1. 13-0159
{NH4}3Cu8{SO3}6*12H2O
13-0159
Tetragon
Groupa 90,113
Dexp. Dcal. d(D) h k l
8.5900 8.6260 -.0360 0 0 1
7.3800 7.4268 -.0468 1 1 0
5.6100 5.6282 -.0182 1 1 1
4.6700 4.6971 -.0271 2 1 0
4.4800 4.4856 -.0056 2 0 1
3.7100 3.7134 -.0034 2 2 0
3.3300 3.3330 -.0030 2 0 2
3.1000 3.0995 .0005 3 1 1
2.9200 2.9130 .0070 3 2 0
2.8700 2.8753 -.0053 0 0 3
2.8100 2.8141 -.0041 2 2 2
2.7700 2.7733 -.0033 1 0 3
a= 10.50306 c= 8.62605
da= .004602 dc= .018137
v= 952
Triklin
8.5900 8.5896 .0004 -1 1 0
7.3800 7.3719 .0081 0 1 1
5.6100 5.6097 .0003 0 -1 1
4.6700 4.6651 .0049 2 0 0
4.4800 4.4772 .0028 0 1 2
3.7100 3.7109 -.0009 1 -2 1
3.3300 3.3303 -.0003 1 -1 2
3.1000 3.1018 -.0018 0 3 1
2.9200 2.9200 .0000 -3 0 2
2.8700 2.8686 .0014 2 0 2
2.8100 2.8098 .0002 2 -1 2
2.7700 2.7699 .0001 1 -2 2
A= 11.435 DA= .004
B= 11.058 DB= .003
C= 10.1661 DC= .0004
GAMMA=122.46 DGAMMA= .02
BETA =115.22 DBETA = .01
ALPHA= 64.404 DALPHA= .002
V= 945.9
2. 13-0165
{NH4}7Cu{SO3}4*5H2O
Triklin
Dexp Dcal d(D) h k l
9.2100 9.2098 .0002 1 0 0
8.4200 8.3909 .0291 0 1 0
7.7600 7.7723 -.0123 -1 0 1
7.4300 7.4207 .0093 1 0 1
6.7000 6.7012 -.0012 0 0 2
6.0600 6.0541 .0059 -1 -1 1
4.2500 4.2581 -.0081 1 2 0
3.8100 3.8102 -.0002 0 -2 1
3.6400 3.6389 .0011 -2 1 1
3.1300 3.1299 .0001 2 0 3
3.0100 3.0104 -.0004 -2 1 3
2.8400 2.8388 .0012 -3 -1 2
A= 9.537 DA= .001
B= 8.827 DB= .006
C= 13.632 DC= .007
GAMMA= 75.21 DGAMMA= .07
BETA = 90.13 DBETA = .03
ALPHA= 79.86 DALPHA= .01
V=1093
3. 13-0177
{NH4}CuSO3
Triklin
Dexp Dcal d(D) h k l
7.7600 7.7373 .0227 0 0 1
4.6200 4.6217 -.0017 1 1 0
4.3500 4.3467 .0033 2 0 0
3.8700 3.8686 .0014 0 0 2
3.6500 3.6426 .0074 2 0 2
2.7100 2.7107 -.0007 3 1 1
2.5800 2.5791 .0009 0 0 3
2.0900 2.0901 -.0001 4 0 3
2.0800 2.0786 .0014 2 0 4
1.9250 1.9251 -.0001 -2 0 3
1.8700 1.8697 .0003 -3 1 2
1.6670 1.6676 -.0006 2 0 5
1.6500 1.6501 -.0001 -4 0 2
1.5730 1.5730 .0000 -2 2 3
a= 9.37 b= 5.4567 c= 8.34 beta= 68.1
da=.01 db= .0006 dc=.01 dbeta=.1
V= 396
4. 13-0285
Cu4+2Ca{SO4}2{OH}6*3H2O
Triklin
Dexp Dcal d(D) h k l p
10.2000 10.2056 -.0056 1 0 0 0
5.8900 5.8731 .0169 0 1 1 25
5.6600 5.6515 .0085 0 -1 1 14
5.3400 5.3448 -.0048 1 0 2 10
5.0600 5.0686 -.0086 -2 0 2 23
4.9600 4.9590 .0010 0 1 2 3
4.8300 4.8361 -.0061 -2 1 1 20
4.6800 4.6983 -.0183 0 -1 2 67
4.5800 4.5676 .0124 -2 1 0 50
