1. 36-0203
Cu3{PO4}2
Triklin
Dexp Dcal d(D) h k l
7.7500 7.7431 .0069 -1 1 0
6.8000 6.8350 -.0350 1 1 0
5.6000 5.5773 .0227 0 1 1
5.4600 5.4476 .0124 2 0 0
4.5200 4.5156 .0044 2 1 0
5.0600 5.0568 .0032 -1 0 1
4.9200 4.8966 .0234 1 1 1
4.5600 4.5645 -.0045 0 -1 1
4.0900 4.0821 .0079 -1 -1 1
3.8300 3.8316 -.0016 2 1 1
3.6300 3.6317 -.0017 3 0 0
A= 10.98198 DA= .00004
B= 10.02936 DB= .00002
C= 5.97911 DC= .00002
GAMMA= 96.8599 DGAMMA= .0001
BETA = 89.3550 DBETA = .0002
ALPHA= 77.2338 DALPHA= .0001
V=637.7
2. 36-0244
Cu3{PO3}6*14H2O
Triklin
Dexp Dcal d(D) h k l
6.9500 6.9523 -.0023 0 1 1
6.2800 6.2780 .0020 1 1 0
6.0200 6.0592 -.0392 -2 1 0
5.5100 5.5039 .0061 2 -1 1
5.0100 4.9941 .0159 2 0 2
4.7500 4.7495 .0005 2 1 0
4.5900 4.5913 -.0013 -3 1 0
4.3600 4.3570 .0030 1 -1 2
3.9200 3.9179 .0021 0 2 1
3.8300 3.8295 .0005 -2 0 2
3.7100 3.7034 .0066 4 0 1
3.6200 3.6208 -.0008 2 0 3
A= 15.1603 DA= .0008
B= 8.14945 DB= .00004
C= 11.2522 DC= .0008
GAMMA=101.72 DGAMMA= .01
BETA = 76.21 DBETA = .01
ALPHA= 83.196 DALPHA= .008
V=1303.1
3. 36-0508
CuH2Se2O6
Triklin
Dexp Dcal d(D) h k l
4.8200 4.8099 .0101 0 1 0
4.1800 4.1788 .0012 0 1 1
3.8000 3.7931 .0069 0 -1 2
3.6200 3.6200 -.0000 1 -1 1
3.2000 3.1961 .0039 -1 0 3
3.1000 3.0958 .0042 -1 1 2
2.8700 2.8696 .0004 -2 0 1
2.8200 2.8164 .0036 1 0 3
2.6700 2.6705 -.0005 2 0 1
2.5600 2.5588 .0012 -2 1 0
2.5200 2.5208 -.0008 -2 1 1
2.2500 2.2485 .0015 2 -1 2
A= 5.8030 DA= .0003
B= 4.8597 DB= .0005
C= 10.684 DC= .002
GAMMA= 93.904 DGAMMA= .005
BETA = 97.61 DBETA = .02
ALPHA= 96.637 DALPHA= .001
V=296.00
4. 36-0509
CuSe2O5
Triklin
Dexp Dcal d(D) h k l
5.4000 5.4242 -.0242 1 1 0
4.7200 4.7166 .0034 1 2 1
4.2300 4.2281 .0019 0 -2 1
3.6800 3.6754 .0046 -1 2 0
3.5400 3.5380 .0020 1 1 2
3.4000 3.3922 .0078 1 -2 1
3.2800 3.2808 -.0008 -1 -2 1
3.0600 3.0579 .0021 0 4 0
2.9600 2.9604 -.0004 -1 3 0
2.9200 2.9210 -.0010 2 2 1
2.8300 2.8311 -.0011 2 0 1
2.6500 2.6493 .0007 2 1 2
A= 5.9391 DA= .0001
B= 12.930 DB= .004
C= 7.36601 DC= .00005
GAMMA= 73.388 DGAMMA= .005
BETA = 69.521 DBETA = .008
ALPHA= 75.93 DALPHA= .01
V=501.87
5. 36-0510
CuSeO3
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
3.8700 3.8716 -.0016 2 1 0
3.4900 3.4911 -.0011 3 0 0
3.0100 3.0087 .0013 1 1 3
2.9300 2.9313 -.0013 3 1 1
