l
13.0000 12.9628 .0372 0 1 0
12.3000 12.2986 .0014 1 0 0
10.1000 10.0924 .0076 0 -1 1
9.5400 9.5383 .0017 1 0 1
8.9000 8.9005 -.0005 -1 -1 1
5.7000 5.6983 .0017 2 0 1
5.5100 5.5140 -.0040 1 -1 2
4.2800 4.2795 .0005 2 2 2
3.4600 3.4595 .0005 -1 -3 3
3.4200 3.4199 .0001 -2 2 2
3.4000 3.4002 -.0002 1 4 0
3.2300 3.2301 -.0001 -3 1 2
2.9200 2.9200 -.0000 2 -3 2
A= 12.9180 DA= .0004
B= 13.635 DB= .003
C= 15.0836 DC= .0001
GAMMA= 72.19 DGAMMA= .02
BETA = 90.82 DBETA = .02
ALPHA= 93.14 DALPHA= .04
V= 2525.5
228. 21-1987
C70H50N16WS3Zn2
Triklin
Dexp Dcal d(D) h k l
14.7000 14.7417 -.0417 0 1 1
13.1000 13.1254 -.0254 0 -1 1
10.3000 10.2810 .0190 -1 0 1
9.7100 9.7180 -.0080 1 -1 0
8.9300 8.9502 -.0202 0 2 1
8.7900 8.7720 .0180 1 1 1
8.2200 8.1952 .0248 0 -2 1
7.5600 7.5454 .0146 -1 1 2
7.3700 7.3709 -.0009 0 2 2
7.0700 7.0813 -.0113 -1 -1 2
6.9100 6.9232 -.0132 1 2 1
6.2700 6.2684 .0016 0 3 0
A= 11.396 DA= .002
B= 18.934 DB= .006
C= 20.72 DC= .01
GAMMA= 90.44 DGAMMA= .04
BETA = 94.45 DBETA = .05
ALPHA= 83.328 DALPHA= .009
V=4425
229. 21-1988
C70H53N19Zn2
Triklin
Dexp Dcal d(D) h k l
11.8000 11.8291 -.0291 0 1 1
9.4000 9.3835 .0165 0 -1 1
8.1800 8.1800 .0000 1 1 1
8.0400 8.0554 -.0154 0 2 1
7.2800 7.2693 .0107 1 -1 1
6.5500 6.5477 .0023 1 2 1
6.0600 6.0620 -.0020 1 1 2
5.7100 5.7178 -.0078 0 3 1
5.0600 5.0615 -.0015 -1 1 2
4.9000 4.8995 .0005 0 3 2
4.5700 4.5700 .0000 2 -1 1
4.4400 4.4475 -.0075 1 -3 1
A= 9.85805 DA= .00007
B= 17.51215 DB= .00009
C= 13.7784 DC= .0001
GAMMA= 87.8754 DGAMMA= .0007
BETA = 78.7845 DBETA = .0004
ALPHA= 76.2501 DALPHA= .0006
V=2266.1
230. 21-1989
C68H40N16O2Zn
Triklin
Dexp Dcal d(D) h k l
13.4000 13.3956 .0044 0 1 1
12.6000 12.6312 -.0312 0 -1 1
9.6000 9.6031 -.0031 1 0 0
9.1100 9.1073 .0027 -1 1 0
7.2500 7.2494 .0006 -1 0 2
6.2800 6.2880 -.0080 1 1 2
5.8200 5.8252 -.0052 -1 0 3
5.6800 5.6783 .0017 1 -2 2
5.3000 5.2950 .0050 1 1 3
5.2100 5.2053 .0047 -1 -1 3
5.0900 5.0899 .0001 1 2 2
4.8800 4.8797 .0003 -2 1 0
A= 9.808 DA= .005
B= 16.590 DB= .005
C= 21.786 DC= .005
GAMMA=101.721 DGAMMA= .004
BETA = 91.59 DBETA = .03
ALPHA= 86.248 DALPHA= .007
V= 3463.3
231. 21-1990
C67H47N19Zn2
Triklin
Dexp Dcal d(D) h k l
11.9000 11.9115 -.0115 -1 0 1
9.2500 9.2468 .0032 0 1 1
8.1100 8.0980 .0120 0 -1 1
7.8600 7.8672 -.0072 -1 -1 1
7.2500 7.2591 -.0091 -1 0 2
6.4800 6.4767 .0033 0 0 2
6.0000 5.9978 .0022 0 1 2
5.6800 5.6666 .0134 -2 -1 1
5.0300 5.0275 .0025 0 -2 1
4.8600 4.8633 -.0033 -1 2 2
4.5000 4.4978 .0022 -2 2 1
4.4100 4.4112 -.0012 2 1 1
A= 13.439 DA= .001
B= 11.6583 DB= .0005
C= 14.7347 DC= .0003
GAMMA= 93.172 DGAMMA= .003
BETA =117.515 DBETA = .001
ALPHA= 81.7799 DALPHA= .0009
V=2026.