4.4700 4.4775 -.0075 -1 1 3 33
4.3800 4.3845 -.0045 -2 0 3 21
4.2600 4.2631 -.0031 1 -1 2 16
A= 11.282 DA= .002
B= 6.513 DB= .008
C= 16.3494 DC= .0007
GAMMA=107.06 DGAMMA= .04
BETA =110.52 DBETA = .07
ALPHA= 81.258 DALPHA= .008
V= 1074
5. 13-0286
CuBeF4*5H2O
Triklin
Dexp Dcal d(D) h k l
5.4500 5.4482 .0018 1 0 0
4.6700 4.6654 .0046 -1 1 1
4.0200 4.0223 -.0023 -1 -1 1
3.7300 3.7325 -.0025 1 -1 1
3.4400 3.4452 -.0052 1 2 0
3.2700 3.2706 -.0006 -1 0 2
3.0400 3.0396 .0004 0 2 2
2.7500 2.7503 -.0003 -2 1 1
2.4200 2.4199 .0001 0 4 1
2.3300 2.3327 -.0027 -2 2 2
2.1400 2.1400 .0000 0 4 2
2.0500 2.0500 -.0000 0 -2 3
A= 5.620 DA= .001
B= 10.089 DB= .001
C= 7.289 DC= .004
GAMMA= 99.01 DGAMMA= .01
BETA =102.02 DBETA = .05
ALPHA= 82.240 DALPHA= .005
V= 397.0
6. 13-0287
CuBOF3*5H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.7500 4.7499 .0001 -1 0 2
4.3600 4.3567 .0033 1 1 1
3.4800 3.4833 -.0033 2 1 0
2.6900 2.6909 -.0009 2 0 3
2.3800 2.3800 .0000 -2 2 1
2.1600 2.1600 .0000 -4 0 1
1.9100 1.9101 -.0001 0 3 1
1.7100 1.7098 .0002 0 3 3
1.5700 1.5698 .0002 2 1 6
1.4200 1.4204 -.0004 5 0 4
1.3800 1.3799 .0001 5 1 4
1.3400 1.3398 .0002 6 1 2
1.2900 1.2901 -.0001 -4 2 6
1.2700 1.2700 .0000 2 0 8
a= 8.715 b= 5.821 c=10.873 beta= 93.91
da=.002 db=.001 dc= .02 dbeta=.09
V= 550
Triklin
Dexp Dcal d(D) h k l
4.7500 4.7585 -.0085 0 0 1
4.3600 4.3601 -.0001 -1 0 1
3.4800 3.4785 .0015 -1 1 1
2.6900 2.6907 -.0007 1 -1 1
2.3800 2.3792 .0008 0 0 2
2.1600 2.1603 -.0003 -2 1 2
1.9100 1.9092 .0008 1 0 2
1.7100 1.7103 -.0003 -3 0 2
1.5700 1.5701 -.0001 -3 2 2
1.4200 1.4200 -.0000 -2 2 3
1.3800 1.3802 -.0002 1 0 3
1.3400 1.3398 .0002 -4 2 2
1.2900 1.2899 .0001 -4 1 3
1.2700 1.2700 .0000 3 1 1
A= 5.791 DA= .001
B= 4.4501 DB= .0006
C= 5.1316 DC= .0004
GAMMA=108.59 DGAMMA= .02
BETA =111.964 DBETA = .006
ALPHA= 84.189 DALPHA= .004
V= 116.2
7. 13-0501
Cu6Si5O16*xH2O
Triklin
Dexp Dcal d(D) h k l
9.9800 9.9587 .0213 1 0 0
4.9700 4.9642 .0058 1 1 1
4.4300 4.4309 -.0009 1 -1 1
3.6300 3.6283 .0017 -2 1 0
3.5000 3.4952 .0048 -2 -1 1
3.3200 3.3196 .0004 3 0 0
3.1200 3.1200 -.0000 2 2 1
2.9000 2.8973 .0027 0 1 2
2.7600 2.7613 -.0013 3 -1 1
2.6800 2.6828 -.0028 3 1 2
2.4600 2.4573 .0027 -2 -1 2
2.3900 2.3896 .0004 3 -1 2
A= 10.693 DA= .006
B= 7.316 DB= .006
C= 6.759 DC= .001
GAMMA= 74.61 DGAMMA= .07