2.8800 2.8813 -.0013 -2 0 3
2.8400 2.8381 .0019 -3 0 2
2.6300 2.6300 -.0000 3 0 3
2.5000 2.5003 -.0003 -4 0 1
2.4500 2.4509 -.0009 -1 2 2
2.2200 2.2193 .0007 3 2 0
a= 10.509 b= 5.750 c= 10.962 beta= 85.30
da= .003 db=.001 dc=.002 dbeta=.04
V= 660.1
6. 36-0562
CuAsF7
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.7300 5.7269 .0031 1 0 1
4.8800 4.9040 -.0240 1 1 1
3.6100 3.6121 -.0021 0 1 2
3.1600 3.1651 -.0051 0 3 0
2.9500 2.9512 -.0012 -2 1 1
2.8700 2.8701 -.0001 2 2 0
2.6800 2.6775 .0025 -1 2 2
2.3400 2.3381 .0019 2 3 1
2.1500 2.1504 -.0004 -3 1 1
2.0500 2.0500 .0000 2 2 3
1.8100 1.8101 -.0001 1 2 4
1.7700 1.7700 .0000 4 1 0
1.6800 1.6800 .0000 2 5 0
a= 7.283 b= 9.495 c= 7.895 beta= 81.65
da=.001 db=.005 dc=.004 dbeta=.04
V= 540.2
Triklin
Dexp Dcal d(D) h k l
5.7300 5.7310 -.0010 1 0 0
4.8800 4.8809 -.0009 0 1 0
3.6100 3.6117 -.0017 0 -1 2
3.1600 3.1596 .0004 1 1 1
2.9500 2.9499 .0001 -1 0 4
2.8700 2.8700 .0000 1 1 2
2.6800 2.6798 .0002 2 0 1
2.3400 2.3396 .0004 0 -2 1
2.1500 2.1500 .0000 -2 -1 2
2.0500 2.0502 -.0002 1 2 0
1.8100 1.8100 -.0000 0 -1 6
1.7700 1.7700 .0000 1 -2 4
1.6800 1.6800 -.0000 3 -2 1
A= 6.1357 DA= .0002
B= 5.1686 DB= .0007
C= 12.7278 DC= .0003
GAMMA=107.933 DGAMMA= .003
BETA =103.609 DBETA = .003
ALPHA= 79.3247 DALPHA= .0002
V= 370.48
7. 36-0566
Cu2OSeO3
Triklin
Dexp Dcal d(D) h k l
5.4900 5.4922 -.0022 0 1 1
5.1800 5.1782 .0018 -1 0 1
4.9600 4.9613 -.0013 0 -1 1
3.9900 3.9918 -.0018 2 1 1
3.6600 3.6578 .0022 -1 2 1
3.1550 3.1558 -.0008 3 1 0
2.9750 2.9751 -.0001 -1 0 2
2.8220 2.8213 .0007 -2 3 0
2.6900 2.6896 .0004 1 2 2
2.5750 2.5753 -.0003 -3 3 0
2.1650 2.1649 .0001 4 2 1
2.0480 2.0478 .0002 0 -3 2
A= 11.766 DA= .006
B= 8.8057 DB= .0001
C= 6.7486 DC= .0006
GAMMA=102.66 DGAMMA= .01
BETA = 78.08 DBETA = .01
ALPHA= 86.864 DALPHA= .002
V= 663.8
8. 36-0660
Li6CuO4
Triklin
Dexp Dcal d(D) h k l
8.7400 8.7320 .0080 0 1 1
6.1400 6.1415 -.0015 -1 1 1
5.2100 5.2054 .0046 0 -1 1
4.6600 4.6642 -.0042 -1 2 1
4.3900 4.3924 -.0024 0 2 0
4.0900 4.0890 .0010 -1 2 2
3.9300 3.9313 -.0013 1 0 2
3.6400 3.6348 .0052 -2 1 0
3.1300 3.1297 .0003 -1 1 3
2.9260 2.9283 -.0023 0 3 0
2.7880 2.7888 -.0008 -2 3 1
2.6250 2.6260 -.0010 2 2 1
A= 7.403 DA= .002
B= 10.299 DB= .006
C= 10.387 DC= .006
GAMMA=104.11 DGAMMA= .05
BETA = 94.34 DBETA = .08