232. 21-1991
C38H23N9Zn
Triklin
Dexp Dcal d(D) h k l
13.2000 13.2131 -.0131 1 0 0
10.6000 10.6518 -.0518 0 1 1
9.1000 9.0975 .0025 0 -1 1
7.2500 7.2473 .0027 -1 -1 1
6.8800 6.8840 -.0040 -2 1 0
6.6800 6.6939 -.0139 0 1 2
5.9200 5.9226 -.0026 -2 1 2
5.7100 5.7105 -.0005 1 0 2
5.5300 5.5290 .0010 2 0 1
5.0900 5.0831 .0069 1 2 1
4.9700 4.9699 .0001 -1 -2 1
4.8600 4.8556 .0044 -3 1 1
A= 14.599 DA= .001
B= 14.843 DB= .007
C= 14.898 DC= .006
GAMMA=111.87 DGAMMA= .05
BETA =106.920 DBETA = .001
ALPHA= 75.69 DALPHA= .04
V= 2831.0
233. 21-1992
C82H53N19Zn2
Triklin
Dexp Dcal d(D) h k l
11.9000 11.9154 -.0154 1 0 0
11.0000 10.9803 .0197 1 1 0
10.5000 10.5044 -.0044 0 0 1
8.6600 8.6279 .0321 -1 1 1
8.1800 8.1989 -.0189 0 -1 1
7.5200 7.5025 .0175 0 2 1
6.2500 6.2391 .0109 -2 0 1
6.0600 6.0604 -.0004 -2 -1 1
5.6200 5.6124 .0076 -1 0 2
5.2900 5.2824 .0076 -2 1 0
5.1400 5.1402 -.0002 -1 -1 2
4.7400 4.7410 -.0010 0 -1 2
A= 12.932 DA= .003
B= 17.82 DB= .01
C= 11.401 DC= .002
GAMMA= 81.17 DGAMMA= .03
BETA =109.23 DBETA = .07
ALPHA= 81.17 DALPHA= .03
V= 2391.6
234. 21-1993
C42H38N10Zn
Triklin
Dexp Dcal d(D) h k l
12.1000 12.1321 -.0321 1 0 0
8.5000 8.5333 -.0333 -1 1 0
7.7500 7.7416 .0084 1 0 1
7.0800 7.0773 .0027 1 1 0
6.1300 6.1369 -.0069 1 1 1
5.4700 5.4743 -.0043 -1 -1 1
4.9900 4.9864 .0036 0 2 0
4.7900 4.7887 .0013 0 2 1
4.3300 4.3337 -.0037 1 2 0
4.1900 4.1896 .0004 -2 -1 1
4.1900 4.1896 .0004 -2 -1 1
4.0800 4.0785 .0015 1 -1 2
A= 12.36 DA= .01
B= 10.299 DB= .002
C= 10.144 DC= .002
GAMMA=100.96 DGAMMA= .03
BETA = 91.47 DBETA = .01
ALPHA= 80.42 DALPHA= .01
V=1245
235. 21-1994
C76H44N22Zn2
Triklin
Dexp Dcal d(D) h k l
17.0000 17.0077 -.0077 -1 1 0
13.7000 13.7144 -.0144 0 0 1
12.6000 12.6049 -.0049 -1 2 0
11.8000 11.8301 -.0301 0 1 1
9.9300 9.9107 .0193 1 -1 1
9.7000 9.6937 .0063 -1 2 1
9.0200 9.0076 .0124 -2 1 0
8.5800 8.5743 .0057 2 0 0
8.3300 8.3366 -.0066 -2 1 1
8.1100 8.1038 .0062 -2 0 1
7.2800 7.2843 -.0043 -2 -1 1
A= 18.3987 DA= .0003
B= 28.1818 DB= .0003
C= 14.0509 DC= .0001
GAMMA=107.2975 DGAMMA= .0003
BETA =101.7024 DBETA = .0002
ALPHA= 90.875 DALPHA= .001
V=6798.9