BETA = 75.374 DBETA = .004
ALPHA= 89.30 DALPHA= .02
V= 492.4
8. 13-0507
3CuSiO3*H2O
Triklin
Dexp Dcal d(D) h k l
12.5000 12.4893 .0107 1 0 0
9.9100 9.9096 .0004 0 1 0
4.9500 4.9533 -.0033 -1 1 1
4.4300 4.4337 -.0037 1 -1 2
3.6300 3.6292 .0008 0 -3 1
3.5000 3.4998 .0002 -1 -3 2
3.4000 3.3999 .0001 2 2 1
3.3100 3.3095 .0005 -2 -3 2
3.1100 3.1088 .0012 1 -1 3
2.9300 2.9296 .0004 4 0 1
2.7700 2.7708 -.0008 3 -2 2
2.6900 2.6902 -.0002 -3 -1 3
A= 12.7761 DA= .0004
B= 11.1521 DB= .0009
C= 9.9800 DC= .0008
GAMMA= 77.914 DGAMMA= .005
BETA = 96.33 DBETA = .01
ALPHA=115.39 DALPHA= .05
V= 1255.8
9. 13-0791
C32H36CuN4
Triklin
Dexp Dcal d(D) h k l
11.7000 11.6908 .0092 1 0 0
10.2000 10.2232 -.0232 0 1 0
8.3500 8.3216 .0284 0 0 1
7.2000 7.2283 -.0283 1 0 1
6.6800 6.6629 .0171 0 1 1
5.8500 5.8454 .0046 2 0 0
5.1500 5.1629 -.0129 -2 1 0
4.6100 4.6172 -.0072 1 2 0
4.1100 4.1149 -.0049 1 -2 1
3.8900 3.8969 -.0069 3 0 0
3.7200 3.7155 .0045 3 0 1
3.5000 3.5005 -.0005 -2 2 1
A= 11.79 DA= .01
B= 10.249 DB= .001
C= 8.404 DC= .001
GAMMA= 91.822 DGAMMA= .006
BETA = 82.81 DBETA = .01
ALPHA= 86.65 DALPHA= .01
V= 1005.2
1. 14-0113
CuAl6{PO4}4{OH}8*3.7H2O
Triklin
Dexp Dcal d(D) h k l
6.8000 6.7969 .0031 1 0 0
6.1600 6.1602 -.0002 1 1 1
4.7300 4.7192 .0108 -1 -1 1
4.5100 4.4897 .0203 1 2 0
4.1800 4.1831 -.0031 1 0 2
3.7170 3.7160 .0010 -1 -2 1
3.4340 3.4311 .0029 1 2 2
3.2490 3.2504 -.0014 -1 -1 2
3.0790 3.0801 -.0011 2 2 2
2.8810 2.8809 .0001 -1 1 2
2.5460 2.5456 .0004 2 2 3
2.5150 2.5158 -.0008 -2 1 1
A= 7.686 DA= .0002
B= 9.374 DB= .006
C= 9.004 DC= .005
GAMMA= 66.70 DGAMMA= .01
BETA = 72.98 DBETA = .02
ALPHA= 83.28 DALPHA= .03
V= 569.7
2. 14-0188
(Cu,Zn,Ca}5{SO4}2{OH}6*3H2O
Triklin
Dexp Dcal d(D) h k l
10.0000 10.0235 -.0235 1 0 0
5.5000 5.5011 -.0011 -1 1 1
5.0000 4.9973 .0027 1 -1 1
4.8000 4.7978 .0022 1 1 0
4.3000 4.2913 .0087 -1 -1 1
3.5400 3.5340 .0060 -2 0 2
3.3800 3.3787 .0013 -3 1 1
3.1500 3.1485 .0015 -2 2 1
3.0100 3.0089 .0011 3 0 1
2.7100 2.7099 .0001 0 1 3
2.6400 2.6405 -.0005 2 1 2
2.5600 2.5597 .0003 3 -1 2
A= 10.6781 DA= .0006
B= 6.8782 DB= .0003
C= 8.933 DC= .001
GAMMA=109.01 DGAMMA= .09
BETA = 97.73 DBETA = .01
ALPHA= 86.27 DALPHA= .01
V= 614.6
3. 14-0479
{Cu,Ca,Si}Sex
Triklin
Dexp Dcal d(D) h k l
3.2500 3.2481 .0019 1 0 0
3.2000 3.2001 -.0001 1 1 0