ALPHA= 61.41 DALPHA= .02
V= 673.5
9. 36-0661
Li2Cu2O3
Triklin
Dexp Dcal d(D) h k l
8.6600 8.6593 .0007 1 0 0
6.1000 6.0880 .0120 1 1 0
5.1800 5.1769 .0031 0 -1 1
4.6500 4.6497 .0003 1 -1 1
4.1600 4.1561 .0039 -1 0 1
3.0700 3.0691 .0009 -2 0 1
2.7750 2.7766 -.0016 0 -1 2
2.6320 2.6317 .0003 0 -3 1
2.5040 2.5054 -.0014 1 3 0
2.3410 2.3409 .0001 -1 3 0
2.2610 2.2606 .0004 0 1 2
2.1000 2.1003 -.0003 -3 1 1
A= 8.8376 DA= .0005
B= 8.0174 DB= .0001
C= 5.62339 DC= .00000
GAMMA= 85.989 DGAMMA= .001
BETA = 81.024 DBETA = .002
ALPHA=108.1495 DALPHA= .0006
V=371.3
10. 36-0662
Li4CuB2O6
Triklin
Dexp Dcal d(D) h k l
6.8500 6.8451 .0049 0 1 1
6.1700 6.1733 -.0033 0 -1 1
5.2000 5.1926 .0074 1 0 0
4.9100 4.9220 -.0120 -1 1 0
4.5100 4.5114 -.0014 1 0 1
4.1200 4.1220 -.0020 -1 1 1
3.7600 3.7560 .0040 -1 -1 1
3.4800 3.4838 -.0038 1 2 1
3.1600 3.1597 .0003 -1 -2 1
3.0300 3.0307 -.0007 -1 3 1
2.9150 2.9162 -.0012 1 3 0
2.8230 2.8236 -.0006 -1 -1 2
A= 5.23474 DA= .00000
B= 11.4779 DB= .0001
C= 7.96527 DC= .00001
GAMMA= 95.5767 DGAMMA= .0001
BETA = 85.93089 DBETA = .00002
ALPHA= 84.14658 DALPHA= .00005
V=472.0
11. 36-0663
Li2CuB4O8
Triklin
Dexp Dcal d(D) h k l
8.8300 8.8283 .0017 1 0 0
5.1200 5.1195 .0005 0 1 0
4.2600 4.2580 .0020 0 -1 2
3.8600 3.8596 .0004 -1 -1 2
3.4700 3.4690 .0010 2 1 2
2.8350 2.8391 -.0041 2 -1 3
2.7260 2.7258 .0002 3 1 0
2.5950 2.5949 .0001 2 -1 4
2.4460 2.4468 -.0008 -2 -1 4
2.3050 2.3052 -.0002 -2 -2 1
2.1230 2.1234 -.0004 0 2 4
2.0770 2.0773 -.0003 -1 -2 4
A= 9.080 DA= .002
B= 5.175 DB= .001
C= 15.5467 DC= .0002
GAMMA= 81.65 DGAMMA= .01
BETA = 79.25 DBETA = .02
ALPHA= 88.61 DALPHA= .01
V= 710.0
12. 36-0664
Li2Cu2B2O6
Triklin
Dexp Dcal d(D) h k l
5.6000 5.6036 -.0036 1 1 0
3.8100 3.8114 -.0014 1 -1 1
3.3200 3.3193 .0007 -1 -2 1
3.1400 3.1435 -.0035 1 3 0
3.0100 3.0084 .0016 1 1 2
2.8800 2.8785 .0015 2 1 1
2.7510 2.7484 .0026 0 2 2
2.7340 2.7365 -.0025 2 2 1
2.6630 2.6668 -.0038 -1 0 2
2.5180 2.5175 .0005 -2 0 1
2.4380 2.4383 -.0003 2 3 1
2.1930 2.1917 .0013 -2 -3 1
A= 6.0397 DA= .0002
B= 9.931 DB= .001
C= 6.51953 DC= .00007
GAMMA= 75.03 DGAMMA= .01
BETA = 81.326 DBETA = .007
ALPHA= 84.439 DALPHA= .007
V=373.0
13. 36-0800
KCu{SCN}4
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
5.5700 5.6040 -.0340 0 2 0