236. 21-1995
C37H21N9Zn
Triklin
Dexp Dcal d(D) h k l
13.0000 12.9906 .0094 0 1 1
12.0000 12.0092 -.0092 0 -1 1
10.3000 10.3041 -.0041 1 1 0
8.9900 8.9893 .0007 -1 1 1
8.3500 8.3532 -.0032 1 0 1
7.0200 7.0212 -.0012 -1 1 2
5.9000 5.8973 .0027 1 3 0
5.7100 5.7014 .0086 -2 -1 1
5.4800 5.4758 .0042 0 0 3
5.1500 5.1521 -.0021 2 2 0
4.9600 4.9650 -.0050 2 1 1
4.7900 4.7899 .0001 0 4 0
A= 11.681 DA= .003
B= 19.352 DB= .002
C= 16.983 DC= .002
GAMMA= 83.315 DGAMMA= .008
BETA =104.00 DBETA = .05
ALPHA= 87.24 DALPHA= .01
V= 3688.0
237. 21-1996
C42N10Zn
Triklin
Dexp Dcal d(D) h k l
14.4000 14.4050 -.0050 0 1 1
12.4000 12.3779 .0221 1 0 0
11.6000 11.5919 .0081 0 -1 1
9.5000 9.5153 -.0153 1 1 0
8.3800 8.3848 -.0048 1 -1 1
8.3000 8.3025 -.0025 0 1 2
7.7500 7.7672 -.0172 -1 0 2
6.7500 6.7559 -.0059 0 3 1
5.7300 5.7279 .0021 -1 2 3
5.6300 5.6309 -.0009 -2 0 2
5.4200 5.4185 .0015 2 -1 1
5.2700 5.2732 -.0032 -2 3 0
A= 13.465 DA= .003
B= 21.821 DB= .003
C= 17.795 DC= .004
GAMMA=108.93 DGAMMA= .01
BETA =108.03 DBETA = .01
ALPHA= 72.755 DALPHA= .009
V= 4590.3
238. 21-1997
C35H25N9Zn
Triklin
Dexp Dcal d(D) h k l
13.2000 13.2085 -.0085 1 0 0
11.4000 11.4012 -.0012 -1 1 0
10.0000 9.9969 .0031 1 0 1
8.3400 8.3209 .0191 -1 0 1
8.0800 8.0845 -.0045 1 1 0
6.6000 6.6043 -.0043 2 0 0
6.0200 6.0192 .0008 2 -1 1
5.5300 5.5231 .0069 -2 2 1
5.2600 5.2602 -.0002 -1 0 2
4.9600 4.9595 .0005 0 -1 2
4.4800 4.4787 .0013 -1 3 2
3.9500 3.9485 .0015 3 1 1
3.5900 3.5903 -.0003 0 -1 3
A= 14.031 DA= .001
B= 14.774 DB= .003
C= 13.36 DC= .01
GAMMA=106.8 DGAMMA= .1
BETA = 86.01 DBETA = .09
ALPHA= 70.86 DALPHA= .03
V= 2463
239. 21-1998
C4H16N10O6S4Zn
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
11.2000 11.1912 .0088 1 0 0
6.4500 6.4397 .0103 1 1 0
5.5900 5.5956 -.0056 2 0 0
4.8000 4.7942 .0058 0 0 2
4.4200 4.4182 .0018 -2 0 2
4.1000 4.0949 .0051 0 1 2
3.9400 3.9369 .0031 0 2 0
3.6000 3.5962 .0038 -1 2 1
3.5200 3.5201 -.0001 -3 1 1
3.2200 3.2199 .0001 2 2 0
3.1000 3.1023 -.0023 -1 2 2
3.0400 3.0425 -.0025 0 2 2
a= 11.833 b= 7.87 c= 10.13822 beta= 108.9
da= .008 db=.01 dc=.00003 dbeta=.1
V= 893.4