3.0400 3.0403 -.0003 1 1 1
2.9900 2.9910 -.0010 0 1 1
2.8500 2.8493 .0007 -1 1 0
2.4900 2.4888 .0012 0 -2 1
2.0000 2.0000 .0000 0 4 0
1.8990 1.8983 .0007 -1 0 1
1.8840 1.8855 -.0015 -1 -1 1
1.8110 1.8108 .0002 -1 1 1
1.7100 1.7097 .0003 1 -1 2
1.6580 1.6582 -.0002 -1 2 1
A= 3.698 DA= .001
B= 8.1510 DB= .0005
C= 3.6035 DC= .0005
GAMMA= 78.98 DGAMMA= .03
BETA = 62.966 DBETA = .008
ALPHA= 84.42 DALPHA= .03
V=94.8
4. 14-0685
{Cu,Mg}SiO3*H2O
Triklin
Dexp Dcal d(D) h k l
10.2000 10.1290 .0710 1 0 0
6.9600 6.9730 -.0130 -1 1 0
4.8700 4.8745 -.0045 -1 0 1
4.0600 4.0619 -.0019 -1 2 0
3.9300 3.9260 .0040 -2 0 1
3.7400 3.7388 .0012 -1 -1 1
3.6000 3.6072 -.0072 1 -1 1
3.3200 3.3209 -.0009 2 0 1
3.1800 3.1796 .0004 1 2 1
3.0400 3.0324 .0076 2 -1 1
2.9600 2.9655 -.0055 3 1 0
2.8800 2.8777 .0023 -3 2 1
A= 10.496 DA= .009
B= 8.691 DB= .006
C= 5.340 DC= .003
GAMMA=101.88 DGAMMA= .02
BETA =102.19 DBETA = .08
ALPHA= 74.61 DALPHA= .07
V= 453.2
5. 14-708
C2H2CuO4
Rombik
Groupa 30,53
Dexp. Dcal. d(D) h k l
4.9000 4.8797 .0203 0 0 2
4.6000 4.5797 .0203 2 0 0
4.2900 4.3066 -.0166 1 0 2
3.6000 3.6039 -.0039 2 1 0
3.3900 3.3807 .0093 2 1 1
2.8400 2.8420 -.0020 0 1 3
2.6100 2.6074 .0026 3 1 1
2.4400 2.4398 .0002 0 0 4
2.2000 2.1982 .0018 2 2 2
2.1200 2.1144 .0056 1 2 3
2.0200 2.0204 -.0004 2 1 4
1.9500 1.9536 -.0036 4 1 2
a= 9.159 b= 5.84 c= 9.759
da= .009 db= .01 dc= .008
v= 522
Triklin
Dexp Dcal d(D) h k l
4.9000 4.9042 -.0042 0 0 1
4.6000 4.5877 .0123 1 1 0
4.2900 4.2971 -.0071 1 1 1
3.6000 3.5997 .0003 2 0 1
3.3900 3.3916 -.0016 -1 1 1
2.8400 2.8395 .0005 -1 -1 1
2.6100 2.6080 .0020 3 1 1
2.4400 2.4426 -.0026 3 1 0
2.2000 2.2016 -.0016 3 -1 1
2.1200 2.1198 .0002 0 -2 1
2.0200 2.0188 .0012 -3 1 1
1.9500 1.9498 .0002 3 2 0
A= 8.3673 DA= .00019
B= 5.6636 DB= .0002
C= 5.349 DC= .001
GAMMA= 81.650 DGAMMA= .003
BETA = 72.815 DBETA = .002
ALPHA= 72.026 DALPHA= .002
V=230.1
6. 14-0804
CHCuO2
Triklin
Dexp Dcal d(D) h k l
7.0800 7.0798 .0002 1 0 0
5.2300 5.2306 -.0006 -1 1 0
4.5400 4.5403 -.0003 1 -1 1
3.0100 3.0084 .0016 2 1 0
2.8600 2.8597 .0003 1 -1 2
2.6800 2.6801 -.0001 2 -2 1
2.5900 2.5903 -.0003 1 -2 2
2.3900 2.3896 .0004 1 2 1
2.3600 2.3599 .0001 3 0 0
2.2700 2.2702 -.0002 2 -2 2
2.1400 2.1399 .0001 1 -3 2
2.1000 2.0996 .0004 3 -2 1
A= 7.1596 DA= .0003
B= 7.29326 DB= .00006