4.4200 4.4181 .0019 0 1 2
3.6900 3.6897 .0003 1 0 1
3.6400 3.6487 -.0087 0 2 2
3.0900 3.0945 -.0045 1 1 2
2.9500 2.9499 .0001 0 3 2
2.5900 2.5900 -.0000 1 1 3
2.4200 2.4208 -.0008 0 4 2
2.3500 2.3502 -.0002 0 1 4
2.1100 2.1095 .0005 0 4 3
1.8800 1.8800 .0000 -1 0 4
1.7900 1.7900 .0000 2 2 1
a= 3.7791 b= 11.208 c= 9.76 beta= 80.26
da=.0002 db=.005 dc=.01 dbet=.09
V=407.1
14. 36-0975
CuBeF4
Triklin
Dexp Dcal d(D) h k l
4.8400 4.8445 -.0045 -1 0 1
3.9300 3.9262 .0038 -1 1 0
3.7300 3.7322 -.0022 1 0 3
3.0980 3.1078 -.0098 1 -1 3
2.9100 2.9090 .0010 1 1 2
2.6900 2.6897 .0003 -1 1 4
2.6200 2.6164 .0036 2 0 0
2.5200 2.5204 -.0004 2 0 2
2.3100 2.3103 -.0003 1 0 6
2.2900 2.2888 .0012 -1 2 0
2.1900 2.1891 .0009 0 2 2
2.1200 2.1200 .0000 1 -1 6
A= 5.4023 DA= .0004
B= 4.6657 DB= .0003
C= 15.0067 DC= .0007
GAMMA=103.94 DGAMMA= .05
BETA = 86.79 DBETA = .01
ALPHA= 88.65 DALPHA= .02
V=366.4
15. 36-1106
Cu4SbO4.5
Triklin
Dexp Dcal d(D) h k l
5.7200 5.7207 -.0007 0 0 1
4.5100 4.5109 -.0009 -2 1 0
2.8760 2.8760 -.0000 2 -2 1
2.7880 2.7896 -.0016 -3 0 1
2.7060 2.7058 .0002 -3 2 1
2.6140 2.6132 .0008 -2 1 2
2.5500 2.5504 -.0004 1 -1 2
2.5080 2.5054 .0026 -2 3 1
2.3800 2.3804 -.0004 -3 3 0
2.2540 2.2555 -.0015 -4 2 0
2.1660 2.1656 .0004 3 1 1
2.0020 2.0024 -.0004 -2 -2 2
A= 9.410 DA= .004
B= 8.3392 DB= .0008
C= 5.80408 DC= .00006
GAMMA=109.50 DGAMMA= .01
BETA = 99.70 DBETA = .02
ALPHA= 87.457 DALPHA= .007
V= 423.2
16. 36-1865
C17H11CuNO2
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
12.6000 12.6457 -.0457 0 0 1
9.6900 9.6897 .0003 0 1 1
8.7500 8.7495 .0005 -1 0 1
5.0400 5.0437 -.0037 1 1 2
4.1800 4.1790 .0010 2 2 1
3.9100 3.9095 .0005 -1 1 3
3.6800 3.6793 .0007 0 2 3
3.3000 3.3000 .0000 -2 3 2
a= 11.325 b= 15.080 c= 12.6800 beta= 94.212
da= .002 db=.001 dc=.0009 dbet=.004
V=2159.6
17. 36-1870
C32H16-xClxCuN8
Triklin
Dexp Dcal d(D) h k l
14.8000 14.6925 .1075 0 1 0
13.2000 13.1382 .0618 1 1 0
8.7800 8.7810 -.0010 -1 1 0
7.3800 7.3463 .0337 0 2 0
6.5100 6.5691 -.0591 2 2 0
5.7500 5.7303 .0197 -1 2 0
5.2100 5.2265 -.0165 3 1 0
4.8500 4.8371 .0129 3 0 0
3.6000 3.6007 -.0007 -1 -1 1
3.3400 3.3394 .0006 -1 -2 1
3.1500 3.1502 -.0002 -2 -2 1
2.9000 2.9022 -.0022 5 0 0
A= 15.89 DA= .01
B= 16.013 DB= .002
C= 3.974 DC= .004
GAMMA= 66.85 DGAMMA= .03
BETA = 81.33 DBETA = .06