C= 6.0238 DC= .0008
GAMMA= 97.973 DGAMMA= .001
BETA = 84.468 DBETA = .008
ALPHA=108.97 DALPHA= .01
V= 294.2
7. 14-0811
C4H6CuO4*xH2O
Triklin
Dexp Dcal d(D) h k l
7.7100 7.7157 -.0057 0 1 1
6.9400 6.9180 .0220 0 -1 1
6.2200 6.1981 .0219 0 0 2
5.9100 5.8985 .0115 -1 -1 1
5.8000 5.7895 .0105 1 1 1
5.4100 5.4017 .0083 0 1 2
5.3000 5.2946 .0054 -1 0 2
4.1100 4.1056 .0044 2 0 0
4.0800 4.0839 -.0039 0 -2 1
3.8700 3.8669 .0031 1 -1 2
3.6000 3.6025 -.0025 0 -1 3
3.6000 3.6025 -.0025 0 -1 3
A= 8.37786 DA= .00035
B= 9.16490 DB= .00037
C= 12.56240 DC= .00186
GAMMA= 81.41376 DGAMMA= .00695
BETA = 96.65655 DBETA = .01993
ALPHA= 84.55717 DALPHA= .01787
V=942.1
1. 15-022
CdCuSO6
Triklin
Dexp Dcal d(D) h k l
5.8600 5.8571 .0029 1 1 0
4.7600 4.7610 -.0010 -1 -1 1
3.3200 3.3202 -.0002 -1 -3 1
3.0900 3.0894 .0006 2 1 0
2.9100 2.9111 -.0011 -2 -1 1
2.8600 2.8608 -.0008 1 -1 2
2.7400 2.7406 -.0006 -2 1 0
2.5800 2.5784 .0016 -2 -3 1
2.5600 2.5593 .0007 1 2 2
2.3800 2.3805 -.0005 -2 -2 2
2.2800 2.2805 -.0005 2 4 0
2.2400 2.2392 .0008 -2 2 1
A= 6.205 DA= .001
B= 11.200 DB= .001
C= 7.01109 DC= .00007
GAMMA= 76.222 DGAMMA= .001
BETA = 94.33 DBETA = .02
ALPHA= 99.912 DALPHA= .009
V= 465.9
2. 15-0073
Cu2Y
Triklin
Dexp Dcal d(D) h k l
3.6570 3.6585 -.0015 2 0 0
3.0370 3.0359 .0011 2 2 0
2.5580 2.5561 .0019 3 1 0
2.4930 2.4931 -.0001 1 -2 2
2.3190 2.3188 .0002 2 3 0
2.2820 2.2820 .0000 -1 -3 2
2.1730 2.1739 -.0009 3 2 1
2.1360 2.1359 .0001 2 2 2
2.1030 2.1028 .0002 -2 1 2
1.9830 1.9826 .0004 1 -3 2
1.8710 1.8711 -.0001 4 2 0
1.7930 1.7937 -.0007 4 0 1
A= 7.6783 DA= .0006
B= 7.593 DB= .001
C= 7.264 DC= .005
GAMMA= 72.607 DGAMMA= .007
BETA = 91.23 DBETA = .05
ALPHA=103.53 DALPHA= .02
V=392.1
3. 15-0157
Cu1.96S
Triklin
Dexp Dcal d(D) h k l
4.2800 4.2788 .0012 2 0 0
3.8900 3.8938 -.0038 0 2 0
3.7520 3.7484 .0036 -2 -1 2
3.5860 3.5863 -.0003 2 0 1
3.3860 3.3810 .0050 1 -2 1
3.3500 3.3499 .0001 -2 0 2
3.2820 3.2835 -.0015 0 1 2
3.1920 3.1926 -.0006 -2 1 1
3.1000 3.1010 -.0010 0 -1 3
3.0400 3.0383 .0017 1 2 1
3.0100 3.0114 -.0014 1 -2 2
2.8900 2.8890 .0010 0 -2 3
A= 9.0964 DA= .0006
B= 8.7915 DB= .0007
C= 9.689 DC= .00196
GAMMA= 72.968 DGAMMA= .003
BETA =106.23 DBETA = .04
ALPHA=115.31 DALPHA= .01
V=659,3
4. 15-0549
CuSeO4*5H2O
Monoklin
GRUPA 3
Dexp. Dcal. d(D) h k l
5.6200 5.6252 -.0052 1 1 0
5.4200 5.4205 -.0005 -2 0 1
4.6600 4.6567 .0033 -2 0 2
4.2600 4.2658 -.0058 2 1 0
3.9200 3.9183 .0017 0 1 3
3.3100 3.3114 -.0014 -2 1 3
3.0600 3.0599 .0001 -1 2 1
2.8500 2.8501 -.0001 1 2 2
2.8200 2.8200 .0000 -4 0 1
2.7200 2.7200 -.0000 2 1 4
2.4400 2.4400 .0000 -1 0 6
2.2000 2.2000 .0000 2 2 4
a= 11.363 b= 6.4795 c= 14.7967 beta= 94.05
da= .003 db=.0007 dc=.0006 dbet=.02
V=1086.5
Triklin
Dexp Dcal d(D) h k l
5.6200 5.6244 -.0044 0 1 1
5.4200 5.4347 -.0147 0 -1 1
4.6600 4.6529 .0071 1 0 0
4.2600 4.2598 .0002 1 1 0
3.9200 3.9163 .0037 -1 1 0
3.3100 3.3098 .0002 0 -1 2
3.0600 3.0641 -.0041 -1 0 2
2.8500 2.8481 .0019 -1 1 2
2.8200 2.8207 -.0007 0 3 0
2.7200 2.7174 .0026 0 -2 2
2.4400 2.4400 .0000 -1 2 2
2.2000 2.2008 -.0008 1 -2 2
A= 4.712 DA= .001
B= 8.506 DB= .002
C= 7.3591 DC= .0004
GAMMA= 84.5089 DGAMMA= .0003
BETA = 97.05 DBETA = .09
ALPHA= 88.72 DALPHA= .09
V= 291.19
5. 15-0670
Cu{OH,Cl}2*3H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
5.8400 5.8498 -.0098 1 1 0
5.1700 5.1772 -.0072 1 1 1
4.1400 4.1356 .0044 -1 1 2
3.9900 3.9898 .0002 -2 0 1
3.4400 3.4402 -.0002 -2 0 2
3.1800 3.1799 .0001 1 1 3
3.0700 3.0717 -.0017 1 2 2
2.8700 2.8711 -.0011 -2 0 3
2.8000 2.8005 -.0005 2 0 3
2.7000 2.6993 .0007 1 0 4
2.6360 2.6359 .0001 0 3 1
2.6020 2.6011 .0009 -3 1 1
2.4500 2.4497 .0003 0 3 2
1.9970 1.9971 -.0001 -3 2 3
a= 8.433 b= 8.124 c= 11.50 beta= 91.43
da= .007 db=.005 dc=.01 dbeta=.09
V= 787.4
Triklin
Dexp Dcal d(D) h k l
5.8400 5.8382 .0018 1 1 0
5.1700 5.1708 -.0008 -1 1 1
4.1400 4.1380 .0020 -1 -1 1
3.9900 3.9938 -.0038 -1 2 1
3.4400 3.4401 -.0001 -2 1 1
3.1800 3.1811 -.0011 2 0 1
3.0700 3.0696 .0004 -2 -1 1
2.8700 2.8694 .0006 1 3 1
2.8000 2.8012 -.0012 2 2 1
2.7000 2.6996 .0004 0 3 2
2.6360 2.6363 -.0003 -2 0 2
2.6020 2.6017 .0003 1 -1 2
2.4500 2.4492 .0008 3 1 0
1.9970 1.9969 .0001 -2 4 2
A= 7.693 DA= .001
B= 9.636 DB= .001
C= 7.013 DC= .002
GAMMA= 92.51 DGAMMA= .01
BETA = 96.122 DBETA = .007
ALPHA= 71.84 DALPHA= .01
V= 491.2
6. 15-0932
C20H40Cl2CuO18*4H2O
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
8.2200 8.2366 -.0166 1 0 1
6.4000 6.4080 -.0080 1 1 0
5.4800 5.4760 .0040 -1 1 1
4.5800 4.5731 .0069 2 1 0
4.3200 4.3154 .0046 2 1 1
4.1600 4.1577 .0023 -2 1 1
3.6200 3.6197 .0003 1 0 3
3.3000 3.3012 -.0012 3 1 1
2.8200 2.8210 -.0010 -2 1 3