ALPHA= 83.24 DALPHA= .09
V=919.1
18. 36-1871
C32Br6Cl10CuN8
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
13.5000 13.1876 .3124 0 1 0
8.7000 8.6868 .0132 1 1 0
6.6000 6.6061 -.0061 0 0 1
6.6000 6.5938 .0062 0 2 0
5.3300 5.2995 .0305 -1 0 1
4.9000 4.9173 -.0173 -1 1 1
4.3500 4.3434 .0066 2 2 0
3.9000 3.9060 -.0060 2 2 1
3.6600 3.6597 .0003 0 3 1
3.5000 3.4973 .0027 2 3 0
3.4000 3.4040 -.0040 -2 2 1
2.9200 2.9207 -.0007 1 4 1
2.6500 2.6498 .0002 -2 0 2
2.5600 2.5594 .0006 2 3 2
2.4900 2.4900 .0000 -1 3 2
a= 11.78 b= 13.19 c= 6.74 beta= 78.6
da= .03 db= .01 dc=.009 dbeta=.1
V= 1026
Triklin
Dexp Dcal d(D) h k l
13.5000 13.5090 -.0090 1 0 0
8.7000 8.6995 .0005 -1 1 1
6.6000 6.5978 .0022 -1 -1 1
5.3300 5.3299 .0001 0 1 2
4.9000 4.8996 .0004 -2 2 0
4.3500 4.3498 .0002 -2 2 2
3.9000 3.8999 .0001 -3 1 2
3.6600 3.6599 .0001 0 -3 1
3.5000 3.4999 .0001 -2 1 3
3.4000 3.4001 -.0001 -4 0 1
2.9200 2.9200 .0000 1 4 2
2.6500 2.6500 .0000 -1 0 4
2.5600 2.5600 -.0000 -3 2 4
2.4900 2.4900 -.0000 2 -5 0
A= 13.891 DA= .004
B= 13.502 DB= .003
C= 11.040 DC= .003
GAMMA= 98.47 DGAMMA= .02
BETA =102.40 DBETA = .02
ALPHA= 73.78 DALPHA= .01
V= 1933.6
19. 36-1881
C32H16CuN8
Monoklin
Dexp Dcal d(D) h k l
12.7000 12.7216 -.0216 0 0 1
9.7100 9.6889 .0211 1 1 0
8.4000 8.4004 -.0004 1 0 1
8.4000 8.5055 -.1055 -1 1 1
7.1000 7.0995 .0005 1 1 1
4.8500 4.8444 .0056 2 2 0
4.1800 4.1798 .0002 -1 1 3
4.0000 4.0047 -.0047 2 1 2
3.8500 3.8482 .0018 3 2 0
3.7500 3.7498 .0002 -2 3 1
3.5400 3.5414 -.0014 4 0 0
3.4000 3.3954 .0046 1 3 2
3.2100 3.2127 -.0027 0 4 1
2.9400 2.9396 .0004 -5 0 1
a= 14.717 b= 13.28 c= 13.22 beta= 105.72
da= .001 db= .02 dc=.02 dbeta=.02
V= 2487
Triklin
Dexp Dcal d(D) h k l
12.7000 12.7484 -.0484 0 1 0
9.7100 9.6996 .0104 1 0 0
8.4000 8.4128 -.0128 -1 1 0
7.1000 7.1072 -.0072 0 -1 1
4.8500 4.8498 .0002 2 0 0
4.1800 4.1794 .0006 -1 -2 1
4.0000 3.9973 .0027 1 -1 2
3.8500 3.8521 -.0021 1 0 2
3.7500 3.7480 .0020 0 0 2
3.5400 3.5413 -.0013 -2 1 1
3.4000 3.3998 .0002 -1 -3 1
3.2100 3.2101 -.0001 -2 2 1
2.9400 2.9404 -.0004 3 -2 2
A= 10.324 DA= .001
B= 13.36 DB= .01
C= 8.030 DC= .002
GAMMA=103.21 DGAMMA= .04
BETA = 72.26 DBETA = .01
ALPHA=104.70 DALPHA= .05
V= 1006.6
20. 36-1883
C32H16CuN8
Rombik
Groupa 16
Dexp. Dcal. d(D) h k l
13.1000 12.0528 1.0472 1 0 0
12.2000 13.2268 -1.0268 0 0 1
8.9700 8.9088 .0612 1 0 1
5.7900 5.8429 -.0529 1 1 1
5.4800 5.4840 -.0040 2 0 1
3.8700 3.8701 -.0001 0 2 0
3.6900 3.6848 .0052 1 2 0
3.5400 3.5496 -.0096 1 2 1
3.3300 3.3402 -.0102 0 2 2
3.2200 3.2189 .0011 1 2 2
2.9400 2.9379 .0021 4 0 1
2.8400 2.8274 .0126 1 2 3
a=12.05 b= 7.740 c=13.23
da= .02 db= .007 dc= .09
V=1234
21. 36-1884
C32H16CuN8
Triklin
Dexp Dcal d(D) h k l
12.7000 12.6756 .0244 1 0 0
9.6700 9.6558 .0142 1 0 1
8.4100 8.4061 .0039 0 1 0
7.0900 7.0907 -.0007 -1 1 0
6.2000 6.1853 .0147 2 0 1
5.7000 5.7028 -.0028 1 0 2
4.8500 4.8529 -.0029 2 -1 1
4.1500 4.1495 .0005 0 2 1
4.0000 4.0042 -.0042 2 -1 2
3.7400 3.7399 .0001 1 1 3
3.3900 3.3886 .0014 2 -2 1
3.1800 3.1789 .0011 1 -2 2
2.9400 2.9402 -.0002 4 1 0
2.7700 2.7701 -.0001 4 0 3
2.7000 2.6998 .0002 3 2 3
A= 13.040 DA= .008
B= 8.503 DB= .005
C= 11.807 DC= .002
GAMMA= 89.45 DGAMMA= .03
BETA = 76.52 DBETA = .04
ALPHA= 81.49 DALPHA= .03
V= 1258.5
1. 37-0217
Cu{As2O7}O2
Triklin
Dexp Dcal d(D) h k l
4.6200 4.6296 -.0096 0 2 0
3.8100 3.8069 .0031 -1 1 1
3.6300 3.6284 .0016 0 -1 2
3.5900 3.5889 .0011 1 -2 1
3.0600 3.0589 .0011 0 -2 2
3.0200 3.0220 -.0020 -1 2 1
2.9400 2.9366 .0034 0 -3 1
2.9000 2.8978 .0022 -1 -1 2
2.7900 2.7863 .0037 1 3 1
2.7500 2.7488 .0012 -2 0 1
2.7200 2.7213 -.0013 -2 -1 1
2.6700 2.6698 .0002 -1 -3 1
A= 6.956 DA= .002
B= 9.320 DB= .001
C= 8.02482 DC= .00006
GAMMA= 84.911 DGAMMA= .002
BETA = 72.878 DBETA = .007
ALPHA= 92.443 DALPHA= .009
V=493.5
2. 37-0218
CuHAsO4*1.5H2O
Rombik
Grupa 19
Dexp. Dcal. d(D) h k l
10.4300 10.3052 .1248 0 0 1
8.4600 8.5769 -.1169 1 0 1
4.0500 4.0558 -.0058 0 1 1
3.2700 3.2753 -.0053 1 1 2
3.1900 3.1881 .0019 3 1 1
3.0800 3.0751 .0049 2 1 2
2.9600 2.9638 -.0038 5 0 1
2.6700 2.6698 .0002 1 1 3
2.5800 2.5787 .0013 6 0 0
1.6100 1.6100 .0000 6 0 5
a=15.472 b= 4.412 c=10.305
da= .009 db= .001 dc= .002
V= 703.5
3. 37-0219
CuHAsO4*1.5H2O
Triklin
Dexp Dcal d(D) h k l
7.8100 7.8092 .0008 0 0 1
5.7300 5.7338 -.0038 -1 1 0
3.9800 3.9799 .0001 0 -2 1
3.9000 3.9024 -.0024 -1 2 0
3.8200 3.8184 .0016 -2 -1 1
3.5600 3.5593 .0007 0 -1 2
3.2300 3.2300 .0000 -2 1 2
3.1500 3.1500 .0000 -1 2 2
3.0600 3.0601 -.0001 2 2 0
2.9400 2.9347 .0053 1 1 2
2.8500 2.8493 .0007 -1 3 0
2.8300 2.8315 -.0015 -2 -2 2