2.7000 2.6993 .0007 -4 0 1
2.6200 2.6219 -.0019 4 1 1
a= 11.332 b= 7.78 c= 11.23 beta= 86.221
da=.005 db=.02 dc=.01 dbeta=.003
V= 988
Triklin
Dexp Dcal d(D) h k l
8.2200 8.2245 -.0045 0 0 1
6.4000 6.4023 -.0023 1 0 0
5.4800 5.4807 -.0007 0 -2 1
4.5800 4.5800 .0000 0 2 1
4.3200 4.3186 .0014 -1 2 1
4.1600 4.1587 .0013 0 3 0
3.6200 3.6201 -.0001 -1 -1 2
3.3000 3.2999 .0001 -2 1 0
2.8200 2.8203 -.0003 -1 4 1
2.7000 2.7000 .0000 0 -2 3
2.6200 2.6200 -.0000 -1 -4 1
A= 6.6537 DA= .0009
B= 13.0111 DB= .0005
C= 8.4355 DC= .0004
GAMMA=102.68 DGAMMA= .01
BETA = 97.256 DBETA = .008
ALPHA= 98.68 DALPHA= .02
V= 694.65
1. 16-0365
Cu4Al2{CO3,SO4}{OH}12*2H2O
Triklin
Dexp Dcal d(D) h k l
10.1000 10.0995 .0005 0 0 1
5.6300 5.6329 -.0029 -1 1 0
5.0300 5.0311 -.0011 0 -2 1
4.2100 4.2090 .0010 1 0 2
3.8900 3.8894 .0006 1 -2 2
3.6500 3.6483 .0017 -1 0 2
3.3300 3.3310 -.0010 -1 1 2
2.9300 2.9301 -.0001 2 -2 1
2.7700 2.7692 .0008 -1 -3 1
2.5100 2.5092 .0008 0 3 2
2.4500 2.4507 -.0007 2 0 3
2.3800 2.3799 .0001 2 2 1
A= 6.326 DA= .002
B= 10.584 DB= .004
C= 10.643 DC= .001
GAMMA=101.49 DGAMMA= .03
BETA = 78.914 DBETA = .002
ALPHA=106.46 DALPHA= .03
V= 662.7
2. 16-0762
CuMnO2
Triklin
Dexp Dcal d(D) h k l
2.8500 2.8559 -.0059 1 0 1
2.7000 2.7119 -.0119 0 1 1
2.5400 2.5358 .0042 0 -1 1
2.4300 2.4357 -.0057 0 2 0
2.2500 2.2489 .0011 -3 1 1
2.2200 2.2206 -.0006 2 2 0
1.9020 1.9012 .0008 -2 2 1
1.7600 1.7588 .0012 4 1 1
1.6160 1.6171 -.0011 6 1 0
1.5590 1.5591 -.0001 2 3 0
1.4440 1.4438 .0002 -2 3 1
1.4280 1.4280 .0000 2 0 2
A= 10.3059 DA= .0006
B= 4.8853 DB= .0002
C= 3.1496 DC= .0002
GAMMA= 89.101 DGAMMA= .004
BETA = 98.46 DBETA = .02
ALPHA= 85.947 DALPHA= .008
V=156.6
3. 16-0763
Cu2{OH}3F
Triklin
Dexp Dcal d(D) h k l
4.6500 4.6501 -.0001 1 0 0
2.7900 2.7910 -.0010 -1 1 0
2.6500 2.6514 -.0014 -1 -1 2
2.4700 2.4705 -.0005 -1 0 2
2.3200 2.3210 -.0010 -2 -1 1
2.2700 2.2721 -.0021 0 2 0
1.8300 1.8316 -.0016 2 -1 1
1.7700 1.7683 .0017 -1 -2 3
1.7400 1.7409 -.0009 1 -2 2
1.7200 1.7196 .0004 1 1 3
1.5800 1.5799 .0001 2 2 2
1.5400 1.5410 -.0010 1 -2 3
A= 4.9765 DA= .0007
B= 5.011 DB= .002
C= 6.337 DC= .006
GAMMA= 69.621 DGAMMA= .006
BETA = 90.67 DBETA = .05
ALPHA=103.96 DALPHA= .04
V= 143.3
4. 16-0811
CuTh2{PO4}3
Triklin
Dexp Dcal d(D) h k l
10.4000 10.4005 -.0005 1 0 0
6.4000 6.3956 .0044 0 1 0