A= 8.2206 DA= .0002
B= 9.501 DB= .001
C= 8.463 DC= .001
GAMMA= 86.838 DGAMMA= .009
BETA =112.56 DBETA = .01
ALPHA= 89.05 DALPHA= .02
V= 609.03
4. 37-0538
CsCu2.4O{CO3}3*5H2O
Triklin
Dexp Dcal d(D) h k l
5.6000 5.6000 -.0000 1 1 0
4.6700 4.6697 .0003 -1 1 0
4.2300 4.2301 -.0001 1 1 2
3.5400 3.5400 .0000 2 0 0
3.4600 3.4599 .0001 2 0 2
3.2100 3.2071 .0029 -1 -2 1
3.1400 3.1377 .0023 0 -1 3
3.0900 3.0900 .0000 -1 1 2
3.0100 3.0092 .0008 -2 -1 1
2.8600 2.8561 .0039 2 2 1
2.5200 2.5229 -.0029 1 1 4
2.3900 2.3898 .0002 2 1 4
A= 7.57077 DA= .00007
B= 7.3899 DB= .0001
C= 10.72068 DC= .00006
GAMMA= 80.084 DGAMMA= .001
BETA = 71.932 DBETA = .001
ALPHA= 89.745 DALPHA= .002
V= 560.9
5. 37-0662
Cu{NH3}4{ReO4}2
Triklin
Dexp Dcal d(D) h k l
6.5100 6.5100 -.0000 0 1 1
5.9900 5.9904 -.0004 0 -1 1
5.3400 5.3391 .0009 -1 1 1
4.9900 4.9884 .0016 1 1 1
4.7000 4.7034 -.0034 1 -1 1
3.9000 3.8999 .0001 -2 0 1
3.6200 3.6192 .0008 0 -1 2
3.4300 3.4329 -.0029 2 1 1
3.2200 3.2174 .0026 1 -1 2
3.0800 3.0791 .0009 1 3 0
2.9200 2.9180 .0020 1 3 1
2.4600 2.4600 -.0000 3 2 0
A= 8.482 DA= .009
B= 9.897 DB= .003
C= 8.114 DC= .001
GAMMA= 89.60 DGAMMA= .02
BETA = 95.65 DBETA = .05
ALPHA= 85.21 DALPHA= .03
V= 675.4
6. 37-0729
CuSeO4*H2O
Triklin
Dexp Dcal d(D) h k l
5.2150 5.2118 .0032 -1 1 0
4.8740 4.8875 -.0135 1 1 0
4.7700 4.7692 .0008 1 0 2
4.3120 4.3306 -.0186 1 1 2
3.6780 3.6813 -.0033 2 0 0
3.5070 3.5069 .0001 0 -1 2
3.4240 3.4170 .0070 -1 0 2
3.3270 3.3269 .0000 2 1 2
3.0180 3.0260 -.0080 0 -2 1
2.7140 2.7112 .0028 -1 2 2
2.5220 2.5198 .0022 1 1 4
2.4550 2.4542 .0008 3 0 0
A= 7.881 DA= .005
B= 7.103 DB= .004
C= 10.186 DC= .005
GAMMA= 88.99 DGAMMA= .06
BETA = 69.42 DBETA = .03
ALPHA= 77.43 DALPHA= .05
V=519.8
7. 37-0843
CuMo2S3
Triklin
Dexp Dcal d(D) h k l
6.4600 6.4587 .0013 -1 1 0
4.8400 4.8404 -.0004 -1 0 1
4.3600 4.3602 -.0002 -1 -2 1
3.4000 3.3998 .0002 -2 0 1
3.0340 3.0339 .0001 -2 -3 1
2.6960 2.6960 .0000 0 -3 2
2.4400 2.4399 .0001 2 2 2
2.4330 2.4325 .0005 2 -2 2
2.2750 2.2752 -.0002 -2 1 2
2.1650 2.1648 .0002 2 5 1
2.1230 2.1227 .0003 3 5 0
1.9910 1.9915 -.0005 1 -5 2
A= 8.856 DA= .004
B= 12.852 DB= .003
C= 6.321 DC= .001
GAMMA= 78.09 DGAMMA= .02
BETA = 86.354 DBETA = .006
ALPHA= 97.80 DALPHA= .01
V= 694.3
8. 37-1028
Cu0.57Te0.43
Groupa 19
romb.
Dexp. Dcal. d(D) h k l
3.6000 3.6091 -.0091 2 1 0
3.4300 3.4323 -.0023 0 4 0
3.3000 3.3025 -.0025 0 2 1
3.2700 3.2679 .0021 1 1 1
3.1200 3.1197 .0003 1 4 0
2.9000 2.8963 .0037 2 3 0
2.0800 2.0794 .0006 3 0 1
2.0200 2.0175 .0025 3 4 0
2.0150 2.0175 -.0025 3 4 0
1.9900 1.9901 -.0001 3 2 1
a= 7.481 b=13.729 c= 3.767
da= .002 db= .003 dc= .001
V= 386.9
9. 37-1037
NdCu4
Triklin
Dexp Dcal d(D) h k l
3.0299 3.0300 -.0001 1 0 2
2.5687 2.5688 -.0001 1 -2 2
2.2322 2.2317 .0005 1 -3 1
2.1824 2.1831 -.0007 0 -3 1
2.0304 2.0302 .0002 1 -3 2
1.8884 1.8889 -.0005 3 0 2
1.7123 1.7125 -.0002 -2 -2 2
1.6676 1.6678 -.0002 2 -3 3
1.6257 1.6254 .0003 3 0 3
1.5593 1.5597 -.0004 -4 1 0
1.5194 1.5192 .0002 -1 4 1
1.4847 1.4850 -.0003 2 2 3
A= 6.4181 DA= .0004
B= 6.8095 DB= .0005
C= 6.5148 DC= .0003
GAMMA=102.200 DGAMMA= .006
BETA = 76.9174 DBETA = .0003
ALPHA=102.173 DALPHA= .008
V=267.1
10. 37-1806
C13H28CuN6Na2O7S3
Triklin
Dexp Dcal d(D) h k l
7.8050 7.8092 -.0042 1 0 0
6.8350 6.8334 .0016 1 -1 0
5.8440 5.8327 .0113 1 0 1
5.1520 5.1471 .0049 -1 1 1
4.6920 4.6886 .0034 0 -1 1
4.3290 4.3288 .0002 1 1 0
4.0810 4.0891 -.0081 1 1 1
3.7250 3.7329 -.0079 0 0 2
3.4480 3.4509 -.0029 0 2 0
3.2550 3.2525 .0025 1 -2 1
3.0740 3.0734 .0006 0 -1 2
2.8770 2.8790 -.0020 -3 1 0
A= 8.680 DA= .001
B= 7.7020 DB= .0007
C= 7.599 DC= .001
GAMMA=114.62 DGAMMA= .01
BETA = 85.40 DBETA = .02
ALPHA= 83.136 DALPHA= .005
V=453.8
11. 37-1808
C6H8CuN6Na2O4
Triklin
Dexp Dcal d(D) h k l
9.4840 9.4823 .0017 1 0 0
7.5350 7.5354 -.0004 0 1 0
5.4800 5.4805 -.0005 -1 -1 1
5.4740 5.4734 .0006 1 1 0
4.3400 4.3386 .0014 1 1 1
3.7250 3.7277 -.0027 -2 -1 2
3.5130 3.5118 .0012 2 -1 1
3.3620 3.3622 -.0002 0 0 3
3.1370 3.1351 .0019 -2 -1 3
3.0010 3.0006 .0004 1 2 1
2.6890 2.6891 -.0001 3 0 1
2.4130 2.4137 -.0007 2 -2 2
A= 10.803 DA= .006
B= 7.6579 DB= .0009
C= 11.333 DC= .002
GAMMA=100.2220 DGAMMA= .0001
BETA =117.12 DBETA = .09
ALPHA= 86.25 DALPHA= .02
V= 821.2
12. 38-0152
{Cu0.3Zn0.7}5{CO3}2{OH}6
TRIKLIN
Dexp Dcal d(D) h k l
6.7900 6.8028 -.0128 1 0 0
5.7900 5.7993 -.0093 0 1 1
5.2800 5.2911 -.0111 0 -1 1
4.6700 4.6751 -.0051 0 0 2
4.5500 4.5529 -.0029 1 0 2
4.0400 4.0471 -.0071 0 1 2
3.7000 3.7004 -.0004 0 -1 2
3.4000 3.4004 -.0004 -1 0 2
3.2600 3.2625 -.0025 2 0 2
3.2000 3.2006 -.0006 2 1 1
3.1400 3.1388 .0012 -1 1 2
3.0200 3.0176 .0024 2 1 2
A= 7.143 DA= .004
B= 6.887 DB= .004
C= 9.863 DC= .005
GAMMA= 88.65 DGAMMA= .04
BETA = 72.26 DBETA = .03
ALPHA= 84.35 DALPHA= .03
v=458.6