5.2400 5.2427 -.0027 -1 0 1
4.8300 4.8311 -.0011 1 -1 1
4.4000 4.4058 -.0058 1 1 1
3.5500 3.5496 .0004 2 1 0
3.5200 3.5193 .0007 -3 1 0
3.4700 3.4701 -.0001 3 0 1
3.3200 3.3161 .0039 2 0 2
3.0100 3.0103 -.0003 -1 1 2
2.9100 2.9116 -.0016 -2 -1 1
2.8400 2.8400 .0000 -3 0 1
A= 11.196 DA= .001
B= 6.704 DB= .001
C= 7.248 DC= .002
GAMMA=106.44 DGAMMA= .03
BETA = 76.73 DBETA = .01
ALPHA= 88.17 DALPHA= .01
V= 505.1
5. 16-0892
C48H40CuN2O12P4
Triklin
Dexp Dcal d(D) h k l
11.4000 11.4393 -.0393 0 1 1
10.8000 10.7801 .0199 0 -1 1
10.1000 10.1009 -.0009 1 0 0
8.0000 8.0037 -.0037 1 1 0
7.8000 7.8155 -.0155 0 1 2
7.0500 7.0338 .0162 0 2 0
6.8600 6.8356 .0244 -1 -1 1
6.0100 6.0157 -.0057 0 0 3
5.7200 5.7197 .0003 0 2 2
5.5200 5.5176 .0024 -1 2 1
5.3900 5.3900 -.0000 0 -2 2
5.1700 5.1707 -.0007 1 2 2
A= 10.327 DA= .006
B= 14.107 DB= .009
C= 18.46 DC= .01
GAMMA= 92.43 DGAMMA= .04
BETA = 78.38 DBETA = .05
ALPHA= 87.06 DALPHA= .01
V= 2626.8
1. 17-0132
Cu4Al2{SO4}{OH}12*xH2O
Rombik
Groupa 29,57
romb.
Dexp. Dcal. d(D) h k l
10.9000 10.9300 -.0300 0 1 0
5.4600 5.4650 -.0050 0 2 0
3.6600 3.6433 .0167 0 3 0
2.6130 2.6136 -.0006 1 2 1
2.4540 2.4540 .0000 1 3 0
1.5350 1.5351 -.0001 1 4 3
a= 3.320 b=10.930 c= 6.713
da= .001 db= .001 dc= .001
V= 243.6
2. 17-0485
K2Cu{SO4}2
Triklin
Dexp Dcal d(D) h k l
9.0800 9.0876 -.0076 0 1 1
8.8500 8.8537 -.0037 1 0 1
6.4700 6.4647 .0053 0 -1 1
4.5800 4.5816 -.0016 0 2 0
4.3000 4.3011 -.0011 2 1 0
4.1900 4.1929 -.0029 -2 1 0
4.0700 4.0683 .0017 2 -1 1
3.4300 3.4309 -.0009 -2 0 2
3.2600 3.2612 -.0012 -2 2 0
3.2200 3.2199 .0001 1 3 2
3.1700 3.1697 .0003 1 -2 2
3.1600 3.1607 -.0007 1 3 1
A= 10.014 DA= .003
B= 9.856 DB= .003
C= 14.246 DC= .005
GAMMA= 82.32 DGAMMA= .02
BETA = 73.22 DBETA = .01
ALPHA= 68.46 DALPHA= .02
V= 1251.5
3. 17-0918
Cu2OCl2
Triklin
Dexp Dcal d(D) h k l
5.2200 5.2239 -.0039 -1 1 0
4.8800 4.8799 .0001 0 0 1
3.3300 3.3294 .0006 0 -2 1
2.9400 2.9405 -.0005 -1 3 0
2.7700 2.7723 -.0023 -2 1 0
2.4900 2.4902 -.0002 -1 1 2
2.4100 2.4101 -.0001 1 2 1
2.3100 2.3088 .0012 -2 3 1
2.1600 2.1598 .0002 0 -2 2
1.9200 1.9205 -.0005 -2 3 2
1.8300 1.8293 .0007 -3 2 0
1.7000 1.6999 .0001 -2 5 0
A= 5.8209 DA= .0006
B= 9.258 DB= .001
C= 5.11788 DC= .00004
GAMMA=105.00 DGAMMA= .01
BETA =107.514 DBETA = .008
ALPHA= 86.592 DALPHA= .003
V= 254.0